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Home My WebLink AboutNCD062555792_19980930_Sigmons Septic Tank Service_FRBCERCLA PA SI_Combined Preliminary Assessment Site Inspection - Volume II References 1 - 28-OCR'I I I I I I , I I I I ·1 I I I I I I I .I '".,...r,, 0 STATE OF NORTH CAROLINA Deparlment of Environment and Natural Resources Division of Waste Management Superfund Section COMBINED PRELIMINARY ASSESSMENT/SITE INSPECTION VOLUME II ' Sigmon 's Septic Tank Service NCD 062 555 792 Statesville, Iredell County, Norlh Carolina Reference No. 06611 September 1998 Donna J. Wilson Environmental Engineer Division of Waste Management Superfund Section I .. I I I I I I I , I I I I I I. 2. 4. 5. 6. 7. 8. 9. 11. 12. References Sigmon's Septic Tank Service Statesville, Iredell Co., NC US EPA ID: NCD 062 555 792 Wilson, Donna, Environmental Engineer, NC Superfund Section. Latitude and Longitude Calculation Worksheet, Sigmon's Septic Tank Service. November 6, 1997. United State Dept. of Commerce, 1961. Technical Paper No. 40: Rainfall Frequency Atlas of the United States. United State Dept. of Commerce, 1979. Climatic Atlas of the United States: National Climatic Center, Asheville, NC. Wilson, Donna, Environmental Engineer, NC Superfund Section. Memo to File. Topic: Tax plat map. September 1, 1998. Moore, Douglas, Environmental Chemist, NC Superfund Section. Memo to File. Topic: Removal evaluation and onsite reconnaissance. December 17, 1996. Wilson, Donna, Environmental Engineer, NC Superfund Section. Memo to File. Topic: Onsite reconnaissance. January 20, 1998. Rhodes, Jerome H., Hazardous Waste Section, North Carolina Department of Environment, Health, and Natural Resources. Letter to Grady W. Burgin, Prism Laboratories, Inc. Subject: Request for data. May 5, 1992. Readling, Scott, Waste Management Specialist, North Carolina Hazardous Waste Compliance Unit. Memo to Keith Masters, Western Area Supervisor, North Carolina Hazardous Waste Compliance Unit. Topic: Site investigation. September 14, 1990. Grayson, Susan C., Project Supervisor, North Carolina Department of Human Resources, Division of Health Services. Minutes of Meeting. June 20, 1980. North Carolina Department of Natural Resources and Community Development. Drilling Well Record. September 8, 1980. Analytical sampling results, September 12, 1980. Sigmon, Henry, applicant. EPA Hazardous Waste Notification Form, Part A, November 10, 1980. Subsequent correspondence: June 17, 1981, April 19, 1982. North Carolina Department of Natural Resources and Community Development, Division of Environmental Management. Monitoring well sampling results. September 24, 1987, June 14, 1990, May 5, 1993. Bold Research Labs. Monitoring well sampling results, February 21, 1991. I .. I I I I I I I , 10 13. 14. 15. 16. 17. 18. 19. 20. 21. 22. 23. 24. 25. Holyfield, Doug. Head, Waste Management Branch, North Carolina Division of Solid Waste Management. Memo to Dexter Matthews, Chief, Solid Waste Section. Subject: Referral. February 11, 1993. North Carolina Department of Natural Resources and Community Development, Division of Environmental Management. Well Construction Record. August 31, 1987. North Carolina Department of Natural Resources and Community Development, Division of Environmental Management. Sample Analysis of Lagoon Sample. March 4, 1987. North Carolina Solid Waste Management Section, Septage Management Program. Applications and permits, A. A. A. Enterprises. May 12, 1989, December 11, 1989, April 21, I 992, December 15, 1995, January 8, 1997, February 20, 1997. DcRoller, Chris, Hydrogeologist, North Carolina Division of Environmental Management. Letter to Barry Sigmon, A. A. A. Enterprises. Subject: NOV. April 8, 1991. DeRoller, Chris, Hydrogeologist, North Carolina Division of Environmental Management. Letter to Scott Readling, Solid Waste Section. Subject: Referral. September 7, 1990. Glaser, Bob, Pete Doorn, Gray Stephens, Laurie Martin, Lafayette Atkinson, North Carolina Hazardous Waste Section. Field Notes and Sampling Analysis. August 31 and September I, 1992. Smith, Brenda J ., Regional Supervisor, North Carolina Division of Environmental Management. Letter to Barry Sigmon. Subject: Notice of Violation. July 13, 1993. Moore, Douglas, Environmental Chemist, North Carolina Superfund Section. Memo to File. Subject: Removal Evaluation. December 12, 1996. Burrows, Steven M., Project Manager, Shield Environmental Associates, Inc. Sigmon Septic Pit Lagoon Sludge Sampling Report. November 3, 1993. Sigmon, Barry D., Vice-President, A. A. A. Enterprises, Inc. Letter to Karen Walker, North Carolina Department of Environment, Health, and Natural Resources. Subject: Lagoon Closure Activities. April 26, 1995. Connell, Karen, Hydrogeologist, North Carolina Division of Environmental Management. Memo to Pat DeRosa, North Carolina Superfund Section. Subject: Waste Pile referral. December 15, I 995. Homesley, T. C., Jr., Attorney, Homesley, Jones, Gaines, & Fields. Letter to Keith Overcash, Regional Supervisor, North Carolina Division of Environmental Management. I .. I I I I I D , D D E I L I I Subject: Termination of A. A. A. Enterprises. February 19, 1996. 26. DeRosa, Pat, Head, Site Assessment and Removal Branch, North Carolina Superfund Section. Letter to Cindy Gurley, Project Officer, U. S. EPA Region JV. Subject: CERCLIS Site Addition. December 12, 1996. 27. Lair, Myron D., Chief, Emergency Response and Removal Branch, U.S. EPA Region IV. Letter to Jack Butler, North Carolina Superfund Section. Subject: Removal Eligibility. April I, 1997. 28. Wilson, Donna, Environmental Engineer, North Carolina Superfund Section. Memo to File. Subject: Preliminary Assessment/ Site Inspection. January 23, 1998. 29. Wilson, Donna, Environmental Engineer, NC Superfund Section. Memo to File. Subject: Onsite reconnaissance. June I 9, 1997. 30. Superfund Chemical Data Matrix (SCDM). Appendix B-1, Table for Non-Radioactive Hazardous Substances. August 19, 1996. 31. Guidelines for Responsible Party Voluntary Site Remedial Action, Inactive Hazardous Sites Program, NCDEHNR. Table C-1: Soil Remediation Goals. October 1996. 32. Al Hanke, Chief, State Programs Section, US EPA Region IV. Memorandum to State Directors, State Authorization Contacts, RPS Unit Chiefs, and RCS Unit Chiefs. Subject: Guidance on Residential Lead-Based Paint, Lead-Contaminated Dust, and Lead Contaminated Soil and Revised Interim Soil Lead Guidance for CERCLA sites and RCRA Corrective Action Facilities. November 16, 1994. 33. North Carolina Department of Conservation and Development. Geology and Groundwater in the Statesville Area, North Carolina. Groundwater Bulletin Number 68. Prepared by Harry E. LeGrand, Geologist, U.S. Geological Survey. 1954. 34. U. S. Dept. of Agriculture, Soil Conservation Service, 1989. Soil Survey of Iredell County, North Carolina. 35. North Carolina Division of Environmental Management. Sampling Analysis for the Cascaddcn well. January 27, 1991, November 13, 1991, September I, 1992, February 22, 1993, March 6, 1995, September 5, 1996, April 8, 1997. 36. North Carolina Division of Environmental Management. Sampling Analysis for the Shepperd well. February 22, 1993, March I 5, 1994, March 6, 1995, October I 0, 1995, October 7, 1996, April 8, 1997. 37. North Carolina Division of Environmental Management. Sampling Analysis for the Davidsons well. September I, 1992, October I 0, 1995, April 7, 1997. I .. I I I I n I I I I, I I 38. North Carolina Division of Environmental Management. Sampling Analysis for the John Lamberth well. August 4, 1994, April 17, 1996. 39. North Carolina Division of Environmental Management. Sampling Analysis for the Steven Lamberth well. October 10, 1995. 40. Wilson, Donna, Environmental Engineer, NC Superfund Section. Memo to File. Subject: Public Water Supply Systems. November 13, 1997. 41. Wilson, Donna, Environmental Engineer, NC Superfund Section. Memo to File. Subject: Water Supply Lines. January 21, 1998. 42. U.S. Census Data, 1990. Average persons per household. 43. Wilson, Donna, Environmental Engineer, NC Superfund Section. Memo to File. Subject: Groundwater population calculation. January 21, 1998 44. Stanley, Jeanette, Environmental Chemist, NC Superfund Section. Memo to Superfund Section Staff. Subject: Update on Status of Wellhead Protection Programs in N.C. December I, 1997. 45. Federal Emergency Management Agency, National Flood Insurance Program. Flood Insurance Rate Maps. Iredell County, NC. May 15, 1980. 46. Wilson, Donna, Environmental Engineer, NC Superfund Section. Memo to File. Topic: Surface Water Drainage Area. February 4, 1998. 47. Wilson, Donna, Environmental Engineer, NC Superfund Section. Memo to File. Topic: Flow Rates 15 mile Surface Water Pathway. March 24, I 998. 48. Wilson, Donna, Environmental Engineer, NC Superfund Section. Memo to File. Topic: Surface Water Intakes. March 25, 1998. 49. Wilson, Donna, Environmental Engineer, NC Superfund Section. Memo to File. Topic: Fishery Identification along 15 mile SWP. July 24, 1997. 50. Wilson, Donna, Environmental Engineer, NC Superfund Section. Memo to File. Topic: Stream Classifications. June I 0, 1997. 51. Wilson, Donna, Environmental Engineer, NC Superfund Section. Memo to File. Topic: Calculation of Wetland Acreage and Frontage. March 25, 1998. 52. Wilson, Donna, Environmental Engineer, NC Superfund Section. Memo to File. Topic: Endangered/Threatened Species. May 22, 1997. I .. I I I D , D D I 53. 54. 55. 56. North Carolina Center for Geographic Information and Analysis. November 14, 1997. North Carolina Administrative Code, Title 15A, Subchapter 2L. Classifications and Water Quality Standards Applicable to the Groundwater of North Carolina. October 19, 1993. Rudo, Kenneth, Ph.D., Toxicologist, Medical Evaluation and Risk Assessment Branch, Occupational and Environmental Epidemiology Section, North Carolina Department of Environment, Health, and Natural Resources. Memorandum to Pat DeRosa, Head, Site Evaluation and Removal Branch, North Carolina Department of Environment, Health, and Natural Resources. Subject: Health Risk Evaluation. November 10, 1997. Wilson, Donna, Environmental Engineer, NC Superfund Section. Letter to Philip H. Vorsatz, NC CERCLA Project Officer, US EPA Region IV. Subject: Sampling Plan for the Preliminary Assessment/Site Inspection. August 12, 1997. I I I I I I , I I I I I I " I I LATITUDE AND LONGITUDE CALCULATION WORKSHEET 12 LI USING ENGINEER'S SCALE (1/60) Ref __ l s I TE NAME, _S-"-''9--'--. l'--'IYl--'--'o'--'-!1-"'.s"'-----='S;z=-1'-t?---'-t-'--i'c...=---Tt.'-0-_A_L ____ cERcu s 1, I.JC.I) a 0 2.-s.ss rl z.. J I AKA: ______________________ SSID: ____________ _ STATE: f-JC. ZIP CODE: 1'---<3 t7b --~-~~--- SITE REFERENCE POINT: _,__N,_,b,c___,U>=_,___r_,___11:...:e.ccr_o-"-.-'P-~!Jj'---,'-"o~o~t1~~a.~r_-e"_tC ________ _ USGS QUAD MAP NAME: Trouffr1tt.f\. TOWNSHIP: N/S RANGE: E/W SCALE: 1:24,000 MAP DATE: 1913 SECTION: 1/4 1/4 __ 1/4 --- MAP DATUM: 1927 ® CIRCLE ONE) MERIDIAN, COORDINATES FROM LOWER RIGHT (SOUTHEAST) CORNER OF 7.5' MAP (attach photocopy) : LONGITUDE: -122._o 5z' 30" LATITUDE: 35 ° ~ 7' 30" COORDINATES FROM LOWER RIGHT (SOUTHEAST) CORNER OF 2.5' GRID CELL: LONGITUDE: _fi_Q_o 57' 3,D" LATITUDE: 3S O 4-2, 30" CALCULATIONS: LATITUDE ( 7_. 5 ' QUADRANGLE MAP) A) NUMBER OF RULER GRADUATIONS FROM LATITUDE GRID LINE TO SITE REF POINT: B) MULTIPLY (A) BY 0.3304 TO CONVERT TO SECONDS: AX 0.3304 C) EXPRESS IN MINUTES AND SECONDS ( 1 '= 60") : 00' 3 2-. cX> " D) ADD TO STARTING LATITUDE: 35 o 4Z... 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I I To: From: Subject: Date: MEMORANDUM File Donna Wilson 'k,ht,~>j,-{,l/.{'su-- Environmcntal Engineer' North Carolina Superfund Section Telephone conversation -Iredell County Tax Assessor's Office Sigmon Septic Tank Service Statesville, Iredell County September I, 1998 On December I 0, 1996, Doug Moore of the North Carolina Super fund Section spoke Ref. 4 with Linda of the Tax Assessor's Office (phone 704-878-3012) regarding the Sigmon property. The property consists of I 5.35 acres and is owned by Mr. Henry Sigmon of I 268 Eufola Road. The parcel is listed as A24 on tax map 3Q. Mr. Sigmon purchased the property in I 970 from Robert C. Hammonds (Book 491, page 389). The property may have been split to Mary Sigmon in I 996; however, the split had not been recorded on the deed at that time. A copy of the tax map is attached. ~~!. c I It I I I Memo Date: December 17, 1996 To: File From: Douglas Moore f)(!)(.t1(fw~~ Environmental Chemist NC Superfund Section Re: Removal Evaluation and On-Site Reconnaissance Sigmon's Septic Tank Service 1268 Eufola Road Statesville, Iredell County, NC US EPA ID: NCO 062 555 792 On Monday, November 16, 1996, Rusty Harris-Bishop and Douglas Moore of the NC Superfund Section trayeled to the subject site to conduct an on-site reconnaissance. We departed Raleigh at 08:45 and arrived at the site at 11 :45. Upon arrival, we met with Mr. Paul Dahlen, Groundwater Section-Mooresville Regional Office, Mr. Henry Sigmon, Jr., site owner and former operator, Ruby Sigmon, Mary Sigmon, owner of Sigmon Environmental Services and current site operator, Mike Gill, office manager of the Sigmon Environmental Services. Doug Moore discussed the purpose of our visit to conduct a preliminary onsite reconnaissance for a removal evaluation. Mr. Henry Sigmon discussed the site history. Sigmon's Septic Tank Service (Sigmon's) has been in business since 1948. Henry Sigmon purchased the property and moved the operation to the site around 1970. Sigmon's business consisted on pumping septage wastes from mostly residential septic tanks, plus some industrial septage from area businesses. Specifically, Mr. Sigmon mentioned that they took septage from Zimmer Industries (a medical supplies company) and Ro-Mac Company (a metal treating business located in Troutman, NC). Sigmon's was a wholly-owned subsidiary of A.A.A. Enterprises. Between 1970-1978, Sigmons emptied wastewaters to the City of Statesville sewer. Around 1973-74, Sigmon's received permits and land applied sludges to area farmlands. Mr. Sigmon stated that the materials they land applied were essentially the same as the materials later placed in lagoons at the site. Around 1978, Sigmons dug several lagoons at the site and began placing septage wastes inside these lagoons. Mr. Sigmon stated that he had received verbal permission from Rawlin Johnson of the Iredell County Health Department and from representatives in the Mooresville Regional Office to construct and use the lagoons for septage disposal. No permits were issued for the lagoons. It is Mr. I Ref 5 D 19 E Sigmo,'s co,~,: ho is ms< =poosiblc fo, MY coo<,mioatio,, fil,re "'= illgooos were verbally approved by the Iredell County Health Department. The lagoons were actively used until around 1992. Mary Sigmon stated that Sigmon's filed Chapter 11 reorganization in the 1980's and operated until 1995, when the company was forced to cease operations by the Internal Revenue Service for "financial reasons". At that time, Mary purchased two trucks from Sigmon Septic Tank Service and started her own business as "Sigmon Environmental Services, Inc." in January 1996. Both Sigmon's Septic Tank Service and it's parent company, AAA Enterprises, are no longer operating businesses. Following the discovery of groundwater contamination at the site, Sigmons provided bottled water to the affected residents until the early I 990's. Mr. Sigmon stated that Florence Russell had a mean dog and that instead of Sigmons transporting the water to the homes, he left the bottled water on the porch of his own residence at 1268 Eufola Road for the residents to pick up on their own. He stated that the residents stopped picking up the bottled water and so he therefore stopped supplying the water. Mr. Paul Dahlen stated that he spoke with Mrs. Rachel Brown that morning, the current resident of the former Russell residence, and that Mrs. Brown is purchasing her own bottled water. Paul Dahlen stated that he had the Iredell County Sheriffs Dept. serve papers to Mr. Sigmon's son, Barry Sigmon, requesting that Sigmons re-supply bottled water to the affected residents again. He stated that he has been unsuccessful in serving the papers at this time. Mr. Sigmon's contention is that he is not responsible for the groundwater contamination at the site. At 12:40, we drove to the former lagoon area. The lagoons were sited on the crest of a east to west trending ridge that appears to be a high point for the general area. Surface runoff from the site could flow radially in several directions from northwest to east- southeast, although the primary overland runoff from the site appears to travel northwest. In 1993, Shields Environmental (Shields) of Winston-Salem was contracted by Sigmon's to address the environmental concerns associated with the site. At that time, Shields had Sigmon's remove the sludge from the lagoons, mix it with sawdust and stockpile the sludge on a plastic sheet near the southeast comer of the site. There are no surface caps or covers on top of the waste pile. A second pit was dug in an open pasture to the north of the former lagoons which Shield intended to line with plastic as a temporary holding pit while they aerate the sludge. Although the pit was constructed, the remedial phase of the project was never started, primarily due to differences between Mr. Sigmon and the project managers of Shields. Mr. Sigmon stated that they excavated all the sludges from the lagoons to a depth of I 0 feet and then backfilled the lagoons with clay fill from the small pond located north of the main office. Mr. Sigmon did not know whether Shield collected post-removal soil samples from the base of the excavated lagoons. Henry Sigmon stated that during the excavation, they encountered large boulders and sandy soil within 2 feet of the base of the lagoons. The presence of bedrock could not be confirmed at this location, but is suggested by the boulders. 2 I I .. I I I Doug Moore measured the approximate dimensions of the former lagoon area. Based on the evidence of backfill, the dimension were measured with a large hand wheel. The areal dimensions are approximately 213 feet long, by 247 .5 feet wide, or 52,717.5 square feet (1.21 acres). The lagoon area is covered with grass and vegetation. The lagoons are surrounded by a three strand barbed wire fence and posted with signs that read "Keep Out. Sewage Disposal Area". However, it was evident that people had been trespassing onto the former lagoon property at the southwest comer and Lauren Drive. A large hole had been cut in the barbed wire fence and tire tracks were visible entering the property through the hole. Mr. Gill stated that they have problems with people trespassing onto the property with either four-wheel drive vehicles or All-Terrain Vehicles from Lauren Drive. At 13:30, Doug Moore, Paul Dahlen and Rusty Harris-Bishop inspected the two downgradient wells at the Mike James and Rachel Brown residences. These two residences are rental properties. The Rachel Brown well is a bored well, roughly 30 inches in diameter. A jet pump and reservoir tank connected to two PVC drops pipes are installed at the wellhead. The depth to groundwater was visually estimated to be approximately 27 feet in the bored well. Mr. James was n9t home at the time of the inspection. We opened the wellhouse to observe the well construction. There were no tags visfble at the wellhead. The well appears to be a 6 inch drilled well with a jet pump and reservoir tank installed at the wellhead. No additional information could be obtained at this time. The two wells are approximately 400 feet southwest of the site. At 13:50, Doug Moore measured the dimensions of the wastepile by pacing the circumference at the base of the pile with the hand wheel. The circumference was approximately 346.5 feet and the pile was approximately 15 feet tall. One estimate was that the pile contained approximately 2000 tons of sludge. I estimated the volume of the wastepile by using formulas for a spherical pile with a height of 15 feet and a radius of 55.147 feet (i.e. circumference/2 x pi). The radius and height were entered into the formula for the volume of a spherical segment: V = 1/6 it•h (3•r2 + h\ or 1/6 1t ( 15) (3•(55.147)2 + (15)2). By my estimates, the figure would be approximately 2,705 cubic yards (or 2,705 tons). The wastepile has a grass cover. There are several small seeps . visible at the base of the wastepile. At 14:05, Doug Moore and Rusty Harris-Bishop walked the overland surface drainage downgradient to the northwest edge of the property. The slopes in this direction have traces of numerous surface seeps and erosion has cut several drainage paths for the seeps. The overland drainage crosses an open pasture to a low drainage feature that directs the runoff to the west-northwest. At the northwest edge of the property, a small earthen berm (roughlyl-2 feet tall) has been constructed to prevent runoff from leaving the site. This area is wet. Deer and cow tracks were observed on the Sigmon property at this location. The surface runoff apparently enters the ground and flows west-northwest where it appears to surface again at the Lamberth property immediately west of the site. The 3 D la E I runoff is then directed to the northwest towards a small pond located on the Wade Lamberth property. At 14:15, we walked back to the wastepile. Observing the slope of the land from this area, there was no visible evidence of surface runoff to the southeast. However, there are several houses along Lauren Drive southeast of the site. One wellhead was observed in the center of an open pasture behind one of these houses that would be downgradient of the site. This well was formerly used to supply drinking water to the Chris Davidson residence. Historic groundwater samples determined that the well had elevated iron and manganese levels above the State of North Carolina drinking water standards. Since that time, Mr. Davidson has moved to a new house further east and the well was not used for drinking water supply. Mr. Davidson constructed another well at his new location which he uses to supply drinking water for the 4 residences along Lauren Drive, southeast of the site. The current Davidson well was recently sampled by DEM and found to contain trichloroethylene below the State groundwater standards. We also observed a small pond directly opposite the houses on Lauren Drive, approximately 700 feet southeast of the site that could feasible receive groundwater to surface water discharge. This pond most likely contains fish species. The small pond is readily accessible to the residents of Lauren Drive and may be used for recreational fishing. At 14:30, we drove from the site to the office trailer. The former background monitoring well (MW-4) was no longer present along the road bed. Mary Sigmon stated that she is the sole owner of Sigmon's Environmental Service, Inc. and that there are no parent companies. We finished our tour of the site with a brief discussion of the future action with the site. We departed the site at 15:05. At 15: 10, we attempted to located the downgradient pond on the Wade Lamberth property. Mrs. Joyce Lamberth granted permission to cross the property and observe the pond. The pond is relatively inaccessible from any nearby roads and Mrs. Lamberth stated that although the pond contains fish species, she has not observed anyone fishing in the pond. We walked to the pond. The pond is located due south from Mrs. Lamberths residence in a low portion of a cow pasture. There was no evidence of any fishing at the pond. This small pond appears to be a watering hole for the Lamberth's livestock. At 15:40, we departed the site for Raleigh. 4 D . : .;,.•·. D D-·--·--------------------------~-----------------t---+--1--------------D I -·--·---------··-----------·------·-----·----- I D ·------·-· •.. I D 1D·---------------------- D-----·-··--·--- V I /I l -------,------------+---+-----+,-/---,L-+----\ ----,---------,------+----L,L---'-------1 V I ------.---+------!---/A----''-------p I I / I / I I / / /I ... D · · · · , ... :~}:::: '.:_}:;;]j(/ --~~;~tJi ;~i{1f'..:: -. ';Jr.~· D 1 0 ... · . : ;, -:-: ; --------'--------'--1-·.---j-----'--------i------- 1 " -------,---af----1---+-+------j----+----+---- • l l I i I , 11 -.1-1-"J-~l l!!!!!!!!!!I --- I I ! \, .... \.' : ,1' ~,-----,-!----,---~ • i\, .. '--~'~---~---- ' '-~ I ' ----,~ ; 11~--- ! ------:--------c"--\ -,,.---------'--'=, ~ .C...-,gt: ~~pt} ~-j--~~-"'~_______;_____:-_--'-'---ci ~':-o -~- ·, . l I I I I i:::::=1 == •== I == I == I I [ -1 !?vl-v..-c. l .. c/4·~ I 1 : 1 1.-...,..., 9:,,~~~=:.!..!:~~_q-,'""or~dL';::I -+--+-- 0,al., J,-. - 7- / I I ; I / I / / / i ,----.---------,!__ __ . ____ _ / ii .~ J • .. ' , f • ,. I I I I I I I, I I I I I To: From: Subject: Date: MEMORANDUM File Donna Wilson ~( Environmental Engineer,. v-\J. North Carolina Superfund Section On-site reconnaissance Sigmon's Septic Tank Service Statesville, Iredell County January 20, 1998 On August 14, 1997, Stuart Parker and I traveled to the above referenced site to conduct an on-site reconnaissance. We arrived at approximately 3:00 and met with Paul Dahlen of the Mooresville Regional Office, Groundwater Division. Mr. Dahlen informed us that a mobile home development (consisting of6 homes) had recently been constructed adjacent to the Sigmon site. His office had not yet sampled any of the wells in the development. On the east side of the Sigmon property there is a opening in the fencing by one of the new trailers. We talked with the resident of the first trailer east of the Sigmon site, Merle Potts, whose address is 1280 Eufola Road. All of the trailers in the new development, including his, have individual private groundwater wells. The former resident of this trailer was Robertson. The Davidson Roofing well was last sampled by the MRO in April. The Davidson home, address 2057 Buffalo Shoals Road, is just north of the Davidson Roofing business. Chris Davidson owns and leases out the four homes west of his business on Lauren Drive. Davidson alleged that an earlier tenant of his, Ellmore, dumped a gas tank on the property (132 Lauren Drive), resulting in semi-volatiles getting into the water lines. Soil was removed and subsequent testing was conducted. As a result of this problem, Chris Davidson installed 2 monitoring wells at 172 Lauren Drive, across the street from 132 Lauren Drive,'and a new domestic well, now located by his business. He gave us permission to sample any of his wells. Ref 6 I I .. I I I I I I I , I Memo to File Sigmon's Septic Tank Service January 20, 1998 Page 2 We stopped and spoke with the resident of 183 Lauren Drive, Tom Shepperd, and received permission to sample the well. Phyllis Frye died since the last sampling of the well. At 3:50, we met with Mary Sigmon. Ms. Sigmon does not know the details of her well, and the top is covered over with concrete. The water from the well is not treated or filtered. She stated that there are 5 workers onsite. The sludges are no longer being landfarmed. They currently take waste from residential pumpers and three grease traps. She doesn't know the contents of the drums that are in and near the shed on the eastern edge of the property. The septic field for the house is directed to the east, and the septic line for the office trailer is directed to the south. She has no knowledge or information concerning the two small open pits that are located in the extreme southeast corner of the site. East of the office, near the entrance road, is a square metal basin, buried in the ground, except for the top edge. Mary Sigmon stated that the basin is used to solidify certain pumpmgs. At 4:20, we drove to an area past the office, north of the shed, that contained drums. Photos 8 -10 were taken in this area. The drums are stored east of the driveway and there is a soil stain on the road nearby that is approximately 3 feet by 6 feet. Eight drums were noted, and are described below: Shcllzone antifreeze -55 gallons full, dated 8/18/89 !!:!gene's Fabulene -approx. 1/4 full. Mamaroneck, NY I 0543. Tank dipping, cleaner. Gray plastic drum -"SON" painted on side, ½ full. Chevron Delo 400 l 5W40 motor oil, possibly empty Hydrotcx Dallas Tex lubricant -empty Rusted drum, oily white, punctured. Full 2 drums, rusted, full, contents unknown At 4:42 we investigated drums in a shed. Photos 11-13 were taken. There were approximately 20 drums, positioned upright and lateral. At least half of the drums were full, all were scaled, and none were marked. The drums were covered with straw and debris. Four above ground storage tanks are near the shed and are used for the storage of septic pumpings. According to Mary Sigmon, when the tanks arc full, the contents are pumped ·O I I I I I la I I I I I I I , I Memo to File Sigmon's Septic Tank Service January 20, 1998 Page 3 and transported to a wastewater treatment facility. Photos 14-15 were taken of the tanks. The tanks are positioned laterally, diameter IO feet, and approximately 20 to 25 feet long. The ports are at the top edge. The bottom of the drums are buried approximately 2 feet. At 5 :00, we drove to the Frances Lamberth residence at 152 Lamberth Ridge Drive (phone 704-528-4623), which is located just west of the Sigmon Property. She gave permission to sample her well and said that her well was sampled about 5 years ago. The well is approximately 56 to 62 feet deep. Mrs. Lamberth stated that the well is on an "underground river" which flows to the small pond to the north, not the pond to the west. The pond to the west, the Williams pond, is downstream. She said that the first house on Lamberth Ridge Drive was owned by Mike Lamberth and the second house was owned by Wade Lamberth. Both of those houses utilize one well which is located under Wade Lamberth's house. She said that the log cabin that is currently being built on Eufola Road near the site is owned by Richard Teague. From 5:30 to 6:00 we conducted a house count along Eufola and Buffalo Shoals Roads. The total number of offsite houses within 1/4 mile was 35. At 6:00, we stopped by 117 Green Valley Road and obtained permission from the owner of the house to walk across the property to sample Norwood Creek. At 6:25, we stopped by 2192 or 2194 Buffalo Shoals Road to get permission to sample the background pond. No one was home. Two mailboxes were near the driveway, apparently including the resident across the street. "Broom" is printed on one of the mailboxes. We left the site at 6:30. ll' . -II - . - _./. . '; m- • I I I h I I I I I I I , I ,~ ~" ·o Q 513""01'! proptrl-~ I I 1J . ' .,1 ~ _. !ti; \' .-: j,'1'" .. ,r. I :~ ~1..· ~:~ •I•• trJ ... ri:1 ···• .. .. , , .. ·+'; ""· ~$:! ::::~ ,tu, , .. ;;i" ;~ ,:-··~ t:~ ~-~ . ~:,:; ••t:, \h ~ .,. ;~! ••• ,,.r. ::a ~ ii 'it• ,:;~ w: .. , v, •· ~ ' ~ f" . ~~~~ .. ;t:'·-• • ' .. '. -~~ ............ ,!.: .. -.•-~::C'.i.,'1( ~· ,!_!, -'"~-.• ·:~~.'#s-f.-,. ~ ..... ,i~·n.':,';~~ . . ·---~..1:t..~l~ ,_,.tt-.,,~•.;••·••,.J:;::!•1:1.r,•i•~•.",:~•..!<1,,;~~ ~\\&iiiiiil~!:'.": &iiiiii, .. .,/!liiiiil ~,---~~:-~.:,";.•:-~~~·:-~--~·1-f ~i:::i4'~:iNK•:ti~4~'it~#ft.,,~. "ltl1ir~li~J1~}.t::gf:f..:1:~={~:i\i:::?=.' • ·-'" '~· ;GJ&~i'ol ,le~ .. ~ ~ ·~ .r:C ·1 I I lt I I I I I I I , I State of North Carolina Department of Environment, Health, and Natural Resources Division of Solid Waste Management P.O. Box 27687 · Raleigh, North Carolina 27611-7687 James G. Martin, Governor William W. Cobey, Jr., Secretary May 5, 1992 Mr. Grady W. Burgin Laboratory Manager Prism Laboratories, Inc. Post Office Box 240543 Charlotte, North Carolina 28224-0543 Re: Request for information -A.A.A. Enterprises, Inc., Sigmon Septic Tank Dear Mr. Burgin: Ref. 7 William L.. Meyer Director 5 In September 1990, this office investigated the reported storage and disposal of waste by A.A.A. Enterprises, Inc., Sigmon Septic Tank, located on Eufola Road in Statesville, North Carolina. The investigation revealed that A.A.A. Enterprises installs and repairs septic tanks, pumps out septic tank wastes and heavy sludges, and provides a variety of waste removal services to various industries in the area. The waste has been stored and disposed of in eight ( 8) active and two ( 2) inactive unlined surface impoundments located on the Eufola Road site. All ten (10) surface impoundments are approximately equal in dimensions, which measure one-hundred feet (100') long by twenty feet (20') wide and ten feet (10') deep. The Division of Environmental Management obtained samples from two (2) monitoring wells located on-site. Analysis of these samples indicated the presence of certain chemicals which exceeded groundwater quality standards. All or some of these chemicals could be present in higher concentrations in the surface impoundments. A waste determination is needed to properly characterize the waste materials in the surface impoundments. On March 26, 1991, the Hazardous Waste Section of the Division of Solid Waste Management issued a Notice of Violation ("NOV") to A.A.A. Enterprises, requiring the facility to submit a comprehensive sampling and analysis report of all waste stored on site. The report was to have been submitted to the Section no later than May 1, 1991. To date, no report or other information has been submitted to the Section by A.A.A. Enterprises. We understand that your company (formerly known as Bold Research An Equal Opportunity Affirmative Acdon Employer I I I I I ,. I I I I I .I I ' I Mr. Grady W. Burgin May 5, 1992 Page 2 Labs, Incorporated) took samples from the eight (8) active surface impoundments and that some of the samples were· analyzed. We understand further that A.A.A. Enterprises may have failed, or was otherwise unable, to pay for the services rendered, resulting in further sampling and reporting to A.A.A. Enterprises being put on hold. Our first concern is the public health and environment and the potential risks imposed by A.A.A. Enterprises' storage and disposal of waste, which we have reason to believe may be classified as hazardous. Depending on the nature of the waste involved, various environmental medias could be affected. We request that all data from and analyses of samples taken at the A.A.A. Enterprises facility be sent to our office to my attention for further analysis and review. Based upon the information submitted, we will assess A.A.A. Enterprises' compliance with the laws and rules governing the treatment, storage and disposal of hazardous waste, and what steps, if any, are necessary to protect the public health and environment. If any of the information requested has been destroyed, please describe such information and the circumstances under which it was destroyed. Thank you for your cooperation. please do not hesitate to call. Sincerely, ~~ .P' .... µ_,9- Jerome H. Rhodes, Chief Hazardous Waste Section c: Henry H. Sigmon, Jr. A.A.A. Enterprises, Inc., Sigmon Septic Tank Kathleen M. Waylett Assistant Attorney General Should you have any questions, I t/ I /le I 0 State of North Carolina Department of Environment, Health, and Natural Resources Division of Solid Waste Management .,.-·Ref. 8 I James 0. Martin, Governor P.O. Box 27687 · Raleigh, North Carolina 27611-7687 William L. Meyer Director William W. Cooey, Jr~ Scactary I I I I I tJ I I I I I I It I I TO: FROM: RE: September 14, 1990 Hr, ieith Masters, Western Area Supervisor Hazardous Waste Compliance Unit Hr, Scott Readling, Waste Management Specialist Hazardous waste Compliance Unit Site Investigation of A.A.A, Enterprises, Incorporated, Sigmon Septic Tank located in Statesville, Iredell County. On Wednesday, September 5, 1990 a visit was made to the A.A.A, en~erprises, Incorporated Sigmon Septic Tank Company located on Eufola Road in Stateville, North Carolina (704) 873-8954, Present during the visit wer~ representatives from the North Carolina Department of Environment, Health and Natural Resources, Hrs. Christine DeRoller, Hydrogeologist with the Division of Environmental Management, Mooresville Regional Office, Hr, Steven Clayton, Environmental Supervisor with the Solid Waste Section and Hr, Karl Shaffer, waste Management Specialist also with the Solid Waste section, The purpose of the visit was to evaluate the site and determine regulatory compliance under the Resource Conservation and Recovery Act, The request for the Hazardous Waste Section involvement came from Hr, Karl Shaffer, Solid Waste Section, Septage program, Mr, Shaffer had been aware of the site and had been overseeing the operations and as a result of new regulations the existing site would no longer be used therefore closure of the site would be needed, Closure of the site would be dependent upon materials present or absent f•~m the surface impoundments located on the property, Mr, Shaffer requested the presence of the Hazardous Waste Section in order to give the owners guidance with the sampling procedures and other requests from the department which may be necessary for closure. Results from groundwater samples collected from the property by the Division of Environmental Management on June 14, 1990 indicated violations with groundwater standards for Iron and Mercury as well as the presence of other constituents such as Lead and 1,1 Dichloroethane,(SEE ATTACIIIIEHTS) . The Sigmon Septic Tank Company is owned and operated by Hr, Henry Sigmon Jr. and his sons. The operation icludes the pick up of septic materials I I I I I I t' I I I I I I I • mainly consisting of wastewaters from various industries located around the StateYille area. These materials are transported and di,s'posited into a total of six (6) unlined surface impoundments located behind the business which is also located in the basement of the owner's residence. The practice of depositing of such materials in this manner has been carried on since 1978 or 1979. Two (2) surface impoundments have been closed out to date and are identified as impoundments numbers eight and nine. Surface impoundments identified as numbers seven and ten contain water run off from the existing six (6) operating ponds and are connected by a septic T, the waters collected in these two ponds are used for irrigation purposes. All of the ten (10) . ponds are appoximately equal in dimensions which are one hundred (100) feet long by twenty (20) feet wide by ten (10) deep. Four (4) groundwater monitoring wells three down gradient and one up gradient have been installed by. the Division of Envitonmental Management about three years ago and are also indicated on the diagram. Hrs. DeRoller indicated that the site does not have a nondischarge permit or. a NPDES permit ana that the site was orginially opened and permitted by the county Health Department. As a result of the evaluation the proper closure of the surface impoundments cannot be determined until laboratory analysis indications are shown, which may indicate either the presence or absence of hazardous waste or hazardous waste constituents. Hr. Sigmon indicated that the company did rrot knowingly transport hazardous waste or any hazardous waste consitituents, however did indicate that the facility did have an EPA identification number NCD062555792 and presente4 it to me. No record of the company was shown on my list of facilities located in Iredell County indicating an invalid number. Any followup action by this department is pending sampling results from the su~face impoundments. Requested sampling requirements were stated to include the following, At least three (3) samples per pond to be taken at various depths, surface, middle and bottom sediment to be analyzed for volitiles and for the presence of EP Tox Metals. t 1r I , /le I I I I I I I t' I I I I n M L I I ' Diagram Company • of Ten (10) surface Impoundments located at the Sigmon Septic Tank as well as the location of the four (4) groundwater monitoring wells • c __ 10 ___ J ----· ---... 1 2 3 4 5 II B E 'II. I "I. T1 ..it.. G,. P-01.UJ t:>\IJ"-Tl.JI:: Motl tTo~ \tl 1.. ~ei..L ltJi-~llFb 6 9 • 7 • 1' 'Ptlorof>.~ l..Oc.A-TIDJ le I JAMES B. HUNT, JR. GOVitRNOR ( STATE OF NORTH CAROLINA DEPARTMENT OF HUMAN RESOURCES Division of Health Services Ref. 9 HUGH H. _TILSON, M.D. D1Rl[C,.0R I SARAH T. MORROW. M.D., M.P,H. Sl[CRK'TARY P. 0. Box 2091 Raleigh 27602 I I I I f I I I I I I It I I Minutes of Meeting in Statesville, NC June 20, 1980 Depth of ponds 10-15 feet (Rollin Johnson) Water table here at 40-50 feet (Steve Steinbeck) Signs of horse dung and hoof prints all over, in between lagoons. Position is upland, only in one direction is there a rise from this area; in all other directions, the landfalls. Trailer located approximately 400 feet downhill. Whole thing in Sigmon's pasture. 1' 15' .J, ' DIRT ROAD OR DRIVEWAY Approximately 15' to fence 15' x 87' green water 15' X 66' green water (obviously some septage addition-tampon casings floating) milky white 15' x 200' Hillcrest --- 217 feet long milky white, scum on surface. (Water level appears to have fallen one foot) iliilky white,hardly any 75' x 9'. green water banked with fill dirt banked at end 220 feet long x 21' wiale scum, tampon casings,. banked a t end level appears to have dropped ,,, about a foot I , Hillcrest --' / 1' tree stump thrown in TeveT appears co .. ~ve 'f' I~ 15' 181 feet long dropped 10-12"., dead 27' --1, lots of bubbling weeds protruding at edges ..j, banked ,, Heavy scum layers, level has I\ 133' X 21 1 water level has dropped 235' X 21' dropped about about one foot 15-18" ... , banked all along this side higher than my head,no slope; sheer cliff, / slope,banks were not seeded. Some were growing weeds. no '-.V " I I I I , I I I I I I I, I I Minutes (Statesvillej -2-June 20, 1980 Dumping occurred at the site while we were there (11:45 a.m.). Sigmon Septic Tank Service office: 873-8954, home: 528-6321. 