NCD003446721_19960801_Celeanse Corporation - Shelby Fiber_FRBCERCLA RA_OU-1 Semiannual Report January - June 1996-OCR

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Operable Unit 1
Semiannual Report
January 1996 -June 1996
Hoechst Celanese Corporation
Shelby, North Carolina
RE.CEIVED
SEP O 3 1996
SUPERFUND SECTION
Document Control No. 026SB-0051
Submitted to
U.S. Environmental Protection Agency
RegionN
Atlanta, Georgia
Prepared/or
· Hoechst Celanese Corporation
Shelby, North Carolina
August 1996
Kubal-Furr & Associates
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Contents
Page
Introduction . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1
Work Performed ................................................ J
1st Quaner 1996 .............................................. 3
2nd Quarter 1996 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4
System Performance .............................................. 6
Inner and Outer Tier Extraction Rates .. ; ............................. 6
Ground-Water Movement ........................................ 7
Treatment Efficiencies .......................................... 9
Maintenance Activities . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 9
Analytical Test Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 11
Data Quality Assessment . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 11
Discussion of Analytical Test Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 12
Review of Selected Historical Water Quality Data . . . . . . . . . . . . . . . . . . . . . . . 13
Closing Comments .............................................. 16
Tables
Table 1. Sampling Matrix-Hoechst Celanese-Shelby, NC
Table 2. Inner Tier Production Data (Jan '96 -June '96)
Table 3. Outer Tier Production Data (Jan '96 -June '96)
Table 4. Inner/Outer Tier TOC Data (Jan '96 -June '96)
Table 5. Semiannual Maintenance Summary (Jan '96 -June '96)
'
Table 6. Summary of Selected Water Quality Constituents (1st Quarter 1996)
Table 7. Summary of Selected Water Quality Constituents (2nd Quarter 1996)
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Figures
Figure 1. Site Plan Showing Monitoring Locations and Geologic Cross Sections
Figure 2. Potentiomettic Surface Map-Shallow Saprolite---January 15, 1996
Figure 3. Potentiomettic Surface Map-Deep Saprolite/Upper Bedrock-January 15, 1996
Figure 4. Hydrogeologic Cross Section A-A', January 15, 1996
Figure 5. Hydrogeologic Cross Section B-B', January 15, 1996
Figure 6. Potentiomettic Surface Map-Shallow Saprolite---April 15, 1996
Figure 7. Potentiomettic Surface Map-Deep Saprolite/Upper Bedrock-April 15, 1996
Figure 8. Hydrogeologic Cross Section A-A', April 15, 1996
Figure 9. Hydrogeologic Cross Section B-B', April 15, 1996
Attachments
Attachment 1. Operation and Maintenance Data (Jan '96 -June '96)
Attachment 2. QA Summary Repon and Analytical Data for the January 1996 Sampling Event
Attachment 3. QA Summary Repon and Analytical Data for the April 1996 Sampling Event
Attachment 4. Selected Water Quality Plots
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Introduction
Hoechst Celanese Corporation (HCC) is currently operating a long term remedial action
(L TRA) system at its Shelby, North Carolina facility. This system, designated as Operable Unit 1
(OU-1) in the Record of Decision (ROD), consists of two ground-water extraction and treatment
systems identified as the Inner Tier and Outer Tier systems. OU-1 became operational in August
1989.
The OU-1 Inner Tier system was designed to extract contaminated ground water from around a
former source area which was remediated as a separate operable unit (OU-2) with its own ROD.
The Outer Tier system was designed to provide hydraulic control over ground water near the
property boundary to prevent the off-site migration of any constituents from the former OU-2
source area. The location of the Inner and Outer Tier systems, the former OU-2 source area, and
the ground-water monitoring points are shown on Figure I.
In the OU-I Annual Operating Status Report dated September 1995, a recommendation was
made to modify the monitoring locations, frequency and parameter list based on a detailed
evaluation of the water-quality database assembled for the HCC L TRA. This recommendation was
reviewed by the EPA and the State of North Carolina, and approval was given to modify the
sampling matrix beginning with the 1st Quarter of 1996. Approval was also given at the time to
change the reporting frequency from quarterly to semiannually. The current report represents the
second semiannual report prepared under the new reporting schedule and the first since
modification of the sampling matrix.
Kubal-Furr & Associates (KF&A) has prepared this semiannual OU-1 operating summary
report for submittal to the EPA on behalf of HCC. It covers the period from January 1, 1996
through June 30, 1996 and includes information on system performance and the results of
analytical testing of samples collected between January 15-16, 1996 and April 15-16, 1996. A
summary of the significant events occurring during this reporting period include the following:
• A revised sampling and analysis plan, approved by the EPA and State of North Carolina,
was implemented during the 1st Quarter of 1996.
• The Lambert domestic supply well was abandoned at their request on February 19, 1996
and the Runyans domestic supply well was abandoned at their request on April 16, 1996;
Kubal-Furr & Associates/Page 1
OU-1 Semiannual Report (Jan '96-June '96)
Hoechst Celanese Corporalion--Shelby, North Carolina
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therefore, these wells are no longer available for sampling. No volatile organics were
reported as present above the detection limit in either of the samples collected from these
wells just prior to their being plugged. These wells were the last two domestic supply wells
to be plugged back as part of an HCC voluntary initiative to provide surrounding residents
with an alternate source of water.
• Outer Tier well OT-2 continued to experience "sanding" problems related to a separation of
the casing from the screen. This well was abandoned and replaced by OT-2R during the
period April 29-May 2, 1996.
Kubal-Furr & Associates/Page 2
OU-1 Semiannual Report (Jan '96-June '96)
Hoechst Celanese Corporation-Shel/,y. North Carolina
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Work Performed
As pan of the OU-1 remedy, samples are collected at selected monitor wells, domestic supply
wells, and at points in the ground-water treatment system. The frequency of analysis and the
parameters to be analyzed are summarized in the sampling matrix (Table 1). A description of the
work performed during this reporting period is provided below.
1st Quarter 1996
During January 1996, water levels were measured in a total of 91 monitor wells, extraction
wells, and piewmeters. Water~quality samples were collected from 2 domestic supply wells, 13
monitor wells, and 6 process points and analyzed for the parameters summarized in Table 1. The
samples were collected and analyzed by Shealy Environmental Services of Columbia, South
Carolina.
Domestic Supply Well Sampling
The Lambert and Runyans wells were the only domestic supply wells sampled during the 1st
Quaner. These samples were analyzed in the field for pH, temperature, and conductivity; and, by
the laboratory for volatile organics by EPA Method 8260A.
As discussed in earlier operating reports, all neighboring residents downgradient of the HCC
facility were provided with county water during the summer of 1995 as part of a voluntary
initiative undertaken by HCC. By the end of 1995, all domestic supply wells, with the exception of
Lambert and Runyans were plugged back by HCC. (The Elliott and Camp wells represent a special
case and their wells were allowed to remain but their use is reserved exclusively for agricultural
watering)
Monitor Well Sampfing
Thirteen monitor wells were analyzed in the field for pH, temperature and conductance; and, by
the laboratory for volatile organics by EPA Method 8260A. Additionally, samples from monitor
wells K-28 and V-23 were analyzed by the laboratory for TOC by EPA Method 415.1.
Kubal-F"" & Associates/Page 3
OU-1 Semiannual Repon (Jan '96-Jw,e '96)
Hoechst Celanese Corporation-Shelby, Nonh Carolina
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Process Point Sampling
One sample each of SBR (sequencing batch reactor) wasted sludge and FP (filter press) sludge
were analyzed for full TCLP. Samples of Inner Tier (IT) influent and effluent, and Outer Tier (OT)
influent and effluent were collected for analysis of volatile organics by Method 8260A. The Inner
Tier influent and effluent samples were also analyzed by the laboratory for TOC by Method 415.1,
and for ethylene glycol by GC/FID.
During the reporting period, influent and effluent samples from the Inner Tier and the Outer
Tier were also collected by HCC personnel for analysis of TOC by the HCC on-site laboratory.
These samples are collected weekly to evaluate treatment efficiency, and the results are suroroario:ed
in the O&M reports provided in Attachment 1.
2nd Quarter 1996
During April 1996, water levels were measured in a total of 92 monitor wells, extraction
wells, and piezometers. Water-quality samples were collected from 1 domestic supply well, 2
monitor wells, and 2 process points and analyzed for the parameters summarized in Table 1. The
samples were collected by Shealy Environmental Services who also performed the analyses.
Domestic Supply Well Sampling
The Runyans well was the only domestic supply well sampled during the 2nd Quarter.
Between the 1st and 2nd Quarter sampling events (on February 19, 1996) the Lambert well was
plugged back at their request, and was no longer available for sampling. It should be noted that the
Runyans well was plugged back at their request following the 2nd Quarter sampling event (on
April 16, 1996), and this well is no longer available for sampling.
The Runyans well was analyzed in the field for pH, temperature and conductivity; and, by the
laboratory for volatile organics by EPA Method 8260A. The samples were collected and analyzed
by Shealy Environmental Services.
Kubal-Furr & Associates/Page 4
OU-1 Semiannual Report (Jan '96-June '96)
Hoechst Celanese Corporatia11-Shelby, North Carolina
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Monitor Well Sampling
Monitor wells K-28 and V-23 were sampled during the 2nd Quaner sampling event. These
wells were analyzed in the field for pH, temperature and conductivity; and, by the laboratory for
TOC by Method 415.1.
Process Point Sampling
Samples of Inner Tier influent and effluent were collected for analysis of TOC by Method
415.1 and volatile organics by EPA Method 8260A. The Inner Tier influent and effluent samples
were also analyzed for ethylene glycol by GC/FID.
Kubal-Furr & Associates/Page 5
OU-1 Semiannual Report (Jan '96-JUlle '96)
Hoechst Celanese CorporaJion--Shelby, North Carolina
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System Performance
Detailed records of system maintenance are kept by HCC and are summarized monthly. The
monthly records for the current reporting period are contained in Attachment 1. Summaries of
physical operating data for the Inner and Outer Tier extraction well systems are presented in Tables
3 and 4, respectively.
Inner and Outer Tier Extraction Rates
During the reporting period, the Inner Tier wells extracted a total of 488,473 gallons. Inner
Tier flows ranged from a low of 78,144 gallons in May, to a high of 91,116 gallons in January.
Pumping from the Inner Tier wells is limited by the capacity of the SBR treatment system, which is
designed to process about 2500 gallons of water per day. With 182 days in the reporting period,
the optimum pumping from the Inner Tier would have been some 455,000 gallons. Based on the
pumpage during the reporting period, the Inner Tier extraction system was producing at a rate of
about 107% of the optimum rate.
The Outer Tier wells extracted 13,331,398 gallons during the reporting period. The flow from
the Outer Tier system ranged from a low of 2,094,269 gallons in February to a high of 2,326,805
in May. It is important for the Inner Tier system to extract and treat contaminated ground-water at a I rate as near the design capacity as possible due to the lengthy clean-up times involved with the
remedy. The Outer Tier system, however, needs to be evaluated somewhat differently than the
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Inner Tier.
The Outer Tier is extracting water primarily to maintain hydraulic control near the property
boundary in order to prevent off-site migration of former OU-2 source area constituents.
Therefore, the primary evaluation criteria for the Outer Tier system needs to be drawdown along
the perimeter of the site. The actual pumping rates and treatment efficiencies, while providing
useful data, are of lesser importance than the demonstration of hydraulic control. A description of
the techniques used to evaluate the ability of the Outer Tier to control ground-water movement
along the perimeter is described below.
Kubal-Furr & Associates/Page 6
OU-1 Semiannual Report (Jan '96-June '96)
Hoechst Celanese Corporatioll-Shelby, North Carolina
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Ground-Water Movement
The purpose of the OU-1 remedial design was to extract contaminated ground water from the
former OU-2 source area and to provide hydraulic control at the property boundary to prevent the
off-site migration of constituents. Along with the water-quality data, one of the best ways to
evaluate system performance in terms of the above objectives is to construct potentiometric maps
which allow inferences as to the direction of ground-water movement
In order to accurately predict the direction of ground-water movement, water-level
measurements were collected from all accessible monitor wells, extraction wells and piezometers
during each of the 1st and 2nd Quarter sampling events. These data were used to construct the
potentiometric surface maps and hydrogeologic cross sections from the January 15, 1996 water
levels (Figures 2, 3, 4, and 5) and from the April 15, 1996 water levels (Figures 6, 7, 8,and 9).
The shallow saprolite maps (Figures 2 and 6) show the water-level contours and direction of
ground-water movement in the uppermost water-bearing zone beneath the site. The direction of
movement in this zone is to the east from upgradient areas along NC 198, towards discharge areas
along the intermittent, unnamed tributaries of Buffalo Creek. Drawdown and a capture zone are
apparent on these figures situated around the Inner Tier extraction system, along the Outer Tier
system, and in the vicinity of the PEW extraction well system (a non-CERCLA related remediation
project).