90 Diesel Chevrolet, 3800 gallon capacity. Waste smelled industrial, liquid, black. Gentleman driving identified himself as Frank Sigmon, nephew of the man who owns the company. According to Frank Sigmon: They have pumped from Barnhardt, Clark Equipment, Union Glass. Do not use lime for odors -puts out vanilla extract. Have filled in a couple of pits "up the hill". Been using this site for septage since the )fr' sewer cut him off and used to put chemicals ,.___ . fY ~-Chemicals would set up solid, doesn't --·--------------··-·-· _____ i:'.,~_t_h_s_e_P_:~g_e_. ------------------ cc: Steve Steinbeck Frank Olive Rick Doby•",,.- ,,,~ ? / I ,,.._.·,Y {-~r!-~ .. . . / ~ Susan C. Grayson Project Supervisor u u D E I I I I I, I I , ( DRILLISG· CO~'?RACTOR t>.O. BO>:. Z/68/ -P.A!_EIGM~ N.C. ti pc.JI l<Sc. ·,o: . 4. TOPOGRi\PHY: draw,valley,slopc,hilltopQ~iJaircl? one) 'S. USE OF WELL: L·/d Dl\TE:. ? -,1--=--J~ ,6. D0?.:S THIS h'ELL REPLACE AN EXISTING WELL? __ 1.=!/:c.-~[~) __ _ 7 •. TOT,\L DEPTH, ,33 , RIG TYPE OR 1-~Tl!OD; /7.-fu '-- 8. FO?.:•LATION SAN?LES COLLECTED: YES NO __ ~•~----------- Depth Inside Wall thick. type Dia. or weight/ft. fror:i ___ to ft ___ _ HT:-'G?.OliT: Depth Material Method F::o;,1 to ft ------- D£?TH FR0-:•1--TO [!-,'.r-' f-/JI /}"" 3' e' ::, -;;i. f , Ref 10 JRILLING LOG FORHATI6N DESC:UP'i'ION It aad1.t:i.onal space is neeoed, us.c oac.< o.:: ::o:m Depth Dia. Type & Oper,ing Fro::i ___ to ft ___ _ LOCJ\1'IOIJ Si<ETCH (Sho,..,, dist.1ncc to nu~:bercd ro~ds, or othc:-r-K1:> :-e:'e;c:i::c: points) .J...2-.-~GRA.VEL: . Depth Size Material ? rom ___ to ___ f t ____ _ . . , 1.-If' ilbOVC . S'i',\TIC W,\TER U.Vl-,L~(s-:-..) f~-1-t;,rzf a~r1 P"J · --H.: OW v / . -L casing is ___ ft. above land surfccc ELtV: .l-5 .• Yif;L[) (9pm) : _____ METHOD OI:~ TESTING: ___ _ J..6, pu;-:?HiG WATER LEVEL: ________ ft. after _____ hout".;. «t _______ gpr.i. rr.--CHLORINATiml: Typc _______ .l\mount _____ _ 18. :-:;SER QU,\r.ITJ.': t~-.-Ldl 20 ·n;~:rr::R,\1'URE(°FJ t::.-C ~- 20. 'i'y~c _______ Cc1.?2.r;ity ______ (gp1:1) !IP ___ _ 1-:,1K.e ____________ In t.:d:c Depth _____ _ Airline Dc;,~h ______ _ li,\S TiiE m;:;c:R BEE:,J PROVIDED A COi'Y OF Tl!IS fff(Oim r.;~o r:;cOK<'·tt:u o::· T!lC DSP,\HT:•:E::,s Hic:QUIR:C:>~::-;-3 ;,~;o l'.::co:-:..,1ENO.\'i' l ON S? Ri;:-~·,;;.::s /~7..,.. z;-_ ~_, Lr..-:i-.:_--=-J:J_:_SZ__c£~..__LL __ /S---~_-________ _ 1 Co ~.::~·ch:.,-c:.::rt:if/ tt,c:t t.:1_;_,; ,,,.~11 .,,,t!; r.:J;t.n1ctec! in cicc0i:C.-,.,,c2 ·~·1:.h· ~;.c. ~-;.~11 Co:.s-.:.::i..:c-..~c:-i Ec:9ul<1tio:1!. ancl ~~::.,1:i,!,1::.-t2s ,1r:d t:1.:1t thic. ·...:~~11 record is trt..:c ,i::C exact. ___ S)'.~,~1.,~~"S'""-?,;~",'f.''· "7<s-f 2-' .·:-; i{CVi!;a::,! J\/J/77_,..,./,' ,:;'.Ji_,,::it ori.ui.r:;d :..:i Gr~)': .;,:;:,._•1 S .. :~::.:..:,,:. ,11\,J cc1:1y u, ·~·,:<~ o·~ '• ..... ~· D ,•'' ( GROUl-ITJl,ATEil. SECTIO:i . ~ . ,,,,/ Driller /L..2 /:dt.c . .vt 1( . . C in.; Cl Casad to ___ ft.; Description Deo~h froi::.. ,!? ::r /3 ~3 .,;) .r (f22ot) ~o I ff-I /3 1 I lo2 J 1 I I <><cl'' ,J I _) :.:, / ...., ~ ?ie:!.d -----Officcc_ ___ _ USGS _____ _ c.bove I-ISL Thickness (i2et) cif I I -----,-.---,-------'-------j-+---i----- lf----,--,---------t----;--;--1--- I I I l ·---. I I /',. -( 1 v / , / I -I fl'>7 1 I--7,7 .. c--Jl h/ 1-I -d--r --5- ,. I ,.. -1-·· ···-·· ···-__ I ... I _ .. __ Gri~ LocaU02 Lt{ 7 ('. -2 t,.__-:._ b Sct=-1-a..l Nu::bf:r g ::._·=-_'--'_·,,_.! __ '-_AL_Y_s_r_s ______________ Odor ______________________ _ 0 .. ~~:c .. Coad • _ _,_-=-0 __ 0 _C __________ AppearaiJ.ce_~------------------ . . l.-=-? ._______ Tas::e. _____________________ _ FOR CONSTITUENTS OR PROPERTIES . .\.S ,I~llZCATED. SECTION, RlcLEIGH N.C. REPORT A1LU.YSIS TO: CHIEF; . .:.:;,-.2.linity (As CaC03) -< / co pa 8.3 .... ;..... □g/l -----:----.to pH 4.5. ...... .. mg/1 .-Ut.:::3.inu:::i.-................. ug/ ! ------- .,.:-senic ..•. ~ •••••.•.• _______ ug/ l X 3:.:-c:,:-bc,:,ate ..•....••• __ /~Jl_· ___ r:,g/ l Ii. , :::::, 5-Jay ..•........ _______ mg/1 ·p~ -·- Ca:-~:;aace •...•....•.. ___ ~_/ ____ mg/1 Ce:-bo:i Dioxide ........ _______ ng/ l :j~oride .•..•..••...• __ ~ ____ bg/1 ;::;:::.£0= (Total MF).. .. / 100.::l ------ l!SE ck: --- Nitrogen Kj elc!ahl. ........ . r;:,g/ 1 -------= Nitrate & ~itrite. □g/1 -------= pE Value (l-ih2n analyz2d {o. Z -~--- Phenol ...••..... : ...• v.g/1 ------· PhCJs?horus, To~al •••• r:.g/1 Potassilliil ................. .. ------rq,/1 Soecific Coni~~ta~ce (cicro;:;ihos at 25°c) .. ------ Silica .....•..... ; ... ng/1 ------· Sodi= .............. . -------= ,::_g/1 Sulfate .•.••..••..••• -----....: 12.g/l Z i ~c ......... -. -.... - - - .. .. ug/l -------= Calci= ..•••....•.•.. _____ __; c-;;/1 Y2.gne.siUI:1 ................ .. r..3/l -------= R~arks: Toe - D D [2d [J n □ 't LJ .-. ' ' ,_, r--1 L.........! 0 n L-1 [J □ D D D D D D DJ\'ISJON OF f.NV!RON·~t:NTAL '-':,,:,;::::~.:=:1H, GROU',D',;ATEP. SECTION r·· .0. BOX 27637 ?./.LEl';H, ll.C. 27611 (-, () A' , · () REG. -~o. W2LL CONS'l'HUCTIO'.'/ PER.MIT ~:o. -n·:2 2. o·.o:s:,, . /1/.r, ..,....r ~~,,, 3. A!lD?c:ss, S':f p,£' /.3 :3 3 ""7,-zo-/4,.,-= ·4. _TOP(X;?.APHY: dr.a·..1,·-1alley~illtop,flat(circle o:-:i!) 5. C5E o, nEU., Hou-f: DATE, 9-s:"-.J'r::> 6. DOES CiHS S"SLL REPLACE AN EXISTING WELL? IV:) 7. 707':-.!. DEP7H: ,;) cf/ RIG TYPE OR METHOD: 121:r·-4< 8. :"O?.!-'_;?IO:-i S~·!PLES COLLECTED: YES ~O L--"" Inside Wall thick. tJ?e Dia·. or weight/ft. Depth Material Metfl.od r:-c::. __ to f::. _____ _ Depth Dia. 'l'ype & O?er,ing o::PTH rR◊-:1--T◊ JRILLING LOG FOTL'-'-;TIQN DESCRIPTIQ:,..i If aaditional space l.S needed, use bac.< of forr.i LOCi\TIO~ SKETCH Fro~ ___ to ___ ft ___ _ (S\o·.r dista.~c<! to nui.:bercd ro.'.ld!:, or cc.her t'.J.? rcf<?ance points) Size Material ?ro::'. ___ to ___ f , ___ _ .-. -' -'1 atlovc . 14. S?A7IC KATER LEVEL:~). Jf~l: .·;t7•"-'-+><;---~ 'L Casi.:-,; is ___ ft. above land surf<.:c r·ELEV: __ _ -i-5,-. YE!.D(gp::i) : _____ METHOD OF' TESTING: ___ _ a!'t~= _____ hou:-s at ______ ,gpr.i. l,,9,--;-.?: .. -.~.,. ... .:. .• I PL?'.?: Date Insti!.llcc! ________ _ GROUXD'.•:ATE?-. SECTIO:i Field ----Office ___ _ uses ____ _ Driller _______ Det2 Drilled ____ _:___ Cased to ___ ft.; Elev.~_ft. ;sc:iov2 l·!SL .,t.:i:::gs _______ Elec. Log __________ Ga= log ________ _ Description ' ;2,d~ (:1::/, .J 5c1/f,J~ n J_ I 2/4Mtu<.-~ " d~bJ. u /:n,?J:d ../ (j_ t;: ' u t/ , u .. . . D D u _fe._,;;,___/ .;i. ,__r,-3 u D ·--- -···----.__. __ ,_.·•· I ·FI /8/ I /r ld'.Y. I .· I I I I I I I I L I L I Thickness (feet) / 7 - /4 ,:/)) "-..1... .. , • I cr::n:uL L<\50:-l-\T0?.Y :'.C:?ORT ( m -.-:.----. L,AL Ys rs ·= .:..~--J p.::. Odor I S;: ~c:. Coed. /<YO Appear a.ice ~~?-oc Taste .?!._~!.3~ T:::ST FOR CO(iSTITUENTS OR PROPER.TIES .-\S L~lJICATED. G?.-::·_;:J·~·-.:._TER SECTIO~l, RALEIGH N. C . REPORT ,\;'!ALYS IS TO: CHIEF, . -'.::.--2.linity (As CaC03 ) ,:: J to pH 8.3 .•..••••. _-_____ __:mg/1 to p:i 4. 5......... .3 mg/1 D ' . . [____; .:...:!... t:::;. in u;31 ••••••••••••• ________ u.g / l i __ ;_,: see;-iic: •.•.•••••••••. ________ ug/ l 3i=arba;-iate .•••••... ··---~---~mg/1 2:::, 5-:Jay ........... ________ ng/1 D -~ ::·,~oride •.•.•...•••• ·---'----,-'rag/ 1 :_-_ ==-::.:.fo= (Total liF). ·-------'--10021 :~??er .... · .... ; ...... _·~==~--ug/1 u-:---;__; D _ =: ................. _______ ug/ 1 D = :..~::,:.= .............. ______ :.,.g/: :~:-.&E.U2Sf! .•.....•.••• ________ ug/1 ~---_: '.'•r=ury.............. ug/1 0 : : ? ::,1~~-T...,\il USE o"-=~:..=, I~.9 i \v g:..o: 'c:.: .-4D-__ .. t.~.e-~---~-' _2;)~ ( t1 .(\ Nitrogen Kj eldahl •••..••••• tg/1 -------Nitrate & Nitrite. r:,g/1 _____ ____: pH \"alue (t-.'h,an ~nalyzed -~---5',2 Phenol. •..••.•••••••• ug/1 ------· Phos?horus, To~al .••.. --------' -c.g/1 Soecific Cond~cta~ce (cic:romhos at 25°C) •. ~/! ------ Silica .••.......•..•. rog/1 _____ __; Sodiu:2. ................. .. c:g/1 _____ __; Sulfate .••.•.•.....•• r.;;/l _____ __; ug/1 Zinc: ..•...••.••.•.••• _____ __; r:.;/ i }';.2,gr~esium .. -............... . ::.-;,/1 _____ __; R~arks: C C Q?: C ~ L r--.__ .- I__ .-I _ ' L--. c:: C C Ci ENVIRON..,,ENT/IL MANJ\GE/\EtlT, GROU,',0',,/,\TER SECTION II OHtLLilJG CO~:TRACTOR 0. BOX 27687 RALEIGH, N.C. 27611 (-" N 1/-<-.!) hCG. -NO. h"ELL CONSTRUCTIO~J ~3 I 0 n D D D D 1. 'n'ELL LOCATI0~l: (Show sketch of the location below) Neare:st Town: (fs1 ./)i-172/ilt' ,.._., ,.-, L- Y& // 3 2 , (Road,Community or Subdivision and Lot No.) .. :2. o:,~:ER: /J-f,.,-, s-f:r-11ac-,,, 0 3. i\DORl::SS: ::-f7: t 'R .:,,, · .. , ·z C'---:(."}U--,£-/Mr/~.;,./ ,.4. TO?OGRAPHi': draw,valley,slo~e,hillto~circlc one)' 5. USE OF WELL: z;__.,✓ DATE: 2-9 cftl 6. DOES THIS WELL REPLACE AN EXISTING WELL? __ _,_/.=V=-._.....ct_)_ 7. TOTAL DEPTH: ,;,,J...fi· 1 RIG TYPE OR HETiiOD: /li.-,;_;, <L 8. FO?.:•lA'i'IO:-J SN·!PLES COLLECTED: YES NO __ -=/ ____ _ ~ASI~G: Depth From to ft Inside Dia. ------------ Depth Material "°all thick. type or weight/ft. Method ·r~o~ to ft ______ _ Depth Dia. Type & 0pcnin9 ,-Ld Ld - County: = Quadrangle tJo. L-c; 2 a L.c .JRILLING LOG DEPTH FRO-i·I--TO FOR.~~TIO~ DZSCRIPTIO~ ' D<f'...-, .f"-/f· - ,2-"_,-<:/' •c r,...-..;2 f-,,,, ~ If adoitional space is neeacd, use back o~ ro:::-::i LOC1\TIOt./ SKETCH rror.i to ft ____ _ (Sho1-1 dist;incc co nur:,herc<l ro:!c!s, or othc::' :c~1p refcr~n::e ?Oi:-:~s) Size Material Fro::i ___ to ___ f t ____ _ 1'1. ST,\TIC WATER Ca.:,ing is , '/ LEV!'.:L -c;:11/, /ft.~ -~ UL-ft. ;ibove land :.:urfcce ELEV: i-,,-:-nELD(gpm) : _____ METHOD or TESTWG: ___ _ aftcr _____ hours at _______ gpn. rr.· C:iLOiUNATION: Typc _______ .l..:nount _____ _ 1a. •,:ATER QUALITY: {~),.,1 ,]..:.-o n;<<?ER1,TUR£(°Fl C..,C 1·,-:-P?.R:·L\~ENT PL1·1P: Date Installed _________ _ Tyy c _______ C.1p<1c i ty ______ ( gpm) HP ___ _ Airline Depth ______ _ 20. l!,\S 'f!!E O;>.'~iEH l!EEN J'ROVIDLD A COi'Y OF Ti!I5 RECORD l\t~D rnrOR!·H:D OF TffE o;:p;,,n~lE~;1·5 R:'.QUIRE:·'.F.:~:Ts J\'.;[) llF.:CO:-'.:•IE<~D;,T I ON S? i C:o hr.!L·r;':',; R<2<;;ulacio:15 ::or::1 c,;,:-1 H~vi5cd i I/' (~. I I I ., I I I I I \':,i{,_;/;:;z: · -2 '-I. 9 &.i7 '--3S-c It I 1--- CROU"'D\JA'.ri:?-. SECTIO'.·i Description 7 ") 7 d ., ? /:-~ (% '),,,,., .. .. / Elev. ft .. ~- I I I I I I I I I I I I I I c.C>OV2 HSL Thickness · (feet) . -. "--<-' ,• , "/. ;. , ,,. I l . · ,',,!) . ( • ,1,,//8 LP2.c2 Collecced_j'~ 7-,',BJ T~c,e,;___ _____ By: /Cv4;_, /~~cfooZ- 73 • r.,,: £ :io::. or site ;?J,,r'.k:'.'-::~_,..v~_4Jc.--,'--'-:;;J0--J.v,>'---=_-"'-="-'·b---:=----:----~-:-------------------m . ::~::::!:ion of Sampling Point_-"{J"-,-=a_=l,"-4'-'d"'-1 ___ --'------------------~--- (?=?ing Ti,;,e, Air Temperature, etc.) .!.S.!.LYSIS ,o::O Odor ---------..,---------------------------------- !aste --------------------,OR CONSTITUEtiTS OR PROPERTIES • .\.S I1'llICP.T!:D. SECTION, RALEIGH N.C • REPORT .01.'.LYSIS TO: CHIEF, . :..:C.:--..2.linity (As CaCO3) ..(/ . to -.,a 8.3 •...•.•.• _. _______ c,g/l to p:l 4.5....... .. '2-mg/l I [:__ _.:.2_;.:::.inu!il. • • •••.•••.• -~ ______ ug/ 1 ' · _!_:-s;e.2ic.............. ug/ l -------1 )<'._ . 3 i.:: c :: ::, ":ia t c., ••••••••• ·----"-----ug / l i __ : :::::, 5-Day........... rog/l px; (£~:,:inace..... .. . .. .. ,,(/ rcg/1 ·; __ : Ce:bon Dioxide •...••. _______ ug/1 I: X; ::-,:.,:)rid-ce. ............. __ s _____ sgl 1 '. :.:-,:,i.fo= (Total MF).. /100:c:l --·- ug/1. Nitrogen Kj eldahl ......... . Nitrate & ~itrite.---7T-'<--sg/1 nz/1 pH Value (\..'hen analyzed -+--'--'--'-''-1--- P~errol. .••.•.••...••• ug/1 ---'--""-----' Pot2.ssil.l.tl ••.. : ...•••• Snecific Co~d~cca~ce (cicrouhos at 25°c) .. tg/1 ,q,/1 ------ Silica .............. . ------Dg/1 .,. Sod.it.:::!:!.. - • - .......... • • ------cg/1 Sulfate ............. . t!';f;,./1 Zinc .................... .. ug/1· ------· cg/1 CalciU2 .••••..••••••• ------ r:,",?,/ l :Mzgnesiui:!. ........... .. ------ R~arks: D D [gJ D i l □ I I I ! f7 L____l 0 D D D I I , I I I I I It I I ',.'ELL P.ECO,:rn OIV!510N.Of [NVfRO:--·~.c•nAL , .... .t,':\G::~=.:·n, G:i.ou•m,.,;,TE{ -"'CT!ON ( .O. BOX 27637 P.AL::JG'-', tl.C. 27611 I n . n -),, (__,. , .<--<--:a.n 1 ( ,1.,Yrt.r-:G. NO. \.;El,L CO'.lSTil,UC'TION PC.RMIT NO. -jT 4 l'. ·,.::LL LOC,\TIO~:: (Sho·,1 s}:Ctch of the loc<1tion belo1,,·) /) /' / Nearcs t Town ;, __ _,I:_;: ,~w~-c:5,.~-'-t:co-~-✓,:· _,,~·~/J/'-'-'~"'~'C.::'--~/__;__· --~,{_c,.,/~--~c-~~---COt!:1 ty :_~,--*=~=-""'~·c...ccc£.<-U,,:::" ~-·~·""',___-_· ______ :_; __ _.:,JY',:•:::__-.Lf?:.::./L...,L"_LcCOL' 2.· •-~-~----c~-~-c------Ouad rang le No. _--;-L _ _,,(;-".'--'7'---{?::C:-,--'--_s"=-------( rtoad, Com.~un i ty or Subdivision and Lot No.) ·2. c;,;:-:E:R: /J-"I,.~ ~-/ <:· J.;10 ,J · .sr /2/ 1 X -i 7;z,,,,<-frzz:,;,,J ~-:OPOGRAPHY: Cr~valley,slope,hilltop~~circle ~ne) 5. USE ·O? WELL: µd DATE: 7-'z-/iv s.·.COES Ti-lIS WELL REPLACE AN EXISTING WELL? __ J;~l/ __ u~·-- I. ?OT.\L DEPTH: -~1,._·-~3'--_RIG TYPE on METf!OD: ~ 8. !OP.!·!-\TION SAflPLE:S COLLECTED: YES NO _______ _ Depth Inside h'all thic,:;. type Dia. or weight/ft. :'ro::i to ft ___ _ ~ GRO!.i"T: Depth Material Nethod Depth Dia. 'l'ype & Opcr.ing D'.::PTi! FRO-:-:--TO &=f ? ' _., ..>RILLING LOG FOR.NATION DESCRIPTION --~&~~~=j~-~~~-'---G6~~~-'<X-='=<=,,J=--~"~~~s.~:~--"'~~-~s,~v-~< 3 33/ 0 Jr aac1t1on~I sp~ce is nP-cdea, use buc~ of for~ LOCATION SKETCH :ro::i ___ to ___ ft ____ _ (S:--.o·-· clis~a::.:~ :o nL:::-.::>er,:,d ro::ids, or other c.:ip reference points) Dep!:h Size Materinl :' ro::s. ___ to ___ f t ____ _ I ~y;-'ii!::LD(gp:n) : ______ METHOD or TESTING: ___ _ .16, P;J:-:?I;,lG h',\TER LEVEL: _________ ft. -l-7-:-· c:n..O?.INATION: Typc _______ Arnount _____ _ :-:.c:~;..;c ____________ Intul:c Deptt 0, _____ _ ~i:-linc Depth ______ _ ~c-:--?'...~,s '!':iE 0'.Jt:ER a~£:-: PROVIDED A. COl'Y OF THJ.S RECO!tD t.::o ;:::-o:-:_:.;;-:D o~· ?ii£ 01::;•,\C'.T!·!Et;Ts REOUIREME~:1·s J...:~r, ;-,2co:.::-:E:-.:□AT-I w s? ::: =:=-!".•.'.!n:!-ly certify th<it t.:hi~ ·-.·..:-11 •,:c1s co:1t,trw.::te-.: i.:-. 2.:~::::::-,::::-.-:c'~ ,,..i_t~: ::.c. •.-:ell Constn:ct.ion ?.e;;'..:latio:1s anci St.:i:~,!:1:·d~ .:in{! th,1t this .... ·s:11 record is ::..:...:c: ,'.::C e~:,:ct. C --.,~ / -· }f3ifrf''m-5t:Ic',±d.~~~c, ,~2'~5'-f"c ,·~---,:-;,.;-~ Rc·:isc.:t:L;~•-· :;~:h:·,!.t. o!·i,_:i::~: :0 c::-,Y.:·,::·-·,:te::· ::l..'c::,ic.,:1 c:nc: co;;y to ·••ell o·-·:1,..'.:. 0 I ·p . ~,_.,,. n.;.,.1.0-:._L.l'\.:.. VJ.' 1',l\l L;t-'1\L A:.'iD ECO~o:-nc R.ESOl?..C:::s ( GROUNDHATER SECTIOci ( Elev .. __ ft. Description Deo-tl,. (f2Et) lfr:: I ~t: I " l I /-3 ,1 / 3'132' l I I Thickness (feet) I l I ''-~-------+--+---+---- I I I I I I I i I I I I l I I I I I I I l •------~:-I_J l -'--..-__ /V/ ]J · Ci::NTR.-U. L<\30?~'-.·;:o:;.Y P~?J,\l" Grid ·LocatC:.0:1 L (, '7 C. -S · ,} . ( ( L"b. # ,, • See4a.J. !;u::~r-3_J'_0_0_2..-_'7_L_ .. :::~::" Cc, :..:'.ec t edJ -9 -,.P-J U."12:....-_____ Ey :_--'--A-"-'a"'--.,,__"'-A--=~~-_.-t..,""-. _,/:..___:;J;_,,~~-o:::O:.::(/\.___,;:_:::::;__ __ . It ·r.~::,s :::.c:: or site /J"°"·=··•~·<---c;,---"v,;,i('=y--,,<nn'-·'=4.__.~b-~-,--------------------l :·~:::::::ioci of Sa:uplinfroint._~r?Ll-<o,.,,_.,..,,1..;..oc('-"--. ________________________ _ {?u::::!?ing Tine, Air Te~perature, etc.) m :;,:C:: Odor ------------------------,.--------------------O'· S:;,;,-::. Co:::l • _ _,_/_ . ..,9.--"-----------'Appearance'---~-~-------------- :.-;:==.?. 0c 'i:as=e --------------------------------11. ?'-'::..,.:::: ::::ST :OR CO:iSTITUEtITS OR PROPE?.TIES AS --'i:IillIC}.7:':D. I) G,.-: ·_--::-;·.·.,_:o::::t SECTIO!!, RAL EICH N. C. REPORT !ol!ALYSIS TO: CHIEF, I iX •x I ,-- L- -- ·~ I _.:..:_',slinity (As CaCO 3 ) . tc pii 8. 3 ......... _. __ -<-=-/ ___ r::g/ l co p:i 4.5....... .. ng/1 . .:....:. ~i.!l u::i .•..•..•••... ________ u g / ! ;..:,senic:....... .• . . . . . ug/i -------- :=:::.::":::-bo:iate .....•.... ________ n_g/ I _e2:. · · · · · · · · · · · - - • • - _______ c3/i 1: ~c:.::·.~c:.::i .............. ___ . .,_,,/\ ' ~-:.::.:-.~-?..:l~S2............ i.:..g/l -------- Nitrogen ,,.,,..---,\ . \mg/1 Kj elda!-ll. •.....•• •-------" Nitrate & ~itrite. ___ ~--// :1'1,>;/1 /11, c; i I I pH \'alue (\.,'hEcn a:ialyzed '----+-...U'--'--,1- ug/1 P ~ea o l .•••••.••....•• ___ .,,___,:_____ Phos?horus, Total •..• mg/! --------= rr.c./T 0 - Pot2ssiur:, . .' .•......•• _____ _: SnEcific Con~~~ta~ce (~crnwhos at 25°C) .• ------- Silica .......... ~---· Bg/! -------· Sodit.2 ........... -.. ... .. r::g/1 ______ ..,: Sulf2te ............. . mg/1 ______ __; Zi~c ................ :. .... . ug/1 _____ _: CalciU2 ............. .. mg/I --------= Y2gnesiun ....... · .... . r:l'l, / 1 _____ __: ,=--:·:c:c:·":c;... . . . . . . . . . . . -,----u-5_/ i _____________ _ l :·: :~ :~;7;?_1 •\0 US2 , CC. : •• .1.1.\ °i I 2. f r1 D D ~ D □ □ I I I ! r--1 L_...! 0 □ D D .. I It I 0 D I I , I I I I I I It ii I -., •. >'--'-'" jll_o<I 1-.'Ell REC0?.0 DIV!510.'l OF ENVfR(l~i.'~.t:NTAL MAMAGEr-'.c:NT, GROUtiDi-i,\TER SECTJO~i 0. BOX 27687 -RALE!GH, N.C. 27611 (~--~ DiULLI!--lG CmITP~:'.\CTOR n . 1y lf.(~L/k?.G. NO. wEr.t coNs·rRucTrON rr::H.'HT ~o. 1. Wf;LL LOC,\T!O~:: (Shr.iw ske::-.ch of the loc.:ition below) - Nearest Town : __ ,,_,/'---"tL"~-~· £~.~::::(,:_,.~· ✓~-i/_·~/.~)~"'~•(l~/~o~~"'----'~l/==--'--'-· _____ coun ty: , ~-~~ «L /( ; ·--~~~=-='-~-=='-------- _-:.,5C-+k_'2.. __ -.,,c,·7c,:/:Z...-,,l(._;[t_-')c._, 2·~'---c---~c--cc-cc------'Ouadrang le No. _ _cLc.__:,0cc. _,?_o,<Z,'-'(_=--~~-(rtond ,Com..~uni ty 'or Subdi~ision nnd Lot No.) .>RILI,ING LOG 2. o;.,-,;2R• /J/1, _sc;:± '-'5"£1,f> '-<.-. · J. · ADDRESS: ~-:-r-c/7~-i.3 ::1 m-E✓£ZU-r>---DEPTH F ROT--, --70 FORMATION DESCRIPTION 4. TO?C(jRAPHY: draw,valley,slope~la::(circle one)· s .. USE O? WELL' h-o ± DATE' ?-c,, -.J-'c) 6. DOES THIS ~ELL REPLACE AN EXISTING HELL? i--? {) 7. TOTAL DEPTH: '"3 .t ,-RIG TYPE OR HETHOD: L;/2r 8. FO?..HATION SA.'!PLES COLLECTED: YES NO t._.; Depth Inside Wall thick. type Dia. or weight/ft. 1-·rora to ft ___ _ -rQ. GROL"?: Depth Material Method Fro~ to ___ ft ______ _ Dia. Type & Oper,ing 1-·ror.i to ft {) -. /2,,~/ .f:-/rf-, It additional space is needed, use oac~ of torm LOCATION SKE'l'CH -----------($ho~ distnncc to nu::-.bcrcd ronds, or o~her i:iar, refcrc:-:r:c poir.ts) Depth Size Material Fro::-i ___ to ___ ft ___ _ 13. W,\TER ZONES (dc;:>th) ~ __ _;'-"~--:,c:_<~'.~l_/ _________ _ 14. STATIC ~ -,,,-above WATER L!::VEL J ft ,,.~~CDC'PP~,;f,,._.~c~,=s~i~a-,7 ~~ l6L-Casing is ___ tt. above land ~urf<.:c~ ELCV: ~ YIELti(gpm) : _____ .HETI-JOD OF 'l'ESTING: ____ _ _l..6-:--PU:•t?ING WATER LEVF.I.: ________ ft. aftcr _____ hours at _______ gpn. n--:-CHLOiU:--IATIO:<: Type _______ .Amount _____ _ 18. V:ATER QU/\!,IT\': £1..:.-_.. {t) TE::-tPERJ\TURE(oF) /./;, Type _______ ca pnc .i. ty ______ ( gpr.-1) f!i' ___ _ Airline: Dcp~h ______ _ 20-: · H,\S Tfif. Oill\ER BCC:--: PROVIDt:D J. COPY OF TllIS RECORU AHO 11;:;c·oru:r.n Of Ti!E DEPAR1;-1£1:Ts REQU!RE.:~:;;~:Ts A::D 1,.zco:-;.:,\_£1; DAT Io:,.; S? DEI',\RTi:lENT OF :-:ATL'RAL !\SD ECO~CJ:·!IC R!/:C\~?,c:s ( GROlhl'Di-:ATE?. SECTIO:-i { L-& 7 (? G. CasEd t:o __ ft.; Elev .. __ ft. · c..bov~ HSL (lt;:i=.5,s ________ Elec. Log __ ~-------Ga~ log _________ _ J ,---~---......;.---..;.! --------'--1 --7 I I I I I I I ·-,..._,_ I -<~- . J '--) . I !~-}'\_ C::u I . I I ' I I I - .. I I I I I :~'-·:=:-_~_· _-_'"-'_-__ !.L_Y_ 5 _ 1 _ 5 ______________ 0dor ____________________ _ I :~::: Co~d . ___ G __ 0 _0_C----------:::::rance_~------------------- --------------------------------:>; :-! 0~ -_, """T --0.° CO''S7 ITUE1""1S OR PROP_ E0• TIES _,5 .. 7 ' •. ,=T_c_;,~_, ED-m c.Z:c:;~-,;_o_r~ ;E~TIO;;, ~ Rl,LEiGH 1{ _ C. "-,.,_ ~ .u - REPORT -~lALYSIS TO: CHIEF, -~ : _,< .:..:~:.z:;_in~ty (As CaC03) co pH 8.3 .... •··-·-· ___ L_/ ___ r:ig/1 ::oprt4.5 .••. -•... 2. r:ig/1 ,--OF '-----' · 1 . · / 1 ~-=inuc, .•.. _ •. _ .... _________ ug _ •0.::s2;,ic ..... __ ....... ug/1 --------~ 3:. : a r b" '1a t 2 •••••••••• ________ og / 1 D' i :CJ), 5-i:Jay..... •• . . . . mg/1 Ca,c:,'.)n2ce........ •. . . -c_/ ing/1 -------- ug/1 -------- Nitrogen Kj c:ldahl. •..•.•..• rc;g/ 1 ------Nicr2te & Nitrite. r:ig/1 -------' pH \'abe (!-.'hE:n analyzed --~--'---t-j? Phenol ...•........... ug/1 Phos?horus, To~al .•.. _____ ---= r::.g/1 Potassiuo ......... _ ..... .. ------mg/1 S02cific Condacta~ce • 0 (oicrowhos at 25 C) .. ------ Silica .............. . Bg fl -------' Sodi= ... _ •.......... ------r::g/1 Sulf2.te ................... .. ------l!lgi l ug/1 Zir,c .....• • .. -.. -.. · . ------· Calciur:, .......•...... cg/1 ------· Y.zgr:esiu:::. ................. . r::,J 1 --------= R~arks: D D ~ D □ □ l I l I I I D □ D □ I I I I I I D D D L I I DJ VISION r ENV I RO,s..:vE •ff J\ L ... ,M:A:; ;::,~.•IT, G ~our;D,_.A T ER (sr_..-,T I ON . BOX 27687 R~LE!~H, N.C. 27611 l..::.. £) kEc. ·r,;-o. \•<ELL co:1sTnucT10:-i Pr.?.:HT t10 . .f:f_ 1-;;;:LL LOC,\'i'IC~:: (Sho·...1 sk(!tc':h of the location belo;;) Nean;st To~n: L2-btc.Z: ,,:_t,-:::::: A-<r_. C~unty: ~ ,' ✓/4 1:-,/ M=·c:1__~&='-Ll..c31.__;;,3,_·2%_~,.....,--.,-,--,--,,----,------•Quadrangle No. L (.? 7 e 7 (~oad,Co:r .. -:iunitr or Subdivision and Lot No.) ·2. c•-..."":;::r\: ffl"'l,. J1,;,u • .:: •• -c1-✓ 3--;,.!>D?.!:SS: //W<<fz::--<1-1..__,, I'='. ,._, ... ?OFW~PSY: draw,valley,slo?e,hilltop~ircle o:ie) CS£ O? >;CLL, 7; _,, ±' DATE, 9-/() -J-'tJ .s. 6 . .-DO~S 7HIS WZLL REPLACE AN EXISTING WELL? ___ _,U=:....U,c___ RIG TYPE OR METHOD: «✓<,.L,,,t., NO ,___.,-j/ 3,3 I , 8 •· ?OA!~..;T ION SA.'1.PLES COLLECTED: YES Depth Inside Wall thick. type Dia. or weight/ft. :re~ to ft ___ _ l.!l--GROtll': D~pth Materinl Method Dia. 'l'ype & 0£:>c:-.ing DEPTil FRO-:•l--TO .JRILLING LOG FOR:'-tATION DESCRIPTION __,_,1,..,,_,.=-~.<....e_c-:=.-L./i..2,,""<'..£1.=<co::--!=..->.<lw:;&e,;y1-=d-~_f;,,~--:f.:c!:'.. ~~ I ?; ~ .,> Ir aadit1onal space is needed, usu bac~ of form LOCAT10tJ SKETCH Frc~ ___ to ft ____ _ (S~o-~· Gist.:incc ro :'l~!::'.~P.rcd ro.:ids, 01· other n.1p rcfe.rcru:e points) Det3th Size Material F ro::: ___ to ___ f t ____ _ , ' --.:C-r":f above -. LEVEL:,-.(..),..> t<C":"";1--_-:-;-t-,;o;:c, 86ft.lftH DJ --~(LL---------~ c,,sing is ct. ctbo\'e land surfl!CC ELEV: /o o::;-1...;-:-· nELD {g;::,:n) : ______ METHOD or TESTING: ____ _ a!ter _____ hours at _______ gp~. 7y2e _______ Amount _____ _ 18, ;.;,\'!'2R QUlJ.lTY :~C,~~-2c•~z~,-~,_\-v~·-· _1'.E:MPERATURE {°FJ (,. {_ :'-'.ii :-:.e ____________ I n lilkc Dcp th'------ .( • I GROlfu'D\·/ATER SECTIO:-i Lt.7<27 -I Log ~.:ell (io. ;,1(1::,. Fic!ld ____ _ Office ____ _ uses _____ _ ,t~i:c:gs, ________ Elec. Log, ___________ .Ga= log _________ _ I Description Deoth (feet) £roo. to Thickness (£ eet) P--------!--1 -----,--1 --!-I __ _ I I I ''----'--------'--;--I ----;-1-+-I --n I [ u I I I 0 I ·u..,.,. /) / 6 ~ I I n c/'l-../,~~ ;! ,f;J I 0 . dn-?7t J.'.z-) I I E f-1 .. --- ':1<) ({I,'. (?=?ing Time, Air Temperature, ate.) I ?I.'.::"""3 f_\"!--I:iSIS ?:: Odor I S:;.~c. Co::d. ~~ Appearar:ce 7~?-oc Tas r::2 I:cST ,OR CO:iSTITUEciTS OR PROPERTIES AS "iSD~CX,ED. REPORT,A..~.U.YSIS TO: CHIEF, SECIIO:i, RALEIGH !LC. ~...:_~...e.linity (As CaC03 ) to pi:! 8.3.. .. . . . .. ..</ □g/1 --------;:c, ):i 4.5......... -< I ::ig/1 .'.2.=ir.uci ...•...••.•.. ________ ug/l : __ ;..=s=:,.ic.............. ug/1 -------- 3:.:s.::,,-o::ate.......... -< J ng/ 1 -------- EJJ, 5-Jay ........... ________ □g/1 Cs.:::>Jilate............ -< / mg/1 -------- Ce.::c,o::t Dioxide....... lilg/1 --------0 ~ ': "l or id a •...••.•....• __ _,_ _____ rag/ 1 ::;::.fo= (Total MF).. /10°"11 _, ---------0 \ ' :: c??er. ....... ; ...... -ug/ 1 1 :·_:a::ide.............. m0 /l :..____: 0 Di _x: ~~55:,~~,,d Solids ••••. __ ro_1 ____ mg/ 1 : , :: ..:.....:•J1:='!.G~:-.............. ________ mg/ l E:_5<_: ~,;::~:,as:; as C?.C03 ..• _. __ 3_3 ____ r;eg/l .:..=.:-..:=.e:ss, ::o:: Car':ion2te..... 33 mg/ 1 --~----- -----· ................ ________ ug/1 -~--................ _______ ug/1 r Ni::roge~ ✓---.... ,. ::(j eldahl. . . • . . . . • . / \ Nit~ate & ~itrite. , / \ / p"!! \'e.lue (\.:hen 2nalyzed i/ L.J. D) . I P!-:eilol. . . . • . • • • . • . . . • \ / ,_=.-,> Soecific Corrd~ctaace (dc.owhos at 25°c) .. r;,g /1 n.7;/l ug/1 -cg/1 rq,/T_ ------ Silica .••.••.••. : .•.. --------' ug/1 Sod!= .....•..••.•.•• r:g/1 Sulfate ..•••.••..•.•. --------' n~/I Zir:?.C--····-·········· --------' ug/1 Calcit.:.2. -............ . c;/i r:-.3/ l R~arks: D D ~ D □ □ D D ! ! 0 □ D □ ,., -.-.----;,. \.'ELL REC0r1D NORTH Cl,?.OL!!-U, D::?;,~iMf.llT OF N,\TUR;d_ P.ES:.n;.;.l_CES C. co:-1:~.vciJTY DEV[LOP,'',~,'{i DIVl$!0N OF ENV!RON:--1ENTAL M/\NAGf.,'-',::'.:tlT, GR□ur:o,:t,TER S_f;.CTJON ( . 0. BOX 27637 -RALEIGH, N.C. 27611 ( I I I I I D I I I L I I r · ;v ,< c_,(Jru::c. ·No:· WELL CONSTRUCTION PER:-lIT NO. it: 7 ·l. \{ELL LOCi\TIO~:: (Sho'w' skelch of the locution below) Nearest Town, 7:Z-(),27 ----/,./0 County, sk ✓I'/// ___,q,,,r::.· L-_ _,/4',c.;"-=</<-_ ______d_---'l--'~·2-·,~:,"'-·, ___ ~ ________ Q,uadrangle No. L i '/ <J J'" (?.o.i.d,Comnunity or subdivi:.ion ,und Lot No.) 2. o·,;.:~rt : __ -"/1-_,·c;1/,'Jtc_.· 'l~~-'-s.J-.· "'---½-'-. ,,.,,_,.,e,; . .L>cc~c:<1"d!J=c."'-<"'--· -~--- ). ~D0?.£5S :...' _:.:,'-V:=._· _,_a,£:,;•4-_ _,/'._c]c'...,}:Je_.. <C.'; ___ --,,µ"-.L'<c.,_/).t.,✓C.,•,<Z:::c,:~_.:,· ""'--· =- -4. 'I'O?W:l-1\PHY: dra•,1,vallcy,slopc,hilltop~irclc one) ·s. usz or WELL: :::Z::::.:-:1 ✓ DJ\TE: 9-/0·-rfu '6. ·DOES 'i'ilIS h'ELL REPLACE AN EXISTING WELL? __ _c.,v_· __ ,_:J __ 7. 70T,\L DEPTH:_~3=-·~)~_RIG TYPE OR HETilOD:~. ,:/ 8 •. FOP.:-F .. TION SAN?LES COLLECTED: YES NO_~L/=----- . -9--7-(:.,\ S I :,; G : Depth Inside Wall thick. type Dia. or weight/ft. Fro::t to ft ____ _ Depth Material Method to ___ ft ______ _ Depth Type & Opening JRILLING LOG m:PTH F R◊-:•l--T◊ FOR.'-'...,\TIQ~; DESC?.IPTION ~ cf , ,;nJc1-~_,.. t?0 -~-Sic1..../2,,-44_ Ir aod1t1.onc1l space 1.s r1cedca, use oac.-: or .::or:a LOCATION SKETCH F::-om ___ to ft ____ _ (~ho•., c!istanc<'-to numbered road5, or othc:-." . ."!.? re~ercr,c~ pc~:1:.:.) Depth Size Muterial ·r ron ___ to ___ f t ____ _ 13, ;-:,\?E~ ZO:,.;'ES (depth) : __ ..,s;,,<...=a:..C. ________ _ ,, 14. STATIC V:ATER LEVEL:~7./tr~b_~lvc~t!-.~ ~2s.iJt(j --~ /i / I(_--. '-~-Casing is ft. above l.J.nd s11rfcce E:Lr::V: r,-:--Y!ELD(gprn) : _____ .H!::T!IOD OF TESTlt~G: ___ _ aftcr _____ hours at _______ gpn. rr.-c:-H.O!UNI\TI0.-1: Ty?e _______ .Amount. _____ _ 18. ',,",!'.,Tf.R. QUAI,ITY:£ei...._ 0--0 • d 0 (.) TEMPERJ\TUIU'. ( F) ~~t:., :-'.a r.c ____________ r n take Depth _____ _ ;,irline Dc;ith ______ _ ! ~-/_q_(,::, l.f ·~ '5: 0 v :;- 1 T fZ-o ._, + ,v.._,-"-.c.J 2. ( .. "" ~- ·-zcr. ;:.--.s T!iS oc,•m.:K ar:EN PROVID:-:[) A CO!'\' OF THIS R.ECOKD AND It;rO!.:..'·'.ED OP Tl!E DEPAR.T,'1£~1·$ llEQUIRE:'·\E'.:Ts l-.~D .R::.co:1~:.am:,-r10::s? __________ . 2 1 . e.c:-c, :z;:s ~_L,,,c,,~L_t..._o ___ ~ ___ f~-s"'·'·'_,,_£-;:(_ ____ , _____ _ ! 2~ hcrcf ~~rtify ttiot tl1is w~ll ~~~ con~tr,ict.cJ i11 ~~corcl~rice wit)1 N.C. Well Con~tr1:c~io~ [{csul.:!t..i0.1c, .:ind St.ind~ircl:; ;1_12d thilt. t;l:i:; 1-.•el l t"(.:Cot."d i:; t.n.H .. ' and ,:-:;;ilCt: ---~/ .. c,.,,)<::::::'.?J":~2., /;'di:%,: -s:~,,, ,.-7 ·;,~:.c/ __ sc, :·0~·::-: c;;-:-1 :'...:vi~;(:,: :;:1L,;ni.l 0l"J.(j.i::::l ':::'.) l;:·:.';.l:'.('.· . .-.:::t:r :;.~.;:;:..io:1 t1:1d -;::o;)J' t.:i ·~·..::1 -::,·.,~.,~,. • ? I I GROlTh'IWA'.TE?-. SECTimi . . IA Driller a,_) /7-, -<..,.-:1 De,.t2 Drilled ~ 0 Cased to. ___ ft.; Elev .. ___ ft. Description c.bov,e HSL Thickness (feet) 01---------+i---+--I ----+-I~ Dr-----------+l-i---1 -i-, --- IJ I I I I I --I I / t (, <• _:..__e,....,_ ~ /,. / I ci,,, __ f'So -I s c_:)_-7. ,;) 7, 7 I I . I I I I I I I __ L __ l. 0 ll :1 i: )" ~-v4_<-,(L ( Grid Lo:::2.cto:1 L(7 C--d '-:--.·'b -S<=~.;cl t;u::b ere C. J J il o 1.. •::---= C::o :-1 S::'--=-::-. _C_:>_::_::l~.--<f".-'.S"~-O--------A;,;,2_2._,:-2_e_c_2 _______________ _ ----'-------~----- s = '? -OC I -- ?:.:::..,.:=.: ~:CST ?O=\ CO::STITUEliTS OR PROPi':?.TIES ::.::.:.·.-:;:·:_,_::3 SEC7IO:J, RALEIGH N.C. _;_3 E; m_y Ca=boa Dioxide....... og/1 -------- ·: :-,2. ~::-:Ld"' •..•••.••... ·--~\ ~:i~ ___ rq,/ 1 :.:-::.:.:o:s,. (Tot;sl ill').. /100=:l ------- =~=-::.2s.s, ~=~~ ~ar~onate ..... __ ~4~®--cg/l --...... -. -· -· -. . . . . . . . . u~:/l -------- -~ -.•............•.. ________ C?, / l _ ::_ ::_::.;,_:_.= .....•......• --~~;: -------- --=---.:.._-.............. cg/! -------- Ni:::-ag2~ :;.::j 2ld2.}-.l ... -......... _ mg/1 --------' ~it~at~ & ~itrite. s~ecific Coniuct~~ce (~co:i!-tas 2.t 25°c) •. · og/1 ug/1 -r..g/1 r;:g/ l ------- Sil.:i.c2.. ..... ---.......... .. ng/1 --:-----.: Dg/1 Sulfa~e ................ . o.g/J.. _____ _, ·zi.::c. -----.... - - ---....... -----..: ug/1 C2.lc:....:2. -.... --........ -. -------· DZ,/;_ r:.2/1 . ?..~c.:-;:s: L C 12 C C r L_ ,-- L .-L ' L._ C [ C [ It I I I I· I D D E I L I I 1\0r!HI Cl\iWL P./( DIV! S lO/\ ,· 'P,\RTl".:';Nl o.=-NATU?...=..L ?.CS.'JUR.Cf.S r. co.~MU( DE'.'ELOP~.c.•ff ·,;.:: LL RECO;{D EN'IIRQ::.v.E~H;..L :-·.;,~:;.~:,:~.::~IT~ GP.OU~:o·rlATER _,t:;CT!O:-. 276Z7 -?.:..t..El';~i~ N.C. 27611 ;)_ . Wf:LL co:iSTRUCTim! rr.rt'HT NO. ' ;.~:.!. LOC,\TIQ::: (Sflow sketch of the locatio:-i b!!lo·,.,.) ~earest To...,n: __ ·772.L__;_,<s,~c:;-:c.:;rJ~L~';-;r.,,_,M,c'.c,,___.,.c=c_ __ --"4'.'-'/'----c__,="-----Cou~ty: ,--1, 1.? .,,.,~,. -c?,/ ---;.¼,'\_+=~:-'-~/Z""'J~~-c/~J~3~J',...-~--,.-,--,-,-,-:,.,.-;-----Quadrangle No. _L_.=t,c._7.,__G--=~'7'--------(~oad,Co~muni ty or Su~division and Lot No.) ·.2 .. c•,c:sA, /th s, -[, _;,.-1,?--,c"---" .>RILLING LOG ~ ,-z.,/(/f?; 3 Tt2L2.c....L , •'-" <c. DEPTH 1 71<D:•~ TO . -. . ':CPC-3? ... :),PHY: draw,valley,slope,hilltoy,ffil}ci:"clc o~e) 9-/o-Sv 5. COE:S 7HIS h'ELL REPLACE AN EXISTING WELL? __ ~j{.?=_c)c.-_ 7. :O?;..L OE?Til: ,;,f-' RIG TYPE OR METHOD: ~ :. • ':O?Y..;..",;-'!0:1 SA,\IPLES COLL~CTEO: Depth Inside Dia. Matc:rinl YES Wall thick. or weigh:./ft. Method :":c~ to ft ______ _ Depth Dia. type r FOPJ-1.ATiml DESCRIPTION i (z/:!J c/, c9 en,-£ °'-~. -<j_,.,.-«-?r:,"'-1 e.') c,J-J'o,.,J! It ac:d1t1onal space 1s neeceo, use bac~ of form LOCAT!O:; SKETCH :":c:-:: ___ to ___ ft ____ _ (S:':o·-· dis:::a~.cc to n·.:::.bc.rcd roads. or o:::her t::ap reference points) Depth Material . ~•"iI"::'.i...D{gp;n) :. ______ Ht:TIIOD OF TESTING: ____ _ ?.::,_·.,_'5 c.J ~-S.j/L... : ~::i ~.-;:rc:,y c~~·ti ::: :::!i-1·_ ~~i~!~tic:1~ ancl Scant!~ ( ) I . ______ ---,1 __ __,l_,Oc:co':'..c~/. ,J33 DEPART:·lENT OF NATL1'-AL AND ECO~:o:-nc R.ESO[?..c;:s ,· ,-( GROlfu'DHATER SECTIOci · ( ,.:;:e:: /?i.,,_, !Jeio t:, d-6 D"-t" Drilled Elev. __ ft. .. 9-/o-fiJ c.bovc HSL lcctt:iue;s ________ Elec. Log __________ Ga= log ________ _ I Description Dev.th (f.eet) to D I I Thickness (f.eet) Or----~--------j------jl---j----1 __ _ I I l I E i I I ---I I f -<'---,-----;::>. (~ t 0 E / I I ~uc]. c:2,Jt. I (~n-, -//co.u I I I It I ·-----. L I I , -I ~~ou~a~ac2~ ~2c~~o~ I I I 0~ ;,<-.. Ir~. ·-·-- u-K . .,,.,-. ~ t . .;,__:_\:2.li.iity (As CaC03 ) // to pH 8.3.......... -:::g/1 --------[ O? ::i 4. 5 ...•..... {e2G cz/1 . • . I I _-_-:..::::::;.::._r-.:: .. !::::! ............... ________ ug - _:...= s :=:!ic. . . . . . .. . .. . .. . . .. ug/ l -------- ==-=~~;s;~r'.:ion2.te..... L { sg/1 ---~---- ---· · • • · · · · · · · · · · · · · · · uz/1 -------- -=-.c --• • • • • • • • • • • • • • • • ,:,z/1 --------. _. -·--···-I, - - - ___ .__;. ••••••• ♦ •••••• ________ "...!~ ,. ·:..c.c.;;~:12s2............ i.:g/1 -------- · · = _ --": •••..•••.•••.• ________ ug/ 1 C,...]fiJo2.1 i;i:::::Jgea i::j e,lc!2.hl .• -....•.. c.g/l ______ _c ~i~r2t~ & ~itrite. Snecific Coud~cta~ce (cic.:-oci:10s 2.t 25°C) .. Silica ................ . ng/1 l.!.'(,/I cg/1 ~fl ------- ng/1 -------.: SoC:it-=:! .................. .. -------C r::.g/I r2g/l. Zi:-.~·················-----~ ug/l cg/1 -...,g/ l L lZ: . Es: C ~ 1::::: G: C r-t .......... ~ .[2 ~ [:: c= L_ 1.-----------------==== I£=~ ~ C '. : :-. ~I. I,) . \ t1 ,Ar ~,7 .. F I I I I I I I , g D D D D I ·.::.L•-RECOiW (__ D!VISIQ~I ( .r OJ" EN'/TRON"E'/TAL .'";,,:,;:;!::'',ENT, G~OU/~D',.'AT6-n SECT 10:-.J P.O. BOX 27637 ?.ALC:IGH, ~LC. 276li( (_ .f~G. ·..:o. WELL CO:JS".i'?.UC?IQ~; PC::?..:H7 ~,o. #:9 1. ;..;:.:;L!.. LOC,\'iIQ~:: (Shol-f·skctch of the loC:ation bdo·,;) Q ?,:ea.rest To·..-n: ·---z:2...,,0(..; -f-M 1-\.11..) rLY (. County: _ _,,~~-/,-,:_:_Yc...-(_'....:c='-_jo.c'._,,,,::....~l"-"£"-·------_...,,c,s,__,✓.+ ___ :,_12.J,=,,_7 _ _:1,,..,_)_-:>_,_, ,_,,_? ___ ~-,-,-----Quadrangle No' __ L _ _,_(c,-,~7'---'<l=-:../_:O:c__ __ (~oad,"Eor:i..':"lunity or Subdivision and Lot l/o.) .2, o·,c:s,,_~b.:...c../A,_,· /t--c.=_ _ __,L~_s,_· .,_r'+(~cc.· lc,,Dc.c,.J ______ _ '3' >c)Di\£5S' IZ~I-I(/ &✓ 3 ,\ c) T ,<,o.c,j{, DEPTH FRO'•\ TO '!'O?OCi?..APHY: draw,valley,slO?e,hilltO?,~irclc o:-ie) . 5. USS o: ~~LL: ___ £.c=~<'.l"'-"'"'~l'--·---DATE: · 6. DOZS 7MIS m:LL REPLACE AN EXISTING WELL? __ ~t,,~/~(~}~- RIG TYPE OR METHOD: 8. ?0?.:-'..;..Tro:-. SA.H?LES COLLECTED~ YES f/ c 15-u ""' so __ ..c'---'=--- Depth Inside Dia. Wall thick. or weight/ft. to ft ____ _ 1 C....-G~OL"?: Depth Material Method !'::o.71 ___ to ft _____ _ ,HULLING LOG FO?-~'.J..TlON DESCRIPTION It aco1~1on~l space is ncecec, use nacK of torrn Dia. 'l.'ype & Opening Fron ____ to ___ f t ____ _ LOCATIO:: Si>:ETC:! (S~.o·-' dist.ance to riu1.-:\;,crcd re::!~~. o: orr.e::-c~? r~fcrcncc poir;ts) Depth size Material : ro::i ___ to ___ f t ____ _ 1.:. S4A7IC ca.sir.; 3 ' ,, 1·1ATr.:~ LEVEL:~ ft.~,ve ~--2f:::::±::s -~-· '-..?( _ _. is ___ ft. above land surfcce ELEV: ·r57 YII:LD(gp:;i): _____ METllOD OF TESTING: ___ _ -:·&;-PU:.-.?1::G WATER LEVEL: ________ ft. l-h--CP.LO?.!:~,\TIO:<: 7y,:ic _______ ./\.mount _____ _ 19. 03,\':'Z'.-{ QUALITY: (/,-.___ t./oo TE:MPER/1TLlKF. (0rL...f___C ·::y~c _______ Capacl ty ______ (9pr:1) llt' ___ _ ~•.a!'.c ____________ ! 11 take Dcp the._ ____ _ z-;;::-::,\S !P.== m:::F.P.· i)E.1:.:-; PROVIOC,D COPY Of THIS R:-~cOc<D ,-..::ri r:ffORN[D OF T;:E D!::P,\~T:-:E.:~\"'J'.S RF.QUiiC:•'.t::rrs 1\:--iD p..2co:-:.:.::.::o;-:r 10::s? "· ?.?.:-,,.,o:s_. '~~ 2.--'-----~----'-----·--------'------::. ~o ~!.:!"'2::IJ C..:!!"tify tr.~t thi!.; ~1-:dl •~·ac: co.:s:::·,:-:::t.t·C i..1 .:1cco::C!a:~c,2 ·~•i.Lh ,:.c. ·,-:c:Jl Co:1:~t.n:ct.io;t ?.c;uL!tio:,s ,1:,(! 5canc!,,.rc!s .:rnd Ut,Lt tili.o; ·,1..:::1 1·-:!con'. i..s true a:-,<! l!Z<1ct.. il/3/7"/ r· /o I I GROi.fu'Di-!A'.!.'E?. SECTIO:-i ~~~ll (·io. =·1f9 Field ___ _ Office ___ _ . uses_--,-__ _ . . d . ' t1_1 Driller 17. . ,,::r:w.z &< Da.te Drilled d Cased .'Co ___ ft.; Elev .. __ ft. Description Thic!<.ness (feet) -,-. -----------'---'-'-----,1--.-1 -;...! __ _ I I I D I I I D I I I .1~,=;2-It~ -, -f 1_,::r:I. :3</ / -1i::-~, I ·1, I -/--/1>0 IC ------- I I i I I L l II I I ;>--______________________ Odo,:-__________ -:--------------,,; 6 5;--:.:-::. Co:;,d. u Appe2i"~ilce __ _,.___ __ -0----~------~-----------------• 7=? ·--~-----C '.i:asre, _______________________ _ ?:.:: . .'.o:C: :;::sr ?OR CO:iSTITUEc,1S OR PROPE:?.TIES . .\S iSD:::cx::.':D. P.Z.?ORT .01:_.;r.Ysrs TO: CHicF, I sc:crro::, R.U.EIGH N.C. , __ _:....:.~i.~~2............. ug/ ! --------:-= s 2 ~ i c .............. ________ u g / l C~=boa Dioxide....... ng/1 -------- C~l~rid~ ............. _~f~Q ___ sg/1 :.:-l:'.co= (Total l:!F) •• _______ /lGO:-ol 0 -~--..... .. . . . . . . . . . c:z./1 -------- It ::-::: .... :..,,• •........ - . . . . t__;g/1 -------- r,.g/1 L r:q,/1 C . !2s= Phenol .............. . cg/1 ------- c.g/1 Po t2ssit1..2 .............. .. -------tc;!;! l Soecific Coni~cta~ce • 0 (ctcror:hos at 25 C) .. -------Silica .............. . ng/1 -------.: Soci.i.t2 .......... -.. -..... . -c.g/1 _____ __, ng/i.. Zi;::c ...•.••....•.•.•. -------· ug/l □,;/1 Y2.gr:esfc..::,__ .......... . r-.g/1 ------......: C ~ L ' ,-- L ,-- L C C C C: C E==-==---==---==---==---==---==---==-==---==---==-==---==---==--===--===---==- - - = = - = = ~ --_ -_--~==--== ·-.0 :.0. c:;,-0.?_T,\o USE I,=='.,; ·-9-;c-ft y_ ~:, . .: .. i • J <'·~ y '-I ]3 {! I ~T":.,c~c·,"c"_' ,r-r'T:::_,---.:...,:,_.;..;B~•~C=;O:U::;N;.T.:_.:Y;;.:N.:.;:A~M:,:E:_,-'-,..;...;:.....;_,--,:::..-,._;:;~:?;.._::;:::..l,:,-.:.• ... c j "- NTINUED FROM THE FRONT \Rlf~ l . ~~~if} :-,';!bl~":~; 11-i,Sl!coNCb~.:; ~f::~·t.i~~·::\~{f-'r-"'A;!:_1.;f_:,?Jf'.i:'? .. 1·-.<'. (specify) -•· ~ -· .• -:t1;;.!titI~i~<'tr1.:;~t;::-i.;~\?i1t~=-.,~-<i-_H1 A'~~~;;7:4~i~~~~-~4}}fi:{:.t;(ftJI;lft•~'1tr :-11:.~:Li_;i12;,:lit:i.~'!J.,. ¢;_~au ~J~i;;f~r~;:::,;}r~~::1it~*:?:ij (specify) s: -····'.. . ... , ....... ,.,,. -·-~-~-,..,._,-..,.,. .... , ·"·~·-~--- : ~j,~~"~:,:~;f~•:1tt7;~~!-~cl-~.~~~};~~i:tf~0~~- 'rJi!ff.4'1.&;it•ct,t/_!;J<11lin&1i!!if~ofi. . _ _ ~--~~~ .c-·T · 1• 9;2 u ii'; C \\ < I I ,Xllll,CEJ'!J"tf.lCA'tlON-{m/~, A, NAME & OFFICIAL TITLE (rype or print) B. SIGNATURE C. CATE SJGNEO I I I Please print or type in the unshaded areas only ·(fi/1-,'n a1·eas are spaced for elite type, i.e •• 12 charactersliC!._,.ch'-"l ... _____ _,-,--,,,.,..,--..,..,..--,,,..----- FORM , . • U.S. EN' .NM ENT AL PROTECTION AGENCY'. 3-..... .·~ED .. ·"·· .. ' HAZARDOI.. _ WASTE PERM ITAPPUCATION' ,, rJ-'\ Consolidated Permits Program- RCRA . IL FIRST OR REVISErnAPPLICATION· Place an···x~•·jn the appropriate box in A or B below (mark one box only_) to indicate whether this is.the first application you,are·submitting. for. your. facility. or . .: revised appliCBtion: If this is your·first applicatlon·and·you already. know-youc facility's-EP.A 1.0:.Number, or.-if. th\s·is·a revised applicat\on,.enter:your. facili~.•.s: EPA 1.0. NUmber in Item I 8bove •. ·· ~-:::. ::;~~'-::t\ ' · · :·~--:•:: ·. -. ' . , ri 2.Ne:vi, P'~~I ~ITV·. (Comptef~:tt~m. bf!l0~.1 )\.;' '-Ji:!, . ·· ' . : ·.· FOR NEW1PAC1LITIE1 . . . PROVIOE'THlrDAT~ A. FIRST APPLICA-TION (place an-. "X.' -b•low-and proulct. the·appropriat• data).a'·:: E8J' i~ EXIS~ING_ FACILITY._-(SH j;,.tructton•· for d«finltion of',.exUtin1,:' facility:.'.· 71 -::-.• :: Completa·it•m·b•lpw~h ,. · ,-,;-:--,-,--:,;;c,r,,:-:-:;,-FOR·EXISTING PACILITIES; PROVIDE THe: DATIi!: (yr., mo:, & day) (yl".,.mo., & day). OP.IUI:. I 'OPERATION BEC.AN·OR;THl!t-.DA~E CONSTRUCTION-COMMENCED, TIONtBS:GAN OR:ISt,·, (IU'!·th• bo:ces,to-tM·left);'-:· : .. ->~. :e:xPECTED TO-BEGIN H,1-1,,.,!,S.d,~!-'Jf;;i,!.J.:Y,.~~!,i.:r,ci:c:c=C"'""',.,::r;:,::-:=,;::,::=:::;::,:e,;:=CT:.::::::::;:----:--:c---:--:,-l'"'-.li' U.Ll!,-"C!..UZ'-!'-"'--,--::,:-:-c':'c-::,::::;-:: □ . M ,-• -• • N,._rpJac.r ~t~~,.;.,b~~~w~and·co_':7'~~!/•·Jte":':.I a~b?ue).:_::,;: .:□•.;. · •. ~--., F'A. c:· ·,:;,T··:., .. -.-·H .. ;_ .. A~.• .. ,R·· .. cR·:',,."{P·~_."·.'RcM:_: .. ,·.T;':·.i.fc.:.;.·.;.~;·•I·,·•·i.,.'.:.,·.f.·::. I I n D I I I '71 ~-.P'ACILIT-~ HAS,l~TERl~."~T~~us~~)'L ::-. ····'.::<,·{:·:·. ·.· ,'. .,·: ···:·.:-.. _;·· ._ •. ~-,,.. _ , III'. PROCESSES'-CODES'AND,DESIGN:cAPACmES' · .. .. :,: • . '_. ... · •. ' -~--~• .. .-i~,., ... ,~:-;::.,·•· '1• .. ::-· .:?~ .. :.':'· .. • ··---'.'.i .. ·., ·.1-. ·-·:, '!' ,;· :,: , , • ;; ,. ,. •. ,, ' .... ·-··-~-•r.::'·' , .. -~:··-· .. ;;~·.' ·-:.,:.; ;. -~·· · .. •._.,.,:><.•:"-:·-, ~--• =--A. PROCESS cooe:...:. Enter.tha·c008·frorwthe·lilt'of,procesa,codes below that bert describes each·procesa.to be-used•atthe:facillty::i.Ten.l1nffare-prov1dadifor:·• '· entering codest. If. mor8 • II nerare-needed;. entei· the code(&J; ii,. the• space· Providect ·: I f-a-proces:s . will: be--. used,_thaf" is-nOT" inctud&d-'in ,tha _list of; codes _bel_OW,1then ~ .. ;~ti~~i~~~~~~~~j~~~,f~~~~~~~~~~ijf~~!~~~~~f~~~£gt~~'.tifr~ll~ {.\,~·'.·U•NIT.OFM~ASUHE-Fo~-•mountanterad:ln,column·.B(1),.anrerth~~.~-~•}~?!;"",~~.~~-~(~,~~.~~~~-~~~~h .EXAA.11'~.fO.R ~P~E!JN_G:1~•-1~1~'pi,~~:!ir}f~.~!Jiin_)f;,"!:}'~t;i_-><_:?;_!»!__iiWJ:fA;~l.ity;~8$,;~.~~~~~~~0ksf#!'i~.f.k~ciuj(_hC?_ld-~·:ga.l_!O~ ~~~itb_~, pth~ can-hold ~-gallon~Z:'·~:~h-~,:_al~_'~~1~~f~n~t,~~~t Cf:!n:~r!!~~~~~-~-~!!~.1!•:~-~o~~;:t:.~ .. ~.'.:t~?;:.::~-]P,:J::;ff;:;_~t:~~1t~,;.:{~'.f'r7ft:.: .... ~'):'P._-:;.:.,:,:;·{'!/'Pt~~-t;~':': " ., 1x-1so2 X-TO 3 600:<\: ··20::::.:; 6 7 2 8 I 3 9 I 4 10 " 11 1• ., .. .. " .. U 19 ,, .. .. EPA Form 3510-3 16-80) PAGE I OF 5 CONTINUE ON REVER Continued from the front. III. PROCESSES continued) C. SPACE FOR AOOITIONAL PROCESS COL INCLUDE DESIGN CAPACITY. - OR FOR DESCRIBING OTHER PROCESSES (cod~ .·04"). FOR EACH PROCESS ENTERED HFRE .. I I I I ··-A.,EPA: HAZARD~ ASTE NO (enter code}- -e:.EsT1MATEo:ANNUAL. gF~"~!.JC-----------'-"---·-·.;D;.::.;Pc.R:.::.:0:.C::.:E=S=S::ES=:.'·-·_-_•_..:•~:.·_· ________ _ . SURE (enter- codei 2.. PRocEss:DESCRIPTION·, (lf a code·U,no~ entered ln.D(l)}: QUANTITY-OF WASTE~. X-1 K 0 5 4 900:- ·x-2 D 0 0 2 400 X-3 D 0 0 1 100 X4 D 0 0 2 ....... _ -·--· p p p 1~ PROCESS·CODESi (enter)¥ T03D80 T03D80 T03D80 \ !... included with above .• \ hi: I . z. __ o _,z· r ... ·., r,_. --D• ., ···i--. -. .. , ~---. -.•. . I'\ I/ , ~t: I I I I I I I ' <:) " .1 ,.,... r fl~ I 2· ~\;. I I I -, ' ' ' I , I I ' I ' I .3 '4 -: ' I I ' ' 7 ' I I 7 ' ' I I ' I s: _7 ' ' ' ' ' 6;- I \}, 7 ' ' I ' I I I I I ' I I I I ' I I I I . I I I I I I I T ' 7 ' ' : IL < ·" ,•;••. ;'12 l ---, ,---, ' ' ' L ~· . I !13' ~ .. I - • ;-i.'!", :"14' .. 7 ---, I ' ' ' I I ' ' I I I 'JS'. :::- rfr;; I ' I I I I I 7 7 I ' ' ' I hi I I I -, ---, 7 ---, ' I ' ' I J8:. l'.'.. • c:J 9' I I I I ' 7 I ' . I 20 I I I 7 7 I ' ' I I I I ' 7 ' ' 21 I 22 I I l 7 7 ' I r 7 ---, ' ' -23 I --, --, 7 I I ' 24 I 25 I I I I I ---, ' ~ 26 I I I I I I -, - EPA Fann 3510-3 16-801 CONTINUE ON REVEAi PAGE. 3: __ OF 5 Continued from the front. IV. DESCRIPTION OF HAZARDOUS W. "ES (continued) E. USE THIS SPACE TO LIST AODITI(. .. ~. All;existing·_facilities:mus :.VE· PHOTOGRAPHS I I I I I [l,All"existing; facilities•must .include photographs· (aerial. or. ground-level) that clearly. delineate· al I existing structures; existing storage;:c",•si:, ·. , i i;'fr8a'tni8'n~a0d.·diSPOS3V3f'etiStand:SiteS:Of:futU-re·:stora'9e;· treatm·enf or disposal·areaS·(see' instroctions for more detail}. · . · -. -~ -Y/::.,., ·. '·"::~ ;vlli:FACILITY:GEOGRAPHIC LOCATION, !VIII:.FACILITY,OWNER•·· f.{'g]\.;,\.~1t:tfi; facifftv··.omi~tis:a1SO thit-facility,operatoi':es !isted.iri:Se<:1:iO.n:v·1 I r-on~-ForTTI-,t:, .. General.Information'', place an "X'.' in the.box tO,the-left·and· .. f ;fJ~1i1i~~!+f~;gJ~:2:t.·;:J;~~ir:t~;il:t;~~:t~~;·:\;·;1:;i;;,tL:l!~~:,1::{,,~'.~~:;-Lm,;_ .. . . ·· · · ·•·• ·.·.··•···.·•tt·\.:"1 ,. ,._ NAME.o'P"'FACILIT:V'S:LEGAi.;-owNER•:f:l : 2; PHONE.'NO .. (area code & no.)· .LJ r. 'IX. OWNER CERTIFICATION· /. /.certify under penalty of.law thatJ;haveper.sonally examined.and am familiar.with·the·information:submitted in this and all attached. . · • ." documents; and;that.based.on my. inquiry of those·individua/s-immediate/y responsiblelor obtaining the information, I believe thlTt the·· ' submitted. information. is·true; accurate) and complete/ I ·am aware that:there are significant penalties for submitting false informatioff; ~.incll.lding:the possibility Offine·and.itn,ii-iSDnment.: ~· .: . · .. -' _ · · ·· 1: : : ., : · · : •, --· ,-. . .. . . A. NAME (print or type) B. SIGNATU!!_g C. DATE SIGNED /-eu r l./ Jj S_. Jc. /',o,'PJ -S::: ( X, OPERA'FOR'CERTIFICATION , /. certify under penalty of law that I have personally examined and am familiar with the information submitted in this and all attached ; documents, and that based on my inquiry of those individuals.immediately responsible for obtaining the information, I believe that the :· ·submitted information is. true; accurate: and complete: I am aWare that there are·significant penalties for submitting-false information, · including.the possibility of fine and imprisanment. A. NAME (pn·nt or type) B. SIGNATURE C. DATE SIGNED ! I I .f .~· CONTINUE ON PA I . , . .:~nMue·J ·from 'paga 4, . m V. FACILITY ~RAWING (see page4)' ~ j.2. L6'J s J 0 , F + !I 1, ,I I . 11 ' I .m D I I ~· l . -~ ~ 11 ]Q Lan, 60 L•ll.f~ I > "' -.~ ,_ 12 U•~ 1 [ ' Ii 110 L On, -~ ~ ~1 \~ I ?O L••z ti ro ~ I I ~~~ ------'-~ "' LO•) ~ Form 3510.3 16-80) I ii ~-"'r I 3 O 11 o~ 1-"'2 ---'---LI ___ I ______.I~ OFFICE -J. □ Oou !,JO Ff PAGE 5 OF 5 Form Approved 0MB No, 158-SB0004 .,, .. -1~·· ... I·,.: . '', ::;.. IJ[f 1}:'· RETURN TO: 0 0 0 I O 2 PAULINE ANDERSON u. s. Environmental Protection Agenc.,yrc-lVED Consolidated Permits Branch he ·-1 • 345 Courtland Street, N.E. [Pl\/f-;EG!ON IV Atlanta, Georgia 30365 , r JUL b Er' I r. ': !\' '' •: U C" • \ 1· V l ~• r_; · • '--. · : SECTION 6@°ro'7~/:R~ QUESTIONNAIRE 1. I have reexamined the definitions for treating, storing or disposing of Hazardous Waste and I wish to withdraw Part A of the permit application. Yes ,.....--· · No ---- I ".~•:: · · 2 I have reexamined the definitions for treating, storing, or disposing II('. . ~!t~~::~~~~-Waste and I wish to add the TSD activity to my original ,. ::f¥ I Mv--i:td(!J4~t.e I.,.. . -~~ . Yes ----No ___ _ /J6]) O G ;2_,S:b5 7 9-)__, /3. 4~ A. £Nf-t~~~,'sc"7 .7,.;c, ftt /Lf · {bD\l 3D0 5-f-rr ~e,_s y/ J ! I!-All .1.g (, 77 . I . .,,: ur:. I m}\ I ,,;; I "-- . "'.,.,,,o ~ :.; ',,, :J -~ i t S;:i'i;2 .; UNITED STATES Ei~VIRONMENTAL PROTECTiON AGENCY "i;._ .._:::-:- :.,'l(pJ.iO\\..:..' REG!Of'-1 IV JUN 5 1981 4E-CP CERTIFIED MAIL RETURN RECEIPT REQUESTED 3.:l.S COURTLAND STREET ATLANTA. GEORGIA 30308 iiCD0G255:) 79~,A-A .. /-/._ f.~~r f rts~ ~,.he.. SlGiib?, 5i.:.t'l;....., 11.1,., ...,c,.,lc:!:: SIGMON MARY bDGKKSEPER RT l'l ll_OX 3:iO STATESVILLE NC~B677 ·---·-··-··-··----·-----· ------------ Re: Section 3007, Resource Conservation and Recovery Act (RCRA) Request for Information Dear Notifier: Our records indicate you filed a notification of Hazardous Waste activity pursuant to Section 3010 of the Resource Conservation and Recovery Act_ (RCRA),.42 U.S.C. §6930. That notification did not indicate that you _either own or operate a facility engaged in the treatment, storage and/or disposal of Hazardous Waste. However, our records show our having received Part A of the application for a permit to operate or continue to operate your facility . . Pursuant to Section 3007 of RCRA, 42 U.S.C. §6927, you are hereby requested to complete and send to this Agency the attached questionnaire in order that we may determine whether your application submission was proper. If we have not received the completed questionnaire from you within ten (10) working days of receipt hereof, you may be subject to appropriate enforcement action. If you have any questions regarding this letter, please contact Pauline Anderson of my staff at 404/881-3446. Sincerely yours, ~ A_cting Direct Enforcement Division Enclosure (1) cc: State Director .. I I I I I I I , I I I D O'i. di. di. cnte~pziJeJ, 9ne. Sipnon Septic 7anh & 7'oot eompang Route 14 · BOX 350 · STATESVILLE, NORTH CAROLINA 28677. (704) 873-8954 1'~\ I"' ".:'.".,_ ;i:?. a' April 19, 1982 "" i:: APR 21 1982 ~ Bill Myer Department of Human Resources Division of Health Services P, 0. Box 2091 Raleigh, N; C. 27602 Dear Mr. Myer: ,,.. .._ ........ ~ "" 1 O April 13, 1982, A, A. A, Enterprises, Inc. received a letter from the Division·of Health Services stating , our Facility I.D. No, NCD062555792 has been deleted as a generator and transporter, We do not want to be re- moved as a transporter. MLS/rs 2eport io: O,\ TE Tl i'.lE PURPC)SE: 8/\SEli NE;• C01'.1PLAli-!T, FlELD AlsJAL YSES pH,: 00 :.~ ·?: ~:L-spec_. Cone. 94 ~~;~~ ,:) a; L •\BORATORY ANALYSES 80D5 "0 mg/I coo HiQh 3'0 mg/I coo t.ow 335 r.-,11/I Colilorm;MF Fecal 3 16 16 1100ml Coliform:/AF T 01al 31504 / 100ml .,__ TOG 680 mg/I Turbidity 71> UTU pH 4<;)3 uni ts A!:.C.alinity !O DH 4. 5 '10 mg/J Al~alioily 1:, 1,H 6. 3 -11:, mQ/1 Ca1bonJ ,,, ,. 4 ~ frlQ/1 Sicar!.ior.ate ·1 40 mg/I :'{ Arsoni c :T 01a I 1002 -(· ') ug/1 Carbon dio~lde '°' mg/I \\ x Chlo:ide 9'0 , , mg/! ,', Chromium:Hox 1032 ug/! Color:True 80 Pt,Co C;anidu 7 20 mg/I G\'/-5t._Revi~•.::o' 7/SS 2s0 c ,- Owner Location or site Samplinq f·:ie1hod Remarks . · · ,; ·, . [c ire I e ( ::-,j;} -, (pumping time, air temp, etc.) Diss. Solids 70300 mg/I r .·•( Ag • Silver 1077 ug/1. Fluoride 951 mg/I H ardness:T 01a I 900 mg/I Hardness (non-carb) '°' men··· X P.rienol s 32730 (/ uolr . \ I Al • Aluminum 1105 / ..:,..,, ") I';/',,·) UQ/1 ",0''-J-------'--,s,c;,3-yCl,!~.L,:::,:_j \~~I··' Be. Barium ·1001 / uQ/1 . 1·~··-+-----~·~' -""'-'-· ·2_) ~ ~-"4-/. Ca Calcium.916 Ct) mg/I i. c·c_-+-'--,:,,:_ _ _:_c:_:,c__~_ar-0'---=~ :<. CCI Cadmium 1027 .. =: ,//) u,;/1 Specific Cone!. 95 uMhos/cm? -./ Su/la111 945 : i moll~ Sul lide 7'5 mg/I K Potassiu,ri 937· ,,..?;../ mo/I Mg Magnesium 927 ':::/(,··mo/I Mo Manganese 1055 ii,, /)I) (")UQ/1 u .. Sodiurn g29 / 0'"/ rng/1 NH3 as N 610 mg/I "' Nic;..e1 1067 -L:.' ~ {) ug /I TKN " N 625 mg/1 PO Lead 105 1 .-:J I (,) ug/1 )</ N02 ..-N03 "N 630 -· ,, mg/I , .. , -'-i~ ,. Selenium 114J -:..<---:: ug /I ', P:Total " p 665 mg/I Zo Zinc 1092 J/110 uo/1- •, For Dissolved An2!/;;i:; -sul~:-:.il fiitcrct'. s:,rnplto 2nd write ·01s· in bluck While copy -Hcadq:rnrters Pink co;;y -Region• Yellow copy -Lab , Organochlorino P,HUcides V 0 rg a no ohos ;i h u r us Pes:icides ·, Acid Herdicides ).: Base I ~,e u 1 r a I E .irac1ab!0 Oroanics 'y Acid Exiracl.it>!o Organic$ .J Purgoable Org.inics (VOA bol ti el •,/ u Oib,omocit,ano (EDB) y' /} ,, ,, ,,, ---, ... ,-: : ., , ' y .; •..._ ./ I ,, , -1 -.• ,,e,S I -d.,;:Q ()\<.l..."l ,..,,1'" r' p;\\f ,c:.\S ~\:..'r ~ -f'_\sl"~ - -N D I) Checked by 8J._c_ Superviso~ ORGANIC Entered ANNx~ by,-,,{~~ 0 Lab No·. . D tG--1,,n\ D D D I D ~ I D D D n f- f-... -, __ f--0 I I ' f_._ I : -- ' [ __ L 0 Iii o.,..I Checked by~ Sample Type /, '~-+,;' Analytical Results n. '" o,+, ·, '·J ,a 01 n Q-o , YO ,A 0, ', G C / t=Pk) ' " Tur lo"\OJ'IT< ·r I,~ 0 ' JAo,.-tid A Ori --n ,,,, ,·~0 ™+,n ;n..o .,--n -In r-On ~ r-Vl .cl 0 I O A ,~c c=.' ' V /\,~ 'lrr-.Rn➔, rn (\\rJ r A. r f", no ~ o , to .o Q •• - V V r.:.c ~J 0 0 11o,v, ' Tin-Om An rrn,. ·ln,, 0 rJ7 (\ .r; _o n Nt r-, ~ ri ro O , -W ' m n./11 n"., ,-/l ro\oto rfo JJ 01---<~ ('-r I M,:. . - t'u-r n r ,· ,Q ~\On I'°'· ; rlQD cl. o-9. Q ,:!l2 d ~-S"-<'.JF.f.-" . 'I ,. .· . J A. .1 l•t·u,f .. 1,,_,,_J,,,1./'~•?:• ;/:;--:;: ~,--J.r.,-,J'(,. --. (, . • ./ ./~,/~,,.✓/( v":· '' ,,r)<•-,s,-/, (_,;r;-_/1__,•, ,,J . .L, , .. ! "2.,(f.J,;;,1~-. .t:;"'9 {,'. / /,;;_./· ,. .,...,,-:.:-~.!.{/ ,. , .., '·' /:' r,;,' ✓/.--.,.,::,,/ -·· :e -f'~.J--<~ ,:; . .' ~~J-'.. _. _j:~: .. ~r /..., /, .~ ·' /,/.: -~-f,{--:----.::a',r._,.:: .T,, / C/HS/DS •.wed Concentr3tion ------{ q.wner <,·,.. PH400 • .(r,,Z 0 soec .. Cond.94tk_£, ~t 2s0c v .Location or·•site Temo.10 lb . 0 c Odor .Aft.117'<-- Appearance ✓o/t.Jjj...,. Ta~te :.,..-,//4 .. _' ( . /~ . /I. ; . Field Arlalysis 6y:·-1-. r~l~ LABORATORY ANALYSES BOO~ 3 1 0 rny/1 .Coo H!gh ·3-10. mg/I coo Low 335 mg/I Colilorm:MF Fecal 3!616 / 1 00ml Colilorm:MF To1al 31504 1100ml TOC 680 mg/I . Turbidlly 76 rnu PH. 403 uni ts Alkalinity lo pH 4.5 '10 mg/l Atkallnl!y ,o pH s:3 4 1-5 mg/I Carbonate '" mg/I Bicarl.lonaie HO mg/I y Arsenic:Tota!" 1002 -< ,.?n ug/1 Carbon dioxide 405 mg/! X. . Chloride 940 .1-.(t mg/I Chromium:Hox 1032 UQ/1 Color:True 80 Pt-Co Cyanide 720 . mQ/1 Lab Comments: G\V-5,~ Rcvis12d 7/85 / 7 (pumping lime, air temp, etc.) . DI ~s. Sol Ids ·,u:iuo my/I Fluoride 951 .· mg/I: .• Hardness:Total 900 mg/I .,. Hardness {non-carb) 902 mg/I· y P_henols 327 30 -, ug/1: .7 ;/. Cd -Cadmiul'!l.1027 ·...:::: /(). UQ/1 Specltic Cond. 05 uMhos/cm·2 ;x Sulfate 9'5 C-j mg/L;, Sut11de 7'5 . mg/I .. V. Hg--Mercury. 71900 ~ · -i / "~ ug/1 mg/I - . mg/I .. NH3 as N 6to p-::; . , : mg/I X /\!i -Nickel 1067 ug/1 TKN " N 625 ·.mg/I• Pb" Lea"d.1051 x N02 -t N03 I .• , as N 630 /.1 ~ ;_,--< _ lnQ/1 ~'"<'. S~ SeleniUm 1147 UI, /I · P:Totai as· P 665 mg/I X Zn ~ Zinc 1Q92: · ug/1-. . . r-or Dissolved Analysis -submit fillr>red sample and write ·01s· in block White copy -Headquarters Pink copy -Region Yellow copy -Lab I y 0rl)ilnochlorlno Pos11t:ldos >( 0 rg a no p hos oh or us pes1icides. , .. · x' Acid Herdicides x Base I Neutral Extraclabl_e Organics . y Acid Extractable Organics )•' Purgeable Organics (VOA bottle) ><' . 1, 2 -Oiolornoo1hane (E06l y {2.__,..,~, -rif':./1r . -✓ I~/,.,,.,,.,. ,/ ";/,. / . .,...,.,_ I • s~ '-'In-. ·•v-11 ,'_''YF,-, u/s A U,?,-, . --~o~ ··VJc~ . Reported by__,(..1.As.of-.T':oe__ I /J-./ r> Checked by n ~ -'--'-'---- Dace ,✓/ d -:j / 8 2, ·--=,1-=:..:_=-,1--=---"'----'~< .... \\ ·:i,. l)Supervisor<J12K ORGANIC ANALYSIS Entered, b~ Checked by.ml u D D g g 0 u , I I I I I, I I Lab No. -11 --\"':l_o~ ---·---... ~ .. \-- i ' -· i r-- i I -- ' ' ' r .. Sample Tvoe : l , --fl-n , Analvtical Results Concentration 'f\,y-,A", h ·; , · _j n ~ ,-Ji~ o -4/-n • a , , • c:,c / r-\Db -, u rn. ,_,..,,-,_-t-";,·_; \-o,,,, ,·,..10 •• -t,·, ,·o-" ' -0 /, °'.' r\n.;;7; 1 in J ' l.i V . -,., -L-.. ,---\n0-n,(m J 0-' . r::c I c ., ' " I I -i ,', ~ 0 ·-,-..PT (l. -~ 0 o. c.? 0.~.1 e rlo 1/-n -h, ,I 0, r::r/,L90 u +,,_ , , • • ; -' n · -\:-; 0 ; n _) ,-n~rh 0 -lo-\t-orTo J V 0' ' • r-.c / I _ 0,? u I'(\-'1 •• JJ ~-4-. . J n ,,.-,,(7 fl-✓-'\ ~..._ I ,,. ~ ,\ ()-1) 0 r -fJn ,rJ Oo -', f lj Cr/ /JTlQ '-- l Y,-• , AA·, _, O ,.,,,--!-·, ·, ,' O I ,~n -Do. rQ n Jo ,·-(.)-o _) .... 0,, <'Cl•~,- 'u ' · r .-,n , "--? n ;;-L :.. . 0 • .\. .. _--\) o _1 Cl.A.. <] , .. T\-~' ·~ h, C\_ !).,,.,-<!,., ,·,,_,,~ D n ", 0 n ()-,. A ,. , ,2. , , · :~--"4 i",; n-0 ~\ I,·'-'-" I e - , , --,' _Q n ~ -J. • 'n · n )I :¼ J.... IC• .r,((2 \J ,. .. :_IA"+,. ,·n fl 1\ -~ 1 '1,.,..,1 e \) 1,rv,;...11, -J.. i ' • n _j --\t ,/ I \ ,_._,--, I (2' V , . ,·A, r\ n~7,_i'o ,'n ,j \.\ ,-C-• 1 r< ,.~.., r c \J , , .. ; ,\ n 01-L ·,, . ;, ,9. -lt C 'l 'l .. U,A, Ip " /'y'!._ ()J •· ,Q _?,n nO ,{ ·,, ~lon r-9n--/. 0/.1:o -.1 Ou✓• ' cc le c ' ' ' GC/MS/DS •.ised ' 11!!!1 \·I/SRO, Ki"nslon EO Other _______ _ □ FIELD ANALYSES Owner cJ ROUTINE PURPOSE: BASELlr-JE, COMPLAINT, (circle COMPL! Ah.ICE, Lus;·' ~~ ()/.. .-L;,..,... o"ne) pH~oo --'--Spec. Cond.9 ,; =----.. at 2s0 c Loe a ti on or si to <.:: ,.:7 Temp. 10 ~/~/:~•--0c De scrip Ii~ n oi sarnp Ii ng poi n 1 __ ,,~·~J,_,,:..c! -'----'fc.·c.'-'·~,.--"'"~'~'------------------------------- '! 'vi ;,1 Tast~ --.c·~•,·~--;7_~;_~-~~--Appearance ,.d..,,..,.. ,'-' , Sa m pl in~ Me th od _ _,C:c,.);,. "'-'·'-'· lc,',""_s<_!./ ~----~----------Sample I nte rva I __ --z_,,~c.C.:, __ , ________ _ ··-r--(pump';" h~iter, etc-.) Fi old Ana I ysi s By: -~/_,~(~·/~,-~•~-•~J;~•-------Rornc:irks -~' c..C'"-''---~---_,:_. ~-:tr::=·~·-__ --.,C?_<i-;:....?"'-_'7,<;.-________________________ ~------- LABORATORY ANALYSES H005 3 10 mg/I COD HiOh J.: o· m (l /I coo Low 335 mg/I Co/ilorrn:Mf-Fecal 3 161 6 1100ml Coliform:MF Total 31504 1100ml roe 680 . mg/J Turbidity 76' !HU . PH. 4 03 uni ts ' Alkalinity to µH -l.5 '10 mg/I Alkallni ly ,o OH 8.3 "5 mg/I Carbonate "' mg/I Blcart,onate HO mg/1 · Arsenic:Total 1002 ug/1 Carbon dioxide 405 mg// Chloride 940 ffiQ/J Chromium:Hex 1032 ug/1 Color:True 80 . Pt-Co Cyanide 120· mg/I ,I (._ .. , G\'l-54 ,Revised 7/85 (pumpi ng time, air temp, c1c.) Diss. Solids 70300 mg/I ug/1 ' Fluoride 951 I Al -Aluminum· 1105. ug/! Hardness:Totar 900 mg/I Ba.-Barium '1007 ug/! Hardnoss (nori-carb) 902 mg·/'.·:t5. Ca 7 Calcium.916 mg/! Ph,rnols 32730 ·U\l/1_, Cd ·•Cadm(u'~ ,1027 :. ; · : _ug/1 ug/1 SpecillC Cond. 95 uMtios'/cm~. ..chro·m1.ufll:Tot~i" 1034.,:_ · · C--1---------~ ---------"'t;<-C-~4"---~-----~~-~-- . m·g(!_<;'.· !t~· eC~ -:,:~o·p-~e·; ·:_1·Q~ 2: ... · SulJato 945 . ug/1 ..ug/1 ; . f--,J-----"~-',-,'::. ,,-'-':: ,.-"'-'--':- . rrig/1 · Fe.-· Jrqfl--1045.-···,_..-,,;:· .. Sulfide 745 · ·ug/1 · --~g/1 .Hg ·_·,Mi:;,ciiry 7 190() _ ... ·· >---+------------!;: :K · -Potassium 93_7:.'. mg.II ug/1 N, SOdium ·929: ... mg/I NH3asN610 Ni Nickel 1067 • ug/1 TKN as N 625 mg// Pb ·L Gad 1051 · u?/1 -mg/I ug/1 . P:To1a1 as P 665 mg/I Zn· Zinc '\092 ug/l . ' For Dissolved Analysis -submit fill(:;red sample· and·write/:01s· in block White copy -Headquarters Pink copy -Region Yell'6w copy Lab Organoctilorine Pes1icldas Organoohosphorus Posticidos AciC Hordicidas Base/ Neutral Extractable Organics Acid E,trac1able Oi"<;ianics · '>{ Purgeable Organics (VOA bo111e) 1,2 Oicromoethane (EDB) ===~~6uw•'--'· .',,.,>+) ~I __ la ___ == __ · · ouAo r,o_i ~712.J'} SERIAL No:fl? !..Ji,7l LAT 7c l)-;(·-_··ot,LO'·JG.XO "Ii' "1')5"" --· .... . . ~ Report 10: ' ARO, FRO.{~ RAO. WaRO, WiRO,: 1/v'SRO,· Kinston ·FO Other FIELD ANALYSES D ROUTINE r:·/ - l.!...:i" _EfvlERGENCY "" .-. I ~ CQivjf\1 AUCE, one)--~ ·~-._,,._,, <:J ' ., iiiD PH 400 C:--:7/spec. Cond.94 b .5: at 2s0c Owner _.')_ ~-,.Y1<=: _, . .,:~-:,., tr. L9cati on o~r site .. C' If. 1 1 ,--.:;-:_~~: ________ ,_-,_:__,f2i--+"-.\,-·._/.,_,.,_\_#=:.e[~'-'1_T:,:)j-::.~ __________________ _ .~ .. 0 do r -'~'~)~,~; ~~~--;~--- A p pea ranee_" ,~,n~-~-~-~--~l~..t_'7v __ Taste , ... I / A .-I -, Field Arialysis By;-~ ii~"?.,. I. LABORATORY ANALYSES 8005 "0 mg/I COD High 3'0 mg/I coo Low :i35 ·. mg// Coli!Cfrm:MF Fecal 31516 1100ml Colllorrn:MF Tomi 3°1504 1100ml I ,./ -TOC 680 mg/I . 7urbldlty 76 NTU )< OH. 403 uni ts Alkalinl!y to µH '. 5 "o mg/I AlkaJinl!y '° oH 8.3 "5 mg// Carbonato '" mg// Bicarliona1e 440 mg/I )( Ars8nic:To1al 1002 --:: n ug/1 ·carbon dioxide 405 mg/I X X Chloride 940 , .. ,, mg/I chromium:Hex 1032 ug /I Color:True 80 Pt-Co Cyanide 720 mg/I Lab Comments: ' ' . I f De script i ·on of samp I i ng point -•'.--..'~'--+I+;-~/~•-•~"-"'"~------------------------------- · Sampling _Me th od Remarks (pumping time, air temp, etc.) Diss. Soll ds 70300 mg/l ';(_ . Ag -Silver 1077 --=:::::2:.-==; ug!! ,< Organochlorine Pesticides Fluoride 951 mg/I x' . Al -Aluminum 1, os /.,..,::) 11 nd ug/1 \.; Organoohosphorus Pesticides Hartlness:Total 900 mg!I -I r V. · Ba -Ba_~lu~ ·,0·01 .. ,4;fAn" ug/I (rion-Carb) .. Hardness 902 ml:!/1 .. v c, Ca!cium.916· J:J'tA .. · mg/I y Acid Herdicides Phenols 32730 r---ug/l ---, x c, Cadmium 1027 .<_.;, r) ug/1 Spoclllc Cond. 95 uMho:;/c,n 1 :~~:' Chromium:Tota! 1034 . 7',C:: ug// x' Gase / Neutral E,Iractable Organics Sulla :e °' 5 (/ mo/I~ " c, Conpor.1042 < :::{:.} . r )( uu/t "' AClcl E,tractoblo Orcanlc, -· Sul!ldo 7'5 mg/I I .Y Fe -Jron·1045. iJ~-,~() . ug/1 ' >< Hg Mercury 71900 _, . ·,>,,:-) ug/I y Purgeaola Or1,anics (VOA bot1le) .. y ' • Potassium 93 7 . /9'. mg/I '< Mg -Magnoslum 927 ::) J mo/I -1.2 -OibroJ1l08lh3nll (ED Bl :56 :x · Mn .-:·1,1anga~~se '°.5.5.-Y.i.lD o. ! ug/_l V _,, r-. ,-.• --.-,. . ' '>( ·Na Sodium 929 9", I -mg!! ' . -,; -----,,J . '" NH3 as N 610· /{:·! ·-mg/I ::< Ni·_-Nickel"1067 <,:;:;o . llgtl X V. I. -· TK r~ as N 625 mg/I So I '-( a Pb -L_aad 10:S 1 I '.""/ r. ug/I / N02 "t-N03 as N 630 :) 7 mg/I ! -./ s, Selenium 1 1 4 7 --<:::J {) ug/1 P:To1.i1 as P 665 ; mg/I r '" Zinc 1092 I 7r> ug/1-. ' E ATTACHED ORGANICS. I ANALYSIS REPORT i ' .:,,._ . ·-•. I _. '. GW-5,; Revise:d 7/85 For Dissolved Analysis -su:.:.,1~it fi/1!3:,-~,1 sample and write ·0_1s· in block White copy -Headquurters Pink cr.py -Region Yellow copy -Lab •· Re.ported by ( Date c;J.//(;,/ ff 7 I \ ·. -~ Checked by A'J-.(2._, 11,supervisor~K I I I I I I ~ I I I E I I I I i I 0 . ' Lab No. 7r--l?,o'-1 I -- Sample Type : /., 1, -1-r-,. Analytical Results 1)1_ •~on1,·,; Jo.-. r-4o'v-n ,{z-,r2 0,' . (', C / i:::'f'\O . V ' 'YI,~ 1'1n-ti ;,.Jo,' _,-,.\n" -t ,a ,-Qr~ -. . -1, ., ·~,-0 o--J~ u.i n, ~or 'To ,0 V , \J " ·"" -(h,, OLM Ge./~ c.. ,'Y\.rr n -0 ~ i-1 ·on rfl /-\..,{"() . A, 1 r /"l rO Q Q-~ r ~ _Q (),,, ·-0 r r J , I -0 0 - Or,· ,.., , , •• ; _1 n '"i-, , _; a ,0 •~n n~ ,--Jln tn ,+n ,.11 n~. \) ' V ,> C / ><rt lo ~'\,-0-A 0 mo, ,+n~ <TL (I r ,• .Ji /lfYITT7n _-(1_0Jo _.., ,, ,.. ·• I ,.. ,,.,. ,..-l~o ,/ro..O 0,.G {-J /f\A\ 0 . 1Y\11· ,.-, r ,· ~ ionO-rir, :On, rQn-f3orvn-~ (), ., r:r_ IF. C / CC/HS/ DS uaed \;/' \ c· Concentration ✓-i '\.:.,_ \ I I I 0 State of North Carolina Department of Environment, Health, and Natural Resources Mooresville Regional Office James C. Martin, Governor William W. Cobey, Jr., Sccret2ry CERTIFIED MAIL RETURN RECEIPT REQUESTED Albert F. Hilton, Regional Manager DIVISION OF ENVIRONMENTAL MANAGEMENT August 9, 1 990 Mr. Henry Sigmon, Jr. Sigmon Septic Tank Service Route 14, Box 350 . Statesville, North Carolina 28677 Dear Mr. Sigmon: RE: Notice of Violation 15A NCAC 2L Classifications and Water Quality standards Applicable to the Groundwaters Sigmon Septi.c Tank Incident No. 3422 Iredell County, N.C. Chapter 143, North Carolina General Statutes, authorizes and directs the Environmental Management Commission of the Department of Environment, Health, and Natural Resources to protect and preserve the water and air resources of the State. The Division of Environmental Management has the delegated authority to enforce adopted pollution control rules. Based upon an inspection of your facilities located on Route 14, Box 350, Statesville, North Carolina, the Division has reason to believe that you are responsible for activities resulting in noncompliance with North Carolina law. Staff of the Mooresville Regional Office (MRO) of the Division sampled two monitor wells at the subject site on June 14, 1990 and the lab results indicated that the North Carolina groundwater standards have been exceeded. Specific violations of 15A NCAC 2L .0103(d) -No person shall conduct or cause to be conducted any activity which causes the concentration of any substance to exceed that specified in 15A NCAC 2L .0202 -are as follows: 919 North ~in S1TCT"1, Moon:;-vil!c, N.C J8115 • Tdcpixmc ~-6t_i3•l&'? • FAX )'(H.,663-60-«) r I I I I I I , I I I I E fl Mr. Henry Sigmon August 9, 1990 Page Two Concentrations of Substance~ Found in Exceedance of 2L Standards on June 14, 1990 (in micrograms per liter, ug/1) -Constituent MW-3 MW-4 2L Standard Iron 590 2300 300 Lead 86 190 50 -Manganese 430 50 --· Mercury 6.0 <0.2 1 . 1 1 , 1 Dichloroethane 1 . 3 ND ND (ND -not detectable; --means not analyzed for) You are responsible for causing, contributing or allowing the continuing violation of the underground water quality standards because you are storing septic tank waste in unlined lagoons. To achieve compliance with the above-cited laws or regulations, you are required to submit within sixty (60) days from receipt of this letter a site assessment report as prescribed in the enclosed outline. As a part of the site assessment, two monitor wells should be installed in the vicinity of the state monitor wells that were accidentally damaged. This data will then be used to submit a remedial action plan which will be due within sixty (60) days after the site assessment report is submitted and approved by this Office. The above violation of 15A NCAC 2L is subject to a civil penalty assessment under the authority of G.W. 143-215.6 of not more than $1·0,000.00. Failure to respond within the time specified and to voluntarily achieve compliance may result in a recommendation for enforcement, the issuance of a special order against you under the authority of G.W. 143-215.2, or a request to the Attorney General to institute an action for injunctive relief. Your response and/or questions should be directed to Chris DeRoller of the Mooresville Regional Office at (704) 663-1699. cc: Office of General Counsel ?erry Nelson Sincerely, Brenda J. Smith, P.G. Regional Supervisor Enclosures: Site Assessment Guidelines Sample Results CMD/pl I '- I I I I ANALYTICAL TESTING & CONSUL TING SERVICES P.O. BOX 31486 • CHARLOTTE NC 28231 • TELEPHONE f704) 527--4183. FAX:(704) 525-0400 March 7, .J'l'll AAA Enterprises Attn:Barry Sigmon Rt. 14, Ba>< 35121 Statesville, NC 28b77 Dear AAA Enterprises: I I I p Below are results of analysis of 2 samples received fat' examination on February 21, 1991: Custo ■er Code: AAAENTER e'hone Number: (701+)873-8954 LAB I. D. AA04173 Bold ID Number G'310Fl-2 Collection Date: 02/l'l/'ll Submittal Date: 02/21/'ll Custom~r Sample I.D#: MW! Submittal Time: 17:4b TEST PARAMETER UNITS TEST RESULT I I I I I Multicomponent analysis: ACID EXTRACTABLES BY GCMS 4-NITROPHENOL '-'9 I l Not Det PENTACHLOROPHENOL ug/1 Not Det 4,b-DINITRO-O-CRESOL ug/1 Not Det 2,4-DINITROPHENOL ug/~ Not Det 4-CHLORO-3-METHYPHENDL ug/1 Not Det 2,4,b-TRICHLOROPHENOL ug/1 Not Det 2,4-DICHLOROPHENOL ug/1 Not Det 2,4-DIMETHYLPHENOL '-' g / l Not Det PHENOL ug/1 Not Det 2-NITROPHENOL ug/ 1 Not Det ·2-CHLOROPHENOL ug/1 Not Det 'Multicomponent analysis: BASE-NEUTRALS BY GCMS N-NITRDSODIMETHYLAMINE ,.19/L Not Det BISl2-CHLOROETHYL)ETHER ug/L Not Det 1.N-NITROSO-DI-N-PROPYLAMINE ug/L Not Det NITROBENZENE ug/L Not Det HEXACHLOROBUTADIENE ug/L Not Det I 1,2,4-TRICHLOROBENZENE ug/L Not Det I SDe'HORONE ug/L Not I)e t NAPHTHA)-ENE ug/1~ Not Det 81512-CHLOROETHOXY)METHANE ug/L ~~ 0 t Dct I HEXACHLOROCYCLOPENTAO l ENE ,_d.0 tJo t Det 2-CHLORO~lAPHTHALEisJ~49 SPRINGBROOK 8/ · • CHARI nrrc: !.If""' ,-,n,.,,~..., DETECTION LIMIT 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 1 0 10 ANAL YT)CAL TESTING & CONSUL TING SERVICES I It I I P.O. BOX 31486 •CHARLOTTE.NC 28231 • TELEPHONE f7D4J 527418.J. FAX (704) 525...()409 AAA Enter·prises I I I I I , I I I I Page: 2 March 7, 1991 BASE-NEUTRALS BY GCMS (continued): ACENAPHTHYLENE ACENAPHTHENE DIMETHYL PHTHALATE 2,6-DINITROTOLUENE FLUORENE 4-CHLOROPHENYL PHENYL ETHER 2,4-DINITROTOLUENE DIETHYL PHTHALATE N-NITROSODIPHENYLAMINE 1,2-DIPHENYL HYDRAZINE HEXACHLOROBENZENE 4~BROMOPHENYL PHENYL ETHER PHENRNTHRENE ANTHRACENE DI-N-BUTYL-PHTHRLATE Fi_UORANTHENE :-•YR ENE BENZIDINE BUTYL BENZYL PHTHALATE BISl2-ETHYLHEXYI_I PHTHALATE BENZ □ la) ANTHRACENE CHRYSENE 3,3'-DICHLORDBENZIDINE DI-N-OCTAL PHTHALATE BENZ □ Cb) FLUORANTHENE BENZ □ (kl FLUORANTHENE BENZ □ Ca) PYRENE INDENO <1,2,3-cd) PYRENE DI PENZ < a, h) ANTHRACENE BENZ □ lg,h, ii PERYLENE 2-METHYLNAPHTHALENE BISl2-CHLOROISOPROPYLI ETHER 4-CHLOROPHENYL PHENYL ETHER HEXACHLOROETHANE •Jg/L ug/L ug /L_ ug/L •Jg/L ug/L ug/L ug/L ug/L ,~,g IL ,_,g /L 'Jg/L ug/L ug/L ug/1.. ug/L ug/L ug/L ug/L ug/L ug/L. •Jg/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L Not Det Not Det Not Det Not Det Not Det Not D et Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det IM,1lticomponent analysis: AROMATIC VOLATILE ORGANICS BENZENE CHLOROBENZENE I 1, 2-DICHLOROBENZENE 1,3-DICHLOROBENZENE 1,4-DICHLOROBENZENE I.ETHYL BENZENE TOLUENE XYLENE I METHYL-TERT-BUTYL ETHER ISOPROPYL ETHER ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L Not Det Not Det Not Det Not Det 3 4 2 6 Not Det Not Det • Multicomponent aCJa!vsi;a; HALOGEN/HE □ 'l!OLATlLE ORGP.N!CS 449 c;PRINGBROO~, ROAD • CHAfiLOTTE, NC 28217 I llZI 1 lZI 1 lZI 1 lZI l lZI 1 lZI 10 1 0 l lZI 10 10 10 10 l 0 10 10 10 10 1 0 10 10 10 10 10 10 10 10 10 1 0 10 10 1 0 1 0 10 1 1 1 1 1 1 1 1 1 I h I I I I I I ANALYTICAL TESTING & CONSUL TING SERVICES P.O. OOX 31486. CHARLOTTE. NC 28231 • l'El.EPHONE (704) 527-4183. FAX.: (704) 52S-0400 ARR Enterprises Page:' 3 Ma,·ch 7, l'l'll HALOGENATED VOLA"f!LE ORGANICS (continued): BROMODICHLOROMETHANE ug/L Not Det l BROMOFORM ug/L Not Det 1 BROMOMETHRNE ug/L Not Det 1 CARBON TETRACHLORIDE ug/L Not Det 1 CHLOROBENZENE ug/L Not Det 1 2-CHLOROETHYLVINYL ETHER ug/L Not Det 1 CHLOROFORM ug/L Not Det 1 CHLOROMETHANE ug/L Not Det 1 DIBROMOCHLOROMETHRNE ug/L Not Det 1 1,2-DICHLOROBENZENE ug/L Not Det 1 1,3-DICHLOROBENZENE ug/L Not Det 1 1,4-DICHLOROBENZENE ug/L Not Det 1 DICHLORODIFLUOROMETHANE ug/L Not Det 1 1, J-DICHLOROETHANE ug/L Not Det 1 I 1, 2-DICHLOROETHANE ,.1g/c. Not Det 1 1, 1-DICHLOROETHENE ug/L Not Det 1 , TRANS-1,2-DICHLOROETHENE ug/l_ Not Det 1 1,2-DICHLOROPROPANE ug/L Not Det 1 CIS-1,3-DICHLOROPROPENE ug/L Not Det 1 TRANS-1,3-DICHLOROPROPENE ug/L Not Det 1 METHYLENE CHLORIDE ug/L Not Det 1 1, 1,2,2-TETRACHLOROETHANE ug/L Not Det 1 TETRACHLOROETHENE ug/L Not Det 1 I 1, 1, !-TRICHLOROETHANE ug/L Not Det 1 1, 1, 2-TRICHLOROETHANE ug/L Not Det 1 TRICHLOROETHENE ug/L Not Det 1 I TRICHLOROFLUOROMETHANE ug/L Not Det 1 VINYL CHLORIDE ug/L Not Det 1 CHLOROETHANE ug/L Not Det 1 I CIS-1,2-DICHLOROETHENE ug/L Not Det 1 ETHYLENE BROMIDE ug/L Not Det 1 I LEAD, TOTAL mg /L 12>. 12>312> 12>. 12>212> IRON, TOTAL mg/L 212>.12>12> 0.02 MERCURY, TOTAL mg /L ( 0. 012>2 0. 002 I~~~~~~===~-~~~~=-----------------:=~=---------------~=~~~-------~ ~ ~ = - - - - -Comments: 'Samples collected VAL:KCR I, I at MW 1 at sludge pool t,49 Sf'RINGBROOK ROAD • CHAc1l.OTTE. NC 2s2·, 7 ANALYTICAL TESTING & CONSUL 11NG SERVICES P.O. SOX 31486 • CHARLOTTE... NC 28231 • TElE.PHONE (70-4) 527-4183 • FAX: [70-4) 525--0400 AAA Enterprises Page: 4 March 7, 1991 Custo ■er Cude: AAAENTER Phone Number: (704)873-8954 LAB I.D. AA04174 Bold ID Number G910Fl-2 Collection Date: 02/21/91 Submittal Date: 02/21/91 Customer Sample I.D#: MW2 Submittal Time: 17:46 I . ' ' ' I Po I I I I TEST PARAMETER UNITS TEST RESULT I I Multicomponent analysis: 4-N ! T_ROPHENOL PENTACHLOROPHENOL 4,6-DINITRO-O-CRESOL 2, 4.-DINITROPHENOL I 4-CHLOR0-3-METHYPHENOL 2,4,6-TFICHLOROPHENOL 2,4~DICHLOROPHENOL ... 2,4-DIMETHYLPHENOL .-P'-iENOL 2-NITROPHENOL 2-CHLOROPHENOL ACID EXTRACTABLES ug/1 ug/1 ug/1 ug/1 ug/~ ug/1 ug/1 ug/1 ug/1 ug/1 I.IQ/ j I Multicomponent analysis: BASE-NEUTRALS BY I I N-NITROSODIMETHYLAMINE BIS12-CHLOROETHYLlETHER N-NITROSO-DI-N-PROPYLAMINE NITRDBEN7.ENE HEXACHLOROBUTADIENE 1,2,4-TRICHLOROBENZENE ISOPHORONE I NAPHTHALENE BIS<2-CHLOROETHOXYlMETHANE HEXACHLOROCYCLOPENTADIENE 2-CHLORONAPHTHALENE I ACENAPHTHYLENE ACENAPHTHENE DIMETHYL PHTHALATE I 2,6-DINITROTOLUENE FLUORENE 4-CHLOROPHENYL PHENYL ETHER 2,4-DINJTROTOLUENE DIETHYL PHTHALATE -NJTROSDDIPHENYLAMINE 1,2-DIPHENYL HYDRAZINE ■ HEXACHLOROBENZENE ■ 4-BRO~OPHENYL PHENYL ETHER PHENANTf'iRENE ug/L ug/L ug/L ug/L ug/L ug/L 1.19/L ug/L ug/L ,.,g/L ug/L ug/L ug/L 1.1g/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L BY GCMS Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det GCMS Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det I 449 SPRlr✓GBROOK ROAD • CHARLOTfE, NC 28217 DETECTION LIMIT 10 . 10 10 10 10 1121 10 1121 10 1121 10 10 1121 10 10 10 10 10 10 1121 10 10 10 10 1121 1121 10 1121 -- 10 10 10 10 1121 10 10 ANALYTICAL TESTING & CONSUL TING SERVICES •• lo I I I I I I P.O. BOX 31466 • CHARLOTTE, NC Z8231 • TELEPHONE (704) 527--4183 • FAX: (704) 525-0400 I , RRR Enterprises Page: 5 March 7, 1991 BRSE-NEUTRALS BY GCMS ANTHRACENE DI-N-BUTYL-PHTHALATE FLUORANTHENE PYRENE (continued): ug/L ug/L ,.,g/L ug/L BENZI DINE BUTYL BENZYL PHTHALRTE BISl2-ETHYLHEXYLJ PHTHALATE BENZ □ la) ANTHRACENE CHRYSENE 3,3'-DICHLORDBENZIDINE DI-N-DCTAL PHTHALATE BENZO lb) FLUORANTHENE BENZ □ (kl FLUORANTHENE BENZ □ la) PYRENE INDENO 11,2,3-cd) PYRENE DIBENZ la,h) ANTHRACENE BENZ □ < g, h, i) PERYLENE 2-METHYLNAPHTHALENE BISl2-CHLOROISOPROPYLJ ETHER 4-CHLOROPHENYL PHENYL ETHER HEXACHLOROETHANE ug/L L<g/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det I I I I Multicomponent analysis: AROMATIC VOLATILE ORGANICS BENZENE ug/L Not Det CHLOROBENZENE ,,g/L Not Det 1,2-DICHLOROBENZENE ug/L Not Det 1,3-DICHLOROBENZENE ug/L Not Det 1,4-DICHLOROBENZENE ug/L Not Det ETHYL BENZENE L<g/L Not Det TOLUENE ug/L Not Det XYLENE ug/L Not Det METHYL-TERT-BUTYL ETHER ug/L Not Det ISOPROPYL ETHER ug/L Not Det IMul t icomponent analysis: HALOGENATED VOLATILE ORGANICS BROMODICHLOROMETHANE ug/L Not Det BROMOFORM ug/L Not Det I BROMOMETHANE ug/L Not Det CARBON TETRACHLORIDE ug/L Not Det CHLOROBENZENE -ug/L Not Det w-CHLOROETHYLVINYL ETHER ug/L Not Det HLOROFORM ug/L Not Det HLOROMETHANE ug/L Not Det . I DIBROMOCHLOROMETHANE ug/L Not Det 1,2-DICHLOROBENZENE ,.,g /L Not Det 1,3-DIC~LOROBENZENE ug/L Not Det 1,4-DICHLOROBENZENE ug/L Not Det I 449 SPRINGBROOK ROAD • CH/\RLOTTE f✓(', ?R?17 10 10 ·' 10 I 10 10 10 10 10 10 10 10 10 10 10 10 10 l<Zl 10 10 10 10 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 ANALY1K::Al TESTING & CONSULTING SERVICES I .. It I P.O. OOX 31'86 •CHARLOTTE.NC 28231 •TELEPHONE(?~) 5?7-4183. FM {704) 525--0,400 I I I I I I AAA Enterprises Page: E, March 7, l'l'll HALOGENATED VOLATILE ORGANICS DICHLORODIFLUOROMETHANE 1,1-DICHLOROETHANE l,2-DICHLOROETHANE 1, 1-DICHLDRDETHENE TRANS-1,2-DICHLOROETHEN E 1,2-DICHLOROPROPANE CIS-1,3~DICHLOROPROPENE TRANS-1,3-DICHLOROPROPEN E METHYLENE CHLORIDE 1, 1,2,2-TETRACHLOROETHANE TE'rRACHLOROETHENE 1,1, 1-TRICHLOROETHANE 1, 1,2-TRICHLOROETHANE TRICHLOROETHENE TRICHLOROFLUOROMETHANE VJNYL CHLORIDE CHLORDETHANE , CIS-1,2-DICHLOROETHENE ETHYLENE BROMIDE LEAD, TOTAL IRON, TOTAL I MERCURY, TOTAL MANGANESE, TOTAL I Comments: Samples collected at MW 2 VAL:ADD I VAL:KCR (continued): ,.,g/L ug/L ug/L ,.,g/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug /l. ug/L ug/L mg/ l. mg/L mg/L mg/L Not Det 1 Not Det Not Det Not Det Not Det Not Det Not Det 1 Not Det Not Det Not Det Not Det Not Det Not Det 2 Not Det Not Det ,'lot Det; ( 0.1212121 0. 1121 ( 0.002 17.50 Please advise should you have questions concerning these data. IR e ~ p ec t f u 1 l y sub m it t e d, I . ~ I I 449 SPRINGBROOK RO/D • CH,\RLOTTC r,ir ~M•·• 1 1 1 1 1 1 1 1 1 1 1 1 1 i 1 1 1 1 1 0.020 121. 02 0.002 0.02 \ \ \ ' I \ I ii I I ', \ Reporl lo: ARO, FRO,~ RAO, WaAO, WiAO, WSFIO, Kinston FO ----~-----cJepartmsm ol Env1ronmsnt, Hea1wnd Natural Resources Division al Environmental Management CtifiltfaaritO~lf tiuY LONG. So<· 5s O .s-" Olher ________ _ ROUTINE SAMPLE PRIORIIY 0 EMERGENCY 0 L,111111.<Hc .. ~ ~ /~ _._ - DATE AECEIVEDsL~3 Time~ (,'-,c: --~ nec"d by: lZ--:? r-·rom: Bu~ Olher DATA ENTRY BY: 111 CK: J;J...s OAT E R EPOA lE D:-::_~:&=/'3_o=/;'[._'.J=--•----Shipped by: Ous.~-ur_ie.~ Olher COLLECTOAfSJ: Ou?,,/1,r h/Jc,!kcroATE !(/5/73 TIME /tJ.l/1).-/0:'(l(pLJAPOSE: BASELINE, COMPLAl~JT. COMPLIANCE, LUST, OTHER (cl,cJe on4,) Pali. r,..,u_ 0 1ELD ANALYSES >H ◄0o 7,U Spec. Cond. D◄ 55l) a 1 -2-s"'c Owner Localion or slle I 5. 12, I I 3 ·C\ emp.1o -I-'-'~-· 0 c Odor _ _,Q..u.O<,f))SY"n,.,_f(,_..scc.·~,_.qny Descrlpli on ol sampling pol nl . j ,u/-·1, \ppearance Ott.:.y /1/ufa;( Tas18 --~-~r.~----> I l • I. Id Ana I y s i s By: -"'tu."-"'"-'l_,_/2'-'-"e...,(_· ------ SamplinQ Melhod ,'3:ke { ballor, ale'.) Remarks (pump, • I /(...(o /),+or -----Ci:i,. ~_;; v2 :, 1± J __________ ./ __ S arnpl e lnlorva I -~~«~~~,_-~3~"'~------ (pumping llme, air lamp, et A □OnATOllY ANAL YS[S -.,."~'Jr~,~-~· ~•~LJG~--r~"---~,JH:=-~s=·~ f .fr..u, C l+c r ,-( /;,L~.Z..• :,;cl.--, ) I Wr:u:f ,l1c {.,...1, ,.,,,cj'.,,..(,,..,..✓ ,-..,,iw ~}, . .( ' BOUf>JI0 ma/I )( o~ ... Solllh 10)00 ,f-)f) mo/I Ag· Sll••t 1011 "'" 01,■nochlo,ln• l"•■llold•• COO HIQl'I J•O moll fluolld1 g~ I moll Al -Al1.mlnum 1106 ug/1 01o•nophoepl'lo1u1 ,.,11lold11 COD Lo• '" mg/I Hudn1 ... :To11I ,., moll )<. •• • 8allum ·1001 710 "'" \( Colllorm:u.F f.c1l J 1618.£' /00 11oom"1 H11dn1u (non•cub) 1l02 mg/I Ca· Calclum 910 moll ,-\Cid H•1dlold•1 Colllorm:l,ff Tot,I J 1~04 / 100ml Ph1nol1 32130 "'" Cd • Cadmium 10 2 J ug/1 TOC 6&0 lflg/1 Sp1clllc Cond. " uLU\01/cm J Ch1omlum:Tol1I IOH uo/1 81 •• I N "-•1111 E1111c11bl• 0,111111!11 Tu1bldllr " HTU Sull111 i ◄!. mo/I Cu • Copp11 1042 ug/1 Acid E1l11cJ1b/1 01g1nlo1 Sutlld1 ,., mg/I fo • Iron I 04 !. ug/1 y Hg • Ll11curr , 1'100 ..::: r-,. ,,,.., ug II X Pu1g11bl1 Oro1nle1 [VOA bolll■J pH ◄ 0 J unlh K • Po1&ulum 9J7 mg/I - A lk 111 nl I 1 lo pH ~, !, <10 mg/I I.lg· Ll&On•,lum 921 mQII 1, 2 Dlb1omo•ll'l1n• (£DIil Ana1tnl1r lo pH I.J ... mg/I Un· L11n1,1•n••• 1056 ug/1 Cubon&II ... mg/I "' . Sodium "' mg/I Blcubon•t• ... mg/I x ""' .. " "' 0, 7;). .. mg/I "' -N le~ 1 I 1061 uo/1 -il~ ... -..... ,:;ae:;• r~, Arunlc:10111 1002 .,,,, TKN .. " "' mg/I )( Pb • LI Id 10!.1 '7'---, Ug/1 fVr.11,1;·1,,:~. _':'''CJ,; . ~. ;c,~l ~'-":.A_JL C11bon dlo,Jth ◄O~ mg/I y NOJ -. N03 •• H 630 7-3 mg·/1 s, • Selenlum I 141 uo/1 "j"'"';;; ,_.,.,. ··.·· Chloride g,rn m11/I P:10111 11 P 61U mo/I '" • Z Inc 10111 ug/1 J!rt i .-, Ch1nmh,m:th • 1032 ug /I '· !'.:'/j Colot:ln ... 10 Pt-Co O/Y/s ~ ... ,, -C 1 • ol de '" mg/I lj f!Ct<'•i,, I ;l!l1//.'r!ft;T. '.! ., ... ., ab Commen11: .,,.ullij-'' ... ., llll OFJJC[ for Dissolved Analysis -submll llllorad sample and wrilo "Pl"" '1 block While Coov • Groundwalar Conlral Olllco Yellow Copy· I · mal Office Pink Conv • Cenlral Flle1 Goldonrod r..,,nv · 1 •h • I EHNR/DEH LABORATORY VOLATILE ANALYTICAL REPORT II LAB NO. JG 101 • .. .BPORTED BY . ~ CHECKED BY. ~ I REViB'iED BY . . . SAMPLE TYPE: WATER I CASI I 15-35-4 15-09-2 I 156-60-5 15-34-3 590-20·1 156-59-4 I 61-66-3 14-91-5 71-55-6 Ii 563-58-6 56-23-5 101-06-2 I 19-01-6 78-81-5 15-21-4 ~ 74-95-3 061-01-5 10061-02-6 79-00-5 I 121-18-4 142-28-9 124-48-1 I 106-93-4 108-90-1 630-20-6 I 15-25-2 19-34-5 I TQL· T· I E· 0- N· I D· H· 1 "COMMENTS: I I VOA TARGET COKPOOND 1,l·Dichloroethene 0,15 Methylene Chloride 0.25 trans-1,2-Dichloroethene 0,15 1,1-Dichloroethane 0.25 2,2-Dichloropropane 0. 25 cis-1,2-Dichloroethene 0.25 Chloroform 0.25 Bro1ochloro1ethane 0.15 1,1,1-Trichloroethane 0.25 1,1-Dichloropropene 0.25 carbon Tetrachloride 0.15 1,2-Dichloroethane 0.25 Trichloroethene 0. 25 1,2-Dichloropropane 0.25 Bro;odichlorouethane 0.25 Dibro101e'-11ane 1 cis-1,3-Dichloropropene 0.25 trans-1,l-Dichloropropene 0. 2 5 1,1,2-Trichloroethane 0, 25 Tetrachloroethene 0.25 1,3-Dichloropropane 0,25 Dibromochloromethane 0.75 1,2-Dibroaoethane 1 Chlorobenzene 0.25 1,1,1,2-Tetrachloroethane 0.25 Bromoform 0, 5 . 1,1,2,2-Tetrachloroethane 0.15 Target Quantitation Limit-subject to change due to instrument sensitivity Tentatively Identified, not confirmed Estimated Value samples analyzed for this compound but not detected Sample not analyzed for this co1pound Detected below quantitation limit GC/HS Analysis performed '"''''''"' ~ DATE !;JS 'i3 ENTERED BY , . CHECKED BY - ANALYSIS RESULTS DETECTED CASI VOA TARGET COMPOUND DETECTED u 1 u I u 96-18·4 1,2,l·Trichloropropane 0.25 u u 108-86·1 Broaobenzene 1 0 u 95-49-8 2-Chlorotoluene 0.25 u 0.41 T 106-43-4 4-Chlorotoluene 0.25 0 u 541-13-1 1,3-Dichlorobenzene 0,25 u 0.51 T 106-46-1 1,4-Dichlorobenzene 1.25 6. 1 u 95-50-1 1,2-Dichlorobenzene 0.25 0. 28 T u 96-12-8 1,2-Dibromo-3-Chloropropane 1 u u 120-82-1 1,2,4-Trichlorobenzene 0.25 u u 87-68-3 Hexachlorobutadiene 0,25 u u 81-61-6 1,2,l-Trichlorobenzene 0. 75 u u 1634-04-4 Kethyl-tert-butyl ether 5 0 u 71-43-2 Benzene 1 u u 108-88-3 Toluene 1 u u 100-41-4 Ethyl benzene 1 D T u 108-38-3 m,p-Xylenes 2 D u 95-41-6 o-Xylene 1 u u 100-42-5 Styrene 1 u u 98-82-8 lsopropylbenzene 1 u u 103-65-1 n-Propylbenzene 1 u u 108-67-8 1,3,5-Trimethylbenzene 1 u u 98-06-6 tert-Butylbenzene 1 u u 95-63-6 1,2,4-Trimethylbenzene 1 D T 0.81 T 135-98-8 sec-Butylbenzene 1 u u 99-81-6 p-isopropyltoluene u u 104-51-8 n-Butylbenzene 1. 6 T u 91-20·3 Naphthalene 3 .1 Other purgeables detected Detected (up to 10 highest peaks) ug/1 ... --"",=_ 1'---",7 • .,,/J_ ,!_,,_ OUAD ND. l. u' G -1<-r.'SEAIAL NO./ -~~7rr_· -- . .Mi.. ;;;:;;; =:I --... u,lpii!ipil_v~--,,•lllcl Department of Environment, Heal111, and Natural Resources ,, Division of Environmental Mana.:iement l!!!!!I -LONG. Groundwater Field/Lab Form Other------------------Repofl to: ARO, RAO, WaAO, WiRO, WSFIO, Kinslon FO Olher ________ _ Shipped by: Gus, Qr., Olher _______ _ CHAl~Jilf E ;~M§lR,DY ~ ROUTINE □ EMERGENCY 0 9f3,/•JCK:fiP DATE REPORTED: __ 177_:_;:c;:_v,._ _ __:_1 _____ _ DATA ENTRY BY: ;oLLE CT OR ( s)' D,f), /t,,, /(v'o /((_, I DATE 'IELD ANALYSES H 400 ___ Spec. Cond.94 ___ a1 2s0c emp.10----oc Odor -------- ppee1ance ______ _ Tasia ______ _ ield Analysis By: ____________ _ AOOrlATOllY ANALYSES BOUf>JlO · mo/I X COO Hlor, )40 moll COO lo• JJ5 mQ/1 Co1110,m:Uf F•c•I J 1618 I 100ml Colllolfn;l,lf Toh I J U04 1100ml Toe 6eo mg/I Turbldlly 16 HTU '" '°' uni•• Alk1llnll1 lo PH 4.S 410 mo/I Alkallnl\y 10 pH I, l . " mo/I C11t1on111 ... mo/I Blc11bon111 .. o moll 1:,( Afunlc:To11I 1002 """ C11t1on dlo11<1• ◄05 moll ,x- Chlorld• 11◄0 moll Ct,romtvm:>h, 1 OJ 2 UQ /I Colo<:ln. .. ao Pl·Co c,,otd• "" "'"" • Cornm•nls: PURPOSE: BASELINE, Ownor Loca1ion or site COM PL A I NT, COMPLI ANGE, (chd• oM) .::±, }( ' -'? 'f,7 2 /? / ,_,//' 1-;./(:__J, LUST, OTHER Descrlplion al sampling point B1c,,-,k Sampling Me lhod ---~B=n~r'/_<-~,•----~-------___ S ampl a lnlel'ta I --',.-u'----_/..'--'c,4"--'----------(pum o. ballor, etcJ Remarks Di"ibUe,I' 1 L,h-f<., po<Ace-c.A /,,.,,../n 0c;,,·fer ±Gek? l..;,,;,:;.-;c"",L.,'rc/ I (pumping llme. air lamp/etc.) Ja l">r.n /i-1·::; {.o:n ·fu.1,'cz4f::i_c=-ic:.__ __ ,_,f,,c,_ _ __:uoec__.1f-11s;e..1.,c:..J. ________________________ _ r , 01 ... Soltd1 10JOO ,S mg/I AO · S11,.•r 1011 ug/1 o,vanochlo,ln• ~•1llolda1 fluoride 051 rnotl Al • Alumlnvm 110, """ Org1nopho1pt:oru1 "•1II0l1:h1 Hardneu:Tol•I 000 moll )<" 0• · Bulum ·1001 l"S """ He1dn••• (non·carb) 002 m·o11 c, • Calcium t U moll PJunoll l21JO """ Cd· C•dmlum 1021 uo/1 Speclllc Cond. " uMhoa/cm 7 Ch10m1um:To1a1 1034 uo/1 e, .. I N,u1nl EattlCUbl• 0,9111.I•• Sulllle 9 ◄S mo/I Cu • Copp•• 1042 uo /I A.Cid E1!1 ■CUbl• o,g1ftloe SuJllde '" mo/I Fa • Iron IO ◄ 5 uo/1 y· Hg· l.hrcur, 1 I QOO ,,,( b ' ug II K • Polaulum 937 mg/I I.lg • Magn .. lum Q27 m.,, 1,2 • 0lbromoalhlna (£011) Mn -l.lanw•n••• 1056 ug/1 Na • Sodium 112Q marl NH311N610 ll,t'J::l mo/I "' • HI C ~ 1 I 1061 ug/1 TKN 11 N 625 moll V ,. • L • • d 10~ 1 L'._ I 0 ug/1 Noa 9 NO3 •• N 6JO ~, OI mg/I ' s, • S•l•nlum I HJ ug I/ I P:Toial •• P 685 moll '" -line 1091 ug ti I/ . :ciiT - i-5-4 REV. ll/90 for Dlssolv&d Analysl& -submll llhorod sampio and wrilo ·01~-·, block I LAB NO. JG 703 It RBPORTBD BY CHECUD BY ~ I ~VIBIIID BY ~ SAKPLE TYPE: WATl!R CASI VOA TARGET COKPOURD EHHR/DEK LABORATORY VOLATILE ANALYTICAL REPORT ANALYSIS RESDLTS SUPERVISOR ~-. DATB .5. ::W . ERTIRBD BY , . ~ CH!ClBD BY DETBCTED CASI VOA TARGBT COKPOUHD DBTBCTID I --~---~-----~~--~u~l__ u l I I I I I 75·35·1 15·09·2 156·60·5 15·31·3 590·20·7 156-59·1 67·66·3 11·91·5 11-55·6 563·58·6 56·23·5 107-06·2 19·01 ·6 18-87·5 15·21·1 74.95.3 0.15 0.25 0.15 0.25 0.25 0.25 0.25 0.15 0.25 0.25 0.15 0.25 0.25 0.25 0.25 .,10061-01·5 10061·02·6 79-00·5 121·18·1 112·28·9 121-48·1 106-93·1 108-90·7 630·20·6 75·25·2 1,l·Dichloroethene Methylene Chloride trans·l,2-Dichloroethene 1,l·Dichloroethane 2,2-Dichloropropane cis·l,2-Dichloroethene Chlorofon Bro1ochloro1ethane 1,1,l·Trichloroethane 1,l·Dichloropropene carbon Tetrachloride 1,2-Dichloroethane Trichloroethene 1,2-Dichloropropane Bro1odichloro1ethane Dibro101ethane cis·l,3-Dichloropropene trans-1,3-Dicbloropropene 1,1,2-Trichloroethane Tetrachloroethene 1,3-Dichloropropane Dibro1ochloro1ethane l,2·Dibro1oethane Chlorobenzene 1,1,1,2-Tetrachloroethane Bro1ofor1 1,1,2,2-Tetrachloroethane 1 0.25 0.25 0.25 0.25 0.25 0.15 D D D D 79.34.5 1 0.25 0.25 0.5 0.15 TQL· Target Quantitation Li1it· Subject to change due to instru1ent sensitivity T· Tentatively Identified, not confir1ed E· 1sti1ated Value U· Sa1ples analyzed for this co1pound but not detected R· Sa1ple not analyzed for this co1pound D· Detected below quantitation li1it K· GC/KS Analysis perfoned · ~ COKK!HTS: 0 0.31 T u u u u u u u u u u u u u u u u u u u u u u u u u u 96-18·4 1,2,3-Trichloropropane 108·86·1 Broaohenzene 95·19·8 2·Chlorotoluene 106·13·1 l·Chlorotoluene 511·13·1 1,3-Dichlorobenzene 106·16·1 1,l·Dichlorobenzene 95·50·1 1,2-Dichlorobenzene 96-12·8 1,2·Dibro10-l·Chloropropane 120-82·1 1,2,l·Trlchlorobenzene 87·68·3 Hexachlorobutadiene 81·61·6 1,2,3-Trichlorobenzene 1631·01·4 Kethyl-tert·butyl ether 11·43·2 Benzene 108·88·3 Toluene 100-11-1 Ethyl benzene 108-38-l 1,p·Iylenes 95·11·6 v•Iylene 100·42·5 styrene 98·82·8 Isopropylbenzene 103-65·1 n·Propylbenzene 108·61·8 1,3,5-Triaethylbenzene 98·06·6 tert-Butylbenzene 95·63·6 1,2,l·Triiethylbenzene 135-98·8 sec-Butylbenzene 99-87·6 p·isopropyltoluene 101·51·8 n·Butylhenzene 91·20·3 Raphthalene ' Other purgeables detected (up to 10 highest peaks! OH! URIDERTl!IED PIAl DITBCT!D BY GC/PID. 0.25 1 0.25 0.25 0.25 0.25 0.25 1 0.25 0.25 0.15 5 1 1 1 2 1 1 1 1 1 1 1 . 1 1 1 1 Detected ug/1 u u u u u u u u u u u u u u u u u u u u u u 0 u 0 u u I .. I I n u D I I I I I I I, I I State of North Carolina Department of Environment, Health, and Natural Resources 512 ~Jorth Salisbury Street • Raleigh, North Grolina 27604 Division of Solid Waste Management Ref. 13 James B. Hunt, Jr., Governor Telephone 9 I 9. 