An attempt was made to separate the uppermost water-bearing zone from the deeper saprolite
and upper bedrock zone. While these maps (Figures 3 and 7) present a reasonable picture of
ground-water movement in this zone, it should be pointed out that these maps are giving a
somewhat more generalized picture of ground-water movement because of the well construction
techniques used in many of the wells and piezometers. The typical construction of these wells was
to have relatively long screens (20-40 ft) and extremely long sand packs in the annular space above
the screens (up to 60-ft). As a result, the lower saprolite/upper bedrock maps have a number of
composite head values measured along a longer screened area. However, the maps are useful for
determining the general direction of ground-water movement
The lower saprolite/upper bedrock maps show movement toward the east from the upgradient
areas west of the plant These maps also show the drawdowns and capture zones around the PEW
extraction well system in the main part of the plant, and along the Outer Tier extraction well system
Kubal-Furr & Associates/Page 7
OU-1 SerroaMual Report (Jan '96-Jwie '96)
Hoechst Celanese Corporatiol>-Shelby, North Carolina
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along the east propeny boundary. These maps indicate that the Outer Tier system was exerting
hydraulic control along the property boundary during the 1st and 2nd Quarters of 1996 although it
appears that less control, or a loss of control, may have occurred in the vicinity of OT-2 during the
1st Quarter of 1996.
As noted in earlier operational reports, OT-2 has developed problems pumping sand similar to
what occurred at OT-1. This well was abandoned and had to be replaced by OT-2R during the
middle of the 2nd Quarter (April 29-May 2, 1996).
To confirm inferences made about the direction of movement and hydraulic control exerted by
the Inner and Outer Tier systems, two hydrogeologic cross sections each were constructed for the
January and April data sets (Figures 4 and 5, and 8 and 9, respectively). The locations of the cross
sections are shown on the site base map, Figure 1. There is one east-west cross sections (A-A')
constructed through the plant from upgradient areas west of the plant to downgradient, off-site
areas east of the plant. The other cross section (B-B ') is oriented north-south, and is situated along
the Outer Tier extraction well system
The hydrogeologic cross sections are very similar for the two measurement periods and show a
general direction of movement in the saprolite and upper bedrock from upgradient areas west of the
plant toward downgradient areas to the east No appreciable downward hydraulic gradients are
apparent on these maps except in the vicinity of the extraction wells, and the movement in the
saprolite and shallow bedrock is predominantly horizontal across the site.
The Inner Tier capture zone is shown on Figures 4 and 9. These figures show that the Inner
Tier is extracting water from beneath the former OU-2 source area in accordance with the remedial
design. The Outer Tier capture zone is shown on all of the cross sections and it can be inferred to
extend entirely beneath the plant in cross sections A-A'. Cross section B-B' indicates that the Outer
Tier wells are exerting hydraulic control along the eastern propeny boundary from near DD-58 in
the south to near PZ-12 at the northern boundary, with the exception of the January and April data
sets for OT-2 which show control at OT-lR and OT-3, but little to no control at OT-2.
Kubal-F"" & Associates/Page 8
OU-1 Semiannual Report (Jan '96-Jw,e '96)
Hoechst Celanese Corporalion-Shelby, North Carolina
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Treatment Efficiencies
Two aspects of the extraction system performance were reviewed for this annual repon: the
production rates achieved during the year, and the removal efficiencies for TOC from the Inner Tier
and from the Outer Tier systems.
Presented in Table 5 is a summary of the treatment system effectiveness of the Inner Tier and
of the Outer Tier in removing TOC during the reponing period. These summaries were prepared
from the water-quality data collected weekly by the HCC on-site laboratory as presented in the
monthly operating summaries (Attachment 1).
During the reponing period, the Inner Tier average removal efficiency for TOC was 96%, with
an average influent concentration of 18 IO ppm (parts per million), and an average effluent
concentration of 74 ppm. Removal rates for TOC from the Outer Tier treatment system were
calculated to be 37%, lower than the Inner Tier but in keeping with historical values. The average
influent concentration during the reporting period was 5.6 ppm, and the average effluent
concentration was 3.5 ppm. The percent reduction ofTOC through the Outer Tier treatment system
is not as high as that for the Inner Tier because of the much lower Outer Tier influent TOC. The
Outer Tier appears to be reducing TOC as well as can be expected.
Maintenance Activities
Low flow from the Inner Tier wells is a chronic problem requiring frequent maintenance. The
actions taken to rectify the low flow problems consisted of replacing bladders, timers, air lines and
such, adjusting the controls and flow rates, and cleaning the strainers. Specific actions taken at
individual wells during the reporting period are contained in the monthly operating summaries
(Anachment 1).
A summary of Inner Tier maintenance incidents is summarized in Table 5. Replacing bladders
at the IT wells was the most frequent maintenance activity during the reponing period, with IT-5
requiring 3 bladder replacements. IT-SR experienced the most frequent number of maintenance
activities, principally related to problems with the Hammerhead pump. This pump problem has
been noted in earlier operational repons as well.
Kubal-Furr & Associates/Page 9
OU-1 Semiannual Report (Jan '96--JUlle '96)
Hoechst Celanese Corporation-Shelby, North Carolina
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No unusual operational problems were experienced during the reporting period in the Outer
Tier recovery well system with the exception of wells OT-IR and OT-2. Replacement well OT-IR
experienced the most numerous maintenance requests followed by OT-2. Cleaning the strainer was
the most frequent maintenance request during the reporting period, principally at wells OT-IR and
OT-2.
As noted earlier, well OT-2 began to experience problems similar to old well OT-1 (i.e.,
pumping sand) during August of 1995. This well appears to have separated between the casing and
screen due to a galvanic reaction between the carbon steel casing and the stainless steel screen,
allowing formation material and sand pack to enter the well. The sanding problem at OT-2 has
recurred on several occasions and it had to be replaced during the middle of the 2nd Quarter of
1996.
Kubal-Furr & Associates/Page 10
OU-1 Semiannual Report (](Jll '96-June '96)
HMchst Celanese Corporatioll--Shel/Jy, Nonh Carolina
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Analytical Test Results
The analytical test results for the 1st and 2nd Quarter sampling events were evaluated using
method specific quality control criteria and, for additional guidance when necessary, the EPA' s
National Functional Guidelines for organic and inorganic data review. The data assessment
su=ary repon for the 1st Quaner sample set is presented in Attachment 2 along with the
analytical test results, field sampling logs, water-level measurements, and chain-of-custody forms.
Similar information for the 2nd Quarter data set is contained in Attachment 3. A su=ary of
selected analytical data for the 1st and 2nd Quaners is presented in Tables 6 and 7, respectively.
Data Quality Assessment
Regarding sample collection, the sampling logs and field information provided was complete.
The chains of custody were incomplete with respect to site specific information concerning client
information, etc. These deficiencies did not compromise the data quality but they will be corrected
in future sampling events.
All TOC data and ethylene glycol test results for the 1st and 2nd Quaners met all method
acceptance criteria and are considered useable for quantitative purposes. During the 2nd Quaner,
acetone and 2-butanone were reponed as present in the field blank. However, the samples
associated with this field blank did not require data flags based on their reponed concentrations.
Therefore, all VOC data met the method acceptance criteria and is considered useable for
quantitative purposes.
The only data needing qualification were the metals barium and mercury for the TCLP tests run
on the Filter Press and SBR sludge samples. In the case of barium, the digested metals blank
contained 0.009 mg/L barium, most likely due to the TCLP filter. All barium results greater than
the quantitation limit but less than 0.09 mg/L were flagged with a "U'' (as non-detect, because of
the presence in the blank). All mercury test results are considered unusable and were flagged "R"
because the test results were obtained without running a daily calibration curve as stated in the
method.
Kubal-Furr & Associates/Page 11
OU-1 Semiannual Report (Jan '96-June '96)
Hoechst Celanese Corporation--Shelby, North Carolina
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Discussion of Analytical Test Results
Domestic Supply Wells
No volatile organics were reponed as present above the detection levels during the 1st or 2nd
Quarters at either of the two domestic supply wells (i.e. Lamben and Runyans) sampled during the
reponing period. As noted in an earlier section, these data represent the final sampling to be
conducted at these two supply wells. The Lamben and Runyans wells were plugged back at their
request during the reponing period and are no longer available for sampling.
Monitor Wells
Of the 13 monitor well samples analyzed during the reporting period, only 5 had any volatile
organics reponed above the detection level. Of these five, only one (V-23) had more than one
individual constituent reponed as present above the detection level.
Monitor well V-23, located downgradient of the former OU-2 source area and just upgradient
of the Inner Tier extraction system, reponedly contained acetone (487 µg/L), benzene (19.3 µg/L),
2-butanone (MEK) (3600 µg/L), carbon disulfide (49 µg/L) and 2-hexanone (282 µg/L). CC-33
and K-28, adjacent to and just downgradient of the former OU-2 source area, reportedly contained
benzene at 10 µg/L and 8.6 µg/L, respectively. Monitor wells HH-48 and HH-77, off-site and
adjacent to the Elliott residence, reponedly contained trichlorothene (TCE) at concentrations of 165
µg/L and 187 µg/L, respectively. Toe presence ofTCE at this location is thought to be the result of
a localized source, unrelated to activities at HCC or the former OU-2 source area.
Monitor wells K-28 and V-23 were also analyzed for TOC during the 1st and 2nd Quarters.
The K-28 test results were similar for the 1st and 2nd Quarters at 222 and 40 mg/L, respectively.
The TOC test results for V-23 were noted to increase from 1237 mg/L to 6100 mg/L during the 1st
and 2nd Quarters.
Process Point Samples
Inner Tier influent and effluent samples were analyzed during the 1st and 2nd Quarters for
ethylene glycol, TOC, and volatile organics. All volatiles in the Inner Tier effluent sample were
below the detection levels. Toe 1st Quarter Inner Tier influent sample reponedly contained the
Kubal-Furr & Associates/Page 12
OU-1 Semiannual Report (Jan '96-June '96)
Hoechst Celanese Corporatiol>--Shelby, North Carolina
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volatiles acetone (342 µg/L), benzene (18.3 µg/L), MEK (352 µg/L), and chlorobenzene (8.8
µg/L). The 2nd Quarter Inner Tier influent sample reportedly contained the volatiles acetone (645
µg/L), benzene (58.5 µg/L), MEK (537 µg/L), carbon disulfide (12.1 µg/L), chlorobenzene (41.1
µg/L), and 2-hexanone (193 µg/L).
TOC test results for both the Inner Tier influent and effluent samples were similar for the 1st
and 2nd Quarter data sets. Inner Tier influent TOC was reported at 1614 mg/Land 1600 mg/L for
the 1st and 2nd Quarters, respectively. Inner Tier effluent TOC was reported at 50 mg/Land 31
mg/L for the !st and 2nd Quarters, respectively.
Two other process point samples were analyzed during the 1st Quarter sampling event. These
included full-TCLP analyses of the FP (filter press) and SBR sludge samples. The constituent
reported .above the detection limits (i.e., barium) was below any applicable State or Federal
regulatory level, and the sludge would not be considered characteristically hazardous, nor would
there be any restriction on disposal into a North Carolina landfill based on the TCLP test results.
Review of Selected Historical Water Quality Data
Attachment 4 contains plots of selected water quality constituents for various monitor wells and
process points. The choice of locations and constituents was based on a review of the water quality
database, in particular those locations having any meaningful data to plot In general, only those
monitoring locations within a few hundred feet of the former OU-2 source area have any
significant number of water quality constituents reported above the detection limits. In an attempt to
assess long-term improvement in water quality conditions resulting from source removal and
ground water recovery, the following locations and constituents were selected:
• Inner Tier Combined Influent TOC and ethylene glycol test results. The Inner Tier TOC
continues to fluctuate in a fairly narrow range of from 1500 to 2500 mg/L, and no long-
term trends have been established. However, during the past year, the TOC results have
been trending downward and may be an early indication of some gradual improvement in
water quality conditions. Similarly, the Inner Tier ethylene glycol data have established an
apparent downward trend although the database is much smaller than the TOC database and
contains several qualified data points.
Kubal-Furr & Associates/Page 13
OU-1 Semiannual Report (Jan '96-June '96)
Hoechst Celanese Corporation--She/by, North Carolina
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• Monitor Well V-23 TOC, 2-butanone (MEK), and acetone. An attempt to plot benzene did
not provide any useful information because more than half the benzene data for V-23 are
either below the detection levels or qualified as estimated
The V-23 TOC data began trending downward from a high of 8000 mg/Lin mid-1989 to
less than 1000 mg/Lin early 1992. Since that time, the TOC data has shown several wide
swings in concentration, and at the present time, no trend has established itself during the
past several years.