73)-2178 February 11, 1993 Jonathan 8. Howes, Secretary MEMORANDUM TO: THROUGH: FROM: RE: Dexter Matthews, Chief Solid Waste Section Jerry Rhodes, Chief/t Hazardous Waste 113ection Doug Holyfield]tkead Waste Management Branch Sigmon Septic Tank Service -AAA Enterprises Eufola (Statesville) I have enclosed for your review a copy of our case development sampling investigation of the noted site. With Mr. Sigmon's failure to comply with our request to sample the septage impoundments, we initiated our own sampling investigation. This investigation included sampling water, liquid, and sludge samples from eight (8) septage pits and three water samples from off-site residential wells. According to Mr. Sigmon, the septage pits have not been utilized since the spring of 1992. Our sampling results indicate the presence of various hazardous constituents, primarily phthalates and phenols, however, no constituent exceeded TCLP levels to indicate a characteristic hazardous waste and we have no information to substantiate the disposal of listed hazardous wastes. Therefore, we cannot establish RCRA land units which would require implementation of closure/post-closure plans or ground water assessment/remediation. As such, our attorneys have advised us that an enforcement action would be very difficult to prove, especially with the site being non-operational. Subsequently, with regards to the septage units, we respectfully refer this site to you for evaluation under your program. In conclusion, by copy of this transmittal, we are notifying the Division of Environmental Management of our results of the off-site residential well sampling which exceeded their 2L Standards. The Munford well (lt9032) contained 0.09 mg/1 manganese, 0.007 mg/1 PO Bo, l7687, R:,bgh, No~h C»olina 17611-7687 Tckphonc 919-733~984 fa,, I 919-733-0Sll --.. /' I I I I m u , D 0 E I ,L I I Page 2. mercury, and 23.35 mg/1 nitrate. The Davidson well (#9033), no longer in use, contained 4.43 mg/1 iron, and 0.83 mg/1 manganese. Please contact me or Bob Glaser of our Groundwater Unit should you have any questions regarding the investigation. Also, Keith Masters and his staff is available for any support in the field. Attachment: cc: Mike Kelly Keith Masters Bob Glaser Judy Bullock Chris DeRoller -DEM Mooresville I .. I I I I I n D I I I, I I TO: FROM: RE: December 30, 1992 M E M O R A N D U M Keith Masters Laurie Martin Site investigation at Sigmon Septic/AAA Enterprises in Eufola. On August 31 and September 1, 1992, Bob Glaser, Pete Doorn, Gray Stephens and Laurie Martin of the Ground Water Unit collected water, liquid and sludge samples from eight septage pits at Sigmon Septic and three water samples from nearby residential wells. Sigmon Septic/AAA Enterprises is located on Eufola Rd. (SR 1333) in Eufola (near Statesville). Lafayette Atkinson, Safety Officer, was also present during the sampling. Eight active septage impoundments were located near the rear of the property. According to Barry Sigmon, no septage had been added to the impoundments since Spring 1992. Two additional ponds, reportedly closed for six or seven years, were also on site. A dirt road, accessed from Buffalo Shoals Rd. (SR 1004), runs behind the property. Several residences with private wells are located along this dirt road. Water samples were collected from the wells located on the Morgan, Munford, and Davidson residences (see attached sketch). Field sample numbers 9031 (inorganic) and 11220 (organic) were collected from the Morgan well. Field sample numbers 9032 (inorganic) and 11221 (organic) were collected from the Munford well. Field sample numbers 9033 (inorganic) and 11222 (organic) were collected from the Davidson well. The analytical results for these samples are attached. The sample collected from the Munford well (#9032) contained 0.09 mg/1 manganese, 0.007 mg/1 mercury, and 23.35 mg/1 nitrate. The sample from the Davidson well (#9033) contained 4.43 mg/1 iron, and 0.83 mg/1 manganese. (According to Davidson, this well is no longer used for drinking water.) These concentrations exceed the North Carolina water quality standards for ground water (TJ.5: 02L I I I I I D D E I I L I I .0200). Liquid, sludge and/or water samples were taken from each of the ''active" ponds (see attached sketch). Field sample numbers 9007 and 9008 (inorganic), and 11196 and 11197 (organic) were collected from pond #6. Field sample numbers 9009 (inorganic) and 11198 (organic) were collected from pond #7. Field sample numbers 9010 and 9011 (inorganic), and 11199 and 11200 (organic) were collected from pond #5. Field sample numbers 9013 and 9014 (inorganic), and 11201 and 11202 (organic) were collected from pond #4. Field sample numbers 9015 and 9016 (inorganic), and 11203 and 11204 (organic) were collected from pond #3. Field sample numbers 9017 and 9018 (inorganic), and 11205 and 11206 (organic) were collected from pond #2. Field sample numbers 9019 (inorganic) and 11207 (organic) were collected from pond #1. Field sample numbers 9020 (inorganic), and 11209 (organic) were collected from pond #10. The analytical results for these samples are attached. Sludges The contaminant concentrations found in the sludges taken from the ponds were below the TC levels. The totals analyses for the organic constituents in the sludges (#11197, #11200, #11202, #11204, #11206) indicated concentrations ranging from not detected (ND) •to 90,000 ppb bis (2-ethylhexyl) phthalate, 25,000 ppb 4-methylphenol, 16,533 ppb toluene, 9000 ppb 2- methylnaphthalene, 8000 ppb dibutyl phthalate, 7000 ppb 1,4 dichlorobenzene, 4000 ppb naphthalene, 2500 ppb chlorobenzene, 1155 ppb xylene, 1000 ppb 2-methylphenol, 624 ppb acetone, 288 ppb ethylbenzene, 200 ppb 1,2 dichlorobenzene, 156 ppb methylene chloride, 100 ppb 1,3 dichlorobenzene, 70 ppb benzene, and 18 ppb carbondisulfide. The totals analyses for the inorganic constituents in the sludges (#9008, #9011, #9014, #9016, #9018) indicated concentrations ranging from ND to 200 ppm lead, 110 ppm barium, 51 ppm chromium, and 0.29 ppm mercury. Liquid (excluding water) The contaminant concentrations found in the liquids taken from the ponds were below the TC levels. The totals analyses for the organic constituents in the liquids (#11196, #11205, #11207) indicated concentrations ranging from ND to 360,000 ppb bis(2- ethylhexyl) phthalate, 11,000 ppb dibutyl phthalate, 7000 ppb phenol, 6000 ppb 4-methylphenol, 1277 ppb toluene, 1273 ppb acetone, 1000 ppb 2-methylnaphthalene, 148 ppb chlorobenzene, 51 ppb xylene, and 33 ppb benzene. The totals analyses for the inorganic constituents in the liquids (#9007, #9017, #9019) indicated concentrations ranging from ND to 2.3 ppm lead, 0.19 ppm chromium, 0.021 ppm cadmium. I I I I I I , I I ·1 .I I ~ I I Pond Water The totals analyses for the organic constituents in the pond water (#11198, #11199, #11201, #11203, #11209) indicated concentrations ranging from ND to 6000 ppb dibutyl phthalate, 1000 ppb bis (2-ethylhexyl) phthalate, 735 ppb 2-butanone, 392 ppb acetone, 208 ppb toluene, 19 ppb methylene chloride, 14 ppb chlorobenzene, 10 ppb xylene, 6 ppb benzene. The totals analyses for the inorganic constituents in the pond water (#9009, #9010, #9013, #9015, #9020) indicated concentrations ranging from ND to 3.58 ppm barium, 2.69 ppm lead, 0.25 ppm chromium, and 0.131 ppm cadmium. I I I I , 1"7,,.,I I I I I ' I I 0 • • D® 11-......,1..,.,.J T,-111( 0 0 0 l) 0 ?i~~·~·· urt" f•"" s,,., .• ,. -- --¥--; • ,. f \ IC ~® i \~ . ' 1 1:>..~,1 ~ .. , "' I I ' ( ,,cr-r'•Jl IM• •~--,<1 u..,,,t, ., ,~ • .-1,"\ .... t:•~,-•,,) t 1,,1-• I ~ t \ ,i ' . ---. f-------l- ----11------ ____ ,_ ___ , ___ _ -------. -----1--- ___ 73-1,.1_ 3-5 f ·-+----+-------------' ·--- I 1----J---~------, -for...t:..-__ : Qr,.c\ 2 ------1--- -----1--- P7· w . . --- ~I ------c ----~~--::-, ' -·-----·. ---. ··---, .rJ""s_ --_ ?e1->0l'_c.__ _r,,...,,-_ -----e------ ~,l '1 Ref 14 :. NO~.Tl", CAROLINA DEPARTMENT OF NATURAL RESOURCES AND COMMUNITY DEVELOPMENT ,_· . .{,,!~t.3lON 0~ ENVIROt~~NT/\L MANAGEMENT -GROUNDWATER SECTION I F0f1 OFFICE USE ONLY Quad. No. _1=__(.,:~ .... li2.. __ Serial No .. J.!..2_9_I_j Lat.::;;-. '-! 3 D½ Long. (;OS~ Pc __ P.O. !:lOX 27687 -RALE:IGHJl.C. 27611, PHONE (919} 733-5083 lie WELL CONSTRUCTION RECORD D DRILLING CONTRACTOR __JJ/_'/? ( 1) ---G' J2Di, ,vcf '''" .\ ('/'- DRILLER REGISTRATION NUMBER __ LQJ=C _____ _ •. \-'JELL LOCATION: (Show .sketch of lho lo-::c1tion tJ•3iow) t~carost Tcwn: -r R,C' ~~ + o, :-, /\,~ I _ .5...!.1..i!Y21.-' :; c..ep ... fl~_1.l:,..!.K S £'_~I~"~;~__,~'------- (Ike.id, Community. or Subdivision and Lot No.) 2. I ADDRESS ~:f}:_f:_(;li r,., i 'r-·, .. \ -C C ~"'-'--'-''-'-c("'s~,r-e_c_\ _o_r~R'o-utc No-.')-------_y;.JlliU'l--'-'-k ______________ _ I DATE DRILi.ED 4. TOTAL DEPTH City or Town State Zip Code '; · d: 'f · f 7 USE OF WELL :Jjy,,-f'--a.Je..s___ 31/ CUTTINGS COLLECTED D Yes D No ..•. _ cor,s WELL nEPLACE EXISTING WELL? • ST/-TIC WATER LEVEi.: J7 ,5;!. FT. D Yes rn i✓o 0 Qbove TOP OF CASING. 0 below TOP OF CASING IS I • 'I> FT. ABOVE LAt,Q SURFACE •. YlcLD (gpnl]. iv',-'/ .. /, TER ZONES (depth) L1ETH0U or-TES~ tJ'i~.S~;· .-CHLORINATION Tyre iO. CASING: I Dep!h F-rom To _2_'!_ F \. I From To Ft. From To r-1. 11. GR0\cH, • '·~•Nlcrvrl---<. ·, Depth From_L __ To ·,)1,,_r-1. ,\mount Wall Thickness Di:imo1er or Weight/Ft. Material c) Material .¾ /?1/l<I\ ,") l :(_ Method /:}, ~,,(~L;: £,.}, j /._ 1J ctd.v From ____ To ___ Fl ______ _ I. SCl'<EEN: Diameter Slot Size I in. ___ in. Frorn ____ To ___ FI. ____ in ____ ,n . •. Cfl;\'VE:[ l'ACK: ~ 11 ,-J(~ Oep\/1 Size MatcriJI r-rorn ,)/, ( To 3 l/ ~~~- r-rom ____ To ___ r-t It Fl . /ll./j. Minor Basin _____________ _ Basin Code ______________ _ Header Ent. ______ _ GW-1 Ent. __ _ MW +::I I STATE WELL CONSTRUCTION PERMIT NUMBER: Gaunt'/ __J____i;, J_L_LJ ____________ _ Depth DRILLING LOG From To r-ormntion Descrip!\on If additional space is needed usci i)ack oi form. LOCATIOi'J SKETCH_ (Sllow direction and d1s1ance :rorat lo;is• two Siate r~oads. or oth8r map reference points) ! I · t' I ~-,! -z ~ s if ' C • ,;F -- -, ~ ') I' ·---··--··-·-• i .1 !: r,. I : ~ _' ._i c, , i ,,, C (. ~ '), / •f I (. •. f1EMAlll'.Soo HEREGY CEr,TIFY fllAT THIS WELL WAS CONSTRUCTED 11,, ACCORDANCE WITH 15 NCl'.C :·;,-, -... ,-~-;:~_-c-,o-,-✓s---iR-UCT10N ST AND ARDS, AND THAT A COP'{ OF THIS flECORO HAS BEEN PROVIDED TQ THE W[l ... L OV·N~Efl ----;;--;,c;a, __ 1:Litf _____________________ _ SIGNAIURE OF COrHHACTOR OR ACErn lw. I Revised 11/84 I N_QR1H C'AfiOUNA DEPARTMENT OF NATURAL RESOURCES ANO COMMUNITY DEVELOPMENT DIVISION OF ENVIRONMENTAL MANAGEMENT -GROUNDWATER SECTION FOR OFFICE USE ONLY P.O. BOX 27687-RALEIGH,N.C. 27611, PHONE (919) 733-5083 .. WELL CONSTRUCTION RECORD I DRILLING CONTRACTOR __ /:)_j!__r;__D DRILLER REGISTRATION NUMBER --~l~D=O~----- 1. WELL LOCATION: (Show sketch or the location below) I Ne a rj?s I Town: __J"'--.!LWD.l'.:n..£'-"''------------------ ~&0/Y. s 5 "-f_L_<-..l.!cl~---"-''-"---'------- (Ro a cJ, Community, or Subdivision and Lot No.J 2. I Re lf_,_,1,-, ~------------------ I City or Town State Zio Code DATE DRILLED .i,__-(). <{ -S 7 USE OF WELL ~r, QI, S ' .: TOTAL DEPTH 3<( CUTTINGS COLLECTED D Yes II;. COES WELL REPLACE EXISTING WELL? D Yes ~ No ~-STATIC \'/ATER LEVEL: 31' I 9 FT. D above TOP OF c.,SING, 131 below TOP OF CASrr,G rs _/_·fl___ FT. ABOVE LAND SURFACE. II,. YIELD (pm) /v fl METHOD OF TEST 8/) I l .ATER ZONES (depth): ') 1 -3 'I I["" CHLOR!f·JA TIQr-.J: Type /1) ft Amount ~o CASING: Wall Thickness Depth Diameter or Weight/Ft. :,\aterial From To .2_'1 Ft.-.-,J __ __1?.J!.S_ I From To Ft. From To Ft. Material MeH10d ¼ FL :: ,')r Jkls I From ____ To ___ Ft. ______ _ 2. SCREEN: I OcpIh From ~-"-)_'-!'------To 3 'I Diameter Sia( Size Ft. .) Fi Jm -~--To. ___ Ft. ____ in. ___ m I From ____ To ___ Ft. ____ ,n ___ in. 3. CRA-1/& PACK: S,i,-,d· I, Depth Frorn _"',;2'---'---To 3 t/ From ____ To __ _ 1114. REMARKS: Si1.e Jr1j(( 1:·1. l't.·~------ Quad. No. I (, 7 J !_2 __ Serial No . .J.g ~ (, 7 · Lat. 35 '-<3 O;l. Long. 8 D 58 <f' Pc __ Minor Basin _____________ _ Basin Code _____________ _ Header Ent ________ GW-1 Ent. __ _ ST A TE WELL CONSTRUCTION PERMIT NUMBER: ___________ _ County: Depth From To DRILLING LOG Formation Description .. :.{· c~F': N ·1P _l_~-Sf-P-~ 1'9cm3~i----~~L~f~:_:~; __ _ 11 additional space is needed use back of form. LOCATION SKETCH (Show direction and distance from at least two State Roads, or other map reterence points) p ,;; ~ 17 ~ S, p I ;, C w<c·--~ s· h-:. (i -,. V 1'ft,J0 S R I.S33 2C, WELL CONSTRUCTION I I DO HEREBY CERTIFY THAT THIS WELL WAS CONSTRUCTED IN ACCOROMJCE WITH 15 NCAC STANDARDS, ANO THAT A COPY OF THIS RECORD HAS SEEN PROVIDED TO I.HE WELL OWt,ER f;-27;.cqX, j,,(,,.,· '-) _________ _£ · 31-. .fl SIGNATURE OF CO/~TRACTOR OR AGENT D1\TE -~--- Revised 1 1 /St, Submit o;igin,11 IC Division o1 En,,ironmentai MHnagemcnt and copy to well owner. , .. I · N9R-fH CAROLINA DEPARTMENT OF NATURAL RESOURCES AND COMMUNITY DEVELOPMENT ,~DN OF ENVIRONMENTAL MANAGEMENT -GROUNDWATER SECTION FOR OFFICE USE ONLY P.O. BOX 27887 -AALEIGH,N.C. 27611, PHONE (919) 733-5083 .. WELL CONSTRUCTION RECORD. I DRILLING CONTRACTOR _/l)_f; ( ~D~--~<~;~!_:_C~O_:_«_cJ~r!~,·~l--~''~"-'~'r DRILLER REGISTRATION NUMBER __ _:_1-"'0'-'C~•-"O _____ _ 1. WELL LOCATION: (Show sketch at the location below) Ne ares! Town: _l___&__(_'.ill_'l.!i..8.=-------------- _brµn.o-&L~j2L:,_il\..,,JJ< s R 3 , 2' {Road, Communi1y, or Subdivision and Lot No.) City or Town State Zi:., Code DATE DRILLED ,..--.) 1-J'7 usE OF WELL /fme oh, j 4. TOT AL DEPTH 3 l/ CUTTINGS COLLECTED O Yes O No .5. DOES WELL REPLACE EXISTING WELL? 0 Yes ~ rio 6. STATIC WATER LEVEL. 3,1,i<;' FT. 0 above TOP OF C.'.Sll✓G. IR below TOP OF CASlllG IS _L 'i 7_ FT. ABOVE LAND SURr•s.:E. 11 YIELD (gpm), ___N_/] __ METHOD OF TEST ~I(. ,WATER ZONES (dep1h) ~! ______________________ _ 9. CHLORINATION. Type f1J fl Amounl __ .,_N"-'-fl~--- 110 CASING, Wall Thickness Depth Diameter or Weight/Ft !,1aterial From ) To _'2':L._ F 1. ;). ?t-'c I From To FI. From To Fi. 11 "GROV !.: Depth Me;hod Ouad. No. L G 7 !} IR Lat. 3.i Lj7, o ;,_~ Long, Serial No. _I:/2. 4bL So $5 OS PC-- Minor Basin _____________ _ Basin Code _____________ _ Header Ent. ______ _ GW-1 Ent. __ _ m "-' 1:1" 3 STATE WELL CONSTRUCTION PERMIT NUMBER: ___________ _ County: Depth From To DRILLING LOG Formation Descri:Jt1on -J ~ :_. ; (i ------\-\cc,--\-;/\_; ,·o.,-c,.-. ~---"'-~"'-+,'-ri~------ ;_,-r: -.::-, . ..,,----------,~,'------- ~ ----~------------- I! additional space is needed use back oi /r,rm. LOCATIOl✓ Si(ETCH (Show direction and distance from a! least two S1ate Roads, or otiier map reference points) n tJ 3 ~j;5 _/ I•,,; J . n f 'l ' ', ( l , f,l~ I i].(1,..,-lor,n. From __ u~•--To ,,)),&- Material F1._¾ ;,,./!ti, ' ..)Z.c,.g,-J 1..-/w....£:.lrtL , I n c! d ;" ,i I From ____ To ___ Fr ______ _ 12. SCRErn, I Depth From ~;),_,_'-I'-_ To $ Y Diameter Sia! Size /.',alerlol Ft. ,) in .. [:;J<.) in. P&'C F!'Jm ____ To ___ Ft. ___ _ in. ___ ,n I From ____ To ___ FL ____ in. ___ in. 13. ~.~-\fµ---f'ACK >11,vcl ;)),(, From :C:: Depth 3 '( Size To_J le' Fi._JY/_c_f_;oc('-• _ ~ From ____ To ___ Ft. ______ _ 114. REMARKS, C 0' wcci' (/,,i, I~ i,s ! Cl 2C. WEI.L C01·1S1RUCTION I DO HEREBY CERTIFY THAT I.HIS WELL WAS CONSTRUCTrn IN ACCORDANCE WITH 15 NCAC STANDARDS, AND THAT A COPY OF THIS RECORD HAS BEEN PROVIOl;D TO THE WEI.I_ OWNER. SIG!t~-:0-1/i?:c~i-r-, -0-Fi_A_G_E_N_'f ______ _ I GW-1 Revised 111a, SutJrnit ,:,:igin;:il lo 01-1isio,; Of f:rwironmental Monaqe.ncn: Jnd coo·r :o -~••Jlt owner I t>rmn1 CAROLINA DEPARTMENT OF NATURAL RESOURCES AND COMMUNITY DEVELOPMENT DIVISION OF ENVIAON"'4EITTAL MANAGEMENT -GROUNDWATER SECTION ~___,.7.0. BOX 27687 -RALE!OH,N.C. 27611. PHONE (919) 733-5083 FOR OFFICE USE ONLY Quad. No. L-(, '/ c, 15 Serial No.}:/? 4/-)J j -.. WELL CONSTRUCTION RECORD I DRILLING CONTRACTOR ----'N'-"--.!\<.-=:...:C...:c.b=-_-__,G'--'11"--"-"-"''-'-N'-'(1/'-C, W=-,1.:...'.:...' ·__c· '''--- DRILLER REGISTRATION NUMBER--~~-~"-----~ Lat.Jr'." 1.1~, OL· Long. Be S"b C~ Pc __ ,".1inor Basin _____________ _ Basin Code _____________ _ Header Ent. ______ _ STATE WELL CONSTRUCTION PERMIT NUMBER: ; /V 1 GW-1 Ent. __ _ 1ll=1=.=W=E=-l=.t=_=L=O=C=.~=-=l'l=O=N=:=(=S=ho=,=,=,=.k~e=1c=h=o=l=lh=e=lo=c=a=1i°o?'c:n=b=c=lo=,=.,)========================c I 12. Nearest Town: -r-Ro,.n-1"' r.-N c-C" ,-~V::\(..Jj.S, -...... fflt I c_ \ tf\Wf, (Head, Community, or Suhdivision and Lot No.) OWNER ~I k. C.j') · C~, ><.1w...il::, ,-ft'\ r,'i'c. AODRESS (Street or Route f✓o. 1-:i .,: , Clly or Town S!JIG Zip Code DATE DRILLED e. 2s-s7 USE OF WELi. IC1-<1'il--~c,~l~,Ls __ 4. TOTAL DEPTH 2,<). G CUTTINGS COLLECTED O Yes (E No 15. COES WELL REPLACE EXU)TIJ'I_ G y;ELL? 0 Yes [8-No .,3':/J.'F . G. STATIC w.:..TER LEVEL: ~, · FT. 0 .i.bove TOP OF CASING, / !;,;"below I TOP OF CASING IS __ .'il_ __ FT. ABOVE LAl·JD SURFACE 7. YIELD (gpm)· I J /f, METHOD OF TEST __ ll_/~(_\ ___ _ '\'/ATER ZONES (dep1h) -~:~~~~''-~~~~ -~~-:~. 9. CHLORINATION: Type 10//t Amounl __ /_,,~/_;,-,_, ____ _ ---.. --.. ·--- lo CASING Wal! Thickness Depth Diameter or Weight/Ft. Material From 0 To Z'i, Ft. ., I"-' c.\ C 3:.· , \ (\ ,; . ( . I From To Fl. From To Fl. ,'.1ethod D From ____ To ___ FL ______ _ 2. SCREEN: \Jc-,:•~~ VJ g!_,'Jl~·il rq//,{',,( 08pth E 1 Cl ?1 .::1 r=rom ~ I To Diameter Slot Size M!!l8ri,il r-1. ·.1.' ,, 1 in ... C> ·· in P ' . .:' · ... ---- r:rJm To ____ in. ___ in. 13 From To GRAVl.'L P.<CK: ___ Ft. ____ 1n. ___ in. __ _ I, From Ooptr1 To s_,9 D FI. From ____ To ___ Ft. ______ _ tiialer1al Deplt1 DRILLING LOG From To Formation Description LOCATI0/1 SKETCH (Show direction and distance from 3! le~st iwo S!ate Rocids. or other map rrerence polnts)c:::::.L __ _ \ r: ... --:,,,-pr ,c J_\\ l fl , ! f"D. , ~-J i...J () ~'..!. ::.'., -.!_ .-· t'•T $ ,,, :;t(:.f>'..'),.,; ::..~·f.-711" 14. REMARKS I DO HEREBY CERTIFY THAT THIS WELL WAS CONSTRUCTED ICI ACCORDAl·ICE WITH I 5 NC!,C ST /,NDARDS, AND THAT A COPY OF THIS RECORD IIAS BEEN PROVIDED TO THE VIEU. OWNER. 2C. WELL COi-.JSTRUCllON I ___:-Tn-a .. .:>11.L'j I ;, 1ii:_f~1; ____ _ SIGNATURE OF CONTRACTOR OR /-.Gm l GW-1 Revised 11 /8,t ~-,,.1· ·! •/_(QUtJTY: ----1· ::.' () ;. -I --- -RIVER 8ASJN: r-,-.P-,. RRO. WoRO WiRO WSRO TS I/ .. D"J ,i.';•: ,, '.'.'!" ·-t~ REM ARKS Station Number Date· Begin, "yy/mm/dd/ lime Begin Dale End Tionc End Dcptn OM D8 DBM Value I ypc Composi!c Sornp/c Type £'2.-. 5, L·L _L_, __ __l __________ ~,.-:,~1:~;,7.~, 1,_'._J_J~,_10_'~_"_·_,_,~J~J_c-_. _t._· -'--~lc.... __ ,_l~_-L ·-~.---',----------'--A---"--~'~~-'---------'----- l s • C G GNXX __ .._ . .:~-::: 0 2 3 4 5 6 7 8 9 10 l l 12 13 14 15 16 17 18 19 20 .· Boo,. 310 COD Hioh 340 COD Low 335 Coli!o,ni: MF F.,col Jl!dt, Coliloim:MF Tatel "'''"04 Coliform· r"ube Fecol 31615 C~lifo,m Tub~ To!ol 31505 Re,idue· Toto!<~" lnH 403 Vo!oii!e" 505 i ended "-30 Volotil.:-S35 ACiditv io nH 4.5 436 >---+A=ci~ to oH 8 J 435 Alkoli11itv to 8 J 415 All,,Qlinilv !o 0H4 5 41() roe 680 mq/1 Chlo,!d., 940 rTIQ/1 "-.( A,~cni<: Total .lQQ2 mQ/1 Chi a: Tri 32217 1100ml Chi c·Corr '\2209 1100ml Pheonh Jin o 32213 /JQ0ml Color: True 80 /\QOml Chromium: Hex. 1037 mo/I Cvonide 710 .. mQ/1 Fluoride9<;] ' :..::.-ma/! Formaldehvd,:-71880 . mo/I Greose ond Oils 556 ma/I mo/1 1 _ MBAS 38760 units ' Phenols· 32730 mo/I mg/I Sulfide 745 mg/I Specific Co"nd.95 mo/I Biomoss:Orv W!. 573 mo/! BiomOss: Pe·,; Ash Free 572 NTU Chi o: Peri Fluro 8?.54 7 Sampling Po;n1 Weier Temperoture("C) D.u. pH A~·. 1; Se(chi (Melen) 8 78 l H,. Se11lcoble C Ma11er(ml/l/H,.l 50066 OM l/ Revi1ed 7.55 10 Air Tempero!ure ("C) 10 Dead Fj,h Severity 1340 300 J. 0.0. % Solurolion 301 Turbidity Severity 13 so 400 1. Solini ! y '.t. 480 Odo,:Atmosphcre Severiry \330 mc:/1 NH1 as N 610 mq/1 .. IKN os N 625 mo/I u<>il ma/I PQ4 as P 70507 mq/1 uci/1 p· foto/ OS p 665 mq/1 Pr-Co · ug/1 .. j( Ag --Silver 1077 ug/1 ~n/1 X: Al -Alu-;,i~um·1105 uq/1 · -'ing /I Be-Ber~llium )012 . .-)f~~ . ;;,q/1 Co -Colciu;,, 916· · n1Q/j )'Cd-Cadmium 1027 me.II · r,. Cu Co;.. er ·1042 UQ/j UQ/ I X . o·,>, Ho-Mercur .·-,1900· <) uo/1 2 uMhos/.;n, Li -Lithiuffi 1132. U~/11 2 9/.',1 2 9/,',-\ r-c;t·"M0\o~-"M'""oe"-o"=•=•ci',_,cm~9c.;1c.7c._-,·0-0-0~,-'.,,~C/ __ ~_9_!J r-)<_.1M=o~-cM=~c"a~'c~c·~c• ~c·•='•c;cOcScSc·_.c-~=~c'_:._.C~C-._._,C/,,_ ~~ X']No Sodium 979 ;;;· ~-'3 m9/M Conductance al 25°( 94 A Igoe: Floating· Mais Severity 1325 Stream Flow s~verity 1351 A!kolinity PH 8.3 82244 Precip1totion (ln_/0oy) . .' 45 Oe1ergent Suds· Severity 1305 , pH 4 .5 431 · . (!oud Cover: 31 Oi1-G_reo1e Severity 1300 ' _,Y Ni-Nickel 1067 ua /) :, :> u Pb-l"od 1051 o< I - Sb-Antimony 1097 uo/J S,-Seb,ium· 11.!Z l!<.J_::J y Zn-line 1092 _ __z ~_-50.u uq/1 Pesticides SoNificollv Scan Orgon6chlorii-ie Scan OrgonophosphoPJ~ .X Orqanics Speci!icolly Scan Bme /.Ncu!rol Extractobles Scan Acid Extractobles . Acidity PH4.5 PH 8 3 82243 877·47 . Wind Direct;on(Deg .) Wino fore e :,d BeoufOn ('I) 36 37 ,.., Floating Deb,;1 Sludge Severity -Severily V< 1]45 13 l5 ' ' ,',, Rep~rted by J?J!J2 I Checked by 1 0 ,M .. ,pervisor C!(:?,(., ORGANIC ANALYSIS Entered by~ ~( Checked by I:)!= I Lab No. Sample Type: hh:z,Y-e,v Analytical Results I 7; 3tJ3' ,/~ /J(L,_ -, /" A _/. ' • " Q I ',,,;, "f ",J : /~ ;½fl, ' d ;J;jJ,.,, AA ........... ('J ,;r--_"" -A~ -_... I "12 0 / d :y{J_ .I T.;::., ,,, ::ti./ / -/ I, -1) 11 I A r (~ / . --k /;-;:._ ' -I>,,,-+· _-+. ti ,,,_ -/2 --I; ; ' " 0 I ;t;;:: ~ J, '-1,..-rJ ,,,-/-_ ./ ,.I, . I A, n 7}T,, (/ /17,-;✓,;'. r I ,I /1 ~ /],./ h ,. . /..,..,.,: .,,.,/ I Alf-, '~ n -hf . ./ / /.,,,, n Q .J 'In / -/-'f'/ ·- ,; . ./, ,.. , _.,. I ' J ~-/ -.... -: ..... ,, ~ .,./· -.,.,, ,.. A fl... • .L.L /} / // Ir, ----.I x, ~x ' ~ --_(', L.:,_,_ .. __ v n ,{.,I,_ f /)JJJ,, A r ' 0 I -t-,.,,, 1/Jo.-./A /I, -1,;,,h;/ L 1 l~c/.4, ~ I,__,__ I A•*' ~*f ~~-/:-r I A ' ' I I I I ~ . I ,_ I ___ GC/HS/DS used .. Concentration I A /~/f , {/ , /d £0 29 /'1/0 ~0 /7 -< 2 - ::? ;, 0 /s-oo -- I .. I I I I I I \ 0 I I I I I, I ••HS T-554 STATE OF NORTH CAROLINA DEPARTMENT OF HUMAN RESOURCES SOLID WASTE MANAGEMENT SECTION SOLID WASTE BRANCH SEPTAGE MANAGEMENT PROGRAM APPLICATION FOR PERMIT TO OPERATE A SEPTAGE MANAGEMENT FIRM 1. 2. 3. 4. 5. 6. 7. 8. 9. 10. Owner's Name Address City ) t-C\:\-:.;..S V> ·. \\ c State_~~ .. ·~---- Business Name Address Phone No. City S+-sJ±-s~u·Yle State '{\. , 7g;'.f-= --~ g''lS( county ,. Q c:e c\ ,-\\ Hazardous Waste No. ( if applicable) I'.\( f) ◊ (p :l 5 S $ 1 q.;) Service provided to: Residences ,._/, Restaurants c/, Industry~ Small Business t/', Other _ilSJ'\'\'S-- Septage disposal method; PretreatmentjSoil application J. Soil application/ Incorporation_<.-/_ Approved wastewater treatment plant __ Name & Location of plant _________ _ Location of all septage disposal sites (S.R.#): /.3 J ·), [,.~:·obf:l ;, Disposal method for washings from the interior of septage hauling containers; he Id,·,, aq (2c· 1,c\ '\ -~o 101,,I Location of the disposal site for washings from the interior or septage hauling containers; fl_,\. I 4 (~ l) -f. •':\ '.)(-. j •+ C, \-c:. ':-> L: . \ \ ·c_ \\ • (,, d,'{ \..o ,-i '\ Do you possess a valid permit to operate yes no ........ ~ I certify that thP. j_nformation provided above .is lrue, r:omplete and correct to the best of my knowledge and b81.j_ef. n C::i , 1\~"'\\"·'--' ,) --I )_ --d (1 Date I .. I I I I I I I , I I I I I I It I I 1. 2. 3. 4. 5. 6. 7. 8. 9. STA TE OF NORTH CAROLINA DEPARTMENT OF ENVIRONMENT, HEALTH, AND NATURAL RESOURCES DIVISION OF SOLID WASTE MANAGEMENT SOLID WASTE SECTION SEPT AGE MANAGEMENT BRANCH APPLICATION FOR PERMIT TO OPERATE A SEPT AGE MANAGEMENT FIRM Owner's Name Address Business Name Address Phone No. City .j k;../e,:. u ;t{,. State //), t:, City 5 ..\.a,+ "'i (,; : 1 \ e State~I'\~, ~<'~·~--- ? uv -~73-£9Sy Coutny ::C::<c ,1, ii Hazardous Waste No. (if applicable) Y\ C Q Q lo ,-il S '.S Sr, c\..J. Zip. ,:i £ C, 7 7 Zip. ex ')' (;, 7 7 Counties of Opera to in; :::r-r c;. c! <-I I . ro ,::_ c. ):, \-'-"' b v: C: Q c, '-'--' c."'-A 6 "-/c;, 1,,J c.: G . ' ' 6 ' 0 1 /l ' G<,-\-n-', 'J:--f"> c,,s;)\.v:,,. ~oc,,,+'s 1 U'\,v(1..6u.<''l<"'-, l\t,..,,\,-,\...11},, ; ) ' ) I F c..c. b C> it 'I,.-,,,, CG:\-Cl"'-' i:J 9, '-'--' ~11<..e..S., yct cl X ,u, =c,•-\-6.J(\ c, J S.\-n "'\. '-\ · Pumper Trucks; Number Operated ct. 1 LicenseNo. 4P-$1J&'. A Q --!l.JJ1 Serial No. C.:f lL\3 S: u 1\0'3q1\ lokC ;:iJ; \-\--Jq <J •~'1-D~----- Capacity 3 Soo gal. 1 s ~ o gal. -----~al. -----~al. Pumping equipment ~, C\ S, . .,-i .. ,.:; -tSS/ <..cl n, »"'(", n r • c:::c ' \ t--' µ.! 1 JJ Service provided to; Residences t...-;"Restaurants__L.6"Industry '--;' Small business ~her.La ,·m '5 Septage disposal method; Pretreatment/Soil application.....:::::;-Soil application/Incorporntion-=::::. Approved wastewater treatment plant __ , Name & location of plant __________ _ Location of all septage disposal sites (State Road#); / '3 3 3 ; L' , >~ Q \-Q Q <1 ,"j -k,+c. ,> u; I\, 0 Disposal method for washings from the interior of septage hauling containers; i--\o i <i . " c f?O i\ sci 'S ~ I I Location of the disposal site for washings from the interior or septage hauling containers; Q ._\. i 1_.l :6of-\50 b:\:c,;4"-Su,\\t,,. \'),<:,. dli'(,']rl ' 10. Do you possess a valid permit to operate yes /no __ . 1 certify that the information provided above is true, complete and correct to the best of my knowledge and belief. OHS :]'.55-4 (lmplcmenLcd 8/89) Solid Wc1stc Scc1ion (RL-....'iC'\,\' 8/91) Date I .. I I I I I I I , I I I I I I. 2. 3. 4. 5. 6. 7. 8. 9. 10. STATE OF NORTH CAROLINA DEPARTMENT OF ENVIRONMENT, HEALTH, AND NATURAL RESOURCES DIVISION OF SOLID WASTE MANAGEMENT SOLID WASTE SECTION SEPTAGEMANAGEMENTBRANCH APPLICATION FOR PERMIT TO OPERATE A SEPT AGE MANAGEMENT FIRM Business Name A-~A C '?Jtrt, pc; 1 .c...'.5· Address O :± 1 lj 0-:,_,:/-:3 <,; 0 City s +a+< s ", ; 1 , State._.,_Y\1.a,wC.._,_.......,~-~--Zip J .£:& 'l 7 Phone No. n o'I) e 7 3 -tr q -:;-y County, _ _., 0 ,..-::..,U,._._r s:,._.,_d ... c--.ul ''-------- Owner's Name H~H : ,; '. C ?' f»'.\ ~ Address /1 :± _I ~{ Jj c! / _ .3 S:O City 5 ta f-c-$ u; I IC, State__,(\...._.,..c( ..... cc. ______ Zip d ,\':t:. 7 7 Hazardous Waste No. (if applicable) ____ _ Volume ofseptage pumped each year {.Jt.,i,1 poc, gallons • C,,unties of operation; _ _,J}--"-'--"-"c..sd.,,cc.-+/-Ll-,,,----'/1,"-'--'olii-'.,,""-l<<-2'-''"'''-r-·.c:•V\=c..""c""°'k'"'/'-'ee...:..,t\..i.W"'· '"':_,t\Hi--'A-'-'-/-"c:c..Lf_,v":\•,,.,,.c\co"-C-10.o.,,,-h.. :\'.\ C."-' Lp,, <!-a +-au,; b C. .., .> Pumper Trucks; License No .. A-5 · :5' {J9 Serial No. ? s :r. ':I 3 y u :, l O 39 ;:. ) .:rv l,{p a O d a q 9 .-z. 10 Capacity ·ye?OO, / $'00 · Pumping equipment (Vacumyb. Diaphragm c. Other ___ · __ _ Number Operated._~~-- Service provided to: Residences_:::,Restaurants..::::.,, Industry__::::' Small business ~ Other_ Septage disposal method; Pretreatment/Soil application_::,'soil application/Incorporation_, Approved wastewater treatment plant_, Name and location of plant, ________________ _ Septage dis osal site permit numbers (SOS#)# dt, ·O<:'), Date issued i \·IC/ ·'/0; # l'/t,·,Y~ Date issued · -00 ; # j '-) (o-G~, Date issued 11 · 19 ·C/n ; Not applirable l'I I '-1lD ·C,6 .1 i I -/11 -'/0 Disposal method for washings from tile interior oi septage hauling containers;,_-l=C'-:..:.(..,_-<_;>c..c.J_L_1 '-'J:/ ____ _ ,,J('5 Ce../:., , Location of the disposal site for washings from the interior of septage hauling containers; (i / /, .C: "-' I certify that the information provided a hove is true, complete and correct to the best of my knowledge and belief. Date DI-IS T-554 (Implemented 8ill9) Solid Was1c Section (Revic-w 8/91) Printed on Recycled P;:ipcr I .. AUTHORIZATION TO DISCHARGE SEPTAGE TO A WASTEWATER TREATMENT FACILITY I I I I I I I D E I I I ll I I I' Robert L. Griffin. System Protection Manager Plant Operator or Authorized Representative Charlotte Mecklenburg Utility Department Wastewater Plant ..... •.-..... ·;:;:;:::;:;:\/\;/)::/\ Bl£~~1;1cb&w1J@1tel:fllrJC 2s216 , 7011 3 94-9 2 84 5100 Brookshire 'iiJM h Address/ Phone i!f~mber EXT 132 do hereby authorize _.,R.,.uu,blJYuiic:i;s"""a ... g-me.oCLnL__ _____ ;"':""!"'L"--------------- Sept<\Q§i Management Firm)I§.:':'ner /Operator .·>:-,:-:-:-:;;:-· ..•. ., .•. , ....• s igmon Environmenta'1,iiiinc. f of This d~lrt! December 31. 1996. Signed Date Note: Falsification of this document by the septage management firm shall lead to permit revocation. tllu\.lµemcm.sep I I I I I I 0 I I I AUTHORIZATION TO DISCHARGE SEPTAGE TO A WASTEWATER TREATMENT FACILITY .Jacqueline A. Townsend, P.E.. System Protection Manager Plant Operator or Authorized Representative Charlotte Mecklenburg.,Utili-ty~Department (704)394 9284 nt until 4 p.m. Sat. This authorization shall be valid until December 31. 1997. I, Signed d \jFacility Operator · Date I Note: Falsification of this document by the septage management firm shall lead to permit revocation. I - ,.-::;:i~-~~rt4r~-1:@-~l~~t;.~.~~,~~~~~ft!i~~-~~~~'lT.tP."!f,"',tJ½~N~-~~11t~~.n,n,-;-..r~ml?~\{tt(1~t:ll.·~':i;>'~~;'iti'tt~~;c:_~}ii:~,~ 11;.'.,~1""!tf'":~·-·} .I '• -... ,. NORTH CAROLINA DEPARTMENT OF ENVIRONMENT, HEALTH, AND NATURAL RESOURCES PERMIT TO OPERATE A SEPTAGE MANAGEMENT FIRM Mary Louise Sigrron (Name orpenon awlYVl8 fur permit) Sigrron Environmental, Inc. (Nameo[Firm) PO Box 6415 Statesville, NC 28677-6415 (Addre:i.a, City, State, Z.ip Code -County ) is hereby issued Pennit Number NCS O0l46 to operate a Septage Management Firm in accordance with the provisions of North Carolina General Statute 130A-291 .I and title 15A of the North·Carolina Administrative Code, Section 13B .0800. This permit expires on Decembec 31, 19 5!2._. This permit is issued to the above named person alone and is not transferable to any other person. This pennit may be suspended or revoked by the Department in accordance with the provisions of North Carolina General Statute 130A-23. This pennit is limited to operations conducted in accordance with the representations submitted in the application.for this permit. The representations contained in the application are incorporated as conditions of this pennit. This permit may be suspended or revoked upon a finding that a .violation of the applicable provisions of the statute, administrative code, or condition of this pennithas occurred. It may also be suspended upon a finding that its issuance was based upon incorrect or inadequate information that materially affected the decision to issue the permit. Date ----"--')._--I-!=]""(! /'--q'-"'7'-------7 7 DHS T-579 lememcd 8/89 Solid Wast, Section ------== liiiii iiiil ---·-- I I I I I I I {' D D E Ref 17 (./) APR 8 199! 2: _J State of North Carolina Department of Environment, Health, and Natural Resou Mooresville Regional Office 'M NA~'V James C. Martin, Governor William W. Cobey, Jr., Secretarv Albert F. Hilton, Regional Manager DIVISION OF ENVIRONMENTAL MANAGEMENT Mr.· Barry Sigmon A.A.A. Enterprises, Inc. Route 14, Box 350 April 8, 1991 State~ville, North Carolina 28677 RE: Dear Mr. Sigmon: Groundwater Sampling Results Sigmon Septic Tank Service Groundwater Incident #3422 Iredell County, N.C. On August 9, 1990 you were issued a Notice of Violation (NOV) from the Division of Environmental Management (DEM) for violation of the North Carolina Groundwater Standards (15A NCAC 2L .0202). In the NOV you were required to determine the vertical and horizontal extent of soil and groundwater contamination and to submit a site assessment report within 60 days of receipt of the NOV. On September 5, 1990 I met with you at the subject site along with.Karl Shafer and Steve Clayton from the Solid Waste Section, Division of Solid Waste Management (DSWM) and Scott Readling from the Hazardous Waste Section, DSWM. During that meeting it was decided that you would conduct, or have conducted on your behalf, a preliminary site assessment which would include the installation and sampling of two monitor wells per the Groundwater Section guidelines and the sampling of the ten surface impound,nents per the Hazardous Waste Section guidelines. Based upon the results of this assessment a determination would be made as to what further actions would be necessary in order for you to achieve compliance with North Carolina law. • I • I I I I I I I i' I I I I I I It I h I / Mr. Barry Sigmon April 8, 1991. Page Two· Staff of the Mooresville Regional Office Groundwater Section received the sampling results for the two monitor wells on March 19, 1991. The results indicate that groundwater at your facility has been adversely impacted. The following constituents were detected in violation of North Carolina's Groundwater Standards: Constituent 1,1-Dichloroethane Vinyl Chloride 1,4-Dichlorobenzene Iron Manganese Concentration* 1 2 3 20,000 17,500 * In micrograms per liter 2L Standard* ND .015 1 . 8 300 so ND -Not permitted in detectable concentrations The DSWM issued a NOV (Docket #91-127) to you on March 26, 1991. In the NOV you were required to characterize the liquid waste from and soil underlying each surface impoundment by May 1, 1991. It is our uriderstanding that if characteristic hazardous wastes are found or it is discovered that Sigmon Septic Tank Service has been operating a hazardous waste disposal facility, the N.C. Hazardous Waste Section will assume jurisdiction of the subject site. We a~e currently holding the DEM August 9, 1990 NOV in abeyance, pending the timely completion of the sampling required by the Hazardous Waste Section. If the sampling reveals that hazardous wastes are not present, the DEM Groundwater Section will re-instate the NOV. We would then require that a complete site assessment be performed to determine the extent of the soil and groundwater contamination. You would also be responsible for developing ~nd implementing a plan to restore groundwater quality based upon information gathered during the site assessment. If you have any questions concerning this matter, please do not hesitate to contact me. Sincerely, _ ... t~ 1)-c::cc! Chris DeRoller Hydrogeologist cc: Incident Management Unit Hazardous Waste Section Solid Waste Section CMD/pl Ref 18 State of North Carolina Department of Environment, Health, and Natural Resources I James C. lvlartin, Governor William W. Cobey, Jr., Secrrtary Mooresville Regional Office Albert F Hilton, Regional Manager I I I I I f' I I I I I I la I I Scott Readling DIVISION OF ENVIRONMENTAL MANAGEMENT September 7, 1990 Solid Waste Management Division Hazardous waste Section 216 Forsyth Street Thomasville, North Carolina 27360 Dear Scott: Please find enclosed the information on Sigmon's Septic Tank. I have included the results of one sample taken from one of the lagoons in 1987. If I can be of anymore assistance, please contact me at (704) 663-1699. ~gt~ Hydrogeologist Enclosures CMD/pl 919 North 1'11..ain Srm:·1, i'-korc-,:vilk. NC n:15 • TclQhonc 70-l-663-1699 • FAX 7f}4.663·ffi40 i 1 ., ' ' t ,,_ "' -, -~ 'j 'tc. iiiiiil - I '---_;_-_-___.--- I --- ' -i---~',--- L I 1·1 --.1---,-- ! ! I -- i . . ! - l -----. ! __ i l I -------·-· ~-----1 i i -r ---- I !. ' I I - r - i !!!!!!!I -- ---1-, -:1,.--~. _ C<--·i..c( /.~/;;i,,,:). II~_. _A);!/~.--!..u~/t;_ i,v14:f~~, _ I ' ' r, I ;/ / ·,I ----~i,,::t :5{<-h><-91,£1:~;J _ fiq-~t-tc~--.)---~:~(-_t.;t£~t- . __ ,,,1,,,,J:z, _ /iv, elf /'Of' r.f.J-11.c St'--"'j"C.:.. t,,0_,(-a..,fu.~w ___ _;Ju. S</-v;'/?:-: _l;;c_~-) C#t,u)_1-1,o_f __ f1.~/1,_71_~c-! o!~ifd-.r!.7 ./2.c {a,Ji.c0_/}cY1c.l 7:_)co.,/_ 1/-.?lR .. /] · '' · 'I '·ii I ___ V«'C&\..t/ ,:i=,-t/e,l_./;,::ucL,!_ bctn/'(_ __ a.{.(,J:fc...L --~( . ~-U[Ot,{1,,d )f. . -----. ---!__ --~-:-~------ ;--· ------------·--· liiliiiiil ------i -------! -I :-. ._~-<: C, I I I J f ,\1--ll---+---+--J 1-+--+---+~c:-+-, ~-I!:= __ ::::!=?_, ~~~---t--1t--1t~=+--, I ' , I I -1./: z -- Vu A' I I ,. (vl-{'J + re =5 [2, ' vese11v1 tJb h, " rle ---liiiii - 11 ,_ z f-tc:-, I 1,./ t-'il"""-'l'--'-'-'-'-+--+----1-----+---1-------:l---1--~"---'---'--+-'----1----1------- ("---"-'-'"'-t-----+---+---4----1-------l,-----f-----+-~fis-+---+---f-'.:7=--- r q 7>_'-'---<d-+<,;..+-----+-----+-----1-----1--........J :; I :I NC. Department of Environment, ~ SAMPLE ANALYSIS REQUEST • I k:illh, & Natural Resources Sohd Waste Management Division ZN State Labontory of Public Hcahh P.O. Box 28047, 306 N. Wilmington Street Raleigh, Nonh Carolina 27611 ... ilc Number _______________ _ Field Sample Number __ ___,_~"-0_,_l...:7 _________ _ Sile Location. __ ~e::,:,,u.:..e(u_""'----------------__ Name of SitcS,~M1Jl\ 5erh,/AA-.4 (W/pl't\l..,l I Collected ByGlc,,;,r (H.ar-1:)'v'-/l::w,1.. ID# I'> /,.J/ 11 Date Collected. __ 1''-l/'--'1-'/_"i'cev<:.-----Time__,/-"3'-=3"-'c"---- ' I I I I u I I I I I I Agency: ~Hazardous Waste Solid Waste _· __ Superfund Sample Type Environmental Concentrate Comments __ Ground water (1) _ Solid (5) __ Surface water (2) ~ Liquid (6) _Soil (3) _Sludge (7) I (1 I·,,._. , Other ( 4) _ Other (8) Organic Chemistry Parameter _P&T:GC/MS _ Acid:B/N Ext. MTBE ---- ---- ---- -- ------ Results(mg/1) Radiochemistry Inorganic Chemistry Parameter _L Arsenic ✓ Barium Results(mg/1)~ L..o.o-\ ~ Cadmium Chloride i/ Chromium __ Copper Fluoride Iron --./ Lead Manganese ,/Mercury Nitrate D, 8 8 0-Qc).\ L....c.:::,"r L..o,aS I ····~~;ameter Results (PCi/1) v Selenium t/ Silver Sulfates Zinc --_pH I I __ Gross Alpha Gross Beta Microbiology Parllmeter Results (Col/IOOml) __ Conductivity TDS --TOC TCLP Compounds Inorganic Compounds Arsenic --Barium --Cadmium Chromium --Lead ·' Mercury --Selenium --Silver Organic Compounds benzene --carbon tetrachloride Results (mg/I) Results(mg/1) --------- -- chlordane chlorobenzene chloroform o-cresol m-cresol __ p-cresol cresol __ 1,4-dichlorobenzene _____ _ 1,2-dichloroethane --1,1-dichloroethylene ______ _ = 2,4-dinitrotoluene __ heplachlor hexachlorobenzene --hexachlorobutadiene ---------hexachloro•elhane ----methyl ethyl ketone nitrobenzene --penlachlorophenol = pyridine __ tetrachloroethylene trichloroethylene --2,4,5-trichlorophenol --2,4,6-trichlorophenol = vinyl chloride . endrin ' ~=- :;:~;._,~rc:~:~r~-~-~~~~~"'~:.-.,~:'=:Ci,if:'o=2~i~·:~_f@'fffttyS:c-"fc~~ifri~,-~~~.~PI;,;,s~1:,:' "''"•W•'~e~*:y'lHio'/'i-',-,, ,;;w;.;;~;,c,,~~.,~;:;;:;c~;;z;;"',t• . -. , . . . -. ---_______ ···-_. -.• . , , -~ lo~ap~e_ne, ·, Dote Extroc'tccl _________ Date-Reported._________ __ 2,4-D ______ ,· _ 2,4,5-TP (Silvex) ______ J I Dote Analy-1.cd Lab Number -.-c-=c----------------l)IIS Jl'Jl (Revised 2/91) N.C. Department of Environment, I I lcalth, & Natural Resources · Solid ~astc ManagcmCnt Division SAMPLE ANALYSIS REQUEST State Laboratory of Public Hcahh P.O. Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611 . 7, wile Number _______________ _ Field Sample Number __ _,_C/_.0:.,0<--J.9 _________ _ __ Name of Sile Si5rrc,,-, .fepf,\/4-li-JJ,-(r,krpr, k4 Sile Location f u.MO- I Collected By (rfi-..~ y /t-1ttrf--/vi Date Collected '&;/JI /fz, Time_,_/7-'--''"'36_,__ __ I Agency: _2{__ Hazardous Waste Solid Waste _· __ Superfund TCLP Compounds -- Sample Type Inorganic Compounds Results(mg/1) Environmental Concentrate Comments Arsenic I --Barium "P7 -/<J --Cadmium __ Ground waler (1) _ Solid (5) --Chromium -- D _L Surface water (2) _ Liquid (6) Lead ----Mercury ·_ soil (3) _ Sludge (7) Selenium -- I Silver _ Other (4) _ Other (8) ---- -- I -- O_rganic Chemistry Inorganic Chemistry -- Parameter Results(mg/1) Parameter Results(mg/1)(,glg Orf!' Organic Compounds Results(mg/1) I _ P&T:GC/MS ,/ Arsenic ..::.:. 0 -ct1 benzene ---- Acid:B/N Ext. ...L Barium D,O-C carbon tetrachloride -- MTBE ~ Cadmium ...-.:....q.o, \...Q. chlordane -- --✓ Chloride Jj' chlorobenzene -- --v Chromium "'-..O_oj chloroform -- --_,L_ Copper <o. o,r: o-cresol -- I ' / iii . le m-cresol ---- / Troe_, p-cresol ---- --...L Lead ..:::....c:,_c,~D cresol --- I --~ Manganese (), '.]?: --1,4-dichlorobenzene --~ Mercury 4...o. aooa --1,2-dichloroelhane v Nitrate ( loo 1, 1-dichloroethylene ------ I ✓ Selenium -"--o-i:.'.:l 2,4-dinitrotoluene Silver L.o_ o'=> = heptachlor _:L._ Radiochemistry ..:,/_ Sulfates LL,_ hexachlorobenzene -- ······--.JL_Zinc <o. o.c hexachlorobutadiene I -- Paramd~r Results (PCi/1) 2._pH '1-0 hexachloroethane -- __ Gross Alpha ~ Conductivity 'jl.o.S ,~~ methyl ethyl ketone -- Gross Beta -'=-iii jg Q r nitrobenzene ---- I _iL TOC 6,o,p½•• + d.Ql':1 __ pentachlorophenol __ pyridine -- Microbiology ----tetrachloroethylene I --__ trichloroethylene Parameter Results (Col/lOOml) __ 2,4,5-trichlorophenol -- ----2,4,6-trichlorophenol --= vinyl chloride ----en,drin liiidanc i I -f ~!:!~~~-~;-~:!::';~';·:·:~:~!:~~~~~~cd:~:i,•:~,~~cc--"••:·~,~'~"'"'''··cc~,,:;, ~S'.2·::£" :~~m,,s~ry~x2:t-1t!<?L·_~ .. _·;, . .i.:~-· ;,.c!"---, :-~· ,···"'·--".,...,,.. .. _-_. ,tox.aphene. . · ··: · · ~:--.. _,,·.,; .. rj.~6?;tt""EXtr'"a7:rc;_f ··--:·--~i--·, - , ..... , ••.• --~. •, .. •• oa'tc"· Report Cd -. . ·. -.... 2,4-0 · .· . · _ 2,4,5-TP (Silvex) ' I Dale Analy,cd Lab Number ; ,Ill IS 3191 (llcv;scd 2/91) -- ~ ') c,..-: A ·• N.C. Department of Environment, · 1 lc.ilth, ~ .Natural Resources &>lid. Waste Management Division SAMPLE ANALYSIS REQUEST State Labora~ory of "fuolic Health P.O. Box 28047, 306 N. Wilmington ·street Raleigh, North Carolina 27611 ! -, .. itc Number _______________ _ Field Sample Number ___ f/,:.oOC-J../.::D __________ _ Site Location eufufe~ _ Name of Sitc,SJ);lmo-o fi.rf,Hc/MA: Drf:«pns(..J I Collected By[tiC<'><,/Ma.fh.,,/))co,.,, ID#l'l/2>t/q 1 I t ; Date Collected 'j /, J ~,z., Time 0"/::lO ~''--'---------------I Agency: _J{_ Hazardous Waste Solid Waste __ Superfund TCLP Compounds I I D I I I I I I I I Sample Type Environmental Concentrate __ Groundwater (1) _· _ Solid (5) _i_ Surface water (2) _Liquid (6) _ Soil (3) _ Sludge (7) _ Other (4) _ Other (8) Organic Chemistry Comments t',S-LJ Inorganic Chemistry Inorganic Compounds Arsenic ---- Barium Cadmium Chromium Lead __ Mercury Selenium Silver Parameter Results(mg/1) Parameter Results(mg/l;(Jllj)~ Organic Compounds Results(mg/1) Results(mg/1) P&T:GC/MS _ Acid:B/N Ext. J Arsenic <, c _p'-\ __ benzene ✓ Barium O, -2 (, carbon tetrachloride _____ _ ✓ Cadmium L. o. 0 , ¼ = chlordane MTBE _i_ Chloride 13 __ chlorobenzene v Chromium <._a_ o'--l chloroform ✓ Copper a . Cr: = o-cresol : 1 Elnnid~ _______ m-creSol ti J a« _______ p-cresol _.!L Lead a_ 1 o4 __ cresol v Manganese D , Y b __ 1,4-dichlorobenzene _____ _ · v' Mercury L.. oA;,a ac ~ 1,2-dichloroethane _iL_ Nitrate 5-Co O __ 1,1-dichloroethylene _____ _ _iL Selenium -"'--o. oj __ 2,4-dinitrotoluene ,----------~---~ _iL. Silver L. o-d~ __ heptachlor ✓ Sulfates "'.I, hexachlorobenzene --Radiochemistry ····--·-------------I__L Zinc Q, 'le) __ hexachlorobutadiene _____ _ P..irameter __ Gross Alpha Gross Beta Results (PCi/1) ✓ pH I..,, ":J hexachloroethane ✓' Conductivity 'I<-. o ...,,.3 2 , __ methyl ethyl ketone _bi: I'7tcfllt / nitrobenzene _jl TOC ef"i(?