The V-23 MEK data have generally fluctuated in a narrow range less than 1 mg/L, with 10
of 23 data points below the detection level. The 1st Quarter data showed a spike for MEK
at 3.6 mg/L. Because the previous quarter's sample was greater than the reported value of
0.767 mg/L (qualified because the test result was out of linear range), it indicates an
increase in MEK concentrations at this location but it's not apparent whether this trend will
continue with the next sample set
The V-23 acetone test results have generally fluctuated in a narrow range below 0.6 mg/L
since 1989. No apparent trend has been established from the reported acetone test results at
this monitoring location.
• Monitor well CC-33 benzene and chlorobenzene data. The water quality plots for monitor
well CC-33, just south of the Inner Tier capture zone, has shown a continual improvement
in water quality conditions as indicated by these two constituents. In the case of
chlorobenzene, this improvement began in late 1989, just after start up of the Inner Tier
extraction system. Both· benzene and chlorobenzene peaked at about the mid-point in the
OU-2 remediation (late 1991), and have continued to decline since that time.
• Monitor well K-28 TOC, MEK, acetone and benzene data. TOC, MEK and acetone have
all shown a decrease in concentration beginning about the time the OU-2 source
remediation began in January of 1991. While benzene has also shown a decline during this
period, this trend is not as readily apparent, and for the past three years benzene has been
fluctuating in a range of from 0.01 to 0.02 mg/L.
• Monitor well HH-48 and Illi-77 TCE data. The Illi-48 TCE test results have generally
fluctuated in a narrow range of from 0.15 to 0.25 mg/L during the past six years, and no
Kubal-Furr & Associates/Page 14
OU-1 Semiannual Report (Jan '96-June '96)
Hoechst Celanese Corporatio,......She/by, North Carolina
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apparent trend is evident in the water quality plots. HH-77 had been fluctuating in the range
of 0.05 to 0.15 mg/L until the August 1995 sampling event when it peaked at 0.332 mg/L.
Toe subsequent sample for HH-77 was below 0.2 mg/L, and it's not apparent if an upward
trend will continue at this monitoring location. As noted in an earlier section, the TCE
contamination in this area appears to be due to a localized source and not related to past
activities at HCC.
Kubal-F"" & Associates/Page 15
OU-1 Semiannual Report (Jan '96-June '96)
Hoechst Celanese Corporatioll--She/1:,y, North Carolina
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Closing Comments
The extraction well production data and the analytical test results for the domestic supply wells,
the monitor wells and process points were generally found to be consistent with historical
information, and no unusual or unsuspected contamination was identified during the reporting
period. Treatment efficiencies at the Inner Tier for removal of TOC remained consistently greater
than 90%, and no volatiles were detected in either the 1st or 2nd Quarter Inner Tier effluent
samples. TCLP test results for the SBR sludge and FP sludge samples were found to be below any
applicable State or Federal regulatory level; the samples were not characteristically hazardous and
are suitable for disposal at a North Carolina landfill site without further treatment.
The present report represents the second semiannual report prepared under a revised sampling,
analysis and reporting schedule approved by the EPA during its review of the OU-1 Annual Report
(August 1995). A revised sampling matrix, approved by the EPA and the State of North Carolina,
was implemented beginning with the 1st Quarter sampling event of this reporting period. The next
sampling events are scheduled for July and October of 1996, with the next scheduled semiannual
report to be submitted to the agency by March 1, 1997.
Kubal-Furr & Associates/Page 16
OU-1 SemiaMual Repon (Jan '96-June '96)
Hoechst Celanese Corporaliort-Shelby, North Carolina
-- - - - - - - - --- -- - - - - -
Table 1. Sampling Matrix-Hoechst Celanese-Shelby
1st Quarter 2nd Quarter 3rd Quarter 4th Quarter
Monllorlng TOO voe Eth. Glycol TOO voe Eth. Glycol TOO voe Eth. Glycol roe voe Eth. Glycol
Location (415.1) (8260) (GCIFID) (415.1) (8260) (GCIFID) (415.1) (8260) (GCIFID) (415.1) (8260) (GC/FID)
PtOCBSS Points
ITCI -I -I -I -I -I -I -J -J -J -J -J -I
ITEF -I -J -I -I -I -I -I -J -I -I -I -I
OTCI -I -I
OIEF -J -I
SBRSIJdge (Full TCLP)
FP Sludge (FullTCLP)
Morrlor Wells
C-49 -J -J
K-28 -J -J -J -I -J -I
P-58 -I -I
T-35 -I -I
V-23 -I -I -I -I -I -I
AA-54 -I -I
CC-33 -J -J
EE-58 -J -I
FF-34 -I -J
FF-62 -I -I
GG-61 -I -I
HH-48 -I -I
HH-n -I -I
Domestic Suee!l, Wells
Lambert11 -I
Aunyans21 -I -I
Notes: 1 / Lambert Well abandoned on February 19, 1996.
2/ Aunyans welt abandoned on April 16, 1996
J/oechst Celanes~helby, NC
OU-1 Semiannual Report (Jan '96 -June '96)
--
_!!!!_
IT-1
IT•2
IT•3
IT-4
IT~
IT-8
IT-7
IT-all
IT-9
• ADF:
- - - - -- ---
Table 2. Inner Tier Production Data
Jan '96 -June '96
Hoechst Celanese Corporadon---Shslby, NC
January 1898 February 1996 March 1990 Aprll 1998
Total Total Total Total
Gallons ~ Gallons ~ Gallon• ~ Gallons ~
5,576 180 5,242 181 8,581 212 5,489 183
1,770 57 2,254 78 2,188 70 2,210 74
3 860 125 3 077 106 4 559 147 3 291 110
1,881 80 3,023 104 2,307 74 3,822 127
11,721 378 11,857 402 9,940 321 8,902 230
4 804 149 4 851 180 4 754 153 4 284 143
4,751 153 3,981 137 6,333 204 5,848 195
37,150 1,198 27,425 840 28,097 842 24,825 831
191823 839 17 492 803 181873 809 221eas 782
81, 1111 78,782 81,110 79,834
Average Delly Aow baaed on HCC production records {Attachment 1),
Ca)culated ae mtaJ flow clvkiad by the number ot days In the month.
- --
May 1998
Total
Gallon• ADP
4,547 147
1,808 58
1 955 83
3,541 114
8,328 289
4 083 132
5,514 178
28,079 881
21 891 700
78,144
----
June 1998 Jan.June '96
Total
Gallons ~ Tolal Gallon•
4,563 152 31,998
1,558 52 11,784
2 880 •• 19 72!!_
2,288 78 U,820
11,052 388 ae,aoo
3 382 113 2a 1aa
5,299 177 31,708
32,908 1,097 175,182
15 181 508 1111,823
78,187 488,473
1/oechsl Cela.nese-SMlby, NC
OU-1 Semiannual Report (Jan '96 -June '96)
-
--- - ---
Janua!I 1996 Febru!!! 1996
Total Total
Well Gallons ADF' Gallons ADP
OT·1R 574,000 18,516 531,600 18,331
OT•2(R) 462,100 14,906 474,100 16,348
OT-3 56 107 1 810 60 384 2 082
OT-4 35,072 1 I 131 34,241 1. 181
OT-5 51,458 1,880 88,840 2,298
OT-II 143 161 4 618 184 421 e 359
OHA 222,870 7,189 198,554 8,847
OT-7 81,428 2,827 77,729 2,880
OT-II 5701900 18,418 466 600 18,090
2,197,092 2,094,289
• ADF: Ava,age Dally Aow baaed on HCC production rec:ords (Attachment 1),
Calculated aa total now divided by the number of days In the monlh.
-- - - -
Table 3. Outer Tier Production Data
Jan '96 -June '96
Hoechst Celanese CorporsUon-Shelby, NC
March 1996 Aprtl 1996
Total Total
Gallons ADP Gallons ADF'
519,900 16,771 48-4,500 16,150
592,200 19,103 549,800 18,320
67 337 2 172 85 358 2 179
41,502 1,339 38,881 1,229
82,733 2,889 78,931 2,631
181 774 5 864 205 532 6 851
194,234 8,288 195,014 6,500
84,377 2,722 82,025 2,734
5591300 18,042 -4851800 15,530
2,323,357 2,183,741
--
•i 1996
Total
Gallons ADF'
820,100 20,003
503,700 16,248
35 339 1 140
39,909 1,287
84,328 2,075
220 779 7 122
207,110 6,681
77,640 2,505
5571900 17,897
2,320,8015
- -- -
June 1996 Jan.Jun• '96
Total Total
Gallons ADP Gollona
591,600 19,720 3,321,700
342,800 11,427 2,924,500
61 309 20.U 345 834
40,873 1,362 228,478
82,642 2,088 406,730
22.§. 379 7 513 1 161 046
266,531 8,884 1,284,313
80,900 2,897 484,097
554 100 18,470 3 174 700
2,228,134 13,331,398
Jloechsl Cekmese-She/by, NC
OU-1 Semiannual Report (Jo.n '96 • June '96)
-
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Table 4. Inner/Outer Tier TOC Data
I January '96 -June '96
Hoechst Celanese Corporation-Shelby, North Carolina
I
(all results reported In mg/L)
Inner Tier Outer Tier
I Influent Effluent %Reduction Influent Effluent % Reduction
Date
I 1/1/96 1428 18.4 99 7 2.6 63 ......... ,_
1/10/96 2707 276.9 90 6 4.1 32
I 1 /15/96 2492 259.7 90 7 6.1 13
1 /22/96 2249 36 98 6 3.3 45 ..
1 /29/96 1854 215.3 88 7 4.2 40
I 2/5/96 1861 75 96 6.1 4.1 33
2/12/96 2083 165.8 92 7.2 5.2 28
2/1 9/96 2275 20.1 99 3.1 2.2 29
I 2/26/96 1570 112.6 93 4.1 5.3
3/6/96 2135 __ 18 99 3.3 3 9 .............. , .. ,_
3/13/96 1424 50 96 5 3 40
I 3/1 9/96 1885 41 98 3 3 0
3/26/96 1538 83 95 5 7 -·--4/1 /96 1333 36 97 3 2 33
I 4/8/96 1309 24 98 5 5 0
4/16/96 1570 45 97 3 2 33
4/22/96 1747 32 98 17 3 82
I 4/29/96 1881 31 98. 8 4 50
5/6/96 1718 1 .. 67 ---~-Q __ 7 6 14
5/13/96 1333 21 98 3 3 0
I 5/22/96 1613 57 96 5 2 60
5/28/96 1778 32 98 3 3 0
6/4/96 1337 10 99 5 3 40
I 6/11 /96 1378 46 97 3 2 33
6/1 8/96 2428 27 99 6 3 50
6/26/96 2126 12 99 5 5 0
I Average: 1810 74 96 5.6 3.5 37
I Note: Outer Tier Average Influent, Effluent, and Percent Reduction do not include 2/26/96 or 3/26/96 data.
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OU-I Semiannual Report (Jan '96 -June '96)
-------------------
Location ID
IT-1
IT-2
IT-3
IT-4
IT-5
IT-6
Table 5. Semiannual Maintenance Summary-1st/2nd Quarter 1996
(Number of Incidents Reported)
Adj Flow/
Strainer Pump Flow Meter Bladder Other
1 1
1 2 1 ........... ,_,, ......
1 2
3
Total
Incidents
2
0
4
3
3
0 -········'"·········· .. IT-7
IT-SR 2 4 2
IT-9 1
Total Incidents: 3 5 2
OT-1R 5 1 1
OT-2/R 4 1
OT-3
OT-4
OT-5 1
OT-6 1
OT-6A 1 2
OT-7
OT-8
Total Incidents: 10 1 6
1
8
N/A
N/A
N/A
NIA
NIA
N/A
N/A
N/A
NIA
N/A
1
8
3 4
7 25
2 9
2 7
0
1 1
1
1
1 4
0
0
6 23
1/oechst Celanese-Shelby, NC
OU-1 Semiannual Report (Jan '96 -June '96)
-------------------
Table 6. Sumn:iary of Selected Water Quality Constituents (1st Quarter 1996)
C-33 K-28 V-23
Total Organic Carbon (mg/L) NA 22 1237
Ethylene glycol (mg/L) NA NA NA
VofaUfe Organics tuq1u
Acetone ND ND 487
Benzene 10 8.6 19.3
2-butanone (MEK) ND ND 3600
Carbon disulfide ND ND 49
Chlorobenzene ND ND ND
2-hexanone ND ND 282
Trichloroethane ND ND ND
Notes: ND = Constituent not detected/reported as below the detection level
NA = Sample not analyzed for indicated constituent(s)
HH-48
NA
NA
ND
ND
ND
ND
ND
ND
165
HH-77 ITCI ITEF
NA 1614 50
NA 11 00 ND
ND 342 ND
ND 18.3 ND
ND 352 ND
ND ND ND
ND 8.8 ND
ND ND ND
187 ND ND
lloechst Celanese-She/by, NC
OU-/ Semiannual Report (Jan '96 -June '96)
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Table 7. Summary of Selected Water Quality Constituents
(2nd Quarter 1996)
K-28 V-23 ITCI
Total Organic Carbon (mg/L) 40 6100 1600
Ethylene glycol (mg/L) NA NA 1070
Volatile Organics fuq/L/ NA NA
Acetone 645
Benzene 58.5
2-butanone (MEK) 537
Carbon disulfide 12 .1
Chlorobenzene 41.1
2-hexanone 193
Trichloroethene ND
Notes: ND = Constituent not detected/reported as below the detection level
NA = Sample not analyzed for indicated constituent(s)
ITEF
31
ND
ND
ND
ND
ND
ND
ND
ND
Hoechst Celanese-Shelby, NC
OU-1 Semiannual Report (Jan '96 -June '96)
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• Monitor well
o Monitor well cluster
Legend ...