~•· f-.£,;,--. pentachlorophenol ,--------------~ __ ____ _______ --pyridine Microbiology __ _____ _______ __ tetrachloroethylene ,--------------~ __ ____ _______ trichloroethylene ------: Parameter Results (Col/lOOml) __ --======= --=========----~-__ 2,4,5-trichlorophenol ' __ __ __2,4,6-trichJorophenol __ ____ ________ __ _____ ________ __ vinyl chloride eildrin -- P .•. =·,··~:: ;,r~.;t:_;¼~;;f.:;7~-f~d-?;.~4:::-::..=:;:;_~:~,,·::~~.?~1.i~ .. ":::;;-::.:r;;i.~~~~:&~: ,;--g-;i,-.,-,-"r./··":.:~~,:;,~~~-:';g 7~; .. ,;,::,.,:ml'.~1;e. ~t-.aH .. ~oi ;c-h_l_o_r_ :-..f~::~:J'.~"' ··--.·:·~.:. •-•-.-.--·~~----_.;_-.· . .,..·.-.. -. -··-. , .. ~-•_,.•.: ;.-- --.. Date Receive -<---•-____ ·-._ _ _ _:_~ _ _R,cp%t!@.\i)' -------·--.. , ------ ·, { ~ :,..,,.,._..;, ,,, ·-·-· ··'•l"'"T"'""••···~---·,n,· ...... :::..~:,;;,_,<_,___ ..... -.:,. __ -:: ... ~ .. ; ": .. :.·:~·.-_:--:--~·:-:· ·-="'toxaphen_e --· •. -- Date Extracted. · Date Reported _____ ;____ __ 2,4-0 2,4,5-TP (Silvex) I Date Analyzed Lab Number ------------------1) l [ S )I')! (llcviscd 2/91) f'\ -4 .t .4 '1 n. C' CC -----1 ------! A Q? .1 N.C. Department of Environment, , I lc.ahh, & Natural Resources Solid Waste Management Division SAMPLE ANALYSIS REQUEST State Labontory or Public Health P.O. Box 28047, 306.N. Wilmington Street _Raleigh, North Carolina 27611 --wile Number _________________ _ _Name of Site-ao/'6' ~lfl!JC ,/f!\f,f>< t;;'l'.twp10¼ Field Sample Number __ ___,1'-"6"--'-'/ 3='----------- Site Location f ½-fuia.. I Collected By 8-(cl.:e_( /rt;u'h"'-/Dc-orr--ID# 17/1i/1 I Date Collected Cf /i / 'f z; I I Time /O/::J I Agency: _£_Hazardous Waste Solid Waste __ Superfund TCLP Compounds -- Sample Type Ino11:anic Compounds Results(mg/1) I Environmental Concentrate Comments Arsenic -- ---:P4- Barium [A) -- Ground water (1) _ Solid (5) Cadmium --Chromium n .J{_ Surface water (2) -- Liquid (6) Lead --' Mercury _Soil (3) _Sludge (7) --Selenium -- m Silver _ Other (4) _ Other (8) ------ I -- Organic Chemistry Inorganic Chemistry -- I Parameter Results(mg/1) Parameter Results(mg/1)(~ Organic Compounds Results(mg/1) _P&T:GC/MS ✓ Arsenic ...:'.o,o'j benzene ---- _ Acid:B/N Ext. (/ Barium O,lfi--carbon tetrachloride --_IL.. Cadmium MTBE LO -0\ \o chlordane -- --....lL Chloride 8.9 chlorobenzene -- --_y_ Chromium L.o,o'-\-chloroform --o-cresol --_Ji_ Copper 12, -;;i 8 -- I EJ:r i..Je m-·cresol --I'. --- --. p_-cresol -- --_L Lead o"o-of:'.) cresol z, 7-lf -- I --___L Manganese --1,4-dichlorobenzene --_IL.. Mercury L.-0-Os:::,<:::>-;}._ 1,2-dichloroethane ---IL-Nitrate < l, D c2 --1,1-dichloroethylene I ___L Selenium L_c,,J;,'.:\ 2,4-dinitrotoluene .....L Silver L..o.os,, __ heptachlor Radiochemistry \/ Sulfates L. \ "")... hexachlorobenzene --/, 08 -- ······-·· 1Zinc hexachlorobutadiene I -- Paramder Results (PCi/1) _JL..PH <..s, ~ 5 hexachlorocthane -- __ Gross Alpha ✓-Conductivity \ :::,a,o .. , S?,., methyl ethyl ketone -- Gross Beta • flil! gr ' 7 nitrobenzene I --..J!_TOC E1,r~•~+-£,>J• ia __ pentachlorophenol __ pyridine --Microbiology --__ tetrachloroethylene I --trichloroethylenc Parameter Results (Col/lOOml) --2,4,5-trichlorophenol --= 2,4,6-trichlorophenol ---- ----__ vinyl ·chloride endrin · -- i~;~;~,:J?{~EI~;::~;:;~f ~~~;;:t ;;~'J;rrr~~;~~,:~\~~~J~,.~~~~:~:~:,~ __ lindanc _ . ~:ZZfi;t," in\~: t-hoxyc h Io _r--~~f.:· ~-;~;~:•:-s=";;:i·i.;:·: ;.;.;;;: ~ ~ ~ .. ;~·~. :...-:-~·,1.•:~-::: toxaphene,. · · . , J . _.·,1... , ...... -. . .. Dale Extracted. . . Dale Repo;ted' .. ' . -----Co -~-·--•~··2,:t.b -· · -• · '. , _ 2,4,5-TP (Silvex) I Dale Analyzed Lab Number ])[ JS 3191 (Revised 2/91) -- " c:--' a -' . •• N. '.C. Department or Environment, , llcalth, & Natural Resources Solid Waste Management Division SAMPLE ANALYSIS REQUEST State Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington Strccl Raleigh, North Carolina: 27611 ,. Mile Number _______________ _ _,Name of Site >fqm,/1'1 x(Yb'o/lABPr irt?rpr1¼,i Field Sample Number o/o I 5 ---'-''-=----------- Sit c Location ¼/(,.., . I Collected ByG{o.'>e1nwhn/Dc,&r/'\, ID# rJ/11/11 Date Collected ~/I J ') 1--Time / 1 lb --"--,'--'-~-'-------'--'--'---'='---- I Agency: ___i.__ Hazardous Waste Solid Waste _· __ Superfund TCLP Compounds Sample Type I Environmental Concentrate Ground water (1) __ Solid (5) Comments Inorganic Compounds Arsenic Barium --Cadmium Results(mg/1) g ..:i,__ Surface water (2) _Soil (3) _ Liquid (6) _________ _ _ Sludge (1) __________ _ Chromium --Lead Mercury --Selenium -- I I I I I Other ( 4) _ Other (8) __________ _ Organic Chemistry Parameter _P&T:GC/MS _ Acid:B/N Ext. MTBE -- -- ---- -- -- -- -- -- -- Resulls(mg/1) Inorganic Chemistry Parameter ~ Arsenic v' Barium Results(mg/l)(ijlll;il,«r L..O_d-\ </ Cadmium __iL Chloride __!c_ Chromium v Copper ....l.E' filami~ • Lua ✓Lead ~ Manganese ✓ Mercury ./ Nitrate Q-\3\ o •. a,s /, S--D 1 -x. :i ei L..o .oo?:, <(oo ✓ Selenium t-----------------1 ~ Silver .<:. a. a':\: Radiochemistry v Sulfates Silver Organic Compounds benzene carbon tetrachloride .Results(mg/1) --------- -- chlordane chlorobenzene chloroform o-cresol m-cresol --p-cresol cresol __ 1,4-dichlorobenzene _____ _ __ 1,2-dichloroethane __ 1,1-dichloroethylene ----~- --2,4-dinitrotoluene __ heptachlor hexachlorobenzene ------, I .... ~~;:meter Results (PCi/1) v Zinc ?,y, Lfr: __!.l.. pH _5'-'·~·;').,____ __ _ hexachlorobu tadiene --------- hexachloroethane __ methyl ethyl ketone nitrobenzene __ Gross Alpha Gross Beta I t-----------------1 ~ Conductivity 5 9 00 .. i,:m,,? ant TOil-1 -. J TOC Er••r~~ ~t: dove. --pentachlorophenol __ pyridine Microbiology __ tetrachloroethylene I --trichloroethylene Parameter Results (Col/lOOml) === -2,4,5-trichlorophenol __ __2,4,6-trichlorophenol _____ _ , .~lt~--------------L~~~-~-------------1 __ :f;i~hloride I·.:: -~;;c1<"'~~~~~-d ----;.:·:-~r~'c: "~.i.:.:s.;.z ... k.~;~ri·tibf:..:,.:,_~_ ~_,,;,;,.;:3=.6',~ " • , ' ~ne~~:~chlor' ,, ,:,;. :·, -::-;~::::.. :;::;-,.z-;:_;,:-, --~. ,_ ., • .. •.. ~~--~ "'.£' .,• -~ •• _. ., •. ·r.: -~·•·-,.;.•;:. "-:T...,./' •'toxaPhene ~ .. --.. ;,:,,,· Dale Exlractc<l _________ Dale Reported________ --2,4-D .· · · · ______ -. ., = 2,4,5-TP (Silvex) I Dale Analyzed Lab Number ------------------ ])!JS 3\'J\ (llcvixcd 2/91) ~ N.C. Department or Environment, ·• l lc:::ilth, & Natural R 0 csourccs SAMPLE ANALYSIS REQUEST State Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611 t Solid Waste Management Division ' ' Field Sample Number ___ q,-'-/J"'-_.q/."'O""----------- Site Location £@le. Date Collected 'l /, / ~ v Time.__,/-"?""CC""---- I Agency: Hazardous Waste Solid Waste __ Superfund TCLP Compounds ---- Sample Type Inorganic Compounds Results(mg/1) Environmental Concentrate Comments Arsenic I --Barium t>/Q-(1\ -- __ Ground water (1) _ Solid (5) Cadmium --Chromium --n _lL Surface water (2) . _Liquid (6) Lead Mercury _ Soil (3) _Sludge (7) --Selenium -- E Silver Other ( 4) _ Other (8) -- ---- I -- Organic Chemistry Inorganic Chemistry -- Parameter Results(mg/1) Parameter. Results (mg/I) ~g 't,el Organic Compounds Results(mg/1) I _P&T:GC/MS ✓ Arsenic -"'-0 -d:l benzene -- _ Acid:B/N Ext. v Barium o. (() carbon tetrachloride ---- MTBE .L Cadmium .L. o. 01 '--" chlordane -- --✓ Chloride a I chlorobenzene -- --...,L_ Chromium Lo. a'-\ chloroform· -- --L Copper <12,0~ o-cresol -- I --_J!._ Slee 'J m-cresol --~ = p-cresol --_L_ Lead L..G, c'-1 c:i cresol -- I --_sL_ Manganese {.,Q,\ --1,4-dichlorobenzene --_L_ Mercury L..o • QC1 C\ d-, 1,2-dichloroethane -- --_,,!_ Nitrate < {, 00 1,1-dichloroethylene -- _IL_ Selenium L.o .. c'.:\ 2,4-dinitrotoluene I v Silver .L.o.oS. __ heptachlor Radiochemistry Sulfates 4-lJ,. hexachlorobenzene ....L.. -- ······-·· _.!L Zinc· o, or-hexachlorobutadiene I -- Paramelt!r Results (PCi/1) _IL__PH (., • "°\ hexachloroethane __ Gross Alpha -L Conductivity \ c~c !:::!::,~~ __ methyl ethyl ketone Gross Beta .,;, 1i!f 3' 7 nitrobenzcne --= pentachlorophenol I ...JL TOC £r,u'/'.,.._,,_ ~-f-J,ow - __ pyridine --Microbiology ----tetrachloroethylene I --__ trichloroethylenc Parameter Results (Col/lOOml) __ 2,4,5-trichlorophenol -- ----__ 2,4,6-trichlorophenol ----. __ vinyl chloride endrin --lindanc a ' · ..... ;:-::.....-........... :.~-·-:i~ .. _ .... , •t-~.-.. ...-~ ••,.· •-,,. -o,;·(c-Rcccivcd~-· . --.... ····. ---·' "' · ... ,. Repoitc-d liy"·"-. . :.:_, -. ... . , .. .. ---...... .. "',"'-.,:,methoxychloL:.c:,. __ .,"'---,:.~c-:.·:, ,:,;· . I> 6otc. E~tract~j .' . . . · · . Dale. Re.ported --toxaphene 2,4-0 I 2,4,5-TP (Silvex) Dale Analy,cd Lab Number DI IS J\91 (Revised 2/91) -- r A I !Icalth, & Natural Resources t fr-./ State Laboratory of Pu;ic ~ P.O. Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611 NC. Department of Emironment~ SAMPLE AN.!,LYSIS REQUEST &lhd, Waste Management D1v,s,o V\ t Site Number ______________ Field Sample Number __ ____,/~/~/~i~'i'---------- .. Name of Site .5/?r,,,,v ijP/7C.. ~ Elv1-/ Collected By u,A</,e' //",:,-a✓-7-77,v ID#/f,,o/ Date Collecte_d_~8;,..//_'.,s+:/;~f'_Z-____ Time /5'3o Site Location._-',f<._-.:l1..(L6-'<o'-'L'-'4---CIL... _____________ _ I I D I I I I I I I I I Agency: , ~rdous Wast6''.' ,-· ('• i;~;;J :a:;J Superfund 1 TCLP Compounds Sample Type uCi O S 19c? Environmental Concentrate Comments ,-.,·r:.~.,.,,,1-: ·1:•_;.i.·:-;~-('rr~,li'~;; _ Solid (5)''·•· . ,;, /'__: ~{J __ Groundwater (1) Surface water (2) VLiquid (6) __________ _ . Soil (3) Other (4) _ Sludge (7) __________ _ _ Other (8) Organic Chemistry Inorganic Chemistry Inorganic Compounds Arsenic Barium --Cadmium Chromium --Lead __ Mercury Selenium --Silver Results(mg/1) Parumt'lcr Rcsults(mg/1) Parameter Results(mg/1) (mg/kg) Organic Compounds Results(mg/1) --,(L:;&T:GC/MS 0cid:B/N Ext. MTBE 1----------------1 Radiochemistry Parameter __ Grnss Alpha Gross Bela Results (l'Ci/1) Microbiology ·par;:1ml'lcr Results (Col/!OOml) Arsenic --Barium --Cadmium --Chloride --Chromium -- --Copper Fluoride Iron --Lead __ Manganese __ Mercury Nitrate Selenium --Silver -- Sulfates Zinc _pH __ Conduclivily TDS --TOC benzene ----car~on tetrachloride ______ _ -- chlordane chlorobcnzene chloroform o-crcsol m-crcsol __ p-crcsol crcsol ----1,4-dichlorobenzene ______ _ 1,2-dichloroethane __ 1,1-dichloruethylcne ______ _ __ 2,4-dinitrololucne __ heptachlor hexachlorobcnzenc hexachlorohutadienc '---------'---hexachlorocthane ----methyl ethyl ketone nitrobcnzcnc ----penlachlorophenol __ pyridine __ tetrachloroethylcne __ triehloroethylcne __ 2,4,5-triehlorophenol ______ _ __ 2,4,6-triehlorophenol __ vinyl chloride · cndrin k ' . SEP 2 6 .!) -~ . '?·-lindane D;ite Rcwvcd 1992. Rcporl_cd Ii · /.~.../-__ mclhoxychlor · . . :;;;;,-;;,x1,.~, l) '1_1 ~ Ex I '"" I ell ;if,;, f ,1, ,.9. :[::j lJtf) '""'"'d!!"~c [) ·a I i.'; R cfii r le d c·.,Vt7. -"V ~,9z::55::.ccc'a .i; =:c:i}~ !'6 '..'.~ "z~:;;c--;,;-,c;;;;;;o::.,.=~-'----'" , .......... ,se.""-"'--"':C'--' :.lf"'=,.,:,,.:..,,.,, ... ,,....,.:/PA,, ~ •-~-f'C•,·. ·. -·' · ·•. ·. "-• · ---~· •·>·•··• ,,, · ·· • -.-.-2,4;5-TP (Silvcx) · ·, " I I ··· ":' Di,te An,il'fi.cU'!·/1/1/JC . 9'/i[-15 . Lah Nun1l,cr :y,;,,:..,::;, s.:,J . --______________ -' C,('l)R'/1• 6&-· 7WF --1:r?z. 2 "? 2-9-92 Z..9c_r-; L--~-------- 1~-~:, Department of Environment, llc.ilth, & Natural Resources Solid,Wastc Management Division SAMPLE ANALYSIS REQUEST State Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611 Sile Number _______________ _ .. Name of Sile .51'/·MPN ,rv?l?f /,<;14;<1 Collected By Kd-fK~-;?/V / ,OiJ ,e;V Field Sample Number __ ...,/,:..L1/,.L1/_7c., 7 ,L.7 ________ _ I I I I I g g n Sile Localion _ __:D=--:C,(c.r,'-'<(}'-'L=,4-,,_ _______ c_ ___ _ ID#%✓ Dale Collecled, __ 8:::./-'.,_ ;:_-=.J,:~.:;,c...l..l_---'_7' ___ z~~~~~-T-i_m_e_}_c._z_· _o __ _, Agency: ~azardous Waste Solid Waste __ Superfund Sample Type Environmental Concentrate Comments Ground water (1) __ Surface water (2) _ Solid (5) _ Soil (:1) _ Other (4) __ Liquid (6) ___________ _ /4udge (7) __________ _ _ Other (8) __________ _ Organic Chemistry Inorganic Chemistry Parameter _ P&T:GC/MS _ Acid:B/N Ext. MTBE -------- ·------- Results(mg/1) Radiochemistry l'animckr __ Gross Alpha Gross Beta Results (PCi/1) Parameter Arsenic --Barium --Cadmium --Chloride Chromium -- --Copper -- Fluoride Iron Lead Results(mg/1) (mg/kg) __ Manganese __ Mercury " Nitrate -- -- Selenium Silver Sulfates Zinc _pH __ Cnnducli\~ty TDS TDC TCLP Compounds Inorganic Compounds Arsenic Barium --Cadmium Chromium --Lead __ Mercury Selenium Silver Results (mg/I) Organic Compounds Results(mg/l) . ,_/ benzene t.L. v carbon tetrachloride --~,J,~~--- ....!L._ chlordane v chlorobcnzcnc ..JL.. chloroform V o-cresol L,/ m•crcsol V p-cresol v crcsol v 1,4-dichlorobenzcne ______ _ V 1,2-dichloroclhane ; , .LL. 1, 1-dichlorocthylene ___ ,,;,I,'-, __ _ .,/ 2,4-dinilrololuene _t.c:: heptachlor V hcxachlmobenzenc .LL hcxachlorohutadicne ______ _ -'-'::'.'.'. hexachlorocthane -~methyl ethyl ketone ""0:.,.,,.,0c..15""·--- ~ nitrobcnzcnc D 1\-licrobiology - 1---~--- .LL pcntachlorophenol V pyridine ,;7' telrachloroethylcne lrichloroethylene [..L., I. u Parameter Results (Col/1001111) r/ 2,4,5-trichlorophcnol ______ _ c/ 2,4,6-trichlorophenol ______ _ _iL'., vinyl chloride , , . ~ cndrin D ' .. ~ .. Department of Environment, J icalth, & Natural Resources Solid. Waste Management Division SAMPLE ANALYSIS REQUEST State Laboratory Of Public Health P.O. Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611 Site Number -----------------Field Sample Number __ _,_/,:..,/:...,/'----''l--'£?""--------- .. Name of Site .,J'//--/'f'0"-7 .Jf&?J/4,9,4 ¢N/-Site Location _ ___,,./c,~c::::r:.,nc.';ea.=4'-'------------- Collccted By 0':AS:£4;,ffe~ ID#-#-Date Collected _ __,8,4f/:....'.3._l',_/ 7 .,1-A__.:9_2-___ Time_,_/--'7--";,lc'-"'O"'--I I I I I I I 0 Agency: ~azardous Waste ___ Solid Waste ___ Superfund Sample Type Environmental Concentrate Comments __ Ground water (1) brfacc water (2) _Soil (3) _ Solid (5) _ Liquid (6) __________ _ _ Sludge (7) __________ _ _ O.thcr (4) __ Other (8) ___________ _ Organic Chemistry Parameter 1/ P&T:GC/MS _V_A Acid:B/N Ext. MTBE Rcsults(mg/1) Radiochemistry P1.1ranll'lcr Results (PCi/1) __ \Jross Alpha ______ _ Gross Bela Inorganic Chemistry Parameter Arsenic Barium --Cadmium --Chloride Chromium -- --Copper -- Fluoride Iron Lead Results (mg/I) (mg/kg) __ Manganese __ Mercury Nitrntc Selenium --Silver -- Sulfates Zinc --_pH __ Conductivity TlJS TOC 0 Microbiology - 1----------------l ------ u Parameter Results (Col/1001111) D TCLP Compounds Inorganic Compounds Arsenic Barium --Cadmium Chromium --Lead __ Mercury Selenium Silver Organic Compounds benzene carbon tetrachloride Results(mg/1) Results(mg/1) --------- -- -- chlordane chlorobcnzcnc chloroform o-crcsol rn-crcsol --p-crcsol cresol __ 1,4-dichlorobcnzcnc ______ _ __ 1,2-dichlorocthane __ 1,1-dichloroethylcne ______ _ __ 2,4-dinitrotolucne __ hcptachlor hexachlorobcnzcnc hcxachlorohutadicnc ---------hexachlorocthane ----methyl ethyl ketone nitrobcnzcnc ----pcntachlorophenol __ pyridine __ tctrachloroethylene __ trichloroethylene __ ·2,4,5-trichlorophenol ______ _ __ 2,4,6-trichlorophenol ______ _ __ ,inyl chloride cndrin N.L. vepartment 01 t:,nvtronment, llca\lh, & Natural Resources · Soiid Waste Management Division Uri.J.T.1.1 .I..JL.r L"1.J. ,_~LJ..I. U.IU ..I.~'\,/_ VJLJU ..I. JU>I'-'-"'UUJ<lLUJJ UJ I UVU'-ll<O<llLU Sile Number ---------------- P.O. Box 28047, 306·!'~. Wilmington Street Raleigh: North Carolina 27611 Field Sample Number __ _,_/~/~/_9~2 _______ _ .. Name of Site Collected By ,.f/,?/Y,:;vv~;?i/f4 #NI-Site Location ,f'cr/tJC..,4 · r~ . -~~~---------------- ~5tf'lf /4,4 t€17,v ID# qfr Date Collectcd __ ~z.,,...4.,1/,~/p_f_z_ ___ Time __ CJ_'?_.Z_O __ 7 .!?oA?/V ,I I I I I I I I I I I I I I Agency: VHazardous Waste ___ Solid Waste ___ Superfund Sample Type Environmental Concentrate Comments _Groundwater (1) __ Solid (5) L Surface water (2) __ Liquid (6) ____________ _ Soil (3) _ Other (4) _ Sludge (7) __________ _ Other (8) Organic Chemistry Inorganic Chemistry Pan,ynetcr : Results(mg/1) Parameter Results(mg/l)(mg/kg) ._{/_ P P&T:GC/MS _LL. Acid:B/N Ext. MTBE Radiochemistry Parameter __ Gross Alpha Gross Beta Results (PCi/1) Microbiology Parameter Results (Col/lO0ml) -- -- Arsenic Barium Cadmium Chloride Chromium --Copper -- Fluoride Iron Lead __ Manganese __ Mercury Nitrate Selenium --Silver -- Sulfates Zinc --_pH __ Conductivity TDS --TOC TCLP Compounds Inorganic Compounds Arsenic Barium --Cadmium Chromium --Lead __ Mercury Selenium --Silver Organic Compounds benzene --carbon. tetrachloride Results(mg/1) Results(mg/1) ---------- -- -- chlordane chlorobcnzcne chloroform o-crcsol m-crcsoi --p-crcsol crcsol __ 1,4-dichlorobcnzcnc --1,2-dichloroclhane ------- __ 1,1-dichloroelhylcne ______ _ __ 2,4~dinitrotolucne __ hcplachlor hcxachlorobcnzcnc --hcxachlorobutadicne ---------h c x a ch lo ro cl ha n c ----methyl e1hyl ketone ______ _ nitrobcnzcnc ----pcnlachlorophcnol __ pyridine __ tctrachloroclhylene __ trichloroelhylcne __ 2,4,5-lrichlorophcnol __ 2,4,6-lrichlorophenol ______ _ __ vinyl chloride cn<lrin --6l lindane ,~ -~ ::,::: ~,:.::!l::,::ICcl:l .. 9 ~/:.,Z:&O~,~~---•~:C~:.~::: P.~:L,~,,--,~~,·~~'~"~--•-,~~c, -c~...-_; ~L--_~l~I:;~: 1 .~,i'·'"'". •.·-. ••·" -,, •. ,.· ·7 .. • ••• • "··.·_. "-· •·. • •• , ,, -""• • ._ ..... _•--•·S -.•e•~H-r-""t, /). 1,4 ·• . •-<--""},_,..:...__ . ,, ., -·-.-·-" c, I --.. P'"., _ -P.'( .. , _,._, .. ~ ·--~-,~-.,,~-,,,,, .,,,,,,-,.,..•=-' Z,~--,f:::1JIJ~j~;l,,,,_ -~----~ Dalc,Ana!yzc<l-!-f~( J.-.5:.h . 9-14--91 -~ l:ah~N u~1bcr,~,_ .... J_.;.., ,._;_. ....::;,_:) :-.,#.-•. _,, •••. , ... -~~,-~ , __ ,.._,:•:--=•:;.;:,,..•-.-•;i,-F,.,_.,_~""t•:.-,,-,~.., ,. -~·~-.•--,-·--··· C:l'llR'JE JJ;J) 7U,Ar ------ I N.C. Department of Environment, liealth, & Natural Resources Solid Waste Management Division SAMPLE ANALYSIS REQUEST State Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington Street Raleigh, North Carolina _27611 Sile Number ----------~-----Field Sample Number_-+-l~/_,,2._o~v _________ _ .. Name of Site .,j/t-/7cJ,v.f_,.:/?(lcfl;.44 /rNT Sile Location lz_V/i:JC-4 l , ;_ Collected By fr4'/S?f'R //Y,1;e??v ID# t}Jfr.'( Date Collected __ ___,'f__,,_~, /_,_'/__,,_/._ ;,9'-"2...-___ Time_C>_f'_3_'S __ I I D u I I I I I I ,;,.,12 ,v / ~ r,.c/?,'rf,v:£. 011 01 L ' , Agency: ~rdous Waste ___ Solid Wasie __ Superfund Sample Type Environmental Concentrate Comments _ Ground waler (!) __ Solid (5) __ Surface waler (2) __ Liquid (6) ____________ _ _ Soil ('.I) _ O_thcr (4) L51udgc (7) _________ _ _ Other (8) __________ _ Organic Chemistry Parameter Results(mg/1) _ P&T:GC/MS __ Acid:B/N Ext. MTBE Radiochemistry l'aramdcr Results (l'Ci/1) _·_ Gross Alpha -------Gross Beta Microbiology Parameter Hesults (Col/l00ml) Inorganic Chemistry Parameter Arsenic --Barium --Cadmium --Chloride Chromium --__ Copper -- Fluoride Iron Lead Rcsults(mg/1) (n,g/kg) __ Manganese __ Mercury Nitrate Selenium --Silver -- Sulfates Zinc -- _pH __ Conductivity TDS ------ TOC TCLP Compounds Inorganic Compounds Arsenic Barium --Cadmium Chromium --Lead __ Mercury Selenium --Silver Results(mg/1) Organic Compounds Results(mg/1) V benzene o. o otf :f V carbon tetrachloride u_ Vchlordane o. o/J, V chlorobenzene Vchloroform o.t>o3:r,f\ Vo-cresol U m•crcsol Vp-cresol l/crcsol C/ 1,4-dichlorobcnzcne -------v 1,2-dichloroethanc u.__ V 1, 1-dichloroethylcnc ~, V 2,4-dinitrotoluene --~---- {,/ hcptachlor t/nexachlorobcnzcnc Vhexachlorohutadiene V hcxachlorocthane _u:: methyl ethyl ketone ..LL_ nitrobcnzc1!e _IL:_ pcntachlorophcnol -"::'._· pyridine . l/ telrachloroethylene ~ lrichloroethylene ------- l-' __02,4,5-trichlorophenol ______ _ // 2,4,6-lrichlorophcnol 7 vinyl chloride ---,-,.--- J.L_ cn<lrin SEP 2 pj) c/ lindanc L D;ilc Received . r£l92 Reported by__________ C/ methoxyehlor • . • • V tox;,iphcm: I ~-=-.:.~.:-.-· .. -~-:.;. D ti 1TI5EXi "riii:tY:,J,.--:.ti.--:/5:·;_.CJ :i_<; fJ £)~::_;_ :-. . , -.:EYJfl'.~~R-~j){-irll:·il~~!';~fL~t.!tZ"~-,;~-:;;·;;:;;;..:;: .: . >-~-·-~-i~4'' E>"C_., .. ·_·:-~'.~"'::-'".:·"'.? .:;'-f: "'~;0·:;'.:i":·:~.v,,..;--=~:-;: _;.i.~z. I ,-fjtv'/+··. ff ·· ··· -,c ;--:-,--c. -,, .·;_ . {/ 2;4,.VfP-(Silvex)h·'"••·,-· .. ,. ,-,,'!"-~'"" c,sec .-Di,te Analyzcu:/:;;,z1:·9-1i./-9;;z_ Lah Number -,,,.;,;:,~i_L3 ··_-_.--.. --,-·• _._ -......... ""'''•"''"" C:1'1)8'11! -t3£J ~ -JV»- rCL/-Y--3t:,··9,."l... N.~. Department of Environment, I lealth, & Natural Resources Solid Waste Management Division SAMPLE ANALYSIS REQUEST State laboratory of Public Health P.O. Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611 •· Sile Number --'-------------- \ Field Sample _Number __ ...,_/,_,/c..::,.Z:...c_o-'-/ ________ _ .. Name of Sile ,ill /'7,:JN ,fjfo/7y::,,1,<J Collected By GL//%'74,f,1?1?,.J Site Localion_~/i"'-'-'(.j=C,....e:0...cl.:.cfi"_,_ ___________ _ I ,9~,V / Agency: ~azardous Waste Solid Waste ___ Superfund TCLP Compounds --- @·· JD# 4,-Date Collcctcd __ .,_71+';..,_~/,,_/2_f_Z-____ Time_.;,,t.r;.ci-"Oc.,.r«>'--- I Sample Type Inorganic Compounds Results(mg/1) Environmental Concentrate Comments Arsenic --Barium I P---f0 --__ Groundwater (1) _· Solid (5) Cadmium ' -- /surface water (2) Chromium --_ Liquid (6) Lead -- I __ Mercury Soil (3) _ Sludge (7) Selenium ----Silver --_ Other (4) I _ Other (8) -- -- --Organic Chemistry Inorganic Chemistry --I P✓Peter Results(mg/1) Parameter Results(mg/1) (mg/kg) Organic Compounds Results(mg/1) P&T:GC/MS Arsenic benzene -;::7 Acid:B/N Ext. ----I Barium carbon tetrachloride ----MTBE Cadmium chlordane ------ Chloride chlorobenzcnc ------Chromium chloroform ------ --__ Copper o-crcsol --Fluoride m-crcsol ---- --Iron __ p-cresol I --Lead crcsol . ------ ----Manganese --1,4-dichlorobcnzene ----Mercury --1,2-dichloroclhane I Nitrate 1, 1-dichloroethylene ------Selenium 2,4-din it rotoluene --Silver __ hcplachlor -- I Radiochemistry Sulfates hexachlorobcnzcnc ----····························-···-·-· ·------··-·-····-··--·--·-··········· Zinc hexac h lo robu lad icne ----Parameter Results (l'Ci/1) _pH hexachloroclhanc -- I __ Gross Alpha __ Conductivity -· methyl ethyl ketone Gross Beta TDS nitrobc.nzcnc ------TOC penlachlorophcnol ---- ----pyridine I Microbiology --__ lelraehloroethylcne __ trichloroethylcne --Parameter Results (Col/IO0ml) __ 2,4,5-trichlorophcnol --I ----__ 2,4,6-lrichlorophcnol ----__ vinyl chloride cndrin --It ') R . I SEP 2 ~92 (3 I --lindt;1nc , ate ccc1vct · Rcport1,;J hy · __ mclhoxychlor . ;"-7:j·~~s~i~~?·[rf!fx~~:·,~~~_:3:;~~i,~-~~;',;:;-·,,; .,c::.,, ; d',:~,,,.•~-o.,._ ~:,,,~·.-:-_. :t\!~:.tphc.:_~S ; ., _ _,_,i_ •.• : _________ ~-.C!'--··· ··-••c,--:1"" 24-D 1,-•;)al:;;~;;,~:;t/;~q-;_·?/'-7:t~<j~ La;;-~um;,~; ~j.'.:,;:~s:J.i. -· · .. l4,S-TP (Silvex) .. --c::J'l)WJJ: (JI) 7Uv I I f\'..~:. Department of Environmcf)-1, Health, & Natural Resources Solid Waste Management Division SAMPLE"ANALYSIS REQUEST State Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington Street Raleigh; North Carolir.a 27611 Field Sample Number __ _,/-'-/_c2_u_2-.---"--------- .. Name of Sile-"'-c-1/"'/'-"-6-/1/:....:..,/)-1/c...::.~.S:=6-"W,'l-'-;<'-C""/4'-'-"-'-'/44""-'--"-E;"',ll'-'-'1/'-,c----Sile Localion. __ ....1..;5":c_-::,lf_,.,,/C"'-'l=--f,f}-""------------- Collccted By ~£./4~ ID#~ Dale Collected __ ...:_f'..,_',,,:.:..'/.,t.'. h_...:_9_2-___ Time / 0 2. u Site Number _______________ _ I I I I I I I I I I I /~~ n .. Agency: ~zardous Waste ___ Solid Waste ___ Supcrfund Sample Type Environmental Concentrate Comments _ Solid (5) __ Ground waler (1) __ Surface water (2) _ Soil (J) _ Liquid (6) __________ _ ,./ Sludge (7) _________ _ _ Other (4) _ Other (8) Organic Chemistry Paramrter _P&T:GC/MS _ Acid:B/N Ext. MTBE Results(mg/1) Radiochemistry Parameter Results (l'Ci/1) __ Gross Alpha ______ _ Gross Beta Microbiology Parameter Results (Col/1001111) Inorganic Chemistry Parameter Results (mg/I) (mg/kg) Arsenic --Barium --Cadmium --Chloride --Chromium ----Copper Fluoride Iron --Lead __ Manganese __ Mcrcury Nitrate Selenium --Silver Sulfates Zinc --_pH __ Conductivity ______ _ TDS TOC TCLP Compounds Inorganic Compounds Arsenic Barium --Cadmium Chromium --Lead __ Mercury Selenium --Silver Results(mg/1) Organic Compounds Results(mg/1) Vbenzcne +mcc. //' carbon tetrachloride LL-7 chlordane ---==---- ✓ chlorobcnzene _L chloroform ✓ o-crcsol V m-crcsol _£,L. p-crcsol V crcsol cJ, o 63 :f,_, ,._i:,~- 0.069 ,3 vl ,4-dichlorobenzcne ______ _ L 1,2-dichloroethane (..L. Vl,1-dichlorocthylene ---'"'--1, __ _ V 2,4-dinitrotoluene V heptachlor c,/' hcxachlorobcnzcne V hcxachlorobutadiene ______ _ ~hcxachlorocthane V m Ct h yl ct h yl ketone .,_n.,,,wQ...o...c"l.,,(fL' --- ..L.::::.. nilrobcnzcne ~pcntachlorophenol ~ pyridine e,,/ lctrachloroelhylene _.s.::::::: trichloroethylene 1t _u:::._2,4,5-trichlorophenol ______ _ ...IL 2,4,6-trichlorophenol ______ _ ~ vinyl chloride c_,/'cndrin L . SEP ('fl ,./ lindanc • D,lle Received 2 fl92 . _ Reported 1,y ✓ mcthoxychlor ;;;~:,:•-':'~i5~itC~E·:1~ ~-t~~y'=-tj.]~,;;;"j_}:;Jk) ~::~;;;:t:t:7~~~~1~ ~~~~-:~¥J::?:,r.-..-,2"--·::•_ ::-:~:-.::;;~.?'d~ :t~~ }1,~:.b~~~. r: S:-· .--.. · -..,., --·-·_·_ ---~-·~--~,--· ~ -'-'l·J:.~:..--;n.~;•~~ ..... ""~; ./,._ ..... --~--/? ~ ........ , ;!~-~-:-_ ........ ~ ...... -~--::: ----••• ----• -.. ~.,=--···""""-.... -:-··,..--,..r-:r·r.-,...,,.._,.,...,..,r;.T;.,,._=-•-,.•?-,,"' •. ~t'.~= -· .----,..~-.:::,,-·.·~~-..... --✓ ..-2,4,5-TP (S1lvcx) Date An.ily1ed'1-/f-7,1.. q-lt-/-9,] Lah Number · • .,. I C:l'll8'J" 8(1. ~ TC<..f' <1-30 -9,2 I- N.C. Department o~ Environment, I lcalth, & Natural Resources Solid Waste Management Division SAMPLE ANALYSIS REQUEST State Laboratory of Public Health r:o. Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611 Site Number · .. Name of Sile ..$'/ ?;v,Yt) f/,()l7c..,/2/,¢,<1 Field Sample Number ___ .L./(,_,,,,2.u=-3"---------- "' -.· l f'~h2-I Collected By 19-Ul5!¥e /1<,-42-p-J JD# 4-Date Collected Time //lo / ,PD,e/l} // ' ' Agency: LHazardous Waste Solid Waste ___ Superfund TCLP Compounds --- £,v/• Site Location I Sample Type Inorganic Compounds Results(mg/1) Environmental Concentrate Comments Arsenic --Barium I t-~,J'tu --__ Ground waler (1) _Solid (5) Cadmium -- VSurface water (2) Chromium -- I _ Liquid (6) Lead --__ Mercury _ Soil (3) _ Sludge (7) Selenium --Silver I _·_ Other (4) --_ Other (8) -- -- --I Organic Chemistry Inorganic Chemistry -- P/peler Results(mg/1) Parameter Results(mg/1) (mg/kg) Organic Compounds Results(mg/1) I P&T:GC/MS Arsenic benzene ✓Acid: B /N Ext. -------Barium carbon tetrachloride ----MTBE Cadmium chlordane ------Chloride chlorobenzcne ------Chromium chloH1form ------ --__ Copper o-crcsol --Fluoride m-crcsol ------I --Iron __ p-crcsol --Lead crcsol ------ ----Manganese 1,4-dichlorobcnzene -- I ----Mercury --1,2-dichlorocthane --Nitralc __ 1, 1-dichloroethylcne --Selenium 2,4-dinit rotolucne ---- I Silver __ hcptachlor --Radiochemistry Sulfates hcxachlorobcnzcnc ----... .......... ··········-··-···-·-···-----······· . ......... Zinc hexach lorohutadicne ----Paraml'll'r Results (l'Ci/1) _pH hcxachlorocthanc I -- --Gross Alpha __ Conductivity __ methyl ethyl ketone Gross Beta TDS nitrobcnzcnc ------TOC pcntachlorophcnol ----I ----pyridine Microbiology --__ lctrachloroclhylene --__ trichloroethylene m Parameter Results (Col/1001111) __ 2,4,5-trichlorophcnol -- ----__ 2,4,6-trichlorophcnol ------vinyl chloride ~- cndrin er) --.. lind,rnc D:1lt,; Received SEP 2 E92 --Reported by methoxychlor ·u,,~~:~~;~;ri;YJ~:rJi;::I§;;~~~t~~f:l;t;:::;;;;~~:~,,~~;::; q•,'~·"''":t~lt)Xaf~ll:flC:-~~~· •~ ·-.. . , ,. :·._-:, <,.t. . ..-.-. ,,• n,-,.s~·-~;~;:,D,-i,t,.,.'c_·l·• • ••··· · s~ .· -· , ... ·. -, ·2;4;5-TP (Silvcx) · · Dale Analyzcd~J-/:,-5'L q:..15-9;:i.., Lah Number S.8ZSJG --D C:l'IJR'JI\ /31!) -7/)JJ N.C. Department of Environment, licalth, & Natural Resources Solid Waste Management Division SAMPLE ANALYSIS REQUEST State Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611 Sile Nuniber _______________ _ Field Sample .Nuinber ___ __,_/..:.'/_J:_::_v....,y'--------- ... Name of Site ,.f/,{hM.JJ;f'PIZC /II~ ,£-vT, Sile Localion, __ .&Ca...::u_F_::·c::_n:;:..!.,4:<-__________ _ Collected By /?42"1"'.,j/-y -?~ 10# # Dale Collected __ _,_f-,L/-'-~.,L,/---'-f'....:2-=---Time / / / 5 I / pc,,e,v / I Agency: [./"'Hazardous Waste ___ Solid Waste ___ Superfund TCLP Compounds I I I I D I Sample Type Environmental Concentrate Comments __ Ground waler (1) __ Solid (5) P-.3S __ Surface waler (2) __ Liquid (6) ____________ _ Soil (3) ✓51udge (7) __________ _ _ Other (4) _ Other (8) Organic Chemistry Parameter _ P&T:GC/MS _ Acid:B/N Ext. MTBE Results(mg/1) Inorganic Chemistry Parameter Arsenic --Barium --Cadmium --Chloride Chromium -- --Copper -- Fluoride Iron Lead Resu Its (mg/I)( mg/kg) __ Mang<rncsc __ Mercury Nitrate --Selenium --Silver --I Radiochemistry ·············•· ·············-···-·-··············-·····················•·· Sulfates Zinc --l'aramctcr Results (l'Ci/1) _pH I __ Gross Alpha ______ _ Gross Beta __ Conductivity ______ _ TDS --TOC I Microbiology - 1-------1--- Parameter Results (Col/IO0ml) I Inorganic Compounds Arsenic Barium --Cadmium Chromium --Lead __ Mercury Selenium Silver Results(mg/1) Organic Compounds Results(mg/1) V benzene +col' g {.,/ carbon lelrachloride ___ Ls,·,_,, __ _ V chlordane c./ ch\orobcnzenc ""v chloroform (_/" o-crcsol L/" m-crcsol V p-cresol v· crcsol LL 0.005 t:O., v 1,4-dichlorobenzene ______ _ V 1,2-dichloroelhane u. V l,1-dichloroelhylcne ___ J..,·'-, __ _ V 2,4-dinilrotolucnc ~ heplachlor V hexachlorobenzene ___LL'.'hexachlorohutadiene ______ _ vhexachloroclhane V methyl ethyl ketone (), Olp L, _t::::_ nilrobcnzene k__ pcn1achlorophcnol _L__ pyridine V lclrachloroelhylcne L lrichloroethylene I, J, i/ 2,4,5-trichlorophenol ______ _ c/ 2,4,6-lrichlorophenol ______ _ c/ ,inyl chloride v cn<lrin . , ,. BD I/ . lindanc D.ole .Received SEP 2 092 Reported hy__________ -£.L. m,·1hoxychlor .. ~ .,...-~, .. ,,,...,,.:;.._......,......_~--~"tl· .~,..__....c,., ___ ,. ___ .........,""'""''i'i"'"'5<-•rn.-"-~~ ...... .-....... ,.. •• .,.;..)~._--i""~ ,., •.• , _l--;::::_tt1x.Jpbcnc --~·· -·· ···-· ... ·-··. i;_s ·-.·. l}Jfc'Exlr':-JCicil-'--I 'iS-· ;.'1'.'i.JiY"==•=i):i7f R~r<>rlcJ°•c=-~""··~··•-._~ ,-;--.u·. ,~: '-·,:_.,--·2 4-i5' -. . ·-•a , . . -· . -,. . I I. -... -.-. ' ': ;·n,-)/J'"'"·.-·. "' ~•n-r:;"" ,.·--,,-,•-x,::::'."'0·t•, ·,:··<;·,·. t~·-3· 'n ,_,,, ....... -·v2'·4 5-Tl'.(Sdv ) •• J -, ~--•• /-:. ·~•• ,t:,~li.--,---• ...._.,."'!!.:-=.~,..._,--,r_..,......,.,-~:::J.-~,r-...,.-;-.,;,,,,l,, ., .. ••---• • • __ 1 , , • CX O,>lc An.oly1.cd/-ll,-Jl-CJ-Jrj'..q;;_, La.h Number__________ __ C:l'IJR'II; 13,._t 7U,lT ----~~- /(U? "1-.'3o-<-!e"J- 1.· N.C. Department or Environment, l lcalth, & Natural Resources Solid Waste Management Division I-Sile Number SAMPLE ANALYSIS REQUEST State Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington Strr:r.t Raleigh, North Carolina 27611 Field Sample Number .2,, c; ----+-~-~---------- .. Name of Site sf//-i<,(),V,..[,£"'1!c'fa,?.4 ff'vT Site Localion _ __,k;:.,_-_.u_,_5_,cJ"--"t..-'-;d"----------- Collccle<l By ~;_;,1,f,(1//,w~ 10# 1.J//V Dale Collcctcd __ :..,,.'lc, /1/;;.h_,f':_:::Z--=-___ Timc_/'--'3"-'-Yi-"o'--_ //)~ ~ ,, Agency: ~Hazardous Waste ___ Solid Waste ___ Supcrfund I I I Sample Type Environmental Ground waler (1) __ Surface water (2) Concentrate Comments _Solid (5) __iLLiquict (6) __________ _ I _ Soil (3) I _Other (4) _ Sludge (7) __________ _ _ Other (8) I u D D D Organic Chemistry Inorganic Chemistry Parameter LP&T:GC/MS v Acid:13/N Ext. Rcsults(mg/1) Parameter Results(mg/1) (mg/kg) MTBE Radiochemistry Paraml'l~r __ Gross Alpha Gross Bela Resulls (l'Ci/1) Microbiology Parameter Rcsulls (Col/lOOml) Arsenic --Barium --Cadmium --Chloride --Chromium -- --Copper Fluoride Iron --Lead __ Manganese __ Mercury Nilratc Selenium --Silver -- Sulfates Zinc _pH __ Conduclivily TDS TOC TCLP Compounds Inorganic Compounds Arsenic --Barium --Cadmium --Chromium --Lead -- --Mercury Selenium Silver Organic Compounds benzene --carbon tetrachloride Results(mg/1) Results(mg/1) --------- -- -- chlordane chlorobcnzcnc chloroform o-crcsol m-crcsol --p-crcsol crcsol ----1,4-dichlorobcnzene ______ _ 1,2-<lichlorocthane __ 1,1-dichlorocthylcne ______ _ __ 2,4-dinitrotoluene __ heptachlor hcxachlorobcnzcnc --hcxachlorohuiadiene ---------h c x a ch lo ro ct ha n c ----methyl ethyl ketone ______ _ nilrobcnzcnc ----pcntachlorophcnol __ pyridine __ tclrachloroelhylene __ lrichloroethylenc __ 2,4,5-trichlorophcnol -------__ 2,4,6-trichlorophcnol ______ _ __ vinyl chloride N.~. Department of Environment, 11.calth, & Natural Resources Solid Waste M~nagemcnl Division SAMPLE ANALYSIS REQUEST State Laboratory of Public Hr.alth P.O. Box 28047, 306 N. Wilmingtou Street Raleigh, North Carolina 27611 Sile Number Field Sample Number __ ____,/~/-,,2~o..,,{, __________ _ le Name of Sile_,d/_/l_&-_~-i4'Y--,f,-if"~--t::-/j_,4,<k7 ____ E,_,,,,,_L_·_ Site Location __ __,_/2"'£--'l/,._· 1-/:_0=t.cct'f:.,_ _________ _ Collected By Cl ,1gtcfa,4~ 1D # /4:i' //.V Date .Collected __ _,'7c,,.~1;L--,,;-/)_:.Y'--'=Z..=--'--Time /_? </o I I I I I · 7 ,{?0 4.N ~ · ' ' Agency: Hazardous Waste Solid Waste ___ Superfun<l Sample Type Environmental Ground water (1) __ Surface water (2) _. Silil (3) _ Other (4) Concentrate Comments _ Solid (5) _ Liquid (6) __________ _ /4udgc (7) __________ _ Other (8) __________ _ TCLP Compounds Inorganic Compounds Arsenic Barium --Cadmium --Chromium --Lead ----Mercury Selenium Silver Results(mg/1) 01----0_r_g_a_n_ic_C_h_e_m_i_s_1ry ___ 4 ____ 1_n_o_r_g_a_n_ic_C_h_c_m_i_s_1ry __ --1 D I I I I I I Paramt'tltr _P&T:GC/MS _ Acid:B/N Ext. MTBE Results(mg/1) . Radiochemistry Parameter __ Gross Alpha Gross Beta Results (l'Ci/1) Microbiology P.aranu~ter Results (Col/l00ml) Parameter Results (mg/l)(mg/kg) Arsenic Barium --Cadmium --Chloride --Chromium -- --Copper Fluoride --Iron --Lead --Manganese --__ Mercury Nitrate --Selenium --Silver --Sulfates Zinc --_pl-I __ Conductivity TDS --TOC Organic Compounds Results(mg/1) {/benzene o,Oo3,"\" ~ carbon tetrachloride __ _.'""----- ...L:::::_ chlordanc l/ c.hlorobenzcne ..J.L:_ chloroform _JL:.O•Cresol -1.L. m-crcsol ..JL p-cresol vcresol v 1,4-dichlorobcnzene Q•Q,; j -------_LL. 1,2-dichlorocthane I , _ (/ 1,1-<lichloroethylenc ---''.._L· __ _ K.. 2,4-dinitrotolucne v hcptachlor ...L:::::_ hexach lorobc nzcnc .JL_ hcxachlorohuta<liene ______ _ _L:::... hcxachlorocthane v methyl ethyl ketone LL_ nitrobcnzcne V pcntachlorophenol V pyridine .LL tetrachloroethylcne .LL.. trichloroethylene V 2,4,5-trichlorophenol // 2,4,6-trichlorophenol .LL_ vinyl chloride ------- ------- · ·· iL_ cndrin L'----. ,-----,-,_~S-EP_2 ____ -_ --B-,i~c'---------'--~,--------,-1 {/ lindane •. Date Rcfrivcd '1'.192 Rq,.ort~d-hy _ _ _ _ V: meti,cixych·lor _ _ _ _ _ _ , ~~-:-~.~~~;~~!~~?~~~!lf-'~;f&~,--,0 , :.is~'t,~ ~R~~!;';'.;·~J':''~,::~:~;·;;;·,_"•:1 ''' ,:,?:r ;J'.:~:n;~~v:~~~~:0 ~'' 0~~,•,¼: '~:::, :"''.~--;~ Date Analyzcd'J'-;C, '7-i. 9-16-4,2 Lah Number .__,,.J,_,_,, • C::l'DRYE /3£>-.. -:,i ?U).r" --- / ( LI· '-I <30 -q ,:J, ~-----------------" I I· N.C. Department of.Environment, I li::alth, & Natural Resources Soli~ Waste Managcmcn~ Division Sile Number ---------------- ,:naie uwonnory or ruouc 11ea11n P.O. Box 28047, 3-06 N. Wilmington Street Raieigh, North Carolina 27611 Field Sample Number ___ ~/i~1/~.;2.o~-,,7.._ ______ _ .. Name ofSile ,:f/,;-;v,;,,.V .Jif;?A[//WA' Collect cd By H&''f0 ~ ffi',CW tf,v t Site Location_~l7<~'i'.~A~o_t.~f'1~------------ ID# #--Dale Collcctcd ___ '°'f~1/;-/.,,_/9~r'_2--___ Time_/~f:~/.~'..7~,...-- I I I I n D I I I I I Agency: ~zardous Waste Solid Waste ___ Superfund Sample Type Environmental Concentrate Comments Ground waler {1) --. _Solid (5) __ Surface water (2) V'Liquid {6) _Soil (3) _ Sludge (7) _,Other {4) Other (8) Organic Chemistry Paramett:r VP&T:GC/MS ~cid:B/N Ext. MTBE Rcsults(mg/1) Radiochemistry Parameter Results (l'Ci/1) __ Gross Alpha -------Gross Bela Microbiology Parameter Results (Col/lO0ml) Inorganic Chemistry Parameter Arsenic Barium --Cadmium --Chloride Chromium --__ Copper -- Fluoride Iron Lead Rcsults(mg/1) (mg/kg) __ Manganese __ Mercury Nitrate Selenium --Silver --Sulfates Zinc --_pH __ Conductivity TDS TOC TCLP Compounds Inorganic Compounds Arsenic Barium --Cadmium Chromium --Lead __ Mercury Selenium --Silver Organic Compounds benzene --carbon tetrachloride Rcsults(mg/1) Results(mg/1) --------- -- -- chlordsnc chlorobcnzcnc chloroform o-crcsol m-crcsol --p-cresol crcsol ----1,4-dichlorobcnzcne --1,2-dichloroclhane ------- __ 1,1-dichloroclhylcne ______ _ 2,4-din iLrotolucne __ hcptachlor hcxachlorobcnzcnc --hcxachlorohutadiene ---------hcxachloroclhanc __ methyl ethyl ketone nitrobcnzcne ----pcntachlorophcnol __ pyridine __ tctrachloroethylcnc __ lrichloroethylene __ 2,4,5-trichlorophcnol ______ _ __ 2,4,6-lriehlorophenol ______ _ __ vinyl chloride cndrin SAMl'L~ ANALrM;:, tu.l,lUl!.-'l ;.")ldlt: Ll:IUUnuury UI ,-uuuL n,;;111111 P.O. Box 28047, 306 N, Wilmington Street Raleigh, North Carolina 276ll N.C. µcpartmcnt of Environment, 1 lcal)h, & Natural Resources I·· &>l;d Waste Management Divis;on Sile Number _______________ _ Field Sample Number ___ _,,./2_,_'/---'='cJ_v~,.,_f _____ _ .. ame of Sile.>/ fr.i</,¥V fl'n7c... /4,4-it £' ,v'/ Site Localion. __ i!icEi-..:l-(LLh_.,O=t-,:,ti.,__ __________ _ Collected By ('Ll?$'E)h~lewirv ID# q}r/4 Dale Collected __ ..!.~.,t.,~:.....'::... /,,,._· /4......:..r:..,,z===-----Time_~/~a:2~cJ_,,o"--_ I Agency: ·t/flazardous Waste Solid Waste __ Superfund I Sample Type Environmental Concentrate Comments I Ground water (1) _ Solid (5) f /Ow _f:'.'.'.'Surface water (2) Liquid (6) _________ _ m _Soil (3) Sludge (7) __________ , _ n _ Other (4) _ Other (8) Organic Chemistry D Parl)Jlleter v P&T:GC/MS I] ::;::?,(cid:B/N Ext. II MTBE -- Results(mg/1) I ===-----------•=--- Inorganic Chemistry Parameter Arsenic --Barium --Cadmium --Chloride Results(mg/l)(mg/kg) Chromium __ Copper Fluoride Iron --Lead Manganese --Mercury · --Nitrate --Selenium Silver --1 ______ R_ .. a_d_io_c_h_e_m_i_s_try ____ ---1 __ i~~:tes I I Paramt>ter __ Gross Alpha Gross Beta Results (PCi/1) Microbiology 1--------------l Parumeter 1--Results (Col/lO0ml) pH = Conductivity TDS ------ --TOC TCLP Compounds Inorganic Compounds Arsenic Barium --Cadmium Chromium --Lead __Mercury Selenium Silver Organic Compounds benzene --carbon tetrachloride Results(mg/1) Results(mg/1) --------- -- -- chlordane chlorobenzene chloroform o-cresol m-cresol p-cresol cresol __ 1,4-dichlorobenzene _____ _ 1,2-dichloroethane --1,1-dichloroethylene --2,4-dinitrololuene __ heplachlor hexachlorobenzene hexachlorobutadiene ------ ---------hexachloroelhane ----methyl ethyl ketone nitrobenzcne __ penlachlorophenol __ pyridine __ tetrachloroethylene __ trichloroethylene __ 2,4,5-trichlorophenol _____ _ __ 2,4,6-trichlorophenol _____ _ __ vinyl chloride endrin L-• -••-·· ·-S_E_P 2,_ · fi;Y. . . · · -lindanc II) Date Received B92 Reported by . . ·--· - · ~ m 0 ~l~oxychlor '_ .. _-·__.__ ____ --_· ~;.,c•:~:~:~~~{~2~~i:!@;;::·.:;~E~£S¥~~~~=~:-~~~:=~-~;~~~ ~~~-·;:r:].;:n;~-ilv:~; *~. :· -.... ~.•; .,,--•;. D,11 c An,ilyzcd 1-/J-9]_, C,-1-5-q;;,., Lab Number -·i• ·-,;;:.; S ,j j_ -· -= . . I llllS 3191 (ltcv;scd 2/91)fJ,,!) 7UU"' 1 ·· I ·I I n D , I I I I I l.1t<·;1L ion or Sampling: N. C. DEPARTMENT OF HUMAN RESOURCES DIVISION OF HEALTH·SERVICES SOLID AND HAZARDOUS WASTE MANAGEMENT BRANCH Chain of Custody Record Hazardous Waste Materials Generator __ TransporLer __ Storage Facility __ Disposal Fncility _L Other : .$' If PJ14f,f /1,ef tdff t( Tn·.1lmt•nl F;i, i 1 i L) Land rill rompnny' s Name ,--fl6-l'f,,v_;¥(7rl7/444 ,f,vz,e',(?e/,p Telephone( __ ) _______ _ Address (Eqr-,_,t.d ) f'C t,</ , p.Jc, ;;,,o , ,;7~,,-7;.5,11«c£; ,9. _;/ ;f<J[~d~ft1;_,,,J._,,..___, Collector's Name4.o:,#-/'1'..'. /_;,.,,h·~,:,, · :1'.J/,i=-Telephone( '71'7 ) ·7:?5-2/76' · signature Ila t e Sampled. __ _.'1,1,,/~;l,1,,i"-/-'y-"~----'q,,,_/-',_/'--'-z...:;:,_c.. ______ Time Sampled _________ _ r I I Type of Process Generating Waste. _______________________ _ Field Information Fie! d Sample No. // / 'J {, //.;2o3 rh,1in of Possession: ., 1. signatur /l!f7 /!If/ __ ,_,· ,,c:'--'-.--'-7!_:!t~"".:'-__ L~_-_-_-_-_-:__-:__ sign.1ture /I :2 oo 1/.Zo z_ /l,2o 7 1/.Zo'/ gJ;-1/2 lf2 inclusive dates (ltfl£'0[,:Lct4;--__ ~9'--· ·+/'------''CC.zc..L/_,_9_,z:,_-_ title inclZsiye1 dates inclusive dates ~ tit le Resu-1 t~s · p:rted ,',, , , , , . , !'/-."7'2-:2-, '12-9-Y.2-. ~ 9 £r / , , , , , , , I, , l11str11cliCJ~S:, ·Coniri·,,rc~;lll applic;bi-e infoi'.niiit'ion incrudinis' s'i0gna(ure,s', :-ind , ... , ., .. -, ~_-_ .. 1 . -~_,..::-~ "..:.,~.~-, ..-: ;:~ ... ~::-~: .. · ~-=-~.~i ~~~ . .: .7 .. ~:':.·1.: J -~·;: ~~}J.J~~-,.~.;J.~~:.~ -::F~::~ ~ ... ;.,..:._--..;;;:~~·~,.:l:';;;~~~~c.7: -;<·.·-o .• , .. ----~":_,.-... ~ .. :-.,-=~-~·:.:::::-:.'_~_; . ,-.. _ ,. · -.. -· · __ _ ·!'. .. · --~ I•• .st~-'--~_. -.~ · •. ;'!_, r ,', . ~, .... -_ .. _ .... _:-,..;:.'..:-:,. •s~. ":". :,,.,.,.::--:~,:i·.C.:·":: •··-~.:;;~ . .::;-r,;:-.,·.,:.t.:=-;';._~•!•£,;;,"->i:, • ...:.w .. ,.,; ·--_., .. :-, ... ; ·. -· ·, _ , .. ~--. •.• · .. , _. ·,_ .,.., ~,·---! ,:: ~) ., . .:. .... ~'4"-",--·•· ~ ~-.. -._.,.. _ _. • ·;-,,•.•.0._-4 -·~··f-~Y-F,!! ""'··~;'-' ;0~.>?"--!'!"~ -·"':-,-· . ~-. · .•• ·~----,·-;;>-,;, ..... • I I N. C. DEPARTMENT OF HUMAN RESOURCES DIVISION OF HEALTI-1 SERVICES SOLID AND HAZARDOUS WASTE MANAGEMENT llRANCII Receipt for Samples ~The· :;,1u1plt'S dl•scribed below we.re collected in conn·ection with the administr:1t inn, ~-nforc~me11L, nnd documentation of the: I North Cnr,1linn Hazardous Waste Management Rules, JO NCAC lOF () North Carolina Solid Waste Management Rules, 10 NCAC lOG I I ( Comprehensive Environmental Response, Compensation and Liability Act (CERCLA) ) Toxic Substances Control Act (TSCA) 15 U.S.C. §2601, ~ ~-, specifically Section 11 of TSCA, 15 U.S.C. H 2610. m 0 Inspector's Name Name of l'Jrm Owner, Operator, or Agent ··-- :;AMPLE COLLECTED SAMPLE TYPE NUMBEP. DATE TIME WATER SOIL //If{, f?/)';/M 151"' fllf7 R///4L /1.-Zo II I f'l:i £ ;,,4,! 17?,• v //l'l'i s!;,/n ofLo ✓ /1 Joo 0'175 /,'_,7c>I . /Ill:, v // ,;;,,2 l/o z" ..... __Lt_ :) <) :J 1 I 10 v /1,;loY' ///', LL-;, oc:-/3:h' I I,, /ll 1.J 'lo Lf_i!Q2_ I If/I> II i1v9 J; 1500 ,/ I K<·cdpl for the sample(s) described :dwvL· is hereby 3cknowledged: I _ i2t& -c £d•{H-tc Signntl1re of Inspector OTI-!ER Ltr!..{,V V :>u .... o,it "1'-itl>.( SLuN( _,, -~1,! L, t>.,p Jew"'-• U l'i,11;? --- /1/. ( lnspec_tor' s Addr Address Title DUPLICATE SAMPLES SAMPLE LOCATION OFFERED ACCEPTED REJECTED ON-SITE OFF-SITE ✓ ✓ // ;/ ,/ / ,/ ✓ / ✓ V ,/ / ✓ ,/ ,/ c/ ✓ ✓ / ✓ v +---+ v -······--·--·-- ✓ ./ ---· ----------- Receipt/rejection of duplicate or split samples is hereby acknowledged: ) . 1 -7:4-/..., ___,; <----;: 112 .~ Signattire of Fi.rm Owner, Operntur, or Agent f I· .. PURGEABLE COMPOUNDS COMPOUND hlororethane rcm:me thane dichlorodifluororethane invl chloride hloroethane rrethvlene chloride 1 richlorofluororethane thene. 1 ·1-dichloro tt,ane 1 1-dichloro- 1 2-trans-dichloroethene hlorofom, thane. 1 2-dichloro- etMne. 1 1 1-trichloro- ,-arbontetrachloride ,rorodichlororrethane rooane. 1 2-dichloro- 1 3-trans-di ch 1 o ne rich loroethyl ene hlorodibrmorethane zene ne. l 1.2-trichloro- 3-ei s-di ch loropropene 2-ehloroethyl vlnvl ether rorofonn STATE LABOMTORY Of PUBLIC HEALTH DIVISION Of HEALTH SERVICES, N.C. OEPAATMENT .Of .HUMAN RESOURCES P.O. BOX 28047 -306 N. 1/ILMINGTON, ST.,.RALEIGH, N.C. 21611 ORGANIC CHEM!CAL ANALYSIS p/oW P•S · P7W f5V✓ LAB NO CJ7::iq JC, q,,n -:in q .::J::,q::,, I q;)dq;;,,, FIELD# II I a lo /IIC/7 JI I -,~ I Jlqu TYPE ( ,. ) 7\ ( .. ( ~ ) ( .., l UNITS uo/1 Mikol uo/1 I .. n/ko) "a/ 1 /uo/ko-, .. ,/\ (\,n/kci? u..-'. II u:;: -I I I ~ ' I -I ,.y ,'/ ' ""' I Af n I ;,. ""'-r, I I '-~ \.' I 'ii ' I Qi+ ".) I i,..L... ! ~ ! i d-. : i ' -'-' \ ' : .)<::---. \ I s;.. '- ' "< i ~ ' i I., ,, -..; i r ..,__ ---, ' "'< : \ I ' I thane. l 1.2 2-tetrachloro-' i ethene. tetrachloro-' \/ .._:/ \I ' toluene ., <-:::, J....,..,...,. ,, c) LJ ,:; '+ --iq h lorob<enzene ~ LL U-,Li thvl benzene "" .i/ !, ·, / '' _, .... cetone ·-~ I' ' . '' / I .-bu ta none " '-i urbondisulfide ' I ., -hexanone I i thv 1-2-'•'ntanone I i stvrene I ' vlnvl acetate .,v (xvlentl l+d-ai) "O ·'-i; '' IL. /.I-L L ' ,,.u, . ,.. ' I . I' ,'/ ,,; ,-,.Li/~ f'nr-" ,..;~_,. nrl "'i I , (-t"!/(-', (~ (-') (-1 (-) PS s w Qo-,C):>::,, Cf .J-7Ci ::, J JI-,,., I) 11,2.L)·I I '71 ( --,, un/1 rtia/kn .. n/ 1 {(,n/en) L<...-' . - ! I i I i I I ' ' : ' -/ -' V 7fl I-'-- I I V \7 ,;_ 633 :r ,Jr.0· .?5co Ii '2.0'. UT I• ?,,CJ,J ,:J7"i j ( .- I ✓I I r, 4-;., ' I l.L--_y (.;_) (.f-I STATE LABORATORY Of f'U8LIC HEALTH I le DIVISION Of HEALTH SERVICES, H.C. DEPARTMENT Of .HUMAN RESOURCES P.O. BOX 28047 -3()-; ~-~!LM!HGTON, ST .. RALEIGH, H:C. 27611 ORGANIC CHEMICAL ANALYSIS f,q-5 . fJw' f35 f2vV PURGEASLE· W1POUHDS LAB NO 'i cl JU :;i,c; q.,., LO')(., r->" ,n 717 q]_Jq -;; ?! FIELD # JI.Jn::J I J,20.';:z, ) J,J,1,Lf J J 771!:J CO'IPOUHD TYPE ( 71 (~ ( 7) ( / o) UNITS un/ 1 ((iQ/k<j) uq/1 /n/l'n' un/ l "'o/ko .. n/1 ,<;';;/kn~ -mhlorcmethane , ' ; ' u... rmonethane dichlorodifluorcmethane \ minvl chloride ~ I hloroethane ..... I '<I ·..y rrethvlene chloride " _;,, 19 /Q/J.. I ' richlorofluorcmethane ~~ I.,(_. I , I • ! I thene 1 1-<lichloro = -! ' thane 1.1-<lichloro-..... 1.2-trans-di ch l oroethene ':---' nhlorofonn ~ ' thane l .2-<lichloro-\, I ' . ' etMne 1 . l 1-trichloro-I i arbontetrachloride . "-.., i n:m:xlichloronethane "· i prooane. 1.2-dlchloro-..... -, I i , .3-trans-dichlo ne 'j'-..,. -, I ! I rich loroethvlene -I chlorodibrcnor.ethane -,:; V V lene C' i +,,,.,,lr P ., 5( ::r :;,, ;\ ne 1. 1 2-trichloro-. " I 0--i_L-i ' I --c i s-<.1i ch 1 o ne ~ ! i 2-<:hloroethvl vinvl ether ·, i I I roroform <:::-..) I ! thane 1. 1 2 2-tetrachloro-) I i I I eth€ne tetrachloro--:,,..,., V --.v 'ii ,i/ I oluene '-\ LJJ57 ,4 '7 I I JJ77 hlorobenzene :')>;t; ; . o?f'.J I £./ 9, , ....... thvlbenzene " _,10 -~/ :?Ll 0. ' (' cetone "'--L,l.--::,,--,n '-10/o L<-.- -bu ta none 0• '7 ::>,", I ' . carbondi sulfide ,;-... I, I -hexanone ~ -rrethvl-Z=ntanone _ .... l styrene .... i I i ii nvl acetate ....._, V .,! / ,'I >.vlenes i+d-a/J ' I, I ,o I "4 I ,e, "'"ih,.1-i-h;,J.,,/ r,}h,,,-I' LL /; '' ,•.,/_J, J ;,,. NI •~ n,.-,'. 0 ~ .J_"\ /'fj/ r-(+) (~) r+ J I.;..) I ' ., Estimated value. -•· · •. . ·. · -Actual value. is.kno,..,n to be less th,rn .. value given. · · · · , Actua~ value· ls known to be greater than· value given. ' · ~~enal was.analyzed for:.but.not detecte<f. The nurber is ·the Minirrun Detection I imit ~:,NA~~~:~~--~~~f_I~f-_:1~-~~-~-i~f_,i;~;;~~:~:~:-~_-::~~~~--:~~:-~~;~?·1·-~-~-.f'.+•·~~~-~~-~~:-·~-~~-:-~ ~_: ~=:· •..•. -•• , --~ . -~:::. •, -,-:.-:.,On ... ~R.QC~ .. llst.o(.-. .-P.CJor~1:ty,..,Pol lutants.:.---;,-.-·--. ., .. ~ ... · · - N.C. Division of llea°lth Services IIIS 3068-0 (t./86 Laboratory) 1°2.S '1 ;1. ::; CJ. -f.j . C, 1;iq 4-{) ;,_J,1 In l li:/0 7 ( 7) (/, 1 .. n/ 1 ,.;;,/kn uo/1 (l]Q/kn"l , ; ' I I I i i I : ' . ' ' ' i I . .. / -;,, (,· --LL - ! \( \/ i·,C3() 1./(1 C( !','7 " ;JS.;,,;;, ,J,r /,"),J, i.J, c:i, i.,,....,, / L- ;p I ,, i ,, I .'55 v Ll,... ,, I+) (+) STATE LASORATOOY Of PUOLIC HEALTH I .. I DIVISION Of HEALTH SERVICES, N.C. DEPARTMENT Of .HUMAN RESCXJRCES P.O. BOX 28047·-306 N. IIILMINGTON, ST., RALEIGH, N.C. 27611 OOGA/IIC CHEMICAL MALYSIS , p loW PURGEABLE 00'1ro.JNDS LAS NO q,-.u,I J FIELD# 1,'>r,C, 00'1ro.JNO TYPE ( _:,) ( ) ( \ UNITS , .. n/ l n,o/ka ua/ l uo/kq un/ l .. n/ko chlorcrrethane brcrrorethane dichlorodifluorcrrethane n vinvl chloride chloroethane ' methvlene chloride '-D trichlorofluorcrrethane ' -~ ethene. l. 1-d\Chloro '--::, ethane l 1--<lichloro--~- l 2-trans--<lichloroethene ,, -m ch l orofonn SC..:: . ethane 1.2--dichlor'O-~ ethane. l l 1-trichloro-'~ I carbon:etrachloride . - brorod1chloronethane \ nr..-v-.ane l 2--<lichloro--'< 11 3-trans--<lichlo, ne ""· trich loroethvlene -\ " chlorodibrmorethane f'~ t:zene ..c"'-I hane. 1. l 2-trichloro-I 1.3-<:is--dichlo ne -.... 2-<:hloroethvl vi nvl ether -----, I brorofonn --..:- ethane l. I 2 2-tetrachloro-I..... ethene tetrachloro-" 1 toluene ,,._<:;; chlorobenzene e thv 1 benzene ,::' "--' .... I acetone ~ 2-butanone ·-\.l carbondisulfide ') 12-hexanone · 7 4-<rethv1-2~ntaoone ~tvrene .vinyl acetate xvlenes l+d-a/1 n1efh ,,f--f.i-,,.J, I p,J../,;,r OJ L ',, /Q n'I ,,,,,, ,;r/-. I I llf-1 Ir-:1 N.C. Division of Health Services · 1011S 3068--0 (s/86 Laboratory) I • ; I ! I ' ' : 'I I"· 'l ;_,___ J,, I ' I ·' ' ' ✓ (+-;) ( l uo/ l .. n/ko ( 1 ( ) un/ l .. n/ko .. n/1 uo/ka ·-- .• NEUTRAl AND ACID XTRACTABLES COMPOUND ~ itrosodimethvlamine . (Z-cr. loroethvl )ether _g-chloronhenol jnol l -dichlorobenzene l 4-dichlorobenzene ll-dichlorobenzene (2-chlorois llether hexachloroethane t. 1 troso-di-n...nrnnvlamine L robenzene i nhorone 2-nitroohenol 1-dimethvlohenol __ , (2-ch loroethoxv)methane 2 4-dichlo~hencl .. 4-trichlorobenzene hthalene hexachlorobutadiene j hloro-rn-cresol ach lorocvclODPntadiene !c.,_ 6-trichloroohenol 2 ronaohthalene hthvlene thvl nhthalate 2.6--dinitrotoluene naohthene -dinltrmhenol ·2 4-dinitrotoluene ii troohenol '1orene "hloroohenvlohenvlether diethvl Dhthalate -dinitro-o-cresol henvlamine azobenzene henvlohenvlether ach l orobenzene =ntachlor~henol H :>nanthrene ~ hracene ( uutvl ohthalate fluoranthene STATE LABORATORY Of PUBLIC HEALTH DIVISION OF HEALTH SERVICES, N.C. DEPARTMENT Of HUMAN RESOURCES P.O. BOX 28047 -306 N. WILMINGTON, ST., RALEIGH, N.C. 27611 . 17-~~GANIC 01EtfJL ANALYSIS f1W f'5vl LAB NO 9;z.;F1c::/'-i "t.'J.,2 '1-·ro '-f,,.(.J. '1, f i ,,2,?-'t._1,-l.. FIELD# lll'H,, Ill 9'7 II 1Cj .lr' //1'!'1 TYPE (In) ('7 ) (o< l (,,Z l UNITS l'f'/\1 I I I I A -r,·,"'-1 .. /Jf)f'VI ,, I J • I A. -I I- \ /,0 IL- '/ 0, I U- I " I ~/ .::? ' 0 '7, _-;-. (,;,' 0 I.I--i,A...--·, IA---- f1-W 7,:/.::!_"}3 ,3 c,,.2.293',f. //.2c.,O /li,Zo/ ( 7) ( • ..2) • A Ff.1/11 f r, r I I LL.- ,v u, I· I, 0 II,-z_ u._ ' ' ~-0 lL-- ·/ ':{ Q L"--· \I/ I· -/NEUTRAL AND ACID EXTRACT ABLES OJMPOUND nvrene zidine b 1 benzvl ohthalate benz(a)anthracene chrvsene 11■-di ch lorobenzi d\ ne hlJ!C2--ethvlhexvllnhthalate di-n-actvl nhthalate mzo(bl fluoranthene zo(kl fl uoranthene benzo(a)nvrene i no ( 1 2 3-cd' nvrene nzo (a. h} anthracene benzo(o h il~rvlene lline t-enzoic acid lzvl alcohol hloroanil ine di~furan ;--1 naohtha 1 ene ; -ethylnheool . ~ ,-,othvlohenol 2-nltroaniline litroaniline itroanillne 2 4.5-trichlorooheool STATE LABORATORY Of PUBLIC HEALTH DIVISION Of HEALTH SERVICES, N.C. DEPARTMENT Of HUMAN RESOURCES P.O. BOX 28047 -306 N. IIIL11!NGTOO, ST., RALEIGH, N.C. ;-)611 pc,, gRGANIC Q-1EPf.Cf:L ANALYSIS ('7W f5vJ LAB NO CJ.-•-~· ,_,q <./J.;?C/30 'I.;/ .'J ';13 I C/,.2.Y-/3 ,, FIELD# ///< ,~ /iltj•7 ///,:_ly II /<f<f TYPE ( ;,,, ) ( 7) (,;l. ) <-~) UNITS /J P/V'I PP/VI /''l"/11 PP,A,1 LC-()_.. \A-I.I . . • \ /} 0,0 '70.,0 ,, , ' ' ; I 'I / '\/ LL L,L ,; u<-- \ u.z.. i,L. ~s-. .s L-L •/ \ ' \ / ' / ,,------•' lr:!JUX(lk. .tic I J>5 + I-( + _! (+) 7-) ( -} --~- I I - p5S P4w q ,;?;),"/ .:f~ Zl..:?;:! ''-.:f i/- /11./JO //.20/ '7) (,2.) , ,.,., ... , ,-r/ l·- "--. \ '--f()J) ilt- \/ \ / L,L, ' l,,{_ \ 3.-0 \,L-· \ / ' / ,.-:-, ~ I .j_) ( -) .___, - .• EUTRAL ANO ACID XTRACTABLES COMPOUND r. ~l■itrosodiirethvlamine b1s(2-chloroethvl)ether ~--~~ ~rooheno l .1 -<lichlorobenzene 1 4-<lichlorobenzene 1-<lichlorobenzene (2-ehlorois llether hexachloroethane ~ i troso-<li -n..nrnnvl amine robenzene is nhorone 2-itrnnhenol g -<liirethvlohenol '2-ehloroethoxvlirethane 2 4-<lichloronhenol l 4-trichlorobenzene hthalene hexachlorobutadiene .I hloro-m-cresol ach 1 orocvc J r-,ru,ntad i ene ··trichlorophenol ronaohthalene hthvlene ,vl ohtha1ate 2 6-<!initrotoluene naohthene -dlnitrfV'lhenol 2 4-<linitrotoluene ~ Ii troohenol J orene 1 -ch l ornnhenv l ohenvl ether l thvl ohthalate -<linitro-0-cresol henvlamine azobenzene ~henvlohenvlether robenzene ""ntachlornnhenol nanthrene ! hracene 1 utvl ohthalate fl uoranthene STATE LABORATORY Of PUBLI•; i!EALTH OIVISiON OF HEALTH SERVICES, N.C. DEPARTMENT Of HUMAN RESOURCES . P.O. BOX 28047 -306. N. WILMINGTON, ST., RALEIGH, N.C. 27611 . p4s riw -pos ·p~vJ . . ORGANIC CHEMICAL ANALYSIS " LAB NO Ji.),~q '? ", l-f,:l,)."f. ·< I~. lf ~ :? / 'I J ::P 3 X . FIELD # //.2 0 ;)._ 1;;-;.03 //,2[)l/ /l-"-0 < TYPE ( '7) ( ,:;2..1 ( ·71 (Ir,) UNITS rrrvt · rF/VI Ff'/VI. f'P/11 J A... LA...-IA IA , ' \ / . I, r l O. I I ri,. 7 I,{ I '-/' 0 (;L. . ' ' I ' C-~ ~ 0 / \ / .v L-L-' / ftvJ C/.:2,2'-j_-?4 L/ .::?,2.9 <I I) //..2-o(p //,}_f;7 ( 'll ( l,,i f-'f-' /V{ Pf'/VI Ii 11 \I/ "· 0 { /4..:, I I I I ' I I I , \ -, I (), < / /. 0 L.C-().__. STATE LABORATORY OF PUBLIC HEALTH DIVISION OF HEALTH SERVICES, N.C. DEPARTMENT. OF HUKAN RESOURCES P.O. BOX 28047 -306 N. WILMINGTON, ST., RALEIGH, N.C. ;-/611 . (14~ . Pl> vJ . ORGANIC QjEMICAL ANALYSIS f35 f2W /NEUTRAL ANO ACID LAB NO 1.1,2.;i.43,-9.2 .2 '-/-? (.,_, '/, .J.:.J. 9. ~ 7 Cl..!.2 "J3 .'? EXTRACTABLES FIELD# I/,.). (J ,J.. //,2(/ '? I /,1-<1<.J //.J.,r-,.::,- --.-CXl'IPOUNO TYPE ( 7) ( ,.z) ( 7 ) ( L-l UNITS rr ,11 l"l'/1-1. I" /Jfv/ .. ,.--;;/VI. ovrene ,,1_ i, . ' 1 I . ~5dine 1 benzvl ohthalate benz(alanthracene . E! sene ' 7 l, -"i ch lorobenzidi ne bi 2-ethvlhexvllnhthalate .. ">-:O (,; ,0 di-n-octvl ohthalale /.,,L-V ~o lb 1 fl uoranthene o(klfluoranthene benzo(a)nvrene ~no(l 2.3-cdlnvrene nzo(a h)anthracene . . ·, benzo(o h il"'-"rviene ' ,11 ' / ., / II arM ine 'A. i ,I LC i ,L...- benzoic add : ~vl alcohol loroaniTine di ofuran ·, 7 2 l0 •0 hthalene c1. u s .thvlohenol ' , . /. u 4-thvlnhenol I .• .o /.~, 0 2-itroanllloe vL.. u...- 3, troani 1 ine 4J troani 1 ioe ' 2 4 5 trichloroohenol I ' \ , ·, 7 ·, / z I RR0X V1 i (' ,,--,__ --Ii c''.;7JS -t-1-I+ J ( -) f-+-7 (-) ' -· - 1 - - I J -Estin'3led value. K~ctual value is known to be less than value given. L ctual value is kn™n to be greater than value given. U terial was analyzed for but not detected. The nUTber is the Hinirrun Detection Limit. ]1, illi~if tE~f 1{Uf i1;~~:~;;;~i::'·•.',': \ \•~~ ; :··.~•. •• • C 'c,., = -->CS :;•; ••• • .- N, C. V.i.v-i..6.i.on 06 He.aUh SViv.i.c.v., VII 3068-0 (4/86 Labo1ta..to1ty) ('25 flW '-7. :1.2 '1. ?'1 C/~.:!-; q Yi) ( /.;LO (,, //.2./17 ( 7) ( / _, f>P/1-1 ,P//v7-. ., v-- ' / \ I/ J-.o -3l-o.o i..L--IA- \ ·, 7 I , I.IL ·, / /, () I A.- /,,J () l,C, ' / \/ --,..--,0.. ( -) ( --r ) ---------~ •:NEUTRAL AND ACID EXTRACTABLES COMPOUND itrosodimethvlamine bis(2-chloroethvllether -~ hlornnhenol nol l -dichlorobenzene _ l 4-dichlorobenzene 1-<lichlorobenzene (2-chlorois l)ether hexachloroethane i troso-di -n ...nrl"V"\vl aml ne robenzene isoohorone ltroohenol -dimethvlohenol b1s(2-chloroethoxvlmethane / ~--<lichlo~henol ___ 4-trichlorobenzene hthalene hexachlorobutadi~ne lh 1 oro-m-cres,) l ach1orocvcl=ntadiene lltrichlo~heno1 ronanhthalene hthvlene w1 phtha1ate ? 6-dinitrotoluene ! nanhthene . -dinitrnnhenol 2,4-dinitrotoluene I it .-nnheno 1 orene 4-ch 1oroohenv 1 ohenvl ether , · ethv1 phthalate '. "-dinitro-o-cresc1 < 1 ,henv1 amine azobenzene l=henvl nhenvlether achlorobenzene oentach1oropheno1 lnanthrene hracene dibutvl ohthalate f, ,oranthene J -Estimated value. STATE LABORATORY OF PUBLIC HEALTH DIVISION OF HEALTH SERVICES, N.C. DEPARTMENT OF HUMAN RESOURCES P.O. BOX 28047 -306 N. WILMINGTON, ST,, RALEIGH, N.C. 27611 ' . . ~ . fl0 ORGANIC QjEMICAL ANALYSIS LAB NO ~1 • .1 .t"T <£ I FIELD# i/,.L0•1 TYPE (~) ( l ( ) ( l UNITS PPM I ( ' ·, / :.?_. 0 vL Actual Value is known to l>e less than value given . . Actual value is_ known to be greater than value given. .. ( ) ( ) ' -- Material was analyzed for but not detected. The nurber is the Minirrun Detection Limit. !'.:,_·· Not analyzed. -=--~--' Tentative Tileriti'ffcafion'""·:'· · ·.-· :-·,"'= ~-;-.:ccc .···.,,,,cc:-•·. ·.cc.cc,.:O·,"':.c,::·.:.= •·a·: , __ :/~:-,:;.'--•.• .:., ;'., / 1 ·· c· ·,-'~. -J.-i"' __ (i; ,1_1 .. . :II ~:o: NR~.Li~!-:-'-'rP.~i.~~,l~·t;;lut,arl~-~61-i/H::tt..;~(l~u~#~ . J'-~ _ l:;,u.... ,,. 1 '-~ .. N.C. V,tv,</2-<.0n 0£ He.a.Uh SVtv-<.cV., 1 .. -. . VIS 3068-0 {4/86 LaboM.ton.y) STATE LABORATORY OF PUBLIC HEALTH ofvisrON Of HEALTH SERVICES, N.C DEPARTMENT OF HUMAN RESOURCES .. _P.O. BOX.28047 -306 N. IIILll!NGTON, ST., RALEIGH, N.C. ?1611 J I \b ORGANIC OlEll!CAL ANALYSIS ' , r · 1 f E/NEUTRAL ANO ACID LAS NO -, EXTRACT ABLES FIELD# 1I.:i. 0<1 I CXJMPOUNO TYPE ( ~) ( l ( ) ( ) UNITS /JPM rene ;, zidine t vl benzvl phthalate benz(alanthracene lsene · · -<lichlorobenzidine · . ... I 2-ethvlhexvl)ohthalate . ,. D di-n-octvl Phthalate I lzo(b)fluoranthene zo(klfluoranthene ben ZO (al nvrene ;I;"° ( l . 2. 3-cd) nvrene nzo(a h)anthracene , benzo(Q,h il=rvlene " iline I,,(_. .izoic acid zvl alcohol hloroaniline d; zofuran hyl naohtha lene thvloheool 4-rrethyloheool litroani line itroaniline itroaniline .. I 2 4 5-trichlorooheool -' . }E.BfJ "i... Vi..,1 <!, I~ Ci .J> .S +I-( -: -- . Estimited value. Actual value is known to be less than value given. Act!J.3.l value is known to be greater than value given . . K.:iterlal was analyzed for but rr0t detected. The nUT'Oc'r is the Hinirrun [):el_ection Limit. ( ) ( l ·--- NA·" Not ·analyzed. · · I -Tentative identification. · :/ · · ;-1 -j;; _·-r, -On NROC List of Priority Pollutants. /31-1/'A-/)u(.;u)_~'1(,:<1/.A.:C~ /i,,:a,~/; 0= .. / )1(!fl-1 c· ,'-I. C. D-<.v-U-<.c111 o 6 lir.o.Uh SVtv-<.CV> ,, 3068-0 (4/86 La.bo1U1-tO/tCfl K.C. I DEPARTMEKT OF ENVIROKIIENT, HEALTH, and NATURAL DIV1S10l( OF SOLID l>'ASTE MANAGEMENT Chain of Custody Record Hazardous Waste Materials GPnerator . __ Transpur lt.:r __ Storage Facility __ Disposal Fncility Landfill D fnmpnny 's Telephone( ___ ) _______ _ I Type FlPl<l of Process Generating Waste ___________________________ _ Information ·•---------------·•------------- (, .. Fielcl Sample No. .._ ' I '/1_·. I ICli:,Jn of Possession: ,, ', i ' : I '· .' I '. .. _signature / .. .,, -~_-, ·title ·1nclusJvc dates 'title inciusive dates r· tit le J.nclus,ive dates /· _..J_ •... S"il',n,1ture t it] C cln t f' Complete all applicable information includinl', signatures, and J I --. " · _ su_~mLt 1wjth ana1·);Ri"s requeSt foims.··-----· .--·:;-:"_.,.~!-•. ;·.,, ... ___ , ..... , -~--r.~-: ---•·,•:-• .,,, _,,,-..·,>;:',.~.;:·.":.'''"::·-··;.·.• ·••'\·_--,·~~,----,.,,~_•_J •. --•--·.·J. •-•,••h :c':,••~h• r::••••...,..;:~-""••,!••:f••,";'• 0 --:-,:,.-~::•-~-,•--•",·<;,.:._, .. "'!.;.• •' I I K.C. DEPART~,E'.\T OF EK\'IRo:;),El\T, HEALTH, and NATURAL RES~•L'RCES DIVISION OF SOLID WASTE MANAGEMENT Receipt for Samples -· ' I. ·. :· .:, . '• ' ·1111 · .. ,1,,1,·n.:4 d\'.S.'i,Iihed bcl01,,,• \..'Pre collc>cted in connectiQn with the ;1c\minf~tr;1tinn, c•11ror1·t·TIH~iii • .:111d dorumC'nt:it inn nf the: m <X; Norri, C;fr,ii°'in:i Hazardous w,,stc Management·Rules, !SA NCAC 13A m North Carol inn Solid Waste Management Rules, ISA NCAC 13B Cnmpr.-hensive Environmental Response, Compens~tion and Linbility Act (CERCLA) U ) Toxic Substances Control Act (TSCA) 15 U.S.C. §2601, !! ~-• specifically Section lJ of TSCA, 15 U.S,C, 6 2610. D °13~v' L-bec(n Inspector's N,,me D ,-W\'."A . c; ( 11:f 'T'cw-.k. t/01 ,'k,; N;ime f Fi rm Firm Address I· i rm O\..lnPr, OpC'r~tor, or Abent Title --.. ---·----- \Ml'LL COLLECTED SAMPLE TYPE DUPLJC I\ TE/SPLIT S/\MPLES 1 SAHPLL LOCATION ' \lMHF.P. IJATE TlME WATER SOIL OTHER OFFERED ACCEPTED REJECTED ON-SITE OH-SlTE ------~ _jQ~:]_ -3.b_ij]_ '--l:?":--0 Ll-j..-..lci ,/ v' ------Ci1.,"'>{''; ·1l:,, .. ------t .. ;:,),..L{4~ •' II -<)cc01 ~ 7?-iJ ✓ V V (Jn ;, a1, 1r.1-('1)~ •. , v V . C _'Jc,_)_!__ . ----· QJ2_';,_ ·-----·---·-.. ' 'it;/' s i ,.,l~f ---____ __1,~--·--------. ----- I•"' fr, ✓ _!k,J IC>C> )_il":(~j~.-'le ,i; ... --------·--- 11 i~ ' - -~j_\;?_ --··-.J.liS. ---·• --.. . . Si~<' </r ;7 I,,,,~ i.-1 Ch, i.( -'le.ii? JNv ··--· \,.d_je .. r1n1'/ H,~ L.i,: ,,cl .. ..':ifJc, J" -II';, ci;, _ I[ __ -----------.. I --- H,·,·<'ipl fnr th,, samplP(s) described ·11,ov" ,;_"cherc,hy ,1cknowled~ed: I 7 -' / f. im~ :-ii1:11:1t11rC' c,f Inspector ~ t.i , !lp,':,1qf1~;51sl. >' ..IL_ .___t~_ V ,, ,/ •✓ --·-···----··. ____ v ---... -----------··-··--·-----·-·· ·-v ,/ __ _L_ __ -·--···----. --. v .. ... •' Ii __ _v _ v· ... . .. ·-. --. -· .. ----- Receipt/rejection of duplicate or split samples is hereby acknowled~ed: /I , / ' ti~~ -~~/---r?.r_.; ---· ·-· ... ···- Signature of Finn Owner, Operatur, or Agent :7 ' -1 . ,.., .,, ... -Title---- D N.C. Oepanmcnt of Environment, J ICalth, & Natural Resources . Solid Waste Mana&C~cnt Division SAMPLE ANALYSIS REQUEST State Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington Street · Raleigh, North Carolina 27611 E .le Number _____ ~~--------Field Sample Number ___ q'--'o"-"'o'-''g"----------- Name of Site lifjC':'f'Yl ~pf, 'e, /AAA:. w/,erpn'>U Site Location ~u{trf CL E Collected By G /e,_c,er !Mart, 'V\ I Doon, ID# 1'3/1,t/i I Date Collected fJ I 3 i /c, j Time !wd-0 1 / F 1 --'-'-ti==•======:...:.=::.-::--:::::-"-::-:=':--::-::-=--=-~ E I I I Agency: _X_Hazardous Waste Solid Waste __ Superfund Sample Type Environment~ Concentrate Comments __ Groundwater (1) _ Solid (5) ]?w-S __ Surface water (2) Liquid (6) Soil (3) _t___ Sludge (7) _ Other (4) _ Other (8) Organic Chemistry Inorganic Chemistry Parameter __ P&T:GC/MS Acid:B/N Ext. MTBE Results (mg/I) Parameter Results~) (mg/t.g) L.. ·:-1 8 ;< Arsenic xBarium xCadmium --Chloride _z;__ Chromium Copper --Fluoride Iron 'I-Lead __ Manganese ..1__ Mercury Nitrate .L...\(g '.} I I 'I Selenium t----------------1 _.:)L. Silver -'-'J. 'o Radiochemistry __ Sulfates I . ·-~~rameter Results (PCi/1) · ~~c __ Gross Alpha _______ = Conductivity Gross Beta TDS ------- 1 --TOC t-----~ - --Microbiology ·1,-------l =-Parameter Results (Col/lOOml) ----- TCLP Compounds Inorganic Compounds ..£_ Arsenic Results(mg/1) ..::'... 0.,C I:\ _x_ Barium ~ Cadmium >< Chromium ,;.. Lead L...o .50 ...6_ Mercury _L Selenium _i::_ Silver Organic-Compounds benzene carbon tetrachloride Res11lts(mg/ll ---------chlordane chlorobenzene --chloroform o-cresol --m-cresol __ p-cresol cresol __ 1,4-dichlorobenzene _____ _ __ 1,2-dichloroethane __ 1,1-dichloroethylene _____ _ __ 2,4-dinitrotoluene __ heptachlor hexachlorobenzene hexachlorobutadiene ---------hexachloroethane ----methyl ethyl ketone __ n.itrobenzcne __ pentachlorophenol __ pyridine __ tetrachloroethylene __ lrichloroethylene __ 2,4,5-trichlorophenol _____ _ __ 2,4,6-trichlorophenol _____ _ vinyl chloride --endrin --lindanc -- --•-. ~~~e Rcc~_v:~: • :'. .':;' .:.~_-'::'."'.~::~:~:.'"'...._";_;R.:2~ .. :~. ~-.d~_\i:•""'.' .. ""'."'-'. =-· --'··~, __ __;·:c.· ---'-" _. -· IT)_et.hory.shlo.r · - -·· . ,,-... :toxaph.ene Dote· ExtracteJ _________ Date Reported 2,4-D I 2,4,5-TP (Silvex) D.ite Analy1.ed Lab Number -,-cc~~-------------~--!)JJS J!1)1 (ltcviscd 2/'JI) n-4 AAA'1 (.."'~·::; .1q? --------- 1. N.C. Department or Environment, I lcalth, & Natural ReSOurccs Solid Waste Management Division SAMPLE ANALYSIS REQUEST State Laboratory of Public Health P.O. Box 28047, 306 f':1. Wilmington Street Raleigh, North Carolina 27611 I .Sile Number ________________ Field Sample Number ___ _,_,,cJ..1-_________ _ Name of Site 'i 1~o-,,1 Yff1<,/AA/t zrAA'!f ,., ~ Site Location_--"'C-"'u,.,_/d.,,,_,_=a.,"---------------- 1 Collected By§(or;r/MrJ1tir./Tocr:,Jskp~D#r3f~J101., Date Collected 'f/i / 9:v Time 0235 E Agency: -/. Hazardous Waste · Solid Waste __ Superfurid TCLP Compounds Sample Type Inorganic Compounds Results(mg/1) E Environmental Concentrate Comments _t_Arsenic L.. o, o'-t x Barium o • '--j 9 _._Ground water (1) Solid (5) "P6,-S _x__ Cadmium ""--Q oR D ....L Chromium LQ-,o __ Surface water (2) · Liquid (6) ....!,_Lead L.o.so _K__ Mercury L.o_ C ,h. _ Soil (3) X Sludge (7) _iL Selenium L..a.a:1 D _k_ Silver L.o _,o _ Other (4) Other (8) -- -- D -- Organic Chemistry Inorganic Chemistry -- D Parameter Resu!ts(mg/1) · Parameter Results~'(mg/kg) Organic Compounds Results(mg/1) _P&T:GC/MS __L Arsenic L.. ""\ • 8 benzene --_ Acid:B/N Ext. ...:1._ Barium \oO --carbon tetrachloride MTBE _.K..Cadmium "---I l.<> chlordane ----Chloride chlorobenzene ----i Chromium --d, I chloroform --__ · Copper o-cresol a ----Fluoride m-cresol ----.. Iron __ p-cresol --_k_Lead --' -\ cresol -- m ----Manganese --1,4-dichlorobenzene --·-_x_ Mercury O. i-'f 1,2-dichloroethane --Nitrate __ 1,1-dichloroethylene -- I _;;t__ Selenium ~7.8 --2,4-dinitrotoluene _x_Silver L.. .:i_o __ heptachlor Radiochemistry Sulfates hexachlorobenzene ---- I ······-·· Zinc hexachlorobutadiene l'aramt!h:r ---- Results (PCi/1) _pH hexachlorocthane -- __ Gross Alpha __ Conductivity __ methyl ethyl ketone I Gross Beta TDS nitrobenzene ------ TOC __ pentachlorophenol -- --__ pyridine I -_. Microbiology --__ tetrachloroethylene --__ trichloroethylene Parameter Results (Col/lOOml) __ 2,4,5-trichlorophenol ----__ ·2,4,6-trichlorophenol --It ----__ vi~yl chloride endrin --. . --lindane· -- ,,,,.,c,Date:Rccciv.cd,;0:,.,_, __ ,, ••• ,.,_, _ ••• '•··"-Rcp_o~te_d._by _ """". -_,....,... --. . ~ ·•~' '---:_z z-~"-· ,,111,e,t~_oxychJ or . • .. :~7•_~;~---~':t:• -::--,...~ r.~-t. '\-· ·-..::.;· .. _,,.. • .:..-.. ·-·--.c.,: . ·-1•:.. .. : . . .. a-~_,·,:· toxaphene -.-.,. ..,. -\'--~-·'-:-"' ... Dote Extrode<l · Date Reported .2,4-0 I __ 2,4,5-TP (Si!vex) Date Analyzed Lab Number J)l!S 3\'JI (Revised 2/91) --~, A C'.-:-U .• C1? i ! : . --. - I ,'\Z.C. Department of Environment, l lcalth, & Natural Resources·. Solid Waste Management Division· SAMPLE ANALYSIS REQUEST State Laboratory o_f Public i'lealth l'.O. Box 28047, 306.N. Witmin.gton Street Raleigh, No~h Carolina 276~ 1 . •• ,ile Number~---------------Field Sample Number __ __;JQ.,=--"----------- Name of Site 5rqrrxm ~M e:,l:yprt'led Site Location _ ___.E"""@.,_,_,·cc/c.,_s= ____________ _ I Collected ByGtase,!t--1t:,rt,vc/,::n:,,,-.,,_ ID#13/44/4, Date Collected 'f /i /92, ' ' Time --·~IO~ZO=--- I Agency: _x_ Hazardous Waste Solid Waste __ . Superfund TCLP Compounds Sample Type Inorganic Compounds Results(mg/1) I Environmental Concentrate Comments ___.!:'.'.'._ Arsenic L.o,a'-1 -P~~s ___.!:'.'.'._ Barium D~3R __ Groundwater (1) Solid (5) --2'.'.'... Cadmium L, Cl a·Q8 _IL. Chromium L.. Q. ·, 0 I __ Surface water (2) _Liquid (6) _JL..Lead L. = ,50 _.!:'.._Mercury L...o,o)-.. _ Soil (3) __L._ Sludge (7) V Selenium ""'-.a.c'::J I i/ Silver . L.o --iO _ Other (4) Other (8) ------ I -- Organic Chemistry Inorganic Chemistry -- -'· I Parameter Results(mg/1) Parameter Result,~ (mg/kg) Organic Compounds Results(mg/1) P&T:GC/MS ...L Arsenic "-1 ,8, benzene = Acid:B/N Ext. --...!:'.'... Barium s·, carbon tetrachloride --MTBE JL.·Cadmium L._ \ lg c!-,lordane ----Chloride chlorobenzene ------v Chromium L. ::i.. 0 chloroform ----- --__ Copper o-cresol -- m --Fluoride m-cresol ---- --Iron __ p-cresol --1Lead ~ :)..q cresol -- I --__ Manganese 1,4-dichlorobenzene -- --...JL Mercury 0-1 1,2-dichloroethane -- --Nitrate __ 1,1-dichloroethylene -- D ...JL Selenium L.,.s 2,4-dinitrotoluene _JL.Silver heptachlor L. :J..o Radiochemistry Sulfates hexachlorobenzene ----······-·· Zinc hexachlorobutadiene D ----ParJ.mt!ttr Results (PCi/1) _pH hexachloroethane --__ Gross Alpha ·-Conductivity __ methyl ethyl ketone Gross Beta TDS nitrobenzene --g --TOC __ pentachlorophenol -- --__ pyridine __ Microbiology --__ tetrachloroethylene m --__ trichloroethylene Parameter Results (Col/lOOml) __ 2,4,5-trichlorophenol -- --2,4,6-trichlorophenol --= vinyl chloride ----eridrin --lindane •.. --methoxychlor 1 . Dale Received :: ~~ .. :~~;::~~~:;~:::-~::i::~--~~.-:~::· ~!:-·•; :::-. . R,P.9'\ed by --.. -. -~. _..... --•·::.' -~~--.. : _· _· -toxaphene ·-· -;-.~-·-~--"'7" ·, -_., _; ~-:-,_:· •· -. -· -----~·' --~ ---· . ... ! ,. Dale Extractc<l Date Reported 2,4-D .. -... ----- I 2,4,5-TP (Silvcx) Dale Analy,cd Lab Number llllS 3191 (llc>iscd 2/9!) -----, l'. ;'\)Is C:F ,c ' (O') n • .. ·-· l I' 7 / I. N.C. Department of Environment; l lcalth, & Natural Resources Solid y.:~sle Manaicmcnt Division. SAMPLE ANALYSIS REQUEST State La_boratory_ :;,£ !1_ublic Health P.O. Box 28047;306_ N.-Wilmingto_n Strccl , · Raleigh; NOrth.Cirolina 276il · .•· :~ _, .. , ... ·; •• Site Nu..;,bei-_· • · . . · Field Sample Number_--"1,"'D.c..·.,_/,.,l.,,z..... _____ -'-_:_-'--___·_·=':.c··'.: . Name of Si.le i½JICM S{pf.-c1/AllA I Collected By(r{r,_c,erMa.1¥-<K/ Dot,·~ [n{e "" I'&, Site Location £u {o (C<. j j I ' I ' ' ID# 1~/,{ /1, Date Collected · 9/1 /9-z. Time II I '5 Agency: I( Hazardous Waste Solid Waste __ Superfund TCLF Compounds i I Sample Type Inorganic Compounds . I . Results(mg/1) 1 Environmental Concentrate Comments J Arsenic ..e..o.o'-l i I ✓ Barium a.·::, a I [3-5 --__ Ground water (1) _ Solid (5) _L Cadmium L..o.ae, _.!:::'.'., Chromium L. .. Q .IQ I __ Surface water (2) Liquid (6) JL.Lead .<:..0.50 v' Mercury <::'.._o. ca,,. Soil (3) i Sludge (7) -;:::;-selenium L..a.a '-\ I 7 Silver L....Q~~Q _ Other (4) _ Other (8) . ---- I -- Organic Chemistry Inorganic Chemistry -- · Pa-rameter Results (mg/I) Parameter Results~mg/kg) Organic Compounds Results(m~/1) I _P&T:GC/MS v' Arsenic L... "'\.?, benzene -- _ Acid:B/N Ext. ✓ Barium )\0 carbon tetrachloride ·• MTBE -- L Cadmium .<C. \ "" chlordane ----I Chloride chlorobenzene ..J:::'.'._ Chromium ·-chloroform --S\ -- --__ Copper o-cresol -- I --Fluoride m-cresol -- --Iron __ p-cresol -- --_\<'._ Lead '"'\ -cresol -- I --__ Manganese 1,4-dichlorobenzeue -- --..JL. Mercury QK 1.5 __ 1,2-dichloroethane Nitrate _._· 1,1-dichloroethylene ---- ~ Selenium L:::::)./:J 2,4-dinitrotoluene I --v Silver L.~o __ heptachlor --Radiochemistry Sulfates hexachlorobenzene ----... ,.,_, Zinc hexachlorobutadiene I Pa rd meter Results (PCi/1) ----_pH hexachloroethane __ Gross Alpha __ Conductivity __ methyl ethyl ketone Gross Beta TDS nitrobenzene ----I TOC __ pentachlorophenol -- --------__ pyridine __ Microbiology --__ tetrachloroethylene I --__ trichloroethylenc Parameter Results (Col/lOOml) __ 2,4,5-trichlorophenol -- --__ 2,4,6-trichlorophenol -- It --__ vir.yl chloride --eridrin --lindanc --Date Received Reportc;d by meth6xychlcr . 1· :.~-~~~·~-;::~~-~~'.;_:·:~~~,:'.·:}:~·~:.:r~:; ·_.. . ,. --... , .. •~:.~(.o.:~~.;:,_:, _:_'"._~;;_ .. ;. • ,::::;,.,," ,, .. .1·= ,_ -"'.""'"'"-.._..;::;·:,,,_.,_ ... , .~/'.:~:~::'fi£~-R~frile:'~ . ··•,· . "· .. .. . '•'." "" .-. ... .. -:.-, .. 'l·,~ ~-·. •"~~-· J..c'.:• ,.::~:.,,.:_ , -•, --·.;. ·-' .. , ~., .. "_'"'" .. ,, ·::-.,,,·.••, ... -.. ~ . Date Extracted Date Reported 2,4-D .. _·_• 2,4,5-TP (Silvex) I . Dale Analyzed Lab Number Dl IS 3191 (Revised 2/91) -- n~ ~ . Cr·,. .... _ • 0 ') 1. • I • N.C. Department of .Environment, I lc:ilth; & Natural Resources ~~id Waste Ma~agcmi:nt·Division SAMPLE ANALYSIS REQUE3T St~tc Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington Street ~lcigh, North Carolina 27~11 • • Sile Number_· ______________ _ Field ·sample Number __ _..9_.D::...i._3.u.... _________ _ _Name of Site SijWn vp./.e, /AAA: 0Wprr¼ Site Location_· _ _.C.e;eofu=,..,k,,=---------------- I Collected By(31@,,/t1o.d, nj12rtv"'-ID# I2jJ:1j(L Date Collected __ : -'q+J.;.,, ;1-/_,_~.=z_,c.,_ ___ Time~l_3_,i/~-o~-- I I I 1- I I I I I I E I ft Agency: _;(_Hazardous Waste Solid Waste __ Superfund -- Sample Type Environmental Concentrate Comments __ Ground water {1) _ Solid (5) va.-s __ Surface water (2) Liquid {6) _ Soil (3) _x_ Sludge (7) Other ( 4) Other (8) Organic Chemistry Inorganic Chemistry Parameter Results(mg/1) Parameter Results (gia,'i) (mrlkg) _P&T:GC/MS ✓ Arsenic .L...:J.'e _ Acid:B/N Ext. --✓--Barium s~-:, MTBE _.l<'...,Cadmium .L.. \ \.i, --Chloride ---- --v Chromium "-\ ") --__ Copper Fluoride ----Iron ------4 Lead ~co --__ Manganese --___'::__ Mercury 0. d-,:l Nitrate --v Selenium L.:J.~ ,/ Silver ""'~Q Radiochemistry Sulfates --..... Zinc --Paramdcr Results (PCi/1) __ pH __ Gross Alpha __ Conductivity Gross Beta TDS ----TOC -- ----. Microbiology ----Parameter Results (Col/lOOml) -- ---- ---- .. _Reported by . . . . . ~ -, -. ' . . .. .. --~ . ' . , :/~~t'c!ret~\>,· ::.: . . " . ,' . .. ,~,:. . ' -. ~ .-,·, . · Date Exl_ractcu · Dale Reporled m Dale Analyzed Lab N"mber . DI IS 3191 (ltc:viscd 2/91) n ~ ,4 A Ar, r C ,-; ; 0? TCLP Compounds ,. Inorganic Compounds Results(mg/1) v' Arsenic L-o-aj ✓Barium Q.3::± vcadmium L.o .06 V Chromium L. C, \0 C V Lead L. c:,_ 50 V Mercury "'-o.o;;L V Selenium 40.0:J _!L Silver L..Q,)O ---- -- -- .O,-;;anlc Compounds Results (mg/1) benzene --carbon tetrachloride --chlordane --chlorobenzene --chloroform --o-cresol --m-cresol --p-cresol cresol __ 1,4-dichlorobenzene __ 1,2-dichloroethane __ 1,1-dichloroethylene 2,4-dinitrotoluene __ · heptachlor hexachlorobenzene --hexachlorobutadiene --hexachloroethane __ methyl ethyl ketone nitrobenzene __ pentachlorophenol __ pyridine __ tetrachlorocthylene __ trichloroethylene __ 2,4,5-trichlorophenol __ 2,4,6-trichlorophenol __ vi~yl chloride cndrin --· lindanc --. . melhoxychlor , .• ,., :tcix;phene:< " . .. .. .. " 2,4-0 . = 2,4,5-TP (Silvex) -- SAMPLE ANALYSIS REQUEST · State Laboratory or Public Health· P.O. Box 28047, 306 N. WilmJngt~ri' Strc·ct' Raleigh, North·Caro1iti8'. ·21611 ~ . . . . . . •• ~ile Number_·_--------------- Name of Site S',~ tfw/-J'e,',UtAf {vterpr,¼ Field Sample Number...;. __ q,_e=Oc..7.._ __________ _ Site Location zuloic I _Collected By Gia.gr /f'1c,_rf, >1. Date Collected R / 31 /'iv I ID# 13 /,f ; Time 1530 -~="---- I Agency: I( Hazardous Wasie Solid Waste __ Superfund TCLP Compounds -- Sample Type Inorganic Compounds Results(mg/1) I Environmental Concentrate Comments Arsenic --Barium pt~0 --Cadmium __ Ground_ water (1) Solid (5) --Chromium I --__ Surface water (2) __x_ Liquid (6) Lead Mercury _Soil (3) _ Sludge (7) --Selenium --I Silver _ Other (4) --Other (8) ---- I --Organic Chemistry Inorganic Chemistry --.. I Parameter Results(mg/1) Parameter Results~)(mg/kg) Organic Compounds Results(mg/1) P&T:GC/MS .1._ Arsenic ""-.\'::> benzene --_ Acid:B/N Ext. ...:t,_ Barium L... I ;;i carbon tetrachloride --MTBE .:L Cadmium .L_ :?:, \ chlordane ----Chloride chlorobenzene ------ --·-....1_ Chromium ..L_ ?:,P, chloroform -- --__ Copper o-cresol --I --Fluoride m-cresol ----Iron p-cresol ------....x_Lead L... ;',8 cresol -- I --__ Manganese --1,4-dichlorobenzene --__;L_ Mercury L... Q • C :) 1,2-dichloroethane --Nitrate __ 1,1-dichloroethylene -- I _:t,_ Selenium "'-\ 5 2,4-dinitrotoluene __L_ Silver .L?,8 __ heptachlor Radiochemistry Sulfates hexachlorobenzene ----······-·· Zinc hexachlorobutadiene I Paramtler ----Results (PCi/1) _pH hexachloroethane --__ Gross Alpha __ Conductivity __ methyl ethyl ketone Gross Beta TDS nitrobenzene --E --TOC __ pentachlorophenol -- --__ pyridine --Microbiology --__ tetrachloroethylene m --__ trichloroethylene Parameter Results (Col/lOOml) __ 2,4,5-trichlorophenol -- ----2,4,6-trichlorophenol --vinyl chloride ----eridrin --lindane :m -..2..aJs.-~c~,s~9 .. ·-· Reported by _. __ · methoxychlor __ .-:;.· '· .-.. -,.-__ :~ toxaphene . . -~ .--<;:•;,. • ' • . ·-. .. .. ------· .. ·----:-. - -Dale ExlractcJ Date Reported _2,4_-D E _ 2,4,5-TP (Silvex) Da!c Analyzed Lab Number DI IS JJ1Jl (Revised 2/91) -- rH,4~-:>c; \r:-P ,1 q? i :-N .. C. Dcpartmc=;~ of Environment, SAMPLE ANALYSIS REQUEST I· .. :.-•·;:J. llcalth, & Natu-ral·Rcsourc_es_ , · . .... -.;·-'~.""'.Soli,d•'?/ast~ t'--f~~a·ge~~~t Divisiqn ; -, _ . . . .. State Laboratory of Public Health P.O.· Box 28047, ~ N. Wilmington Street Raleigh, North C-arolina 27611 I I I I I I I I I I I I I . :-,. •. ; .. Field Sampl·e Nurriber ___ . ..t'7,.,6CL/_'}1----------- .. Site Location __ ·-"~"''1"""bf'""'a ______________ _ Date Collected __ q,_,· /::1:/~7:'.:v'.::::::::::::::-_T_im_e _ _j!:ll __ s__ __ :::_ Agency: ~Hazardous Waste Solid Waste __ Superfund Sample Type Environmental Concentrate Comments . Ground water (1) _. Solid (5) Surface water (2) ,lL Liquid (6) ___________ _ Soil (3) _ Sludge (7) _________ _ Other (4) _ Other (8)-__________ _ Organic Chemistry Inorganic Chemistry Parameter P&T:GC/MS = Acid:B/N Ext. Results(mg/1) Parameter v Arsenic I/ Barium vCadmium --Chloride Results~ (mg/kg) L.\ ~ MTBE dChromium Copper --Fluoride -Iron _k'.'.,Lead __ Manganese v' Mercury --Nitrate ?selenium t---------------1 J Silver Radiochemistry Pardmetcr __ Gross Alpha Gross Beta Results (PCi/1) Microbiology -- Parameler Results (Col/IOOml) Sulfates Zinc pH __ Conductivity TDS TOC ""'-38 TCLP Compounds Inorganic Compounds Arsenic Barium Cadmium Chroinium Lead _ ·_Mercury Selenium Silver Organic Compounds benzene carbon tetrachloride chlordane chlorobenzene chloroform o-cresol m-cresol p-cresol cresol Results(mg/1) ResulL~(mg/1) ------ = 1,4-dichlorobenzene _____ _ 1,2-dichloroethane --1,1-dichloroethylene _____ _ __ 2,4-dinitrotoluene __ heptachlor hexachlorobenzene · hexachlorobutadiene hexachloroethane methyl ethyl ketone nitrobcnzene --pentachlorophenol --pyridine ------ tetrachloroethylene trichloroethylene --2,4,5-trichlorophenol _____ _ __ 2,4,6-trichlorophenol _____ _ ,---------------...... ----------------j vinyl chloride --endrin lindane Dole Rccciv~d Reported by Dote Extracted Date Reported Date Analyzed Lab Number DIIS 319) (l!cvi:;cd 2/91) nt4"-.'1f; ( r .. ': .,rt 4 9? __ methoxychlor __ toxaphene _2,4-_D . -~ 2;4;5-TP (Silvex) I .. I I I I I D I I I L I I State of North Carolina Department o'·'"'rwironment, Health and No,ural Resources Mooresville Regional Office James B. Hunt, Jr., Governor Jonathan B. Howes, Secretary Vivian Burke, Regional Manager CERTIFIED MAIL DIVISION OF ENVIRONMENTA~ MANAGEMENT July 13, 1993 RETURN RECEIPT REQUESTED Mr. Barry Sigmon A.A.A. Enterprises, Incorporated Route 14, Box 350 Statesville, North Carolina 28677 RE: Notice of Violation 15A NCAC 2L Classifications and Water Quality Standards Applicable to the Groundwaters cy Sigmon Septic Tank Service (~i'.t\\i!i~~JM\~AVt,::·;;· Groundwater Incident W 3422 • · · · Iredell County, N.C. Dear Mr. Sigmon: On August 9, 1990 you were issued a Notice of Violation (NOV) from the Division of Environmental Management (DEM) for violation of the North Carolina Groundwater Standards (15A NCAC 2L .0202). In the NOV you were required to determine the vertical and horizontal extent of soil and groundwater contamination and to submit a site assessment report within 60 days of receipt of the NOV. The NOV was held in abeyance pending a review by the Hazardous Waste Section of the Division of Environmental Management. In April of 1993, the Hazardous Waste Section concluded that the site did not fall under its jurisdiction. On May 5, 1993 staff from the Mooresville Regional Office Groundwater Section resampled two of the monitor wells at the subject site and found that groundwater standards violations still exist at the site. Specific violations are as follows: 919 North Main Street. Mooresville, North Ccrolina 28115 Telephone 704-663-1699 FAX 704-663-6040 An Equal Opportunity Affirmative Action Employer sat recycled/ 10% post•consumer paper I .. I I I I I I I , 0 n AAA Enterprises, Inc . July 13, 1993 Page Two Constituent dissolved solids nitrate mercury lead 2-chlorotoluene 1,4-dichlorobenzene benzene 1,3,5-trimethylbenzene n-butylbenzene naphthalene Concentration* 650,000 54,000 29 75 2 6. 1 2.3 1 1. 6 1 . 3 * 2L Standard 500,000 10,000 1 • 1 50 ND 1 • 8 1 . 0 ND ND ND * Concentration in micrograms per liter (parts per billion). ND Not permitted in detectable concentrations. The Groundwater Section staff also sampled two downgradient water supply wells.in February of 1993 and found that both wells contained nitrate levels above the groundwater standards. You are responsible for causing the continuing violation of the underground water quality standards because you have stored and/or disposed of septage waste in unlined lagoons. According to 15A NCAC 2L .0106 (c)(1), you are required to assess the cause, significance and extent of the violation, submit a plan and schedule for eliminating the source and for restoration of the groundwater; and implement an approved plan in accordance with a schedule established by the Director. In establishing a schedule, the Director shall consider any reasonable schedule proposed by the person submitting the plan. To achieve compliance with the above-cited laws or rules, you are required to submit within sixty (60) days from receipt of this letter a site assessment report in accordance with the enclosed guidelines. This data will then be used to submit a corrective action plan which will be due within sixty (60) days after the site assessment report is submitted and approved by this Office. In addition, 15A NCAC 2L .0106(b) states that any person conducting or controlling an activity which results in the discharge of a waste, hazardous substance or oil to the groundwater, or in proximity thereto, shall take immediate action to terminate and control the discharge, mitigate any hazards resulting from exposure to the pollutants and notify the Department of the discharge. To comply with this section of the rules, you must provide an alternate drinking water supply for the residents who use the wells at Route 14, Box 356 and Box 357 (the last two wells on the dirt road behind your facility) within seven days of receipt of this letter. I: .. I I I I I I I , I I I You should be aware, however, that the above violation of 15A NCAC 2L may subject you to a civil penalty assessment under the authority of G.S. 143-215.6a of up to $10,000 per rule violation. each day that the violation continues may be considered a separate violation. Failure to respond within the time specified and to voluntarily achieve compliance may result in a recommendation for enforcement, the issuance of a Special Order against you under the authority of G.S. 143-215.2, or a request to the Attorney General to institute an action for injunctive relief. Your response and/or questions should be directed to Chris DeRoller of the Mooresville Regional Office at (704) 663-1699, ext. 235. Sincerely, ~1.~-lh Brenda J. Smith, P.G. Regional Supervisor cc: Groundwater Section, Raleigh Laurie Martin, Hazardous Waste Section Julian Foscue, Solid Waste Section Rhonda Morgan, Well user Bill Munford, Well user Enclosures: Site Assessment Guidelines Sample Results I It I I I ' . Ref. 21 Memorandum Date: December 12, 1996 To: Pat DeRosa . Head, Site Assessment and Removal Branch From: Douglas Moore 4-~ . Environmental Chemist, Site Assessment and Removal Branch NC Superfund Section Subj.: Removal Evaluation Sigmon Septic Tank Service 1268 Eufola Road Statesville, Iredell County, NC. EPA ID: NCD 062 555 792 Sigmon's Septic T:.nk Service operated a septage removal business located on a 15.35 acre property at 1268 Eufola Road (S.R. 1333), Statesville, Iredell County. The company operated at the site from the late 1970's until September 28, 1995, when both Sigmons Septic Tank Service and its parent company, A.A.A. Enterprises, ceased operations for financial reasons (Figures I, 2). The operation included pick up of septage wastewaters from various industries located around the Statesville area which were transported and deposited in lagoons at the site until Spring 1992. As of September 1992, tell lagoons were present on site; two unlined lagoons were inactive and eight unlined lagoons were active. The estimated total dimensions of all ten lagoons are 225 feet wide by 180 feet long, by 12 feet deep, or 486,000 cubic feet (18,000 cubic yards). Sludges remaining in the lagoons were mixed with sawdust and stockpiled in lagoon #3. A estimated 2,000 tons of sludges are reported at the site. Historic aqueous and sludge samples from the onsite lagoons demonstrate the presence of CERCLA hazardous substances. Elevated levels of aluminum (14,000 ug/1), copper (350 ug/1), iron (11,000 ug/1), mercury (0.8 ug/1), magnesium (3.7 ug/1), manganese (350 ug/1), lead (50 ug/1) and zinc (2,300 ug/1) were detected in an aqueous lagoon sample collected on March 25, 1987 by North Carolina Division of Environmental Management (DEM) On August 31, and September I, 1992, the N.C. Hazardous Waste Section sampled liquid and sludge from the eight active septage lagoons and analysed for volatile organics, semi- volatile organics, total inorganics and toxicity characterisitic leachate procedure (TCLP) inorganics. The aqueous sample results contained elevated levels of bis(2- ethylhexyl)phthalate (360,000 ug/1), diethyl phthalate (11,000 ug/1), phenol (7,000 ug/1), 4-methylphenol (6,000 ug/1), toluene (1,277 ug/1), acetone (1,273 ug/1), 2- methylnaphthalene (1,000 ug/1), chlorobenzene (!48 ug/1), xylene (51 ug/1), benzene (33 ug/1), lead (2.3 _mg/I), chromium (0.19 mg/I), and cadmium (0.021 mg/I). None of the contaminants exceeded the RCRA TCLP levds for 1oxici1v characterisitic . . -. ·•. -. . --. . . ' ' -~ . -. -·. •-· ... , . -. ., •·. .. ., -. .. . ... ~ •• , ,,J--;.