....
+ Inner ner Extraction Well --I
e A-39
PEW Extraction Well
Piezometer
Stream/Creek
♦ Outer ner Extraction Well 1!11!1 HCC Building/Structure
o Domestic Supply Well ♦ Abandoned Outer ner Well
• Abandoned Inner ner Well A-A' Location of geologic cross-sections
_,
~
Kubal-Furr & Associates
-Environmental Consultants-
--Ai --' --~
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' \
~
-----~ ---
Scale in Feet
0 400
Figure I. Site Pl~n
Hoechst Celanese Corporation
Shelby, North Carolina
800
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.------------------------::---------:------------=--=--=----=----_-_-_-,
B 0
830
BOO ,
111 ___ ,._ ____ ,,
Legend --• Monitor well I Stream/Creek
Water Level (fl msl)
0 Monitor Well Cluster -HCC Bulldlng/Slructure
.... Plezorneter / Water-Level Contour 750
Inner Tier Extraction Well I (Dashed where Inferred) + (See Table for Water Levels) -+-PEW Extraction Well
♦ Outer Tier Extraction Well
• , 770
~
770 T-17
764.13
750
G
~·1 Crotts
" \\
Kubal-Furr & Associates
-Environmental Consultants-
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Inner Tier Water Levels
IT-I = 792.15
IT-2 = 795.18
IT-3 = 794.66
IT-4 = SA
IT-5 = 788.6-l
IT-6 = 781.90
IT-7 = 789.88
IT-SR = 791.10
IT-9 = <797.73
Outer Tier W atcr Levels
OT-IR = 755.94
OT-2 = 763.61
OT-3 = 745.03
OT-4 = 741.63
OT-5 = 744.75
OT -6 = 729.45
OT -6A = 729.38
OT-7 = 729.98
OT-7A = 773.96
OT-8 = 760.81
OT-10 = 779.07
PEW Water Levels
PEW-I = 769.25
PEW-2 = 788.69
PEW-3 = 801.60
PEW-4 = 806.82
\
Figure 2. Potentiometric Surface Map
Shallow Saprolite -January 15, 1996
(See Table for Water Levels) " Domestic Supply Well
Hoechst Celanese Corporation
IL.::;;;;;;:;;;;:;;;;:;;;;:;;;;:;;;;:;;;;:;;;;:;;;;:;;;;:;;;;:;;;;:;;;;:;;;;;;;;;;;:;;;;:;;;;:;;;;:;;;;:;;;;:;;;;:;;;:_ ________________ ....1 _______________ ..J, _______ s_h_e_Ib.;,.y_, N_orth __ c_aro_Ii_n_a _____ .....,
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--
i ', \ \
i ·.
---------
~ -:.--
-.:-0
_,
-
!:,:: .
_ • Monitor well
Water Level (ft msl)
o Monitor Well Cluster
♦ Outer Tier Extraction Well
/,
750 Water-Level Contour
1 (Dashed where inferred)
.._ Piezometer
--, Stream/Creek
Ill HCC Building/StructUre
Kubal-Furr & Associates
-Environmental Consultants-
/
0
Scale in Feet
400 800
Figure 3_ Potentiometric Sunace Map
Deep Saprolite / Upper Bedrock -January 15. 1996
Hoechst Celanese Corporation
Shelby, North Carolina
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850.00 o--------Piant Area----------0------------------Wastewater Trestment Area----------------◄
830.00
810.00
790.00
770.00
D-'.!7
(829.20)
D-35
(828.95)
D-56
(828.71)
750.00 C
730.00 -
710.00
69000
Potenciometric Surface -Inferred direction of ground-water movement
Inferred capture zone-Outer Tier Wells
* Not used in contouring
---, ---' Saprolite
G-50
(809.13)
Screened Interval of Well
T
• • J-28
(805.14)
• •
Kubal-Furr & Associates
-Environmental Consultants-
LAND
SURFACE
850.00
..: 830.00
~ 810.00
790.00
770.00
A'
1 750.00
730.00
710.00
" 690.00
C 670.QO
Figure 4. Hydrogeologic Cross-Section A-A'
January 15, 1996
Hoechst Celanese Corporation
Shelby, North Carolina
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830.00
810.00
790.00
no.oo
750.00
730.00
710.00
690.00
I I i
I !
I i
' L
;
I I
,-
;
' c
i I
' I i '
r
760
Line of equal fluid potential (ft msl). Dashed
where inferred.
Potentiometric Surface
' Inferred direction of ground-water movement
Not used in contouring
Bedrock
,---, . ___ , Saprolitc
Screened Interval of Well
LAND
SURFACE Of-4
Kubal-Furr & Associates
-Environmental Consultants-
-I 830.00
J
i J '
810.00
790.00
no.oo
750.00
730.00
710.00
690.00
670.00
Figure 5. Hydrogeologic Cross-Section 8-8'
January 15, 1996
Hoechst Celanese Corporation
Shelby, North Carolina
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850 840 830
820 • A-39 814.00
810 800
\\~'.,=2 .\\~L:~:~~1:~~::~j=~~F~====:::::==:~=,g"=":=±+=:::::--...'i
' ~
790
\\\ J\\ /,---\ \ \ --+----
\\\ • --t----f I \\ \ \ ---+---;\ \, ', ~'<----• -\', \ '
C ,...\\\ '\ --JI-----
--!'•.
0 \ \\ \ +-----
.[_: \ \ \ ) r--------
·, \ \
. \ I ' . I \
· .. c\ \
·.<JI ' \:i:\ \_ \~\ .'.
'-' \ \
Legend
-----
780
-' • Monitor well I Stream/Creek ~
Water Level (ft msl)
0 Monitor Well Cluster 11111 HCC BulldlnglStructure
A Plezometer / Water-Leve! Contour 750
Inner Tier Extraction Well I (Dashed where inferred) + (See Table for Water Levels) -+-PEW Extraction Well
♦ Outer ner Extraction Well
(See Table for Water Levels) C Domestic Supply Well
00-see1
\ Crotts le
\ \\
Kubal-Furr & Associates
-Environmental Consultants-
0
Inner Tier Water Levels
IT -I = 785.42
IT-2 = 785 . .50
IT-3 = 783.78
IT~ = 78-tl9
IT-5 =
IT-o =
IT-7 =
IT-SR =
IT-9 =
793.93
781.98
786.09
789.94
<783.75
Outer Tier Water Le .. ·els
OT-IR = 758.54
= 761.91
= 728.73
= 747.80
= 738.05
= 739.00
OT-2
OT-3
OT-4
OT-5
OT-o
OT-oA =
OT-7 =
OT-7A =
OT-8 =
OT-10 =
Scale in Feet
400
735.63
730.98
773.68
765.03
779.60
800
Figure 6. Potentiomenic Surface Map
Shallow Saprolite -April 15, 1996
Hoechst Celanese Corporation
Shelby, North Carolina
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' \ \ . \~\\=='. \t\ \-==• S\\_j-I
\ • ,1
I
/
,,,,.-
/
' _ ,,,_ ---
/ -
810
Legend
• Monitor wet
Water Level(ft mal)
o Monitor Wei Cluster
♦ OUter Tier Exb&Cllon Wei
1fi' Waler-Level Contour
I (Cashed where b,fe11ed)
a Do.uewac ~ Wei
♦ PEW Exlrac1lon Wei
A PlezoitW,tei
-~. Sbean~c•
• HCC BulldlnglStJuc1
830
-_, , '
' '
, _____ ..
rC·~•-.~ · soo:::::~::=:,':",
i:i: .... :,.'
,
, --
,
' '
-----
750
I
' '
'
0
,, 720
730
----
' I
Scale In Feet
400
---
--- -
,,JP r "---~~:-
____ ___.:...u..._....:.. ___ __, ______________ ---1
Kubal-Furr & Associates
-Environmental Consultants-
Figure 7. Potentiometric Surface Map
Deep Saprolite / Upper Bedrock -,.\pril 15, 1996
Hoechst Celanese Corporation
Shelby, North Carolina
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850.00 -
830.00 "
810.00
790.00
770.00 r C
750.00;
i
730.00 -
710.00 r
690 00 -
-
oooao
---------Plant Area-----------
D-'.27
(830.41)
D-35
(830.21)
D-56
(830.09)
* Not used in contouring
--------------------Wastewater Treatment Area----------------
G-50
(809.40)
-Environmental Consultants-
LAND
SURFA·:E
C 850.00
830.00
810.00
790.00
770.00
A'
.:. 750.00
-730.00
-
710.00
690.00
: 670.00
Hoechst Celanese Corporation
Shelby. Nonh Carolina
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830.00
810.00
i
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8
790.00
[
770.00
;-
I
' I
' ' ' I
'
750.00 ,-
i
730.00 ;
' t
i !
c
710.00
690.00
l '
Line of equal fluid potential (ft msl). Dashed
where inferred.
• Potentiometric Surface -Inferred direction of ground-water movement
Not used in contouring
I I
T-17
(764.51)
Saprolite
Screened Interval of Well
LAND
SURFACE
750
Kubal-Furr & Associates
-Environmental Consultants-
750
830.00
810.00
790.00
770.00
750.00
730.00
710.00
690.00
670.00
Figure 9. Hydrogeologic Cross-Section B-B'
April 15, I 996
Hoechst Celanese Corporation
Shelby, North Carolina
I January WELLS3.WK1
JANUARY
I i 996: IT-1 IT-2 IT-3 IT-4 IT-5 IT-6 IT-7 IT-8 IT-9
01/01/96 0 50 0 43 428 107 11 0 1094 581 I 01/02/96 0 57 o 29 490 134 140 1245 780
01/03/96 11 3 55 0 22 338 139 150 1295 810
01/04/9 6 0 46 0 1 1 229 11 9 1 .13 1082 5978 I 01/05/96 229 50 96 1 6 447 134 149 1146 658 01/06/96 INCLEt'v1ENT WEATHER NO READINGS 5 INCHES SLEET & SNOW
I 01/07/96 425 101 214 41 968 267 293 2289 1163
01/08/96 220 57 11 8 21 0 158 156 1251 661
01/09/96 196 50 1 1 1 1 5 456 159 152 1205 482
I 01/~')/96 209 54 122 7 266 166 159 1291 507
01/11/96 192 50 11 0 1 5 205 147 143 1208 593
01/12/96 188 47 11 3 · 1 6 307 138 150 1186 601
I 01/13/96 182 49 121 1 7 325 143 143 1188 465
01/14/96 1 91 47 176 1 7 425 144 149 1225 403
01/15/96 227 47 1 21 20 460 147 152 1268 319
I 0 1 / 1 6 /9 6 235 57 291 136 592 167 160 108 210
01/17/96 237 63 177 127 643 182 228 1401 95
01/18/96 237 68 2d2 0 611 179 1 91 1471 108
I 01/19/96 217 64 201 288 235 169 175 1358 178
01/20/96 233 75 152 96 232 193 196 1508 86
01/21/96 211 68 142 84 180 181 1 91 1440 1 2
I 01/22/96 223 73 145 88 310 195 202 151 9 4
01/23/96 218 74 143 68 623 191 205 1557 0
01/24/96 207 72 137 70 417 1 78 139 121 8 758 I 01/25/96 185 57 11 3 59 248 130 138 1255 691
01 /26/96 1 78 52 155 128 429 11 9 129 1137 624
01/27/96 1 71 50 156 129 348 11 4 11 1 964 569 I 01/28/96 176 59 1 21 76 277 126 129 1099 653
01 /29/96 164 57 92 75 415 11 9 109 1029 609
01/30/96 170 62 163· 79 432 139 111 1122 655 I 01/31/96 142 59 128 68 385 120 98 991 570
I AVG: 186 57 129 62 391 153 158 1238 661
I TOT: 5576 1770 3860 1861 11721 4604 4751 37150 19823
I
I
I OUTER TIER DAILY FLOW
Page 5 of 9 I
I January WELLS3.WK1
I JANUARY
1996: OT-1 OT-2 OT-3 OT-4 OT-5 OT-6 OT-6A OT-7 OT-8 I 01/01/96 30700 100 2187 1068 2143 3375 9238 2606 24800 01/02/96 17300 17100 1744 1082 1618 3026 6966 2641 18200 I 01/03/96 16300 18900 1723 1090 1589 3386 6942 2650 . 1 7300
01/04/96 17200 17300 1770 1072 1 611 3267 7011 2618 17600
I 01/05/96 19500 14600 1904 1090 1667 3224 7387 2630 18800
01/06/96 INCLEMENT' WEATHER NO READINGS 5 INCHES SLEET & SNOW
01/07/96 40500 20100 4007 2288 3376 6887 15431 5538 39300
I 01/08/96 17000 0 1722 971 1443 3227 6568 2332 16900
01/09/96 16500 17500 1772 1074 1498 3842 7101 2648 18500
01/10/96 16400 18000 1781 1069 1520 5100 7030 2624 18500 I 01/11/96 16500 18000 1785 1086 1593 7309 7001 2628 18500
01/12/96 16600 18600 1816 1110 1667 7814 6903 2628 18700
01/13/96 16500 17100 1800 1087 1591 6315 7029 2584 18500 I 01/14/96 16600 17900 1813 1130 1558 5147 7279 2597 18800
01/15/96 16500 17900 1808 1150 1587 4547 7019 2619 18700
01/16/96 16000 17300 1743 1144 1552 4284 6931 2603 17700 I 01/17/96 15300 17400 1680 1149 1520 4134 6756 2606 17300
01/18/96 16000 18400 1748 1152 1564 4010 7057 2618 17700
01/19/96 17300 17700 1715 11 61 1572 3757 6992 2655 17700 I 01/20/96 17500 17000 1697 1151 1572 3462 6899 2621 17400
01/21/96 18100 16800 1737 1170 1588 3606 7004 2647 17700
01/22/96 18100 15900 1731 1156 1653 3716 6916 2596 17500 I 01 /23/96 20200 13700 1821 1175 1563 3837 7213 2630 18300
01/24/96 21000 12300 1852 1181 1631 3536 7311 2629 18300
01 /25/96 17500 16500 1706 1183 1604 4130 6948 2654 17400 I 01/26/96 17900 17700 1772 1172 1701 5816 7171 2636 181 00
01/27/96 18200 18000 1773 1177 1700 5771 7111 2641 17900
01/28/96 20000 15500 1845 1186 1 81 0 5913 7285 2636 18100 I 01/29/96 28500 3100 2156 1179 2105 7491 8192 2591 20800
01/30/96 19600 15400 1775 1195 1904 6701 7177 2672 18200
01/31/96 18700 16300 1724 1174 1956 6531 7002 2648 17700
I AVG: 18516 15403 1870 1169 1715 4772 7429 2714 19030
.TOT: 574000 462100 56107 35072 51456 143161 222870 81426 570900
••
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-- --- - ------- --- - --
GfOU)WATEA UONl)I.Y MONITOAN'.i: GROLN)WAlER UONHLY MOJJTOANG: 11-N:H I EA COMBV--.IEO N=LUENT #2 ITCI OU!cR TEA COMBlr-ED l>Fl.1£r,tT; 111 OTCI PAGE N0.1 PAGEN0.1 JAN.1996 JAN.1996 DATE: FLOW; Pit COO: TSS: TOC: DATE: FLOW: PH TOC: CR) pH ppm ppm ppm CR) ptl ppm
01/01/96 2413 5,5 6000 14 1428 01101/96 76217 5.9 7 01/02/96 2875 01 /02/96 69677 5.9 01/03/96 2922 5,7 ◄230 3 01/03/96 69880 5. 7 0 1/04/96 2227 5.8 3870 7 01/04/96 69449 5.6 01/05/96 2925 5.9 37◄ 0 10 01/05/98 70802 5.5 01/06/96 5.8 3700 8 01/06/96 5.6 01/07/96 5761 5.9 5430 9 01/07196 137427 5,7 01/08/96 2642 5.7 6170 11 01 /08/96 50163 5.6 01/09/96 2826 5.7 6350 13 01/09/96 70435 5.6 01/10/96 2781 5.6 9750 29 2707 01/10/96 7202 ◄ 6, 1 6 01/11/96 2663 5.9 8960 20 01/11/96 74402 6.0 01/12/98 2746 5.7 8700 16 01/12/96 75838 6. 1 01/13J96 2833 5.6 5800 21 01/13/96 72506 5.6 01/14/96 2777 5.5 8000 23 01/14/96 7282◄ 5.6 01115/96 2761 5, 7 8950 10 2492 01/15/96 71830 5,9 7 01/16/96 1856 5.7 7100 • 01116/96 69257 6.1 01/17/96 3163 5.4 8210 1 ◄ 01117196 67845 5.6 01/18/96 31D7 5.5 5700 24 01/18/96 70249 6.1 01/19/96 2885 5.6 5610 20 01119/96 70552 6.2 01/20/96 2771 5.5 8390 9 01/20/96 69302 6.0 01121196 25D9 5.6 8410 10 01121/96 70352 5,7 01/22196 2759 5.7 8950 10 2249 01/22196 69268 6.0 6 01123196 3079 5.7 9350 • 01/23/98 70439 5.6 01 /24/96 3246 5.8 6500 17 01/24/96 69740 5.7 01125/96 2876 5.7 7110 16 01 /25/96 69625 5.6 01/26/96 2951 7,5 6400 4 01/26/96 73988 6.1 01/27/96 2612 5.4 5100 18 01127/96 74273 5,7 01128/96 2716 5,5 5060 21 01/28/96 74275 5.7 01129/96 2669 5.4 6260 6 1854 01/29/96 76114 5.6 7 01 /30/96 2933 5.5 6340 8 01 /30/96 74624 5.6 01/31/96 2561 5.6 6620 6 01/31/96 73735 5.5
AVG: 2858 5.7 6692 13 2146 AVG: 73236 5.8 7 MAX: 5761 7.5 9750 29 2707 MAX: 137427 6.2 7 MIN: 1956 5.4 3700 3 1428 MIN: 50163 5.5 6
Jenuery 1996 Pege 1 ol 10 Jenuery 1998 Page 2 ol 10
----- -- -- --- -------
GfO.UlWAl Ell MONII L V MONJTOAJ-tl: GftOI. H:JWA 1 i:A MONII I .Y MOIIIORNG: Sl!HMIXfl)l OU)R; S8fM. At-71:A Pl AIE SEPARATOH BEFORE S8R: PAGE NO. 4 PAGEN0.3 JAN.1996 SETT. SlJJGE 6/0AY JAN.1096 UAlt:: fH Nll3N: P04; 00; MISS: MLVSS: SOUllS; WASTED F/M: F/M: DATE; Pl t C,CX); TSS: pl I ppm ppm ppm ppm ppm ml/I 9•1 r8.tlo re.llo pH ppm ppm
01101/96 8.0 114 39.5 1.• 2616 190 121 0.15 01/01/96 6.3 4400 12 01/02/96 7.9 126 25.◄ 1. 7 2552 200 121 D.17 01102/96 6.7 4750 16 01/03/96 -, .9 110 18.4 1.9 270◄ 1856 200 106 0.18 D1/03/96 7.3 4970 40 01/04/96 7.9 92 15.1 1.9 2HO 190 105 D.13 01/04/96 6.9 3550 44 01/05/96 7.6 64 17.4 1.6 3276 110 94 0.10 o.u D1/05/96 6.0 3610 40 01106/9 6 7.9 110 19.-4 1.6 3200 170 135 0. ,o D.13 D1/08/96 6.9 3540 48 01/07/96 7.7 100 18.◄ 1.6 2960 170 106 0.15 0.13 01107/96 6.0 5064 40 01/06/96 7.9 116 19.8 1.9 262◄ 160 121 O.UI 0.13 01/08/96 6.9 6110 46 D1109/96 7.9 87 6.6 1.6 312◄ 160 100 0.17 0.13 01/09/96 0.0 6800 40 01/10/96 7.8 121 40.2 1.6 2400 1876 160 1,21 0,22 0.16 01/10/96 6.9 69D0 66 01/11/96 6.0 100 12.8 1.5 2860 150 108 0,20 0.18 01/11/96 6.9 6630 94 01/12/96 8.0 62 11.8 1. 7 2620 165 108 0.2◄ 0.20 01/12/98 5.6 7200 20 01113/96 6.0 105 31.2 1.8 25◄◄ 185 108 o. 19 0.20 01/13/98 5.7 5◄60 16 01/1 ◄/96 6.0 121 2◄.◄ 1.7 2◄0 ◄ 160 81 0.21 0.21 01/1 ◄/08 6.8 6760 28 01/16/96 8.0 116 17.0 ,.. 268 ◄ 180 100 0.20 0.21 01/15/06 8.0 5700 44 01 /16/98 8.0 116 12.0 1.8 2760 160 94 o. 18 0.21 01/1 8/98 5.7 6060 46 01/17196 7.9 167 16,0 1.• 3◄22 2372 140 84 0.15 0, 19 01/17/98 6.9 6950 60 01/16/86 6.0 166 56,8 1.1 3000 140 100 o.u 0.18 01118/96 0.0 6560 eo 01119/98 7.9 145 48.6 ,.. 3400 160 81 0.1

◄

0.17 01119/96 6.8 6480 60 0 1 /20/96 7.8 140 40,0 1.8 3200 160 94 0.17 0.16 0 1/20/08 5.6 6080 80 01/21/96 7.8 130 20.4 1. 7 30◄0 176 10• 0,11!1 o. 18 01/21/98 6.9 8140 80 01/22/06 8.0 144 14.3 1.8 2960 190 136 0, 19 0.17 01/22/08 5.P 8◄50 68 01/23/08 6.0 130 14.4 ,.. 3800 196 121 0.19 0, 18 0 1/23/00 0.0 82iO 40 01/2◄/98 7.9 167 37.2 ,.. 350◄ 2404 186 106 0,20 o. 19 01/2◄/98 6.4 7800 20 01125/98 7.1 160 38.0 1. 7 308◄ 180 1 21 0.21 0.20 01 /26196 5.8 7360 40 01126/98 6.0 200 17.2 1.8 3052 200 100 0.18 0.19 01/26198 8.0 6050 18 01127/96 6.0 177 40.4 1.9 3008 220 148 o. 18 o. 19 01/27186 8.1 5400 20 01/20/86 6.0 169 36.0 1. 7 2798 200 100 0.17 0,18 O 1 /28198 6.3 5250 26 0 1 /29/96 8.1 169 38.0 1.8 3100 200 100 0, 14 0.17 01 /29/96 8.1 ◄810 108 01/30/96 8.0 130 32.0 1.9 30◄0 200 108 0.1