· I lie m D 1D 1D I I 1• 1• • , 1• •• -- ' ' .It I Removal Evaluation Memorandum Sigmons Septic Tank Service December 11, 1996. Page 2. The 1992 sludge samples taken by the Hazardous Waste Section from the lagoons co9tained elevated levels of bis(2-ethylhexyl)phthalate (90,000 ug/kg), 4-methylphenol (25,000 ug/kg), toluene (16,533 ug/kg), 2-methylnaphthalene (9,000 ug/kg), dibutyl phthalate (8,000 ug/kg), 1,4-dichlorobenzene (7,000 ug/kg), naphthalene (4,000 ug/kg), chlorobenzene (2,500 ug/kg), xylene (I, 155 ug/kg), 2-methylphenol (1,000 ug/kg), acetone (624 ug/kg), ethylbenzene (288 ug/kg), l ,2-dichlorobenzene (200 ug/kg), methylene chloride (156 ug/kg), 1,3-dichlorobenzene (100 ug/kg), oenzene (70 ug/kg), carbon disulfide (18 ug/kg), lead (200 mg/kg), barium (I 10 mg/kg), chromium (5 I mg/kg) and mercury (0.29 mg/kg). None of the contaminants exceeded RCRA TCLP levels for toxicity characteristic. In early September 1993, Sigmon contracted with Shield Environmental Associates, Inc. (Shield) of Charlotte, NC to sample and characterize ,Judges in the eight active lagoons. The sludge sample results detected elevated concentration~ of toluene ( 45 mg/kg), xylenes (5.8 mg/kg), carbon disulfide (1.1 mg/kg), 1,4-dichlorobenzene (47 mg/kg), ethylbenzene (I.I mg/kg), chlorobenzene (22.8 mg/kg), TPH (diesel range) (2,950 mg/kg), TPH (gasoline range) (81 mg/kg), and total TPH (2,950 mg/kg). None of the contaminants exceeded the RCRA TCLP levels for toxicity characteristic . Despite the low TCLP results, releases to groundwater have been repeatedly detected in onsite monitoring wells. In I 987, four monitoring wells were installed at the li!goons; three downgradient of the lagoons and one upgradient (Figure 2). Groundwater was encountered at 24-34 feet below grade. Groundwater samples collected by the North Carolina Division of Environmental Management (DEM) on September 24, 1987 detected levels of barium (6,600 ug/1), chromium (55 ug/1), iron (87,000 ug/1), manganese (16,000 ug/1), lead (210 ug/1) and mercury (1.2 ug/1) in excess of North Carolina 2L Groundwater Standards. On June 14, 1990, additional groundwater samples collected by the NC Division of Environmental Management (DEM) detected elevated levels of iron (2,300 ug/1), lead (190 ug/1), manganese (430 ug/1) and mercury (6.0 ug/1) in excess of the North Carolina 2L Groundwater Standards. The groundwater sample also detected the presence of 1,1-dichloroethane (1.3 ug/1). On August 3, 1990, a Notice of Viclation letter was issued to Sigmon for violations of the 2L groundwater standards. Sigmons rcsampled two monitoring wells on the site and submitted the results to DEM on March 19, 1991. The sample results detected elevated levels of 1,1-dichloroethane (1.0 ug/1), vinyl chloride (2.0 · ug/1), 1,4-dichlorobenzene (3.0 ug/1), iron (20,000 ug/1) and manganese (17,500 ug/1) in excess of the NC 2L groundwater standards. On May 6, I 993, DEM collected additional groundwater samples from monitoring wells #1 and #2, downgradient of the lagoons. On July 13, 1993, a second Notice of Violation letter was d lie D 1D 11 I E 1• •• •• 1' 1/ •• •• -:' f f ' . ·•'·--· I. - Removal Evaluation Memorandum Sigmons Septic Tank Service December I I, I 996. . - Page 3. issued to Sigmon for releases of 2-chlorotoluene (2.0 ug/1), benzene (2.3 ug/1), nitrates · (54,000 ug/1), dissolved solids (650,000 ug/1), 1,4-dichlorobenzene (6.1 ug/1), 1,3,5- trimethylbenzene (1.0 ug/1), n-butylbenzene (1.6 ug/1), mercury (29 ug/1) and lead (75 ug/1) in excess of the State 2L groundwater standards. The sample results also detected elevated levels of I, 1-dichloroethane ( 1.6 ug/1), cis-1,2-dichloroethane (2.3 ug/1), trichloroethane (0.25 ug/1), chlorobenzene (5.5 ug/1), 1,3-dichlorobenzene (0.38 ug/1), barium (710 ug/1), and m.p-xylenes (2.1 ug/1) in the onsite monitoring wells. Historic groundwater sample results from two nearby drinking water wells (Allen Cascadden residence and Florence Russell residence) demonstrate that offsite drinking water wells have also been affected by releases from the site. The wells are located southwes_t of the site as depicted in Figure 3. A summary of the groundwater sample results is presented below in Tables 1 and 2 . Sam le Date 2-22-93 3-I 5-94 10-1-94 3-6-95 10-10-95 10-96 NC 2L Std EPAMCL Table I. Rhonda Morgan/Florence Russell/Rachel Brown Well Historic Sample Data Nitrates (ug/1) 1.1-DCA (ug/1) cis-1.2-DCE (ug/1) TCE (ug/i) 11 8.2 0.59 7.2 0.65 D D 9.4 0.72 0.43 0.27 8.6 0.65 0.67 D NA NA NA NA 10.0 700.0 70.0 2.8 10.0 none issued 70.0 5.0 1,4-DCB (ug/1) 0.53 0.72 0.87 0.74 NA NA 75.0 Shading indicates a concentration exceeding NC 2L GW standards or EPA MCL drinking water standards. NA:::: sample results not available at time of report. I .. 1• I I I I I ..) ~ <;._ I~ ,. •• --,, ' ' ~ I Removal Evaluation Memorandum Sigmons Septic Tank Service December I _I, I 996. Page 4. Table 2. Allen Cascadden (or Munford)/Mike James Well. Historic Sample Data Samnlc Date 1,1-DCA (uc/ll cis-1.2-DCE (ue/1) TCE (ue/1) PCE (ul!ll) I ,4-DCB (ue/1) 1,2-DCB (ue/1) 1/23/91 D D 0.35 0.29 ---- 11/13/91 0.57 D 0.89 0.53 · 1.5 0.3 -- 10/01/92 ----D D ---- 03/06/95 1.5 3.5 D ------ 09/20/96 1.2 3.4 ----D -- NC 2L Std. 700 70.0 2.8 0.7 none issued none issued EPAMCL none issued 70.0 5.0 5.0 75.0 600.0 Samnle Date m,o-Xvlene (ul!/1) o-Xvlene (ue/1) Mn (ue/1) He (ue/1) Nitrates (me/I) 1/23/91 ---------- 11/13/91 5.1 1.3 11m11,ro--j;3--- 10/01/92 -----®-B!IW7f.Oll!li -23!{f511!W 03/06/95 ------!El'ii!if R !!ii-J® ,ITTAtlf¼l .l wt . ... 09/20/96 --. -----1~3-!IElif:~-. ~-- NC 2L Std. 530.0 530.0 50.0 I. I 10.0 EPAMCL 10,000 10,000 none issued 2.0 10.0 Shading indicates a concentration exceeding NC 2L GW standards or EPA MCL drinking water standards. --= not analysed, or not detected. D -detected below the sample quantitation limit. Both offsite drinking water wells have exhibited levels of manganese, mercury and nitrates in excess of the State 2L Groundwater and/or EPA's Maximum Contaminant Level Drinking Water standards. As a result, the State of North Carolina Environmental Epidemiology department has recommended that the occupants discontinue use of the water from these wells for drinking or cooking purposes. Both wells are located at rental properties. In September 1994, the Sigmons ceased supplying bottled water to the Rhonda Morgan trailer per Ms. Russell's request. Since that time, Ms. Russell has vacated the trailer and a new tenant, Rachel Brown, is occupying the residence. According to DEM, Mrs. Brown, who is nearly 9 months pregnant, has been a resident of the Rhonda Morgan property for at least 6 months. Mr. Allen Cascadden has also recently vacated the rental trailer and the residence is currently occupied by Mr. Mike James. According to DEM, neither the State of North Carolina nor the Sigmons are currently supplying bottled water to either of the two residences. DEM has notified both residents of the previous recommendation regarding use of their wells. I .. I I 11 11 11 11 1D ., 11 -- ' ' ' la I Removal Evaluation Memorandum Sigmons Septic Tank Service December 11, 1996. Page 5. A groundwater sample collected from a third offsite well at Mr. C:hris Davidson's property, also demonstrated elevated concentrations of iron (4,430 ug/1) and manganese (830 ug/1) above the North Carolina 2L groundwater standards. The Davidson well is reportedly not used for drinking water (Figure 3). I contacted Mrs. Rhonda Bost, West Iredell Water Corporation (704) 873 .. 1658, who indicated that there are no public water supply lines available in the vicinity of the site. She stated that the closest public water supply lines are located approximately 5 miles from the site near Interstate 70. Sludges and lagoons present an actual or potential exposure threat to nearby human , . populations, animals or the food chain from CERCLA hazardous substances. Bis(2- ethylhexyl)phthalate was detected in sludge samples at a concentration exccedir,g the current EPA Superfund Chemical Data Matrix (SCDM) human health-based soil screening benchmark of 46 mg/kg. According to DEM, several of the nearby residents have small children. The lagoons are currently empty and covered with vegetation. No covers or caps are present on the sludges or lagoons to prevent contact with the conte!lts. A three strand barbed wire and electric fence reportedly surrounds the lagoon property, restricting access by neighboring livestock which have repeatedly broken through the site fence to eat the grass. There is a small pond located along the overland drainage pathway within 1000 feet west of the site containing food chain species that may be taken for human consumption (Figure 3). Considering the potential human contact threat, potential food chain threat and the actual contamination of drinking water supplies by hazardous substances attributable to the site, I recommend that the site be referred to the EPA Emergency Response and Removal Branch for evaluation. If you have any questions, please contact myself at ext. 315. Contacts for the site: Henry H. Sigmon, Jr. (704) 592-2176 (owner and fonm:r operator) Paul Dahlen, (704) 663-1699 (DEM-Groundwater Section). (w/attachmcnts) cc: Doug Moore File --~---------!-- I --___ Q Q -:-----i----._,.-,..Jf'ivl~ I .. ·-i· -- 1 ---·i- i I I I I '-····-··-· I I -.!-. .. ?r,o*. !I . ,1 ·---1-- ··----·--\---, -~ \" ... November 3, 1993 Ms. Chris DeRoller, Hydrogeologist State of North Carolina Department of Environment, Health, and Natural Resources Division of Environmental Management Groundwater Section 9 I 9 North Main Street Mooresville, North Carolina 28115 Reference: Septic Pit Lagoon Sludge Sampling Report Sigmon Septic Tank Service, Inc. A.A.A. Enterprises, Inc. Eufola Road Site Iredell County, North Carolina Groundwater Incident Number 3422 Shield Job Number 930133 Dear Ms. DeRoller: Ref. 22 -E"NVIRN.c. DEPT. OF ONMENT I & NAruru,L R' IEALTH -ESOURCEs' NOVO 5 199.3 During early September 1993, Si(;,.non Septic Tank Service, Inc. (Sigmon) contracted Shield Environmental Associates, Inc. (Shield) of Charlotte, North Carolina to sample and characterize the sludges in eight septic pit lagoons at the above referenced site (see Figures 1 and 2 for site location map and site plan). On September 9, 1993, Mr. Steven M. Burrows of Shield contacted you by telephone regarding the required sludge sa.,,pling parameters. You requested that samples be collected from the sludge present in the bottom of each lagoon. You also indicated that sludge samples should be analyzed for total petroleum hydrocarbon (TPH) compounds, volatile organic compounds (VOCs) and Resource Conservation and Recovery Act (RCRA) metals according to the Toxicity Characteristic Leachate Procedure (TCLP). You indicated that two or three samples of sludge should be collected from each of the lagoons and that TPH and VOCs should be run on each of these samples. You also indicated that one sample should be composited for analysis of TCLP RCRA metals per lagoon. In a letter dated August 26, 1993, the Division of Environmental Management (DEM), Mooresville Regional Office (MRO), Groundwater Section requested that Sigmon close the sepJic lagoons at the site by October 31, 1993 . .,, The following report documents the septic sludge sample results and Shield's recommendations regarding proposed corrective action measures and recommended lagoon closure activities. -, ,, I I .I ,, i •· Septic Pit Lagoon Sludge Sampling Report Sigmon Septic Tanlc Service, Inc. Page 2 Iredell County, North Carolina lie . . n Field Activities D D E On September 21, 1993, an environmental technician and a geologist from Shield mobilized to the Sigmon site. Prior to beginning sampling activities, the environmental technician numbered each septic pit (see Figure 2). Shield personnel then collected sludge samples from the bottom of each septic pit (see Figure 3 for sludge sample locations). Three samples each were collected from lagoons#! through #6; two sludge samples were collected from lagoon #7; and, one sample was collected from lagoon #8. The collection of a second sample from lagoon #8 was not possible due to pit access problems and the small amount of sludge present in the lagoon bottom. Sludge samples were collected using a clean 15-foot long section of PVC pipe. The PVC pipe I was driven into the septic pit bottom until refusal. Strips of duct tape were then placed over the open end of the PVC pipe and the pipe was withdrawn from the pit. The pipe was then placed on a clean flat surface and the duct tape was removed. A clean PVC ram was inserted into the I sample pipe and a sludge core was slowly extruded. The bottom 18-inches of the core was collected and three sample aliquots were prepared. Two of the aliquots were placed in laboratory I supplied glassware for TPH and VOC analysis. The remaining sludge sample aliquot was placed in a new plastic mixing bowl. After all sample aliquots had been collected from an individual septic pit, a single composite sample was prepared by thoroughly mixing the contents of the bowl. I I I I I This composite sludge sample was then placed in laboratory supplied glassware for metals analysis. Each sludge sample was labeled with sample number, depth, time, d2'.~, analysis to be performed and sampler's name. Sample bottles were placed in an ice-filled cooler, chilled to approximately 4° C and delivered to the analytical laboratory using EPA chain-of-custody procedures. At the laboratory sludge samples were prepared for TPH analysis by gas chromatograph according to SW-846 Extraction Methods 3550 and 5030. Sludge samples were also analyzed for VOCs according to SW-846 Method 8240 and for RCRP 'Iletals according to the TCLP. Sludge Sample Laboratory Analytical Results Septic pit sludge sample results for TCLP RCRA metals are summarized in Table I (see Appendix A for laboratory documentation). The sludge samples exhibited arsenic, barium, cadmium, chromium, and lead; however, no sample result exceeded the TCLP regulatory limit. I Septic pit sludge sample results for VOCs are summarized in Table 2 (see Appendix A for laboratory documentation). Sludges from lagoons # I through #7 exhibited various VOCs, L including toluene (0.09 mg/L to 45 mg/kg); ethylbenzene (below detection limit to 1.1 mg/kg)-;- • xylenes (below detection limit to 5.8 mg/kg), carbon disulfide (0.006 mg/Land 1.1 mg/kg), 1,4- dichlorobenzene (below detection limit to 75 mg/kg), and chlorobenzene (below detection limit to I 22.8 mg/kg). Toluene, xylenes and 1,4-dichlorobenzene were the most common VOCs detected in the sludge samples. I \ i ! i i • j j . ·. Septic Pit Lagoon Sludge Sampling Report m Sigmon Septic Tank Service, Inc. Iredell County, North Carolina lie Page 3 n Septic pit sludge sample results for TPH compounds are summarized in Table 3 (see Appendix A for laboratory documentation). Sludge samples from lagoons #I through #7 exhibited diesel range TPH compounds. Diesel range TPH compounds ranged frcim 2.07 (sample IB-8, lagoon D #1) to 2,950 mg/kg (sample 3A-4, lagoon #3). Gasoline range TPH compounds were detected in lagoons #3 through #5. Gasoline range TPH compounds ranged from 24 (sample 3B-5, lagoon #3) to 8 I mg/kg (sample 4B-8, lagoon #4). Total TPH compounds are plotted versus sample o location on Figure 4. E Site Sensitivity Evaluation 11 Shield has prepared a Site Sensitivity Evaluation (SSE) for the site (see Appendix B). The DEM, I) Groundwater Section guidance manual indicates that: "The purpose of the SSE is to evaluate the sensitivity of groundwater to contamination by release of petroleum related substances from the I unsaturated zone" (Groundwater Section Guidelines For The Investigation and Remediation of Soils and Groundwater, State of North Carolina, DEM publication, March 1993). Generally, the SSE has been applied to soil cleanups at petroleum underground storage tank sites; however, the • SSE can be applied to the sludges at the Sigmon site based on the need to determine the "sensitivity of groundwater to contamination by the release of petroleum related substances from 4 unsaturated zone." Shield has prepared the SSE to determine the sensitivity of groundwater r contamination by the release of petroleum related substances from sludge that resides in the unsaturated soil at the site. The following paragraphs document the results of the SSE .preparation. Soil Grain Size Characteristic lrhe soil grain size characteristic was given a rating score of I 0. This score is based on the DEM soil bore logs for monitoring wells MW-2 through MW-4 (see Appendix C). The soil bore logs ■ndicate that soil encountered during drilling was red and tan clay at monitoring well locations ll-fw-2 and MW-3. However, sandy clay, silty clay and silty sand was encountered durmg the drilling of monitoring well MW-4. A rating score of IO was assigned to the grain size llharacteristic based on the various soil grain sizes encountered and fact that clay alone was ~ncountered in two of the three monitoring well borings. telict Stroctures Characteristic lfelict structures were encountered during the drilling of monitoring well MW-4. Based on the !l}EM bore logs, relict structures intersect the groundwater table at monitoring well location MW-4. A relict structure rating score of 10 was assigned to this characteristic based on the MW-4 soil ~re log. ? ~epest Contaminated Sludge Versus Depth to Groundwater Characteristic lhe septic pits at the Sigmon site were excavated to a depth of 8 to 12 feet below grade. I !I ' 110. Ci .. e II> I It I _I .,,.r ... , •. · · Septic Pit Lagoon Sludge Sampling Report Sigmon Septic Tanlc Service, Inc. Iredell County, North Carolina Page 4 Therefore, 12 feet below grade is the deepest sludge burial depth. On September 23, 1993, Shield collected depth to water level readings at monitoring wells MW-2 through MW-4. Water levels ranged from approximately 27.5 to 34.2 feet below the top of the well casing. The top of the well casings are approximately 2.5 feet above the ground surface. The shallowest groundwater measured occurs at a depth of approximately 25 feet below grade. Therefore, the distance between the deepest known sludges and the level of shallow groundwater is approximately 12 feet. A rating score of 10 points was assigned to the distance between groundwater and the sludges. Top of Bedrock Characteristic The DEM bore logs for monitoring wells MW-2 through MW-4 indicate that bedrock was not encountered during drilling. This indicates that the level of groundwater is above the level of bedrock at the site. A rating score of zero points was assigned to this characteristic. Artificial Conduits Characteristic The Sigmon septic pits are located south ofEufola Road in a grassy field. This area was formerly rural farmland before the septic pits were installed. No public sewer or public water lines are present in the area. Based on Shield's conversations with Sigmon personnel, no subsurface uti'.ities or artificial conduits are present in the subsurafce below the septic pits. Given this information, Shield has assigned a value of zero to the artificial conduits characteristic. Total Site Score A total site score of30 was calculated on Table 1 of the SSE (see Appendix B). Site Category The Sigmon site meets the criteria for assignment as a Category A site (see Table 3 of Appendix B). This indicates that water supply wells in the area are affected (with nitrate only) and that the area is not served by public water supplies. Initial Cleanup Level Table 2 of the SSE indicates that a Category A site with a total site characteristic score of 30 will have an initial cleanup level of 100 ppm for gasoline range TPH compounds and 400 ppm for diesel range TPH compounds. Final Cleanup Level Table 2 of the SSE indicates that the initial cleanup levels are equal to the final cleanup level. Therefore, the final cleanup level for gasoline range TPH compounds is 100 ppm and for diesel range TPH compounds the final cleanup level is 400 ppm. Septic Pit Lagoon Sludge Sampling Report Sigmon Septic Tanlc Service, Inc. Iredell County, North Carolina Recommendations for Lagoon Closure Page 5 Based on a meeting between Shield and Sigmon on October 18, 1993, Sigmon personnel are prepared to properly close the lagoons as soon as possible. However, closing all lagoons by October 31, 1993 is not possible because some of the sludges are affected with elevated levels of TPH compounds and volatiles. Shield recommends remediating these affected sludges prior to permanent lagoon closure. The following paragraphs suggest a plan for lagoon closure at the site. Lagoons #1 and #8 -Sludge Characterization and Recommendation for Oosure Sludge samples obtained from lagoon# 1 exhibit low levels of TPH compounds, VOCs and RCRA metals. The sludge sample obtained from lagoon #8 exhibited no TPH compounds or VOCs, and low levels RCRA metals. These sludge samples do not exceed the North Carolina Soil Cleanup Level for diesel (40 ppm) and gasoline (10 ppm) range TPH compounds. Also, toluene and carbon disulfide concentrations in the sludge samples do not exceed the U.S. Environmental Protection Agency (USEP A) RCRA surface impoundment clean closure target concentrations (see Table 2 for summary of USEPA target concentrations) (Surface lmpoundment Clean Closure Guidance Manual, USEP A, October 12, 1987). Metals concentrations in these sludge samples are also well below the TCLP regulatory limit. Based on the sludge sample results, Shield recommends closing lagoons #1 and #8 by adding lime to the sludges and capping the area with soil backfill. This technique of septic lagoon closure has been recommended by the North Carolina Division of Solid Waste Management (DSWM), Septics Management Branch (see Appendix D for guidance letter to Sigmon from the DSWM). Lagoons #4 and #7 and Southern Two-Thirds of Lagoon #3 -Sludge Characterization and Recommendation for Oosure Sludge samples obtained from lagoons #3, #4 and #7 exhibit moderate levels of TPH compounds, VOCs and low levels of RCRA metals. These sludge samples exceed the North Carolina Soil Cleanup Level for diesel (40 parts per million (ppm)) or gasoline (IO ppm) range TPH compounds. However, the sludge sample results for lagoons #4 and #7 indicate TPH concentrations that are less than the final SSE cleanup level for TPH compounds. Sludge sample results for lagoon #3 indicate that two of the three lagoon sludge samples exhibited TPH concentrations that are less than the final SSE cleanup level for TPH compounds. In addition, VOCs detected in the sludges are well below the USEP A RCRA surface impoundment clean closure target concentrations (see Table 2 for summary ofUSEPA target concentrations) and no metals exceed the TCLP regulatory limit. Based on the sludge sample results, lagoons #4 and #7, and the southern two-thirds of lagoon #3 -- contain septic waste with moderate amounts of TPH and VOCs and minor amounts of RCRA metals. The moderate levels of TPH compounds detected in the lagoon sludges are below the final SSE cleanup level. Based on the sludge sample results and the SSE,· Shield recommends closing lagoons #4 and #7, and the southern two-thirds of lagoon #3 by adding lime to the sludges ' 1., 11 Septic Pit Lagoon Sludge Sampling Report Sigmon Septic Tanlc Service, Inc. Iredell County, North Carolina and capping the area with soil backfill. Page 6 Lagoons #2, #5 and #6, and Northern One-Third of Lagoon #3 -Recommended Remediation Sludge sample results indicate that lagoons #2, #5 and #6, and the northern one-third of lagoon #3 exhibit TPH compounds above the SSE cleanup level for diesel range TPH. Shield recommends remediating the sludges in these lagoons to a TPH concentration below the SSE level for diesel range TPH. Shield recommends that Sigmon bioremediate the sludges at the site. Shield recommends the following plan for closure/remediation of the septic pit lagoons: • Immediately begin closure activities at lagoons#!, #4, #7, #8, and ihe southern two-thirds of lagoon #3. These lagoons will be closed by liming the sludges and capping the area with soil backfill. The septic pits will be closed but not completely filled with soil backfill. A depression will therefore be left at the former pit locations. These depressions can then be used to help remediate the sludges from the other pits. • Use the space created by the lagoon closures to remediate the· sludges from lagoons #2, #5, #6, and the northern one-third of lagoon #3. The depressions left in the ground by the lagoon closures will be lined with polyethylene sheeti,3. The polyethylene sheeting will act as an impermeable barrier to further migration of sludge constituents into the subsurface. After lining the depressions, a layer of sand and perforated PVC pipe will be installed in the depressions. The piping will then be covered with coarse sand or fine gravel. Sludges tl:..c need treatment will then be mixed with sand, soil and mulch. Mixing will provide air pathways and absorb excess. sludge moisture. After the sludge is sufficiently mixed, it will be placed in the lined depressions, on top of the pipe and sand layer. Sludges will be added to the lined depressions up to the approximate level of the grade. Sand and perforated PVC pipe will then be installed above the mixed sludge layer. The depressions will then be capped with polyethylene sheeting and soil backfill over the sludgP ••eatment unit. • Shield proposes to use a rotary blower to sparge air into affected sludges through the perforated PVC piping underlying the sludge layer. We propose to use a rotary blower to create a vacuum within the perforated PVC piping overlying the sludge layer. This method of remediating the sludges will allow the sludge layer to be aerated. In addition, any volatiles or off-gases will be vacuumed off and discharged to the air. The aerated environment within the sludge layer will activate the aerobic bacteria and increase biologic activity. Once sufficient numbers of aerobic bacteria are present, the bacteria will start to feed on the petroleum compounds that are present in the sludges. Eventually the level of petroleum hydrocarbons within the sludges will be reduced to an acceptable level. A cross section of the proposed sludge aefation unit is illustrated in Figure 5. • After mixing the sludge but before beginning aeration, Shield will collect samples of the mixed sludge to send to the laboratory for TPH analysis. This will provide Sigmon and the DEM with data regarding the mixed-sludge TPH levels prior to the start of ID lilt ID ID 10 ID I D I~ I I ,, I I r m 11 11 11 1i 1 la 11 . Septic Pit Lagoon Sludge Sampling Report Sigmon Septic Tank Service, Inc. Iredell County, North Carolina remediation. Page 7 • Shield proposes to collect sludge samples at 6-month intervals to gauge the effectiveness of the aeration technique. Shield and Sigmon believe that this sludge aeration plan can be earned out successfully and that the TPH compounds in the sludges can be reduced to acceptable levels. Shield and Sigmon believe this technique is advantageous for the following reasons. • The implementation and start-up costs for this type of remediation are reasonably low and affordable to Sigmon. • The maintenance and operating costs for this type of remediation are reasonably low and affordable to Sigmon. • The remediation plan can be quickly implemented. • The affected sludges will remain on-site and no transportation costs will be incurred to transport the sludge off-site for land application or disposal. • The polyethylene sheeting under the sludge aeration unit will inhibit migration of slu0ge constituents into the subsurface. • Groundwater downgradient of the aeration treatment unit can be monitored using the existing monitoring wells at the site. • Bioremediation ofTPH compounds is a proven and accepted technology. Shield and Sigmon request that the DEM, :lv!RO, Groundwater Section reply to this report and the proposed corrective action measures. .,:gmon and Shield are prepared to begin lagoon closure and sludge remediation immediately, based on your acceptance of this report. If you have any comments or questions regarding this report, please contact me at (800) 395-5220. Sincerely, SHIELD ENVIRONMENTAL ASSOCIATES, INC. Steven M. Burrows, P.G. #! 184 Project Manager John Brown, P.G. Chief Operating Officer .lw.wAMA&df+Gl'ifs;;------. ·--. . --. t&t#f_,.WWWW<Ji U!1 .I &f ~ I ,... ------·-- -·-------.-I!!!!!!!! l!!!!!!I I!!!!!! i== i== 2 5-10 0.01 I 1.114 0.024 <0.005 0.235 <0.0002 <0.007 <0.010 3 4-5 <0.007 0.614 0.015 <0.005 0.031 <0.0002 <0.007 <0.010 4 3-4 0.014 0.875 0.012 <0.005 0.045 <0.0002 <0.007 <0.010 5 5-8 0.015 0.698 0.012 <0.005 0.156 <0.0002 <0.007 <0.010 6 5-<S <0.007 1.569 0.029 <0.005 0.208 <0.0002 <0.007 <0.010 7 8 <0.007 1.248 0.040 <0.005 0.071 <0.0002 <0.007 <0.010 8 3 <0.007 0.794 0.019 <0.005 0.017 <0.0002 <0.007 <0.005 none 5.0 100.0 1.0 5.0 5.0 0.2 1.0 5.0 (}) \ All samples collected September 21, 1993. (2) · Depth range below sludge surface for the composited sample. Analyticiil laboratory: Hydrologic, Inc., Frankfort, Kentucky --.. ---- - - -,.----!!!!!I I!!!! l!!!!!!I 8 0.11<3> BDL BDL BDL BDL BDL 0.11<3) 8 0.09(3) BDL 0.006(3) BDL BDL BDL 0.096(3) 2 5 8.0 1.4 BDL. l.l BDl BDL 10.5 2 8 15.0 1.6 l.l 15.0 BDL BDL 32.7 2 10 23 2.8 BDL 4.8 0.6 BDL 31.2 3 4 20 1.5 BDL 2.9 BDL 1.3 25.7 3 5 1.9 2.7 BDL 2.4 0.5 3.5 11 3 5 2.0 5.7 BDL 10.9 l.l 1.6 21.3 4 3 3.8 5.8 BDL 47.0 BDL 18.0 74.6 4 4 7.8 2.4 BDL 14.8 BDL BDL 25 4 4 8 BDL BDL 15 BDL BDL 23 5 5 2.2 BDL BDL 9.8 BDL BDL 12 5 8 2.6 1.4 BDL. 75 BDL 10.4 89.4 5 6 2.8 1.4 BDL 33.7 BDL 22.8 60.7 6 6 12.5 BDL BDL 10 BDL BDL 22.5 6 6 9 BDL BDL 5.5 BDL BDL 14.5 6 5 45 4.5 BDL 7.5 BDL BDL 57 7 8 7 BDL BDL BDL BDL BDL 7 7 8 1.8 BDL BDL 1.4 BDL 1.0 4.2 8 3 BDL BDL BDL BDL BDL BDL BDL none none 400 not 100 100<6) not specified 40 none specified (/} All samples collected September 21, 1993. (2) &epth below sludge surface. (3) Sample exhibited very low solids content and was analyzed as a liquid. Sample result units are mgll. (I) Below Detection limit (5) Surface J111pound111ent Clean Closure Guidance Manual (USEPA, October 12, 1987) (6) Concentration cited is for 1,2-dichlorobenzene. Concentration/or 1,-1-dichlorobenzene was no/ specifif!d. ___ .·lnoltlt<~al l.nh~>ry: ..!.!J;;Jro!agi<:_ fJ!_c., Frnnl-.:(ort, ~icky ID=WI ~ ,_ __,,_ ....,., - D D I I , I I I I I I I, I I :·.<..\ .. : .. ; .. •.-:-·_·:·.-.. :•:·::-;. ': .··. >: :· • '•·IA,8:. ?·>• ?·) : .. •, 1 B'-Si.i'.C??,? ·. : .• •.:·1ccs:·••>• · 2A'5•>•·.: · 2 L ? ·2Bcs• :..::? 2 ·.-·,;, •· 2c:io •····· 2 .· 3A4 •.::ii:. 3 ··3B,s•.:•.i< 3 .. .. :Jes ,:.:< 3 4A,3.:• ·< 4 I••·•.·. :'4B~8:':: ;:::.=,: 4 4G4(.: 4 .. sA,s:.·<•:i 5 sB,8.••·•· 5 · SC.,6 ·•··(:: 5 •·• ·6A'6>.:• 6 • ·'····6B'.:6?•· ·••· 6 ? .• 6c:5. 6 ·1Ac8:·. \: 7 7B'8 ··• .:.:: 7 .. #SCJ :· . .: 8 ... · ijj~ij~i~1f ~~b~i~,;j < Total.l'efroleumHydrocarboni(:orii'pounds sw"8iii; •. Jifu,;~iitn Mei:iiilcif:i5so & soJ<h :f'.il!.~.i~l~f1~f;~t~~1~f: ; ;r .:.:••Grouiidwatei'•IiidderitNwnber.3422(: ,•·••••(\siii.;,a;N,;;;;l)ef9301:i:\•···•··'•' ):.,,.,., .. ,., ......... . 8 6.42(3) BDU4l 8 2.07Pl BDL 8 7.06(3) BDL 5 1,080 BDL 8 552 BDL IO 1,410 BDL 4 2,950 BDL 5 129 24 5 113 35 3 262 59 8 209 81 4 221 BDL 5 1,000 BDL 8 565 BDL 6 600 27 6 1,950 BDL 6 555 BDL 5 439 BDL 8 206 BDL 8 348 BDL 3 BDL BDL (I) All samples collected September 21, 1993. (2) Depth below sludge.surface. (3) Sample exhibited very low solids content and was analyzed as a liquid Sample result units are mgll. (4) Below Detection limit Analytical laboratory: Hydrologic, Inc. Frankfort, Kentucky 6.42(3) 2.07(3) 7.06(3) 1,080 552 1.4 IO 2,950 153 148 321 290 221 1,000 565 627 1,950 555 439 206 348 BDL l I 11 I I 1. I I I I I ; I I I ll i II i • I i I .. a - KILOMETERS I 0 I 2 l · ( $ 11 7 11 I 10 MILES I 0 Scale 1:150,000 f lnc_h represents 2.◄ mlles SITE LOCATION MAP SIGMON SEPTIC TANK SERVICE, INC. !REDELL COUNTY, NORTH CAROLINA DATE : 11-02-93 DRAWN BY : RM SCALE : AS SI !OWN FIGURE : l S 1-1 f ELD -ENVIRONMENTAL ASSOCIATES, )NC 0 ,j 0 I () 1 ~ ,l ,, ,.; •.:! 1 ·, j , i ' p ~ • .. "' Ill. ' o· "'-IP LCM , -,----Property Lloea.,_.•L-C:-= ~(>>---'-'-"··=-c-=·=-'--=·-·=-cc-=~~<-~===--=·=,.'? r-"-· ... ;.. Scale: I "=65' ...... ·. Site Plan Figure 2 Sigmon Septic Tank Service, foe. Iredell County, North Carolina ' S 1-[ I .E J_,D ENVIROIIMENTAL ASSOCIATES. INC. 0 0 0 " 0 • '=-IP C<'..H -~~---=.-=-::.-=--=-=-=-Property Line=-=~•~~ <t> · -------- ....;..,_ ,. /. (1> . --------·--.:---:. " "'' "e, Legend • -Sludge Sample Location Scale: 1 "=65' Sludge Sample Location Map Figure 3 Sigmon Septic Tank Service, Inc._ Iredell Count North Carolina · s I-I I E I-1 D ENVIROHMEIITAL ASSOCIATES. I/IC. - ' 0 0 J Y x1puaddtt --~ I!!!!!!! \ \' V if Legend • (6.34) Sludge Sample Location Sludge Sample TPH Result (6.34) -m1il<c (6.◄2( -m1/L Scale: I "=65' : Sludge Sample TPH Map; __ , Figure '4 Sigmon Septic Tank Service, Inc. Iredell Count North Carolina ' s I-I I E I...J D ENY/ROIIMEIITAL ASSOCIATES. INC. .. - -- VACCUUM EXTRACTION PVC PIPE . , ..... STORMlt'ATER CONDUIT PIPING SOIL COVER MIXED :JLUDGE (SLUDGE, SOI!. & MULCH) .. \-----------POLYETHYLENE UNER-----------1 SAND l.AYER ... 0 SOIL COVER CLOSED LA.GOON SLUDGE SPARGING PVC PIPING .. SLUDGE DIOREMEDIATION CROSS SECTION SIGMON SEPTIC TANK SERVICE, INC. !REDELL COUNTY NORTH CAROLINA DATE : 11-02-93 DRAWN BY : RM SCALE : !" = 5' FIGURE : 5 s I--I IE L D ENVIRONMENTAL ASSOCIATES INC. I I I I I I I f I I I I I I It I I Ref. 23 !< ,--:-: ~: di. di. di. €11teepeueJ, 911c. El..;-,;~;---.·:;. ENVIRONMENTAL SERVICES Route 14, Box 350 • Statesville, North Carolina 28677 (704) 87~954 • Fax (704) 528-4911 April 26, 1995 State of North Carolina Department of Environmental, Health and Natural Resources Ms. Karen Walker 919 North Main Street Mooresville, NC 28115 Dear Ms. Walker: Re: Lagoon Closure Activities GW Incident# 3422 L'. ·. In accordance with OEM's Notice of Regulatory Requirments for 15A NCAC 2L .0106 (F)(3) and (4), which requi~ed that primary and secondary pollution sources be removed, treated or controlled prior to or concurrent with assessment activities. Seven (7) of the eight (8) lagoons located at 1268 Eufola have been perma tley and properly closed. Lagoon# 1 used as a storage receptalbe for run off in the initlal plan submitted by Shield Environmental Services will be closed permantley by the 1st week of May. The total area will be sowed in grass to stablized the ground in the affected area. The seven (7) lagoons were closed by April 3rd 1995 per the extension issued by your office. Thank you for your corporation concerning the lagoon closures. If you have any questions regarding this letter or the site please feel free to contact me at 704-873-8954. Sincerely, ~;J~ Barry D. Sigmon Vice-President BDS/mls •• I I I I I I , I I I I I I I, I I Ref 24 State of North Carolina RECEIVED Department of Environment, Health and Natural Resources DEC 1 8 1995 Mooresville Regional Office SUPERFUND SECTION AVA James B. Hunt, Jr,, Governor Jonathan B. Howes, Secretary DEHNR MEMORANDUM To: From: Pat DeRosa DIVISION OF ENVIRONMENTAL MANAGEMENT December 15, 1995 Division of Solid Waste Management Superfund Section Karen Connell, Hydrogeologist KC,, Division of Environmental Management Groundwater Section Subject: Sigmon's Septic Tank Service Groundwater Incident #3422 Iredell County, N.C. This memo is in response to recent telephone conversations I have had with you regarding the subject site. I originally contacted Jeanette Stanley to determine if the sludge at the site would qualify for "emergency removal." A.A.A Enterprises (Sigmons's) agreed to hire a soil scientist to determine if the sludge and the site were suitable for land application. Based on telephone conversations with their soil scientist, the nitrogen levels in the soil are such that approximately 90 acres of land will be required to land apply the estimated 2,000 tons of sludge. The site is situated on 4 acres. Please be aware that this Office has not made a request for emergency removal of the contaminated sludge, only a request for the options available. A Final Notice will be sent to Sigmons's requiring that a plan for removing the sludge be submitted to this Office. If the sludge is not removed or the schedule proposed is unacceptable, DEM will formally request emergency removal of the sludge. DEM plans to continue to work with Sigmon's toward the completion of the site assessment activities. Brief Site Description: Sigmon's Septic Tank Service operated ten lagoons at the site located on Eufula Road (S.R. 1133), Statesville in Iredell County since approximately the late 1970 1 s. As of September 1990, a total of ten lagoons were present on-site; two were inactive and eight unlined lagoons were active. During an n 919 North Main Street, Mooresville, North Carolina 28115 Telephone 704-663-1699 FAX 704-663-6040 An Equal Opportunity Affirmative Action Employer 50% recycled/ 10% post-consumer paper I I I I I I I I , I I I I I I L I [I MEMORANDUM Pat DeRosa December 15, 1995 Page Two August 23, 1995 meeting with representatives from Sigmon's, DEM staff were informed that the sludge in the lagoons was mixed with saw-dust, and the sludge was removed and was stock-piled in lagoon #3. Brief History: On August 9, 1990, DEM issued a Notice of Violation to Sigmon•s. That Notice required that the extent of soil and groundwater contamination at the site be determined. On September 9, 1990, DEM held the Notice in abeyance pending review of the site by the Hazardous Waste Section, as there were some questions regarding jurisdiction. In April of 1993 the Hazardous Waste Section concluded that the site did not fall under its jurisdiction. Therefore, after resampling the monitoring wells at the site, a Notice of Violation was reissued to Sigmon•s on July 13, 1993. In September of 1990 staff of the Solid Waste Section, DEM, and Barry Sigmon met at the site to discuss closure of the eight lagoons, and to determine if the wastes in the lagoons were hazardous prior to land applying. Samples were collected by the Solid Waste Section in August and September of 1992. I found no documentation in the incident file from the Solid Waste Section concerning land application of the sludge. It is understood that because the samples collected from the lagoons do not exceed the TCLP levels, the sludge is not considered hazardous and can be land applied. As stated, there are only 4 acres on-site and an estimated 2,000 tons of sludge, so the Sigmon's will not be able to land apply the sludge on-site. In addition, the presence of the contaminants in on-site monitoring wells as well as in downgradient supply wells may indicate that the contaminants are leaching from the sludge. The most recent groundwater sampling results are attached for your review. In addition, the laboratory results from sludge samples collected by Shield Environmental, on the behalf of Sigmon•s, are attached for your review. If you have any questions and/or comments, please call me at (704) 663-1699, ext. 243. Attachments --- - -,_ . \ '11(•~ ~\ .) .' ,::"'' .· . .._ ., ! - - ·-' -., V C --•• ;iii -·. ~-:c.-cu ~ ~' I . , -_ I ) • ,, '\ _ . " ... \ / ; ~yl ', I-~. '', ~\' I ' /""; \ . ;) fr;:• , • 1 '-'1,,,,.., 1 "" 1 ,.~,,-,.,,..,.,,._ ·--<,,.,.. . L. 1 -, ~ _ . \ --1..:____ y _ - -. . "' • ' . -.. , .r ' r,J -. '.'iv • . ~, •. • . -•. i _u~· ' \ • - IOLOMETfAS 1 MllES J -,1· ,,,-:;, '. -• ' • • • I ,r ''tc: __ , __ r '':/di ~"it::~) ... , I '-'1'... " -s.._ . - "'1 l ---~ I __ .,... I _../'. ) . -/' ' .;11 J; , / ~; i'- ., ... , .. • I ,_ I ( ' -, . --=. /, .'."" ,t~~. ' ', .,, .. . ' . , 0 ' ' ' . ' . . .. ' 0 1·150000 Scale · 10 2'4 mil•• ' • 1 Inch represen . ~) OCATION QUAORANGl[ l SIGMON SEPTIC T~A~ORTH CAROLINA !REDELL COUN • DRAWN BY : RM DATE . 11-02-83 WN FIGURE : I SCALE : AS SI 10 s 1-1 I ELD ENVIRONMENTAL ASSOCIATES, INC. • 0 0 I /'17 • • tr: ~ .. "'*> ~ rJ • ··> Q~\9 "'-Ip -_---Property Unt .. 4 . -= eo.::C.:.:G~. M.c.,--ac-..a· --aa·~-·-==""-'•IL-'·"'·-===---, -"·· .. ~ L • (6.3◄) Legend Sludge Sample Location Sludge Sample TPH Result (6.3 ◄) • m1/lia (UJ( • msfl, Scale: 1 "=65' : Sludge Sample TPH Map;_· Figure 4 Sigmon Septic Tank Service, Inc._ Iredell Count North Carolina · s I-I I E L D ENVIRONMENTAL ASSOCIATES. INC . . ~--.--------_,;------~~~---llliiiiiiiiiiiiiiiaiii ...... ____ j i I t --•--- JtrJ ff " ,. +- ...c: r ~ C. "' ... 