◄

o. 16 01/30/96 6.5 495D 144 01/31/96 1.9 156 30.7 1.7 3904 2724 210 106 0.12 0.16 01/31/96 6.0 5◄60 172
AVG: 1.U 131 26.1 , .-, 297◄ 2206 175 106 0.17 0.17 AVG: 6.0 5625 66 MAX: 0.1 200 56.8 1.9 3904 272◄ 220 148 0.2◄ 0.21 UAl(; 7.3 8220 172 "'"' 7.1 82 6.6 1.5 2400 1878 140 61 o. 10 0.13 MIN; 6.4 3540 12
J11mi111y IUUtl P11g111 3 of 10 Jtmuttry 1 U06 Pugo ◄ ol 10
-- - ---- ---- --- - -- --
GFO.WWAl EA MOtlll-L Y MONITORt-G: GROLN)WATEA MONTI I.Y MO-UTORNG: SBA EFFLUENT:(DECANT) "4 SBRE INl'-EATIEA EOUALlZATION TANK: ITEOT PAGE NO. 5 PAGEN0.2 JAN.1996 WAS. NH3N PHOS. JAN.1996 DATE: Fl.OW: COD: TSS: 1SS ADDED: AOOED: DATE: PH CCX): OTWATERADDEO GO ppm ppm ppm gal Iba pH ppm· gal
a 110110e 2267 190 120 99-40 0 0 01/01/98 7.2 4200 01 /02/96 2255 230 105 10800 0 0 01/02/96 7.3 ◄550 01/03/96 226-4 206 60 10600 0 0 01/03/98 7.3 5010 01/0-4/96 2262 190 6◄ 13200 1 01/04/96 7.2 3490 01/05/96 2256 209 60 10400 0 01/05/96 7.1 3580 01/06/96 22-48 200 6 ◄ 11600 0 0 01/08/96 7.0 3480 01/07/96 2226 200 60 10800 01/07/96 7.1 6080 01/06/96 2220 175 72 12200 1 01/08/98 7.2 6180 01 /09/96 2223 160 90 12240 3 3 01/09/96 7.3 5600 01/10/96 2217 2◄0 66 1-48-40 1 0 01/10/96 7.◄ 5700 01/11/96 2253 227 96 12000 0 0 01/11/96 7.3 6-410 01/12/96 2175 260 166 14880 3 3 01/12/96 7.3 6700 01/13/98 2188 2◄0 120 11880 2 1 01/13/98 7.1 5150 01/1-4/96 2178 265 1 ◄◄ 12660 1 0111 4/96 7.2 6520 01/16196 2277 266 120 12440 1 01116/96 7.2 6300 01/16/98 2330 296 1 ◄0 16 ◄00 2 3· 01/16/96 7.3 6700 01/17/96 2276 280 1 ◄0 12800 3 0111 7196 7.0 6260 01118/96 2269 260 90 13580 0 01/18/98 7.3 6750 01119/98 2287 316 ◄O 12000 0 01/19/96 7.◄ 5540 01 /20/98 2231 259 66 12◄00 1 01120/98 7.2 6030 01/21196 2233 300 60 12000 2 01121/98 7.0 6190 01122/96 218◄ 271 96 11600 1 2 01/22/98 7.7 6810 0 1 /23/96 2206 270 10 ◄ 116◄0 3 3 01 /23/96 7.◄ 8310 0 112◄/96 228◄ 2◄0 135 1 ◄220 3 1 01/2 ◄/96 7.◄ 6350 01/25/96 2231 261 60 11860 3 01/25/98 7.2 65 ◄ 0 01126/96 2231 235 110 8520 0 2 01/28196 7.3 5◄00 01127/98 2281 235 92 10600 01127/98 7.3 5050 01/28/96 2171 250 12◄ 9980 01/28/96 7.3 4700 01/29/96 2250 250 120 11500 01129/96 7.3 5070 01/30/96 2205 2◄0 136 11 ◄20 0 0 01/30/96 7.2 5060 01/31/96 2267 226 172 12260 0 01131/96 7.3 5420
AVG: 2240 242 10 ◄ 12015 AVG: 7.3 5449 #OIV/01 MAX: 2330 316 172 15400 • 3 MAX: 7. 7 8310 0 MIN: 2164 175 40 8520 0 0 MIN: 7.0 3480 0
January 1996 Page 5 of 10 January 1996 Pege 6 ol 10
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GACXN)WATF.n MONTl-L Y MONfTOANl: GROLN)WATER MONTH.Y MOOfTORNG: N-EATIEA c.ARBOl'J FUEA EFfll.ENT 18 ITEF OUTEATERCARBONFLTEREFFU£NT: ll70TEF PAGE NO. 7 PAGEN0.3 JAN.1996 JAN.1996 DATE: Pit COO: TOC: TSS: DATE: PH: TOC: TSS: ... ppm ppm ppm pli ppm ppm
01/01/86 18.◄ 01/01/96 2.6 01/02/96 01/02/96 01/03/98 6.2 206 66 01/03/96 6.7 0 1 /04/98 01 /0 ◄/98 01/05/96 01 /D 5/96 01/08/96 01/06/96 01/07/98 01/07/96 01/08/96 01/08/96 01/09/96 01/09/96 01/10/96 6.2 340 276.9 01/10/96 6.4 4.1 01/11/96 01/11/96 01/12/98 01/12/98 01/13/98 01/13/98 01/1 ◄/96 01/14/98 01/16/96 259.7 01/15/96 6.1 01/16/96 01/18/96 01/17/96 6.1 290 01/17/96 6.9 01/18/96 01/18/98 01/19/98 01/19/96 01/20/96 01/20/96 01/21/98 01/21/96 01/22/96 36.0 01/22/96 3.3 01/23/96 01/23/96 01/24/86 6.3 255 01/24/96 6.5 01/25/96 01/25/96 01/26/96 01/26/96 01/27/96 01/27/96
01128/96 01/28/96 01/29/98 215.3 01/29/96 4.2 01/30/96 01130/96 01/31/96 6.3 220 01131196 7.7
AVG: 6.2 262 161 56 AVG: 6.6 4.1 MAX: 8.3 340 277 56 MAX: 7.7 6. 1 MIN: 6.1 206 18 56 MIN: 5.9 2.6
January 1996 Pago 7 of 10 January 1996 Pago 8 ot 10
---- --- - - -
GFOl.NJWATEA MONTH. Y MONrTOANG:
RAINFALL DATA
DATE ctl:.S'OAY
01/01196 0.10
01/02/96 0.20
01/03/96 0.00
01/04/96 0.00
01/05/98 0.00
01/08/96 O. ◄O
01/07/96 0.50
01/06/96 0.00
01/09/96 0.00
01/10/96 0.00
01/11/98 0.20
01/12/96 D.00
01/13/96 0,00
01/14/96 0.00
01115/98 0.00
01/16/98 0.00
01/17/98 0,00
01/18/96 1. 10
01/19/96 0.00
01/20/96 0.00
01/21/98 0.00
01/22/98 0.00
01/23/96 0.10
01/24/96 0.30
01125/98 0.00
01 /26/96 1.50
01127/96 0.00
01/28/96 0.00
01/29/96 0.30
0 1 /30/96 0.10
01/31/96 0.00
TOTAL 4.80
AVG 0.◄ 4
January 1996 Page 9 of 10
- --
GfOJNlWAlEA TREAlMENT Pl.ANT
NEAlEASYSTEM
JAN.1996
ITEM 1/fLUENT
FLOW -TGD 2.9
COD • mg/I. 6707.1
TSS • mg/I. 13.6
LOW 5.4
pH
HIGH 7.5
GAOUl-llWATEA TREATMENT PU\Nf
OUfEA lEA SYSTEM
ITEM ffllJENT
FLOW • TGO 73.2
TSS . mg/I.
LOW 5.5
pl I
HIGH 6.2
t-olES
- -
EfFLUENf %RED.
·······-......
2.9
262.2 96.1%
6B.0 .. ,
B.3
EfFLLENT %RED.
73.2
1.0
5.9
7.7
LEAK IN INNER TIER INFLUEN r LINE.NO SAMPLES.01/02196
NO WEU READING 01/07195 INCLEMENT WEATHER
January 1996
- - --
Pago 10 ol 10
I January ITMAINT1.WK1
I MAINTENANCE ACTIVITIES-GROUNDWATER OPERABLE UNIT #1
INNER llER SYSTEM
I DATE LOCATION PROBLEM
I NO MAINTENANCE ACTIVITIES REPORTED IN JANUARY
I
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Page 1 of 1
ACllON
DATE ACTION MECHANIC
I January OTMAINT1 .WK1
I MAINTENANCE ACTIVITIES-GROUNDWATER OPERABLE UNIT #1
OUTER TIER SYSTEM
I ACTION
DATE LOCATION PROBlEM DATE ACTION MECHANIC
I NO MAINTENANCE ACTIVrTlES REPORTED IN JANUARY.
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I Page 1 of 1
I February WELLS3.WK1
INNER TIER
I DAILY FLOW:
FEBAJARY
I 1996: IT-1 IT-2 IT-3 IT-4 IT-5 IT-6 IT-7 IT-8 IT-9
02/01/96 172 71 136 85 335 153 118 1239 711
02/02/96 343 74 445 245 0 156 119 1289 767 I 02/03/96 227 74 183 129 0 147 85 1443 840
02/04/96 151 75 157 158 50 147 154 1238 877
02/05/96 167 76 150 169 150 154 129 1279 175
I 02/06/96 172 83 158 201 230 178 158 1400 1
02/07/96 166 82 156 61 570 182 152 1296 0
02/08/96 172 84 155 4 625 187 144 1273 0
I 02/C 9/96 182 90 161 77 505 184 151 1329 884
02/ 1 0/96 170 81 138 79 571 156 122 953 863
02/11 /96 201 88 148 96 512 164 141 908 932
I
02/12/96 198 91 142 97 280 157 145 874 904
02/13/96 205 95 150 144 576 161 197 1008 448
02/14/96 199 94 145 156 602 161 186 568 891
02/15/96 209 93 127 149 627 162 134 204 948
I 02/16/96 195 85 96 124 305 139 152 56 892
02/17/96 137 60 35 102 336 108 100 0 590
02/18/96 204 85 0 152 287 166 135 0 30
I 02/1 9/96 157 68 15 130 462 144 122 0 626
02/20/96 198 81 18 142 538 159 157 0 30
02/21 /96 182 77 0 85 506 169 121 1172 1
I 02/22/96 192 84 0 0 582 193 170 1474 721
02/23/96 190 83 0 5 592 197 175 1482 965
02/24/96 191 78 0 134 542 194 138 1467 944
02/25/96 154 61 0 1 6 490 161 131 1198 769 I 02/26/96 11 6 61 0 103 403 141 81 1028 647
02/27 /96 122 62 118 12 409 140 89 1065 672
02l'-8196 126 61 122 72 372 143 89 1065 673
I 02/29/96 144 57 122 96 200 148 166 1117 691
I AVG: 181 78 106 104 402 160 137 946 603
I TOT: 5242 2254 3077 3023 11657 4651 3961 27425 17492
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OUTERTIER
I DAILY FLOW:
FEBAJARY
1996: OT-1 OT-2 OT-3 OT-4 OT-5 OT-6 OT-6A OT-7 OT-8 I 02/01 /96 24100 5900 1926 1171 2119 6842 7332 2656 18600
02/02/96 21300 10800 1821 1169 2025 6701 7175 2657 17600
I 02/03/96 21500 12200 1840 1180 1998 6839 7297 2667 17900
02/04/96 23200 9600 1920 1175 1757 7072 7538 2616 17500
02/05/96 17100 16600 1659 1186 1740 6330 6767 2668 15900
I 02/06/96 17900 17600 1752 1193 2001 6606 7072 2679 16100
02/07/96 17700 17400 1752 1192 2150 6557 7024 2665 16000
02/08/96 17700 17400 1772 1179 2240 6558 7053 2686 16300
I 02/09/96 18300 16300 2211 1195 2166 6602 3077 2693 16700
02/1 0/96 17300 16500 2179 1185 2239 6420 10878 2646 16000
02/11 /96 17700 16300 2209 1188 2382 6539 7003 2678 16500
02/12/96 17500 16600 2201 1196 2403 6599 7063 2680 16500
I 02/13/96 17300 16500 2202 1214 2494 6564 7020 2679 16300
02/14/96 17200 16100 2199 1208 2556 6563 7022 2689 16200
02/15/96 17100 15900 2172 1250 2628 6503 6962 2658 15800
I 02/16/96 17400 16300 2175 1217 2594 6684 7155 2649 16500
02/17 /96 17600 16300 2199 1255 2493 6732 7228 2690 16900
02/18/96 17600 16400 2193 1192 2540 6728 7232 2685 16500
I 02/19/96 17800 16700 2192 1182 2552 6648 7143 2721 16700
02/20/96 17800 16700 2180 1148 2429 6353 6836 2669 16500
02/21 /96 18000 17300 2169 1114 2431 6258 6728 2681 15800