'I" (;' -1 0 0 , ..c: "' ~ '3 ;, -., ;::> 'l. ;J-.. ~ • ... --. liiiiiw == == == I!!!!!! ~ • 111111 • I I ,c:. I .. Law Offices of JHLome::sJey, Jolllle§, Gaiiilllle§ & fiieldLs 383-387 North Main Street . Ref 25 m 1~ C. Homesley, Jr. Walter H. Jones, Jr. Edmund L. Gaines T. Eric Fields Post Office Box 1235 Mooresville, NC 28115 704/664·1l27 · Facsimile 704/664-6596 Offices· Mooresville Statesville II Clifton W Homesley IJ L. Ragan Dudley February 19, 1996 E Mr. B. Keith Overcash Regional Supervisor State of North Carolina Division of Environmental Management 919 North Main Street Mooresville, North Carolina 28115 Dear Mr. Overcash: RE: A.A.A. Enterprises, Inc. Ground Water Incident /3422 Iredell County, NC Reference is made to your letter of December 15, 1995, to the attention of Barry Sigmon of A.A.A. Enterprises, Inc. I have been requested to answer your letter in order that you would know that they are not just ignoring you. However, A.A.A. Enterprises, Inc. ceased doing business for financial reasons on September 28, 1995, and they simply have no funds available to do anything further with respect to the problems outlined. As you may or may not know, A.A.A. Enterprises, Inc. was primarily owned by Henry H. Sigmon, Jr., and his only income is his social security income which is limited. We have gone over many alternatives with respect to this problem, but it does not appear that they are financially able to try to comply with any of the alternatives. Accordingly, they wanted me to let you know that they simply are not in a position financially to proceed to do anything further with respect to this problem. I do want you to know that they are being sued by people who have previously tried to assist them with these problems, but they do not even have the money to try to pay those people for their prior assistance. Sincerely, GAINES & FIELDS .~- T. C. Homesley, Jr. TCH/vc I I I 1D I I 1• ., •• •• -f I ' It I State of North Carolina Department of Environment, Health and Natural Resources Division of Solid Waste Management James B. Hunt, Jr., Governor Jonathan B. Howes, Secretary William L. Meyer, Director Ms. Cindy Gurley NC CERCLA Project Officer U.S. EPA Region IV Atlanta Federal Building 100 Alabama St., SW Atlanta, Georgia 30303-3140 December 12, I 996 SUBJECT: CERCLIS Site Addition Sigmon's Septic Tank Service, NCD 062 555 792 (RCRIS) 1268 Eufola Road Statesville, Iredell County, NC Dear Ms. Gurley: Please add the subject site to CERCLIS. Preliminary data gathering has established the following about the site. I. The site name is Sigmon's Septic-Tank Service. The site is located at 1268 Eufola Road (S.R. 1333), southwest of the town of Statesville in Iredell County, North Carolina. The geographic coordinates of the site are 35° 43' 01" north latitude and 80° 58' 11" west longitude. The site is currently owned by Mr. Henry H. Sigmon, Jr. 2. The site was operated from the late 1970's until September 28, 1995, when the company ceased operations for financial reasons. The operation included pick up of septic wastewaters from various industries located around the Statesville area which were transported and deposited in lagoons at the site until spring 1992. As of September I 990, ten lagoons were present on site; two unlined lagoons were inactive and eight unlined lagoons were active. The estimated total dimensions of all ten lagoons are approximately 225 feet wide by 180 feet long, by 12 feet deep, or 486,000 cubic feet (18,000 cubic yards). Sludges remaining in the lagoons were mixed with sawdust and stockpiled in lagoon #3. A estimated 2,000 tons of sludges are reported at the site. P.O. Box 27687, FAX 919-715-3605 Ref 26 Raleigh, North Carolina 27611-7687 Voice 919-733-4996 ~uc::c Rei.Jee An Equal Opportunity Affirmative Action Employer 50% recycled/10% post-consumer paper b I I 11 1D 1 D 1• 1• ., 1• •• -I I ' It I Letter to Ms. Gurley December 12, 1996 Sigmons Septic Tank Service Page 2 3. Historic aqueous and sludge samples from the onsite lagoons demonstrate the presence of CERCLA hazardous substances. On August 31, and September 1, 1992, liquid and sludge samples were collected from the eight active septage lagoons and analyzed for volatile organics, semi-volatile organics, total inorganics and toxicity characterisitic leachate procedure (TCLP) inorganics. The aqueous samples contained elevated levels of bis(2-ethylhexyl)phthalate (360,000 ug/1), diethyl phthalate (11,000 ug/1), phenol (7,000 ug/1), 4-methylphenol (6,000 ug/1), toluene (1,277 ug/1), acetone (1,273 ug/1), 2-methylnaphthalene (1,000 ug/1), chlorobenzene (148 ug/1), xylene (51 ug/1), benzene (33 ug/1), lead (2.3 mg/I), chromium (0.19 mg/I), and cadmium (0.021 mg/I) in liquids collected from the lagoons. The sludge samples contained elevated levels of bis(2-ethylhexyl)phthalate (90,000 ug/kg), 4-methylphenol (25,000 ug/kg), toluene (16,533 ug/kg), 2-methylnaphthalene (9,000 ug/kg), dibutyl phthalate (8,000 ug/kg), 1,4-dichlorobenzene (7,000 ug/kg), naphthalene (4,000 ug/kg), chlorobenzene (2,500 ug/kg), xylene (1,155 ug/kg), 2-methylphenol (1,000 ug/kg), acetone (624 ug/kg), ethylbenzene (288 ug/kg), 1,2-dichlorobenzene (200 ug/kg), methylene chloride (156 ug/kg), 1,3-dichlorobenzene (100 ug/kg), benzene (70 ug/kg), carbon disulfide (18 ug/kg), lead (200 mg/kg), barium ( 110 mg/kg), chromium (51 mg/kg) and mercury (0.29 mg/kg). None of the contaminants exceeded RCRA TCLP levels for toxicity characteristic. 4. Despite the low TCLP results, releases to groundwater have been repeatedly detected in onsite monitoring wells. In 1987, four monitoring wells were installed at the lagoons; three downgradient of the lagoons and one upgradient. On June 14, 1990, groundwater samples collected by the NC Division of Environmental Management (DEM) detected elevated levels of iron (2,300 ug/1), lead (190 ug/1), manganese (430 ug/1) and mercury (6.0 ug/1) in excess of the North Carolina groundwater standards (!SA NCAC 2L). The groundwater sample also detected the presence of 1,1-dichloroethane ( 1.3 ug/1). On August 3, 1990, a Notice of Violation letter was issued to Sigmon for violations of the State groundwater standards. On May 6, 1993, DEM collected additional groundwater samples from monitoring wells # I and #2, downgradient of the lagoons. On July 13, 1993, a second Notice of Violation letter was issued to Sigmon for releases of cis-1,2-dichloroethane (2.3 ug/1), benzene (2.3 ug/1), barium (710 ug/1), mercury (29 ug/1) and lead (75 ug/1) in excess of the State groundwater standards. The sample results also detected elevated levels of I, 1-dichloroethane ( 1.6 ug/1), trichloroethane (0.25 ug/1), chlorobenzene (5.5 ug/1), 2-chlorotoluene (2 ug/1), 1,3-dichlorobenzene (0.38 ug/1), 1,4- dichlorobenzene (6.1 ug/1), m.p-xylenes (2.1 ug/1) in the onsite monitoring wells. I .. I I ti 1• 1 • 1• 11 ., 1R 10 11 " I I ' I I Letter to Ms. Gurley December 12, 1996 Sigmon's Septic Tank Service Page 3 5. Groundwater sample results from two downgradient drinking water wells (Mike James residence and Rachel Brown residence) demonstrate that offsite drinking water wells have also been affected by releases from the site. Both offsite drinking water wells have exhibited levels of manganese, mercury and nitrates in excess of the State of North Carolina's groundwater standards and/or EPA's Maximum Contaminant Levels for drinking water. As a result, the North Carolina Occupational and Environmental Epidemiology section has recommended that the occupants discontinue use of the water from these wells for drinking or cooking purposes. Both wells are located at rental properties. 6. Sludges'and lagoons may present an exposure threat to nearby human populations, or animals from CERCLA hazardous substances. Bis(2-ethylhexyl)phthalate was detected in sludge samples at a concentration exceeding the current EPA Superfund Chemical Data Matrix (SCDM) human health-based soil screening benchmark of 46 mg/kg. Although the site is not located in a highly populated area, several of the nearby residents have small children. No covers or caps are present on the sludges or lagoons to prevent direct contact with the contents. A three strand barbed wire and electric fence reportedly surrounds the lagoon property, restricting access by neighboring livestock which have repeatedly broken through the site fence to eat the grass. A small pond, located within 1000 feet west of the site along the overland drainage pathway, contains food chain species that may be taken for human consumption. Attached is a CERCLIS site addition form and a copy of the site maps which show the immediate area of the subject site. If you.have any questions, please call me at (919) 733-2801. Attachments cc: Pat DeRosa File Scott Ross Pat DeRosa, Head Site Assessment and Removal Branch NC Superfund Section 0 1E 1• I I 1 • 1• •• ., •• •• I I I ' ,. I LATITUDE AND LONGITUDE CALCULATION WORKSHEET. #2. LI.USING E.NGINEER'S SCALE (1/60) r SITE NAHE: .S/6mo,-JS Sel>TIC 77+N/C SEl<VICt CERCLIS I: AXf> Ob;;J SS5' 7'1,;/_ AKA '----------'--',~~-----------ss ID'-------,---------- ADDRESS : / ;;u,~ [::(,I F'O LA--f<o~ STATE: NC- SITE REFERENCE POINT:. lrf'l'Ro)(/ /Vllr'Tf= lD CA-'176,v ZIP CODE: cxftb77 OF. LA60o/oJJ USGS QUAD.HAP NAHE: T/i?ocrrmA-rv' NC.. TOWNSHIP:· . ' .. N/S RANGE:· __ E/W . SCAL~. ~p· DATE:~96,,C, SECTION: ___ if{ ___ l/4 __ 1/4 HAP DATUH: ~i9!33 (CIRCLE ONE) HERIDIAN:~·----------------- COCRDINATES FROH LOWER RIGHT (SOUTHEAST) CORNER OF 7.5' HAP (attach photocopy): LONGITUDE: .fu___o S"'Z_.' .3.Q__" LATITUDE: 3S o 37 3o " COORDINATES FROH LOWER RIGHT (SOUTHEAST) CORNER OF 2.5' GRID CELL: LONGITUDE: LATITUDE: :,5 ° 4-,_ ' 3c CALCULATIONS: LATITUDE (7.5' QUADRANGLE HAP) A) NUHBER OF RULER GRADUATIONS FROH LATITUDE GRID LINE TO SITE REF POINT: Ji_ B) HULTIPLY (A) BY 0.3304 TO CONVERT TO SECONDS: AX 0.3304 3o . 73" ---- C) EXPRESS IN HIHUTES AND SECONDS ( 1 '= 60") : l!)O '3 l 00" ---- D) ADD TO STARTING LATITUDE: ?,5 ° Lj--Z. '~•Q_Q__" + 00 '.°St .. OD . _ Cl~CULA'I'IONS: LOt~GITUDE ( 7. 5' QUADRN,GLE HAP) .A) NUHBER OF RULER GRADUATIONS FROH RIGHT LONGITUDE LINE TO SITE REF POINT: t·.:z . .'l-- B) MULTIPLY (A) BY 0.3304 TO COINTRT TO SECOIWS: AX 0.3304 C) EXPRESS IN MINUTES AND SECONDS ( l '= 60") : (')cJ ' 4-/ . OO " D) ADD TO STARTING LONGITUDE: 'ifo o..2.l'~-Q...£_" + Oo '..!ti_. Ob I ~----------------__J SITE LONGITUDE: .8.Q_0 5'g'•([ .Oo" ------ I E-11 I .. I 1' l D I I •• •• I f SITE DISCOVERY FORM Part I: Information necessary to add a site to CERCLIS ACTION: A EPA ID: NCO 062 555 792 SITE NAME: Sigmon's Septic Tank Setvice STREET: 1268 Eufola Road CONG DIST: 9 (optional) CITY: Statesville ZIP: 28677 CNTY NAME: Iredell CNTY CODE: 49 (optional) LATITUDE: 35/43/01 LONGITUDE: 80/58/11 (optional) INVENTORY IND: Y REMEDIAL IND: Y REMOVAL IND: N FED FAC IND: N RPM NAME: RPM PHONE: (EPA Project Officer) SITE DESCRIPTION: (optional) Sigmon's Septic Tank Service operated a septage removal business located on a 15.35 acre parcel at 1268 Eufola Road (SR 1333), Statesville, Iredell Co., N.C. from the late 1970's until September 28, 1995, when the company ceased operations due to financial reasons. The operations included pickup of industrial septage wastewaters that were transported to the site and deposited in ten unlined and unsecured lagoons. Sludge and aqueous samples from the lagoons contain elevated concentrations of CERCLA hazardous substances, including mercury and manganese which have been detected in groundwater from monitoring wells adjacent to the lagoons and in drinking water wells near t!1e site at levels exceeding the North Carolina groundwater standards and EPA Maximum Contaminant Levels for drinking water. Although the company had been providing bottled water to the affected residences, they are currently out of business and no longer supplying bottled water. In addition, there are children living iri nearby residences that may have access to the site and a small pond downgradient of the site in the overland drainage pathway that contains food chain species that may be taken for human consumption. l in I U I D lg 10 D , 1D 11 -I I f t- i Part 2: Other site information DATE SITE FIRST REPORTED: 12/12/96 REPORTED BY: NC Superfund Section REASON FOR LISTING: Actual contamination of drinking water supply. Potential food chain threat. Potential human contact threat. I :I I I I I •• I 'I I I I la I I UNITED STATES ENVIRONMENTAL PROTECTION AGENCY REGION4 ATLANTA FEDERAL CENTER 100 ALABAMA STREET, S.W. Ref 27 ATLANTA, GEORGIA30303-3104 RECElVED 4WD-ERRB Mr. Jack Butler, Deputy Director Solid Waste Management Division North Carolina Division of Solid SUPERFUND SECTION Waste Management P.O. Box 27687 Raleigh, N.C. 27611-7687 SUBJ: Sigmon's Septic Tank Service, Statesville, N.C. Dear Mr. Butler: The U.S. Environmental Protection Agency's Emergency Response and Removal Branch (ERRB) reviewed the available information for the above referenced site to detennine its eligibility for a potential removal action under the National Contingency Plan (NCP). Sigmon's Septic Tank Service is located at 1268 Eufola Road in Statesville, Iredell County, North Carolina. The site operated from the late 1970's until September 28, 1995. The operation included pick up of septage wastewaters from various industries and were transported and deposited in lagoons at the site until 1992. On January 24, 1997, On-Scene Coordinator John Nolen reviewed the available information and spoke with the state of North Carolina and concluded that the above referenced site does not meet the criteria for removal eligibility. This detennination does not preclude any other investigation activities or response actions by other parties -which may still be appropriate for this site. Should site conditions change or additional infonnation become available, ERRB will re-evaluate this site as necessary. Should you have any questions concerning detennination, please contact John Nolen, On-Scene (404) 562-8750 or Michael Norman, Chief of Remov Section, at (404) 562-8720. Recycled/Recyclable• Printed with Vegetable OU Based Inks on 100% Recycled Paper (40% Postconsumer) at I I I I I I I I f I I I I I ' I I Memorandum Date: April 10, 1997 To: Paul Dahlen GW Section, NC Div. of Environmental Mgmt. -Mooresville Reg. Office From: Douglas Moore ~ Environmental Chemist, Superfund Section Subj.: Sigmon's Septic Tank Service Eufola Road, Statesville, NC US EPA ID: NCO 062 555 792 (RCRIS) On January 23, 1997, the NC Superfund Section referred the subject site to the Environmental Protection Agency -Emergency Response and Removal Branch (ERRB) for removal evaluation. A copy of the removal request memo was previously faxed to you on March 10, 1997. At that time, we had not received a written response from ERRB regarding the disposition of the site under their program. On April 4, 1997, our section received ERRB's response indicating the site did not meet the criteria for removal eligibility. A copy of their written response is attached to this memo. On December 12, 1996, the site wasadded to the CERCLIS database as a site that may require further investigation in the near future. This site has been assigned to Donna Wilson, an Environmental Engineer with the Superfund Section. Mrs. Wilson will be reviewing the file to determine if additional sampling will be required in order to assess the potential threat the site may pose to human health or the environment. If you have any questions, please contact Donna at (919) 733-2801, ext. 317. cc: Pat DeRosa Donna Wilson File Aeporl 10: ARO, FAo~-:B-. RAO, WaAO. WiAO. WSAO, Kinslon FO Olhar _______ _ ,-- Shipped by: Ous.~~ud✓r, 01hor · ______ _ CAA~ ·@wo®bf6TODY (:Zl ROUTINE O EMERGENCY · 0 Olhar -------------=-,,,,-- DATA ENTRY BY: 1-11 CK: J):._~ DATE REPORT ED: __ 4.=c,/..eso"'/__,v""------ COLLECTOA(SJ: Oe&fl_ /1,,~(!(,t,1 DATE 5/:ii;i? ' TIME PURPOSE: BASELINE, COMPLAINT, COMPLIANCE. LUST, OTHER (cltcle on-el FIELD Al':).AL YSES 70 ~-~-Spec. Cond.9 ◄ gco rl Ownor I}()(+ G,ic. c Pr/ SC5 (s,f,2-Y'n .0 ,! frc 12, etc I/ -«"/.;.Jr(!') 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N 6 lo n.9<1- TKN "N .,, N0,1 '9 H03 11 N OJO <</, P:Toial 11 P 64'5 mg/I moll moll V moll """ uMho1/cm 1 mg/I mo/I x mot/ mg/I X mg/,l mg/I Ag -Sll•er 1077 Al -Alt,ml~um 110, Oa • Bui um ·1001 cc::ci n c, • Calclum I" Cd • Cadmium 1027 Chromlum:To1al 1034 Cu· Copp■t 1042 ,. • Iron 10,s Hg • l.hrcu,1 71900 -:../'-1 K • Po1aulum 937 Mg -IJagn .. lum 821 Mn • l.l1nu1n11■ 1056 Na • Sodium ai 1J NI t,/1 Cl• I I 061 Pb • LI ad I 0 !i I 1 1 n s, Sal■nlum 1147 lo • line IOV1 1-/-5-'o REY, 919() for Olssol\/9d Analysis -submll littered sample and wrila "DI"' !n block White Coov ~ Groundwaler Gnnlr.ll Offlr..A Vn!l,-iw r.nnv. I rn-.1 ('\I/I,-,., 01~1, ,-. --· uo/1 Orw1nochlo,ln• "•■IIGl411 uo/1 01u•nopho1phoru1 ,. •• 11014•• "'" moll Acid H ■tdli::ild•■ 1.111/1 ug/1 81•• I N ,uiral (1lt1Clabl• o,,.,., •• llOII Acid E.1lr1cl1bl• 01g1n101 uo/1 ug/1 X Puru11bl1 Org1nlc1 {VOA bolll•J -motl m<>'I ''' -Olbroll'IO•th•n• (£0111) ug/1 moll -·- ug/1 ~ -.._...,,. ... • .. r ... i'IJ.,'TTJRAL . . ..,.,. ~ ..... ·-. ,~.' ., ug/1 ~M?°Y!UNiTi., ··.,,:·, ,:r .. ,, uQ/1 / u011 .Pii : / H>T~ I • 1;rir<• ,, --~i:;,i:;,. ' p; "' . ,~ .. -·' I LAB NO. 3G~01 -~BPORTBD Bl'u- CHBCKED BY . I RBVIBWBD BY aJJ? SAKPLB TYPE: WATER I · CASI VOA TARGET COKPOUND I 75·35·! 1,l·Dichloroethene 75-09·1 Methylene Chloride 156-60·5 trans-1,1-Dichloroethene I 75.34.3 l,l·Dichloroethane 590-20·7 2,1-Dichloropropane 156-59·4 cis-1,2-Dichloroethene I ,1·66·3 Chlorofon 74.97.5 Bro1ochloro1ethane 71-55-6 1,1,l·Trichloroethane 563·58·6 l,l·Dichloropropene I 56·23·5 Carbon Tetrachloride 107-06·1 1,1-Dichloroethane 79-01·6 Trichloroethene I 78·87·5 1,2-Dichloropropane 75-17-4 Broaodichloroaethane 14.95.3 Dibro101ethane ,10061·01·5 cis-1,3-Dichloropropene. 10061·02·6 trans-1,3-Dichloropropene 19-00·5 l,l,1·Trichloroethane 121·18·4 Tetrachloroethene I 142-18-9 1,3-Dichloropropane 124-48·1 Dihromochloro1ethane 106·93·! 1, 2 · Dibroa.oethane I 108·90·7 Chlorobenzene 630·20·6 l,l,1,2·Tetrachloroethane 75-25·2 Broaofon I 79.34.5 l,l,2,2·Tetrachloroethane 0.75 0.15 0. 7 5 0 .15 0 .15 0.15 0.15 0.75 0.15 0.25 0. 75 0 .15 0.25 0.25 0.15 1 0 .15 0.25 0. 2 5 0. 25 0,25 0,75 1 1.15 0. 25 0.5 0.75 TQL· Target Quantitation Limit· subject to I change due to instru1ent sensitivity T· Tentatively Identified, not confirmed B· Bstiaated Value BHNR/DBK LABORATORY VOLATILE ANALYTICAL REPORT ANALYSIS RESULTS '"'''"''"'~ DATB BHTBRBD· BY - CHECKED BY DETECTED CASI VOA TARGET COMPOUND DETECTED u 1 u 1 u 96·18·4 1,1,3-Trichloropropane 0.15 u u 108·86·1 Broaobenzene 1 u u 95-49·8 2 ·Chlorotoluene 0.25 1 I. 6 106·43·4 l·Chlorotoluene 0,25 u u 541·13·1 1,3-Dichlorobenzene 0.25 0.38 1, 3 106-46·7 1,4-Dichlorobenzene 0.25 4. 8 B u 95-50·1 1,1-Dichlorobenzene 0.25 4. 2 B u 96·11·8 l,1·Dibroao·3·Chloropropane 1 u u 110·81·1 1,2,4-Trichlorobenzene 0.25 u u 87-68·3 Hexachlorobutadiene .0.15 u u 87·61·6 1,1,3-Trichlorobenzene 0.75 u u 1634-04·4 Kethyl-tert-butyl ether 5 u 0.25 71-43-1 Benzene 1 2. 3 u 108·88·3 Toluene 1 u u 100·41·4 Ethyl benzene 1 u u 108·38·3 m,p·Xylenes 1 1.1 u 95-47-6 o-Iylene 1 D u 100·41·5 Styrene 1 u u 98·82·8 Isopropylbenzene 1 u u 103-65-1 n· Propylbenzene 1 u u 108·61·8 1,3,5-Trimethylbenzene 1 1 B u 98·06-6 tert-Butylbenzene 1 u u 95·63·6 1,1,4-Triaethylbenzene 1 u 5. 5 135·98·8 sec-Butylbenzene 1 u u 99·87·6 p·isopropyltoluene 1 u u 104-51-8 n·Butylbenzene 1 u u 91·10·3 Naphthalene 1 u Other purgeables detected Detected [up to 10 highest peaks) ug/1 BIGHT UNIDBNTlFIBD PBAKS DETECTED BY I U· saaples analyzed for this co1pound but GC/PID. H· I D· K· " COKKEHTS: I I not detected sample not analyzed for this compound Detected below quantitation limit GC/KS Analysis performed I --1 I I I I I I ,. I I I I I I It I 11 To: From: Subject: Dale: MEMORANDUM File CJ'\ . Q_ LJ.;.' (;S,()-Donna Wilson vfA'LIVI'-d '.J'-\, Environmental Engineer North Carolina Superfund Section Preliminary Assessment/Site Inspection Sigmon's Septic Tank Service Statesville, Iredell County January 23, 1998 Ref. 28 On August 25 and 26, 1997, PA/SI sampling was conducted at the above referenced site. The sampling was conducted by two teams: Team I -Donna Wilson, Harry Zinn, and Stephanie Kozel Team 2 -Jeanette Stanley and Doug Moore The following notes were taken for Team 1. We arrived al the site at 12:45 and spoke with Mary Sigmon about the schedule of the samples. At 12:50, we began setup of the Little Beaver power auger at the background soil sample location SS-29-SL, SS-30-SL, and SS-31-SL. The plan originally called for the samples to be taken on the adjacent property of Merle Potts, but I was not able to reach him to obtain permission. An alternate location was chosen, after obtaining permission from Mary Sigmon, in front of the Sigmon's home approximately 20 feet from Eufola Road on the crest ofa slight hill, and approximately 65 feet west of the Sigmon entrance. Sample SS-29-SL was collected at 13: 17 from a depth of2 inches to 2 feet by Stephanie Kozel. The sample was red clay. Photo #1 was taken of SS-29-SL. At 13:25, Harry Zinn and Stephanie Kozel began augering with the Little Beaver. At 13:37, sample SS-30-SL was collected at a depth of3.5 to 4 feet by Stephanie Kozel. The sample was red clay. Photo #2 was taken of SS-30-SL. At 13:47, augering was resumed. At 14: I 0, sample SS-31-SL was collected at a depth of 12 feet by Stephanie Kozel. The sample was red weathered saprolite with clumps of \ n u , n u 0 0 0 Memo to File Sigmon's Septic Tank Service January 23, 1998 Page 2 yellow and black. Photo #3 was taken of SS-31-SL. At 14:45, we drove to the lagoon area and began setup of the Little Beaver over the area that appeared to be lagoon #2. At 15:10, augering began. At a depth of8.5 feet, an impenetrable substance was encountered, most likely saprolite. At 15: 15, thundering began, so the equipment was packed back into the trailer. At 15:30, we drove to the new mobile home development located just east of the Sigmon property and knocked on the door of the trailer located closest to the lagoon area to inquire about sampling their well. The person who answered the door was not the owner. The owner is Matt Frye, who was away at work. At 15:45, we arrived at the Sigmon home. The well appeared to be a dug well, covered over at the ground surface with concrete. We began purging water from a spigot on the side of the house at 15:48. No information was available on the details of the well. Time Temp ph Conductivity 15:48 19.6 6.52 314 15:54 18.5 6.81 361 15:59 19.4 6.86 70.3 16:04 18.3 6.89 300 16:09 18.5 7.06 83.6 16: 14 18.1 7.22 405 Sample SS-32-PW was collected at 16: 18 by Harry Zinn. It rained very hard beginning about 15:50. We were able to stand in the garage of the Sigmon residence as we monitored the groundwater parameters. We drove at the home of Tom Shepperd (SS-03-PW). Because there was no outside spigot, we began purging the water at the kitchen sink at 16:52. No information was available on the details of the well. Mr. Shepperd buys his own bottled water. Time Temp pl-I Conductivity 16:53 21.3 8.85 149.6 16:58 20.2 10.44 143.7 17:04 20.2 I 0.5 130 17:09 20.3 I 0.53 122.5 Because of the high pH readings, we began to question the accuracy of the pl-I meter. At 17: 12, sample SS-03-PW was collected by Stephanie Kozel. As the water was being u g 0 0 g g Memo to File Sigmon's Septic Tank Service January 23, 1998 Page 3 added to the pre-preserved VOA vial, a visible gas vapor was formed, The rain stopped while we were sampling SS-03-PW. We walked next door to the Mike James well (SS-02-PW) and began purging at 17:36. The 2-foot diameter bored well is contained in a well house, with water visible at a depth of about 30 feet. Time Temp pH Conductivity 17:37 19.4 13.51 266 17:42 18.9 10.76 212 17:47 20.2 13.07 203 17:52 19.6 13.49 227 Because of the high pH readings, we concluded that the pH meter was not working properly. At 17:53, sample SS-02-PW was collected by Harry Zinn. Photo #4 was taken at this location. At 18:28, we drove back to the lagoon area. At 18:35, augering began at a location north of the previous hole in lagoon 2. An impenetrable substance was again encountered at a depth of 8.5 feet. The auger was moved about 20 feet east. An impenetrable substance was also encountered. The decision was made to abandon lagoon #2. At 19:20, the auger was moved north to lagoon #3, which was covered with dead vegetation. An impenetrable substance was encountered at 7 feet. The auger was moved approximately 10 feet to the west. At a depth of 5 feet, light gray saprolite with an odor was encountered. At 19:50, sample SS-21-SL was collected at 5.5 feet. Photo #5 was taken at this location. HNU reading at the breathing zone was 1.5. HNU reading at the hole was 8. HNU instrument No. 3 was used. We left the site at 20:30. We arrived at the site on August 26, 1997, at 8:30 and began setup of the Little Beaver over lagoon #5. At 8:55 the tripod was setup and angering begun. At a depth of 10 to 11 feet. black-brown odorous sludge-like material was encountered. At 9: I 0, sample SS-35- WS was collected. Photo #6 was taken. Augcring continued in the same hole. At 9:50, sample SS-22-SL was taken at a depth of 12 feet. The material was gray saprolite mixed with brown moist sludge-like matter. Photo #7 was taken. I .. I I D D E I Memo to File Sigmon1s Septic Tank Service January 23, 1998 Page 4 At I 0:00, the Little Beaver equipment was cleaned and the sampling equipment was loaded. At I 0:35, we climbed up the waste pile on the north side to a height of approximately 6 feet. The total height of the pile is approximately 20 feet high. At 10:42, sample SS-23- WS was collected at a depth of 9 to 18 inches with the use of a hand auger. The material was dark brown and had a septic odor. Photo #8 was taken. At 10:59, sample SS-25-WS and duplicate sample SS-125-WS were collected on the top of the pile at a depth of 3 feet with the use of a hand auger. Photo #9 was taken. At 1 1: 18, we moved to the west side of the pile to a height of approximately 10 feet. Sample SS-24-WS was collected at a depth of2 feet. The material was brown sludge like matter, fine grain with red clay. Photos #10 and 11 were taken. At 11 :44, at the tank area, sample SS-26-SL was collected at the third tank from the north, at a depth of 2 to 6 inches. The material was poorly sorted dark brown/black sand and was odorous. Photos # 12 and 13 were taken. At l l :46, sample SS-27-SL was collected at the fourth tank from the north, at a depth of 2 to 6 inches. The material was light brown medium sand and was odorous. Photo # 14 was taken.The area surrounding the tanks is estimated to be 40 feet x 3 feet, or 120 square feet. At 12:05, sample SS-28-SL was collected, with the use of a hand auger, behind the third tank at a depth of 3 to 3.5 feet and a distance of approximately 5 feet from the tank. The material was red sandy clay. Photos# 15 and 16 were taken. At 12:30, we left for lunch and purchased locks for the monitoring wells. After returning to the site, we proceeded to the two open pits in the extreme southeast corner of the site. The pits were surrounded by thick tall brush and vegetation. Harry climbed into open pit #1, which was about 15 feet deep, 12 feet wide and 40 feet long, and oriented 40° east of north. No water was present in the pit. At 14:45, sample SS-18- SL was collected at a depth of 0 to 6 inches. The material was red clay with no odor. Photo # 17 was taken. Harry climbed into pit #2, which was oriented north-south, and was about 10 feet wide and 20 feet long. The area was covered with thick brush. At 15:05, sample SS-19-SL was collected at a depth of0 to 6 inches. The material was stiff red clay. 4 I It I I I I u , '' 0 D E I Memo to File Sigmon's Septic Tank Service January 23, 1998 Page 5 At 15:21, we arrived at the home of Matt Frye and Sheila Tenney (SS-34-PW) and met Team 2. At this home, there are three people who drink the water, including a 17-month old baby. Their address is 130 Mustang Drive, Statesville 28677. Team 2 stayed at the site to sample the well. At 15:31, we drove to the south side of the property on Lauren Drive and walked to the ditch to collect the background ditch sample (SS-13-SL). The direction of surface water runoff appears to split south of the Sigmon property. We chose to sample on what appeared to be the crest of the road and ditch; however, the sample location may receive runoff from the site, and may not actually be a background sample. The location was west of the trailers. At 15:35, sample SS-13-SL was collected at a depth of 3 to 6 inches in the ditch. The material was brown, organic, clayey sand. Photo #18 was taken. While we were assessing the location for sample SS-13-SL, I spoke with Team 2, Jeanette and Doug, about the location of SS-12-SL. The sample was chosen in order to characterize any contamination that may enter the drainage ditch from the east side of the culvert inlet to the pond. At this time, however, the telephone utility company had disturbed the length of the ditch east of the culvert for the installation of telephone lines; therefore, it was not possible to sample SS-12-SL. At 16:42, we drove back to the Sigmon property to the monitoring well located in the southwestern portion of the site. The water level was measured to be 35.5 feet from the top of the casing. The column of water was determined to be 4.5 feet, one well volume was calculated to be 0. 73 gallons, and three volumes was calculated to be 2.2 gallons. At 16:55, we began bailing the well. Gallons 1.5 2 pH 6 7 Cond ucti vi t y 1150 1401 Temp 22.9 19.9 At 17:25, the trip blank and the post preservative blank were prepared. At 17:28, after collecting 2.25 gallons of water, sample SS-05-GW was collected. The sample was very turbid. We left the site at 17:45. 5 I -I I I I I I ., \m g I I I I I ' I I I I ~ H u I Memo to File Sigmon's Septic Tank Service January 23, 1998 Page 6 The following notes were taken by Team 2, Doug Moore and Jeanette Stanley. At 12:45, they met with Mrs. Peggy Burris, 194 Green Valley Road, Statesville, and obtained permission to cross her property to collect the background surface water/sediment sample on Norwood Creek. The sample location was downhill from the house, along a meadow. The creek was 6 to 8 feet wide and 8 inches deep. At 13: I 0, Jeanette Stanley collected sample SS-09-SW. The sample location corresponds to GPS #RO82517A. At 13:15, Jeanette collected sample SS-09-SD. The sediment was medium brown fine silt with little sand, little organic content, and no obvious odor or sheen. They decided to switch GPS units because the R-unit was not functioning properly. GPS readings will be taken using the C-unit. Photos# 2 and 3 were taken at this location. At 14:00, they drove to the background pond location (SS-08-SW/SD). The pond is approximately 150 feet across at the dam and approximately 200 feet in length. Jeanette collected sample SS-08-SW. The sample location corresponds to GPS #CO825 I 8A. Photo #4 was taken at this location. At 14: 10, Jeanette collected SS-08-SD. The material was gray silty sand with light to moderate organic content and slight odor of hydrogen sulfide (rotten eggs). The sample location corresponds to GPS #CO82518B. Photos# 5 and 6 were taken of the sediment location. The sediment sample was collected on the extreme eastern side of the pond, opposite the dam. The water sample was collected on the southern side of the pond, near the dam. At 14:50, they drove to the Joe Anderson residence, 297 Carriage Road, to obtain access to the creek below his home for sample location SS-07-SW/SD. At 15:15, Jeanette collected sample SS-07-SW, at a distance of approximately I 00 feet below the confluence of the two intermittent streams. The sample location corresponds to GPS #CO82519A. At 15:20, Jeanette collected SS-07-SD. The sediment was a light brown silty sand with little organic content and no obvious odor or sheen. Doug inspected the creek for 250 feet downstream of the confluence. The stream bed is 8 to IO feet wide and 8 inches deep on average. No hydric soils, nor hydrophilic type vegetation was observed downstream of the confluence at SS-07-SW/SD. Photos# 7 and 8 were taken. From 15:40 to 17:00, there was a rainstorm. The sample plan was modified for sampling point SS-16-SW/SD. After studying the aerial photographs and talking with Doug Moore about our observations of surface water flow to the west of the site, we concluded that the pond next to the Frances Lamberth I -I I I I I I I , 0 D m It I I . Memo to File Sigmon's Septic Tank Service January 23, 1998 Page 7 house was not shown on the topo map, and that the surface water drainage from west of the site did not enter below the Williams pond, but between the Lamberth pond and the Williams pond. Therefore, SS-16-SW/SD was moved to the drainage channel that receives surface water runoff from the site, before it joins the runoff from the Lamberth pond. Sample location SS-116-SW/SD was added, at a point downgradient of the Lamberth pond, but upgradient of the confluence with the runoff from the Sigmon site. At 17:00, they met with Talmadge Williams. At 17:35, they walked the tributary upstream from the Williams pond to determine if wetlands were present. For a distance of 305 feet, as measured by the wheelie, the soil parameters suggested a very high probability of wetlands. A push probe was used to obtain a vertical section of soil. The soil exhibited an olive-gray, low chroma soil color with a slight sulfide odor. Oxidized rhizospheres were present in the upper 6 inches. Wetland hydrology was present along both sides of the stream bank, as evidenced by the water table at a depth of 6 to 8 inches. The vegetation present indicates a probability of wetlands. Overstory consists of red maple, hickory, iron wood, and sweet gum. Understory contains grasses including some type of saw grass like vegetation, ferns, arrowheads, and cardinal flowers. Photo# 9 was taken of the wetland area facing downstream toward the Williams pond. Photo #10 illustrates the soil color and wetland hydrology on the southeast bank of the downstream tributary above the Williams pond. Photo# 11 was taken of the soil color and hydrology on the northwest branch of the tributary draining below the site above the Williams pond. Oxidized rhizospheres are present in the picture. Photo #12 show cardinal flowers in the wetland. At 17:25, Jeanette collected sample SS-17-SW from downstream of the Williams pond darn. The sample location corresponds to GPS #CO82523A. At 17:35, Jeanette collected SS-17-SD near the head of the Williams pond. Photo# 13 was taken at sample location SS-17-SD. The material was a gray fine silt with little sand and no odor. Mr. Williams address is 1170 Eufola Road, Statesville 28677, phone 704-528-6722. The sample location corresponds to GPS # CO825238. At 18: 15, Doug Moore collected sample SS-16-SW downstream of the runoff from the Sigmon site, and approximately 40 feet upstream of the confluence with the runoff from the Lamberth pond. The sample location corresponds to GPS #CO82522A. At 18:25, Doug collected sample SS-16-SD. The sediment was gray fine silt, organic rich muck, with a slight hydrogen sulfide odor. Photos #14 and 15 were taken. At 18:20, Jeanette collected sample SS-116-SW from the tributary downstream of the Lamberth pond, approximately 40 feet upstream of the confluence with the tributary 1 I -I I I I I m n , 0 I I I It I I Memo to File Sigmon's Septic Tank Service January 23, 1998 Page 8 which receives runoff from the Sigmon site. The sample location corresponds to GPS #CO82522B. At 18:25, Jeanette collected sample SS-1 I 6-SD. The sediment was a gray fine silt with a small amount of sand, and exhibited a hydrogen sulfide odor. Photos #16 and 17 were taken. Photo # 18 was taken of the small spring that drains to the tributary below the confluence. Because a wetland was discovered upstream of the Williams pond, this wetland was now considered the first wetland encountered by surface water runoff from the site. Samples SS-14-SW/SD and SS-15-SW/SD were no longer needed and were canceled. At 19:00, they arrived back at the Sigmon site and helped Team I load equipment. At 20:30, they departed the site for the hotel. At 8:05 on August 26, 1997, Doug and Jeanette arrived at the site and began preparing equipment and sampling jars. They drove to the Davidson pond, which is southeast of the site, and south of Lauren Road. The pond was covered with duck weed and algae. At 8:20, the volatiles samples (SS-10-SW and SS-110-SW duplicate) were collected. It was difficult to collect the VOA sample without a bubble because of the duck weed and algae. At 8:30, the metals and BNA water samples were collected. At 8:45, sediment samples SS-10-SD and SS- 110-SD were collected. The sediment was an olive gray silt with sand, with heavy organic content and a slight odor. The sampling location was at the western edge of the pond, at the dam. Photos # 19 and 20 were taken of the sediment and surface water samples. At 9:45, they arrived at the Potts residence, 1280 Eufola Road. After talking with Mrs. Potts, they began to purge the well for 15 minutes. The well plate contained the following information: Rcg.#203 Well completed 4/95 Depth 50 feet Casing depth 50 feet Diameter 20 inches Pump intake 48 feet Static water level 36 feet Yield 5 gpm Jim Steele Reg #54 7 Jet Pump °by Goulds .J!305 I -I I I I I D D E I • '9 1 I Memo to File Sigmon's Septic Tank Service January 23, 1998 Page 9 Calibration check of equipment: Turbidity 5. I 9 on 5.21 check standard Conductivity background calibration to zero at 22.3 (21.9 C) 1419 uS on 1413 uS standard TDS 704 ug/1 on 706 ug/1 standard at 23.1 C The pl-I probe was malfunctioning. Time Turbidity Conductivity 10:00 0.26 NTU 76.1 uS 10:25 3.78 61.9 10:30 5.6 64.5 10:32 4.65 59.6 At I 0:35, sample SS-04-PW was collected. Temp 19.5 C 21.5 19.3 I 9.3 TDS 38.3 at I 9.9 C 31.8 at 20.8 31.8atl9.6 30 at 19.4 At 11 :00, they drove to Chris Davidson's properties and waited for him to deliver the well keys. He arrived at 11 :20. He had three monitoring wells on the property. Sample SS- 06-G W is located on the northwest corner of the lot at 173 Lauren Drive. The lock was rusted closed, so the lock was cut with a bolt cutter. 1-INU 970163 was checked. Span setting of 1.94. They zeroed the meter to local air and uncapped the well. The meter read no volatiles in the well headspace. The water level was measured to be 19 feet and 1.5 inches below the top of the casing. The bottom of the well was measured to be 30 feet and 8 inches below the top of the casing. The casing height is I foot and 5 inches above the ground surface. One well volume was calculated to be 1.87 gallons, and three well volumes was calculated to be 6 gallons. At 11 :35, purging of the well began. The water was very muddy. The tag on the well included the following information: Reg. 888 Date completed 5/29/94 2 inch diameter casing depth 15 feet Well depth 30 feet Gravel 30' -13' I It I I I I I I I , D I Memo to File Sigmon's Septic Tank Service January 23. I 998 Page I 0 Time Volume purged 12:00 2 gallons 12: 10 2 gal + 2 liters 12:50 2 gal +8 liters 13:05 2 gal+ IO liters 13:20 Turbidity Conductivity TDS 181 NTU 38. 7 uS at 26.3 C 19.6 mg/I at 24.9 C 75.9 12.3 35.9 at 26.6 18.2 at 25 4.50 35.7 at 23.6 17.9 at 22.8 4.2 36.8 at 27.6 18.7 at 25.4 At 13: I 0, Jeanette collected SS-06-GW. The sample location corresponds to GPS #CO826 I 7B. At 13:20, the pH of the water was measured to be in the range of 5.0 to 6.0, based on the pH paper. Photo #21 was taken. Soil ditch sample SS-11-SL, north of Lauren Drive and west of the culvert inlet, was moved from the original sample plan location because there was minimal flow during the heavy rainfall the prior afternoon. At 13:00, Jeanette collected SS-11-SL in the ditch along Lauren Drive at the southeast corner of the Sigmon property. The sample was a reddish brown loamy clay, collected at a 2 inch depth. The sample location corresponds to G PS #CO826 I 7 A. Photo #22 was taken. At 13:40, Jeanette collected an equipment rinsate blank of the peristaltic pump after rinsing with two liters of deionized water. At 14:00, they drove to the Davidson drinking water wells located by the Davidson Roofing Company business, and began purging the well. Chris Davidson told them that there were two wells side by side to increase the yield. Both were approximately 60 feet deep, 24 inches in diameter, and contained approximately 40 feet of water. The wells serve 4 homes and 8 people. Chris Davidson's address is P.O. Box 5602, Statesville 28687, and 2058 Buffalo Shoals Road, Statesville, 28677. Time 14:30 Turbidity 2.65 NTU Conductivity 40.7 uS at 24.9 C TDS pH 20.6 mg/I at 23.2 C 6 At 14:30, Jeanette collected sample SS-0 I-PW from the wellhead tap located closest to the intersection of Buffalo Shoals Road and Lauren Drive. They drove to the Lamberth well, located on Lamberth Ridge Drive just west of the Sigmon property. At 14:50, well purging began. John Lamberth, 152 Lamberth Ridge Drive, Statesville 28677, was home. The well is a bored well. The well house could not be entered because of the presence of bees. ID I -I I I I I I I , D D m I I " I I Memo to File Sigmon's Septic Tank Service January 23, 1998 Page 11 Time Turbidity 15:10 0.9NTU Conductivity 39.9 uS at 24.3 Sample SS-33-PW was collected at 15: I 0. TDS pH 20.4 mg/I at 22.2 C 6 They drove to the Sheila Tenney/Matt Frye well and began purging the well at 15:20. The well tag provided the following information: Well depth 363 feet Casing depth 43 feet Gravel interval 21 Static water level 40 feet Yield 3 gpm Date completed 7/18/97 Reg.#960 Pump at 280 feet Due to positioning of the faucet at the well head, the sample was collected at the end of the hose. Time Turbidity 15:40 0.48 NTU Conductivity 51.9 uS at 20.6 C Sample SS-34-PW was collected at 15:40. TDS 26.2 mg/I at 19.5 C At 16:20, Doug walked from the Burris residence to the background stream sample location on Norwood Creed to obtain a new GPS reading. The sample location corresponds to CO82620A. At I 6:50, they met Team I at the Sigmon property and left the bolt cutters. They left the site at 17:00. I\ I .. I I I I I I I , I ffl D 0 D m It I I SS-08-SW C082518A SS-08-SD C0825 I 8B SS-07-SW/SD C082519A SS-16-SW /SD C082522A SS-116-SW/SD C082522B SS-17-SW C082523A SS-17-SD C082523B SS-11-SL C082617A SS-06-GW C082617B SS-09-SW/SD C082620A Sigmon Septic Tank Service NCD 062 555 792 OPS Readings August 25 and 26, 1997 80° 58' I 0.0726 35° 42'31.5695 80° 58'07.3031 35° 42'31.0965 80° 59'10.8742 35° 42'30.8135 80° 58'17.7630 35° 43'06.6646 80° 58' 18.2660 35°43'07.7242 80° 58'25.2469 35°43'06.7460 80° 58'23.6189 35° 43'07.1673 80° 58'05. 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