I 02/22/96 18500 17900 2214 1102 2429 6115 6630 2747 15300
02/23/96 19600 16000 2194 1133 2423 6126 6634 2695 15700
02/24/96 17300 19700 2197 1084 2382 5817 6313 2718 14600
02/25/96 16000 18100 2148 982 2175 5276 5749 2655 13400
I 02/26/96 17700 20000 2192 1180 2268 5654 6140 2703 14500
02/27/96 17900 20000 2180 1191 2274 5608 6159 2707 14700
02/28/96 17800 20700 2183 1279 2291 5605 6183 2719 15100
I 02/29/96 17700 20300 2153 1301 2461 5522 6141 2673 14500
I AVG: 18331 16348 2082 1181 2298 6359 6847 2680 16090
I TOT: 531600 474100 60384 34241 66640 184421 198554 77729 466600
I
I
I
I Page 4 of 8
I
-- - -- - - - - - - - - - - ----
GfD.NJWATERMONlll.VMONITORN3: GFD..NlWATEA MONTI·LY MO,UTORNG:
l>I-ERTERCOM8"'Ell >FLUENT #2 ITCI OUTER TEA COMBl>ED l!fl.LENT: #1 OTCI
PAGEN0.1 PAGEN0.1
FEB.1996 FEB.1996
DATE: FLOW: Pit 000: TS& TOC: DATE: FLOW: Pit TOC:
CH) pH ppm ppm ppm GR) pH ppm
02/01/96 3020 5.4 5450 13 02/01/96 70646 5.9
02/02/96 3438 5.7 6340 10 02/02/96 71248 5.6
02/03/96 3128 5.6 6410 10 02/03/96 73421 5.6
02/04/96 3007 5.7 6550 10 02/04/96 72378 5.6
02/05/96 2449 5.6 5718 18 1661.0 02/05/96 69950 5.5 6.1
02/08/96 2581 5.7 5690 10 02/06/98 72903 8.5
02/07/96 2665 5.7 7150 32 02/07/96 72440 5.8
02/06/96 264◄ 5.5 10000 64 02/08/98 72888 6.0
02/09/96 3563 5.4 11000 73 02/09/96 69244 6.1
02/10/96 3133 5.6 6900 14 02/1 0/96 75347 6.1
02/11/96 3190 5.5 6350 12 02/11/96 72499 5.7
02/12/96 2888 5.6 7910 13 2083.0 02/12/98 72742 5.8 7.2
02/13/96 2984 5.5 7150 19 02/13/96 72273 6.7
02/14/96 3002 5.5 6240 34 02/14/96 71737 5.5
02/15/96 2653 6.7 6000 60 02/15/96 70973 6.3
02/18/98 20,4,4 5.8 6740 24 02/18/96 7287-4 5.5
02/17/96 1468 . 5,8 6130 14 02/17/96 73397 5.8
02/18/96 1059 5.5 5840 10 02/1 6/96 73070 5.7
02/19/96 1724 5.6 7130 8 2275.0 02/19/98 73838 5.8 3.1
02/20/98 1323 5.5 5660 8 02/20/98 72815 5.8
02/21/96 2313 5.5 6570 17 02/21/96 72481 6.0
02122/96 3-416 5.7 6730 • 02/22/96 72937 5.6
02/23/96 3669 5.7 4700 13 02/23/96 72505 6.3
02/24/96 3688 5.5 4950 6 02/2-4/98 72111 6.0
02/25/96 2960 5.7 4200 15 02/25/96 66465 5.6
02/26/96 2560 5.5 5050 9 1570.0 02/26196 72337 5.6
02/27/96 2689 5.6 4820 7 02/27/98 72719 6.1 4.1
02/28/96 2723 5.5 5410 9 02/28/96 73660 6.3
02/29/96 2741 5.6 6340 7 02/29/96 72751 5.7
AVG: 2717 5.6 6453 19 1947,3 AVG: 72216 5.9 5.1
MAX: 3689 5.7 11000 84 2275.0 MAX: 75347 6.7 7.2
MIN: 1059 5.4 4200 7 1570.0 MIN: 66465 5.5 3.1
February 1996 Page 1 of 10 February 1896 Page 2 of 10
---- - - - - - - - ----- - --
GFD..N>WATER MONTI-l. V MONITORN3: GFPLNJWATER MONTH..Y MO\IITORN3:
SBRMIXEDUQUOA: --AFTER PLATE SEPARATOR BEFORE SBA:
PAGEN0.4 PAGEN0.3
FEB.1996 SETT. SU1lGE 5/DAV FEB.1996
DATE: PH: Nfl3N; P04: 00: MlSS: MLVSS: &X.DS:WASTED F/M: FIM: DATE: PH cco: TSS:
pH ppm ppm ppm ppm ppm ml/I gal ratio retlo pH ppm ppm
02/01/96 8.0 147 5.0 1. 7 2988 210 135 0.14 02/01/96 8.1 4700 28
02/02/96 8.0 184 23.3 1.9 3524 200 87 0. 14 02/02/98 8.2 5450 32
02/03/96 7.9 180 22.4 1.9 3200 200 81 0.15 02/03/96 8.0 5360 44
02/04/96 7.7 195 19.4 1.8 3200 180 108 0.15 02/04/96 8.2 5410 78
02/05/96 7.8 160 17.6 1.9 3892 200 81 0.12 0.14 02/05/96 8.0 5280 124
02/08/96 7.9 108 16.7 1.6 2660 210 81 0.19 0. 15 02/06/96 5.9 5580 92
02/07/96 7.9 148 12.1 1.8 3796 2640 190 81 0.14 0.15 02/07/98 6.5 5990 28
02/08/98 7.9 207 47.3 1.5 3200 190 81 0.18 0.15 02/08/96 5.5 6350 32
02/09/96 7.9 140 42.2 1.8 3260 190 67 0.15 0.16 02/09/98 5.4 6660 18
02/10/96 7.9 144 40.2 1.6 2268 230 81 0.25 0.18 02/10/98 5.1 8300 38
02/11/96 7.9 148 35.1 1.9 3168 210 81 0.19 0.18 02/11/98 5.8 6650 20
02/12/96 8.0 152 20.0 1.3 3880 210 81 0.15 0.18 02/12/96 5.7 6410 18
02/13/96 7.8 160 27.5 1.9 3340 220 81 0.15 0.18 02/13/96 5.2 5700 20
02/14/98 7.8 147 15.5 1.9 "4240 3600 220 81 0.15 0.18 02/14/96 5.7 7030 72
02115/96 8. 1 177 47.8 1.5 3284 240 54 0.16 0.18 02/15/96 5.7 5950 24
02/18/98 5.9 184 44.0 1.8 3372 250 94 0.17 0.16 02/18/98 5.8 6590 16
02/17/98 7.8 180 42.4 1.9 3200 245 94 0.14 0.15 02/17/96 5.7 5070 40
02/18/98 7.7 154 40.4 1.8 2662 250 94 0.19 0.16 02/18196 5.8 5730 28
02/1 9/98 8.1 150 42.0 1.8 3388 260 81 0.14 0.16 02/19/98 5.5 5190 40
02/20/98 7.9 200 44.4 1.4 2210 270 94 0.21 0.17 02/20/98 5.7 5260 40
02/21198 7.9 138 14.0 1.7 3580 2560 270 84 0.14 0.18 02/21/98 6.4 5700 48
02/22/98 7.9 134 15.2 1.7 3400 270 94 0.18 0.17 02/22198 5.5 6090 40
02/23/96 8.0 154 32.9 1.8 3480 280 94 0.13 0.18 02/23/96 7.0 5000 40
02/24/96 7.9 115 37.6 1.3 3340 270 108 0.13 0.15 02/24/96 8.7 5050 20
02/25/96 7.9 113 16.0 1.0 3148 230 64 0.14 0.14 02/25/96 7.1 4850 32
02/28/96 8.0 127 15.6 1.6 3428 260 64 0.13 0.14 02/28/98 7.0 4850 38
02/27/96 8.1 107 21.2 1.8 3480 270 94 0.12 0.13 02/27/96 5.6 4690 20
02/28/98 7.9 135 33.2 1.5 3360 2120 290 100 0.12 0.13 02128/96 5.8 4710 •• 02/29/96 8.2 135 26.6 1.8 3496 300 100 0.13 0.13 02/29/96 5.7 5180 40
AVG: 7.8 149 28.2 1.7 3290 2730 234 88 0.15 0.16 AVG: 5.9 5579 39
MAX: 8.2 207 47,6 1.9 4240 3600 300 135 0,25 0.18 IAAX: 7.1 7030 124
MIN: 5.9 107 5.0 1.0 2210 2120 180 54 0.12 0.13 MIN: 5. 1 4690 18
February 1996 Page 3 of 10 February 1996 Page 4 ol 10
---- - - - - ---- - - - - - --
GFOLN)WATEAMONll-LYMONITORN3: GA'.X.N>WATER MONil-1.. Y MOOITORNG:
SBA EFFLUENT~DECANT] #4 SBAE INt-EA TIER EQUALIZATION TANK: ITEOT
PAGE NO. 5 PAGEN0.2
FEB.1996 WAS. NH3N PH06. FEB.1996
DATE: FLOW: COO: TSS: 1SS AOOED: ADDED: DATE: PH COO: OTWATEAADDED
CH) ppm ppm ppm gal lbs pH ppm gal
02/01196 2192 220 100 10300 3 02/01/96 7.3 4800
02102/96 2356 217 64 10440 0 02/02/96 7.3 5090
02/03/96 2524 220 120 12000 1 02/03/96 7.4 5240
0 2/04196 3270 269 186 12610 1 1 02/04/96 7.2 5380
02/05/96 2226 228 164 10680 1 2 02/05/96 7.3 5190
02/06/96 2279 252 124 10640 2 3 02/06/96 7.7 5510
02107196 2282 203 125 10000 2 4 02/07/98 7.5 7020 500
02/08/96 2291 190 150 11820 0 0 02/08/96 7.7 6700
02/09/96 2275 220 60 12000 1 ·O 02/09/96 7.4 5900
02/10/96 1939 220 104 13180 0 02/1 0/98 7.4 6350
02/11/96 2156 255 140 9600 0 02/11 /98 7.4 6350
02/12/98 2226 224 200 16200 1 02/12/96 7.3 6520
02/13/96 2211 215 120 11340 1 02/13/96 7.1 5600
02/14/98 2232 228 132 14800 2 4 02/14/96 7.1 7110
02/15/98 1917 240 120 10920 0 02/15/98 7.3 8000
02/16/98 2274 283 128 12020 0 02/18/96 7.2 6090
02/17/96 2140 182 120 12000 1 02/17/96 7.1 5160
02/18/96 2172 258 100 10200 0 02/18/96 7.2 5860
02/19/96 2265 225 92 15600 0 02/19/98 7.7 5080
02/20/96 2273 253 120 12880 0 02/20/98 7.6 5410
02/21/96 2282 274 196 11400 2 02/21/98 7.7 5640
02/22/96 2386 263 126 11600 2 02/22/96 7.2 6340
02/23/96 2554 295 125 11840 0 02/23/96 7.5 4900
02/24/96 2945 310 92 8920 0 02/24/96 7.5 4550
02/25/96 3053 320 124 8600 1 02/25/96 7.8 4550
02/26/96 2264 260 110 10640 1 02/26/96 6.0 4700
02/27/96 2289 240 160 11000 2 02/27/98 6.1 4710
02/28/96 2291 242 160 10000 0 02/28/98 7.4 4670
02/29/96 2264 246 124 12400 1 02/29/96 7.3 5260
AVG: 2338 243 129 11560 1 AVG: 7.4 5575 500
MAX: 3270 320 200 16200 2 4 MAX: 6.1 7110 500
MIN: 1917 162 80 8800 0 0 MIN: 7.1 4550 500
February 1996 Page 5 of 10 February 1996 Page 6 of 10
--- - - - - - ---- - - - - ---
GROlNJWAlER MONTI LY MONITOANG: GAOLN)WATEAMONTH.YMONITORJ.IG:
IN'ERTIERCAR!lONFILTEREFFUENf #8ITEF OUTER TEA CARBON FL TEA EFFLLENf: 17OTEF
PAGE NO. 7 PAGEN0.3
FEB.1996 FEB.1996
DATE: PH: COO: TOC: TSS: DATE: PH: TOC: TSS:
pH ppm ppm ppm pH ppm ppm
02/01/96 02/01 /96
02/02/96 02/02/96
02/03/96 02/03196
02/04/96 02/04/98
02/05/96 75.0 02/05/96 •• 1
02/06/96 02/06/96
02/07/98 6.1 164 38 02107/96 7.2 5
02/08/96 02108/98
02/09/96 02/09/86
02/10/96 02/1 0/96
02/11/96 02111/98
02/12/96 165.8 02/12/96 5.2
02/13/96 02/13/96
02/14/96 8.3 2<0 02/14/96 7 .•
02/15/96 02/16/96
02/16/96 02/16/96
02/17/96 02/17/96
02/18/96 02/18/96
02/19/96 20.1 02/19/96 2.2
02/20/96 02/20/96
02/21/96 8.0 275 02/21/96 6.2
02/22/96 02/22/96
02/23/96 02/23/96
02/24/96 02/2-4/96
02/25/96 02/25/96
02/26/96 02/26/96
02/27/96 112.6 02/27/96 5.3
02/28/96 8 .• 226 02/28/98 6.6
02/29/96 02/29/96
AVG: 8.2 232 93.4 38 AVG: 6.9 4.2 5
MAX: 6.4 275 165.8 38 MAX: 7.4 5.3 5
MIN: 6.0 184 20.1 36 MIN: 6.2 2.2 5
February 1996 Page 7 ol 10 February 1996 Pago 8 of 10
-- --·--- -- - - - - - - ----
GAOLN)WATEA MONTl-1.. Y MONfTOAN3: GFD.JMJWATER TREAlMENT Pl.ANT
UERlERSVSTEM ( 1)
RAINFALL DATA
FEB.1996
DATE Q-ESIDAY
ITEM NFLLENT EfFLLENT %RED.
02/01/96 0.40 ·····--·····-····
02/02/96 1.80 FLOW • TGD 2.7 2.7
02/03/96 0.00
02/04/96 0.00 COD • mgll 6452. 7 231.B 96.4%
02/05/98 0.00
02106/96 0.00 TSS . mgll 19.3 38.0
02/07/96 0.10
02/08/98 0.10 LOW 5.4 8.0
02/09/96 0.00 pH
02/10/96 0.00 HIGH 5.7 8.4
02/11/96 0.00
02/12/96 0.00
02/13/98 0.00 GlnJl,DWATER TREATMENT PUWf
02/14/96 0.00 OUTERlER SYSlcM (2)
02/15/98 0.00
02/18/98 0.00
02/17/98 0,00
02/18/98 0,00 ITEM NFLLENT EFFLLENT %RED.
02/19/96 0.70
02/20/96 0.20 FLOW • TGD 72.2 72.2
02/21/96 0.00
02/22/96 0.00 TSS • mgll 5.0
02/23/96 0.00
02/24/96 0.00 LOW 5.5 6.2
02/25196 0.00 pH
02/26/96 0.00 HIGH 6.7 7.4
02127196 0.00
02/28/96 0.10
02/29/96 0,00
TOTAL 3.40
MIN. 0.10
MAX. 1.80
AVG. 0.◄ 9
February 1996 Page 9 of 10 February 1996 Page 10 of 10
-------------------February ITMAINT1 .WK1
MAINTENANCE ACTIVITIES-GROUNDWATER OPERABLE UNIT #1
INNER TIER SYSTEM
ACTION
DATE LOCATION PROBLEM DATE ACTION MECHANIC
02/20/96 PLATE SEPARATOR SLUDGE PUMP 02/21 /96 REPLACED KEY ON SHAFT TO PUMP JPPP
02/21 /96 IT-8 NO FLOW 02/21 /96 REPLACED FLOW METER JPPP
02/21 /96 IT-9 NO FLOW 02/21 /96 CLEANED PROBES JPPP
02/22/96 IT-9 NO FLOW 02/22/96 REPLACED PUMP JPPP
02/22/96 IT-3 NO FLOW 02/27 /96 REPLACED EXHAUSTED JPPP
02/22/96 E.O.TANK VENT LINE 02/26/96 REPLACED VENT LINE JP
02/23/96 IT-3 NO FLOW 02/23/96 REPLACED BLADDER FP
02/23/96 IT-4 LOW FLOW 02/28/96 REPLACED REFIL TIMER CONTROL
REPLACED EXHAUST CONTROL JPPP
02/26/96 PH.PROBE CALIBRATION 02/27/96 CALIBRATED RPBH
02/29/96 IT-7 LOW FLOW 02/29/96 REPLACED BLADDER JPPP
Page 1 of 1
-------------------February OTMAINT.1.WK1
MAINTENANCE ACTIVITIES-GROUNDWATER OPERABLE UNIT #1
OUTER TIER SYSTEM
DATE LOCATION
02/22/96 OT-2
PROBLEM
LOW FLOW
ACTION
DATE
02/23/96
Page 1 of 1
ACTION MECHANIC
CUT OFF 18 IN.OF PIPE TO GET ABOVE
SAND.REPLACED PUMP. JP PP
I March WELLS3.WK1
INNER TIER
I DAILY FLOW:
I MARO-I
1996: IT-1 IT-2 IT-3 IT-4 IT-5 IT-6 IT-7 IT-8 IT-9
I 03/01/96 147 59 124 1 211 153 196 1125 702
03/02/96 136 57 118 88 204 146 188 1067 653
03/03/96 149 69 137 54 126 161 211 1181 647
I 03/04/96 157 51 95 55 112 116 149 847 532
03/05/96 218 63 118 79 336 132 180 1029 414
03/06/96 254 61 239 20 341 157 177 1009 460
I 03/07 /96 219 50 209 80 255 116 135 784 218
03/08/96 275 75 155 0 173 184 223 1299 93
03/09/96 292 71 147 0 252 207 253 1420 6
I 03/1 0/96 283 71 144 0 230 200 253 1383 0
03/11 /96 292 75 150 0 312 199 255 1422 0
03/12/96 284 77 150 0 339 204 248 1374 681
I 03/13/96 223 62 124 37 452 122 196 1089 744
03/14/96 251 71 141 43 489 145 212 571 808
03/15/96 244 · 74 136 6 537 174 219 135 828
03/1 6/96 256 83 143 0 588 191 244 1 926 I 03/17 /96 244 86 144 0 552 190 241 51 550
03/18/96 275 84 203 150 493 193 243 605 913
03/1 9/96 262 85 196 224 495 185 243 0 931
I 03/20/96 252 83 147 88 345 176 236 384 910
03/21 /96 243 83 147 74 282 154 223 486 900
03/22/96 246 83 143 74 291 156 212 888 884
I 03/23/96 206 73 126 121 369 135 185 803 782
03/24/96 176 67 113 127 315 86 168 0 657
03/25/96 168 66 114 119 310 113 172 899 638
I 03/26/96 202 77 137 157 328 149 210 1297 783
03/27 /96 151 66 113 137 255 126 1 81 1019 665
03/28/96 144 65 149 136 259 129 178 1007 658
03/29/96 62 62 117 120 249 118 168 978 637
I 03/30/96 63 59 117 124 247 121 173 999 650
03/31 /96 207 58 263 193 193 116 161 945 603
I AVG: 212 70 147 74 321 153 204 842 609
I TOT: 6581 2166 4559 2307 9940 4754 6333 26097 18873
I
I
I
Page 3 of 8
I
I March WELl.S3.WK1
I OUTERTIER
DAILY FLOW:
MARCH
I 1996: OT-1 OT-2 OT-3 OT-4 OT-5 OT-6 OT-GA OT-7 OT-8
03/01/96 17700 20400 2180 1330 2404 5603 6253 2724 15200
I 03/02/96 18200 20900 2226 1359 2572 5779 6422 2767 15300
03/03/96 17000 19600 2118 1298 2343 5494 6121 2618 14600
03/04/96 15600 17900 2026 1257 2230 5062 5670 2479 13600
I 03/05/96 17400 20000 2194 1342 2370 5584 6316 2734 17700
03/06/96 16900 19400 2167 1324 2570 5505 6288 2734 18300
03/07 /96 16600 19400 2157 1330 2386 5490 6241 2702 18200
03/08/96 16800 19600 2175 1331 2441 5621 6358 2722 18300 I 03/09/96 16700 19200 2171 1335 2472 5659 6358 2704 18200
03/10/96 16700 19100 2163 1345 2505 5684 6466 2725 18300
03/11/96 18000 20600 2204 1339 2825 6160 1863 2693 20100
I 03/12/96 16300 18700 2182 1338 2551 5686 2809 2710 18000
03/13/96 20300 13600 2187 1348 2889 6176 9927 2701 19700
03/14/96 16700 20000 2184 1328 2662 5813 6485 2747 18600
I 03/15/96 16200 18900 2151 1337 2685 5949 6403 2717 18400
03/1 6/96 16600 19400 2184 1350 2772 6007 6442 2741 18500
03/17 /96 16900 19700 2174 1359 2838 6159 6649 2770 19100
I 03/18/96 16500 19000 2197 1353 2757 5922 6461 2720 18500
03/19/96 16600 19100 2191 1359 2822 6090 6546 2750 18800
03/20/96 15800 18100 2184 1349 2684 5803 6239 2733 17800
03/21 /96 15700 18000 2147 1329 2703 5749 6311 2682 17900 I 03/22/96 16200 18600 2265 1338 2773 6001 6522 2729 18600
03/23/96 16700 19000 2089 1355 2871 6007 6594 2767 18900
03/24/96 16600 18900 2181 1348 2844 6043 6556 2758 18700
I 03/25/96 16500 18800 2166 1329 2819 6116 6516 2730 18500
03/26/96 16900 19300 2185 1357 2870 6177 6651 2768 18900
03/27 /96 16900 19000 2165 1325 2843 6053 6542 2739 18600
I 03/28/96 16900 18900 2167 1355 2819 6076 6528 2741 18500
03/29/96 14700 20400 2139 1325 2831 6110 6586 2685 18600
03/30/96 16800 19500 2222 1365 2796 6117 6584 2796 18500
I 03/31 /96 16500 19200 2196 1365 2786 6079 6527 2791 18400
AVG: 16771 19103 2172 1339 2669 5864 6266 2722 18042
I TOT: 519900 592200 67337 41502 82733 181774 194234 84377 559300
I
I
I
I
Page 4 of 8
I
- - ---------- -------
GAOlN)WA1ER MONl1-L Y MONITORNG: GAOIN)WA1ER MONTH. Y MONITORl<G:
NERTERCOMBNED N'l.lJENT #2 ITCI OUTER TEA COM811ED IN'l.LENT: 111 OTCI
PAGEN0.1 PAGEN0.1
MAA.1996 MAR.1996
DATE: FLOW: PH: coo TSS: TOC: DATE: FLOW: PH: TOC:
GO pH ppm ppm ppm GO pH ppm
03/0 1 /96 2718 5.5 5530 14 03/01/96 73794 5.6
03/02/96 2657 5.6 6180 9 03102/96 75525 5.7
03/03/96 2735 5.5 5770 9 03/03/96 71192 5,6
03/04/96 2114 5.6 5170 26 03/04/96 65624 5.9
03/05/96 2569 5.6 4900 17 03/05/96 75640 5.8
03/06/98 2718 5.7 6550 18 2135 03/06/96 75188 5.8 3,265
03/07/96 2088 5.6 5570 7 03/07/96 74506 5.9
03/08/96 2477 5.6 6350 8 03/08/96 75348 6.0
03/09/96 2648 5.6 8420 9 03/09/96 74799 5.9
03110196 2564 5.6 8400 11 03/10/96 74988 6.0
03/11/96 2705 5.6 8600 28 03/11/96 75764 6.1
03/12/96 3357 5.6 8360 23 03112/96 70276 5.9
03/13/96 3049 5.6 6410 8 1424 03/13/98 78828 5.9 5
03/14/96 2731 5.6 5900 11 03/14/96 76519 6.9
03/15/96 2353 6.5 7220 10 03/16/98 74742 5.6
03/16/96 2432 5.4 7210 6 03/18/98 75996 5.6
03/17/98 2058 5.5 7380 10 03/17/96 77649 5.6
03/18/98 3159 5.4 9990 6 03/t 8/96 75410 5.9
03/19/98 2621 5.4 6070 10 1885 03/19/96 78593 5.9 3
03/20/96 2621 5.4 6000 6 03/20/98 72692 6.0
03/21/96 2592 5.6 7110 10 03/21/96 72521 6.1
03/22/96 2977 5.5 7700 6 03/22/96 75028 6.0
03/23/96 2800 5.5 8000 23 03/23/98 76283 6.0
03/24/98 1709 5.6 6350 6 03/2•'196 75930 6.0
03/25/98 2599 5.6 5300 17 03125/98 75476 6.0
03/28/96 3340 5,6 5550 11 1538 03/26/98 77108 5.7 5
03/27/96 2713 5.7 6690 10 03/27/98 76167 6.0
03/28/96 2725 5,5 5540 6 03/28/96 75988 5.7
03/29/96 2511 5,6 6550 13 03/29/96 75376 5,6
03/30/96 2553 5.5 5690 10 03/30/98 76680 5.6
03/31/96 2739 5.6 6090 11 03/31/96 75884 5.5
AVG: 2633 5.6 6669 1 2 1746 AVG: 75024 5.6 4
MAX: 3357 5.8 9990 26 2135 MAX: 78826 6.1 5
MIN: 1709 5,4 4900 6 1424 MIN: 65824 5.5 3
March 1996 Page 1 of 10 March 1996 Page 2 ol 10
-- - --- - ----- - - - - - --
GFKX..tOWATEA MONTl-L Y MONITORN3: GAOLN)WAlEA MONTH. Y MCNITORNG:
SBA MIXED l.Xll.OR: SBIM_ AFTER Pl.Al£ SEPARATOR BEFORE SBA:
PAGE N0.4 PAGEN0.3
MAA.1996 SETT. SUJJGE 5/OAY MAA.1996
DAlE: PH: NH3N: P04: DO: MLSS: MLVSS: SCU)S: WASTED FJM: F/M: DATE: PH: COO: TSS:
~ ppm ppm ppm ppm ppm ml/I gal ratio ratio ~ ppm ppm
03/01/96 8.1 130 25.0 1.8 2844 200 94 0.17 03/01/96 5.6 5340 80
03/02/96 8.2 134 24.4 1 ,7 3408 240 g4 0.15 03/02/96 5.5 5790 46
03/03/96 8.3 132 22.2 ,.. 3200 250 108 D.16 03/03/98 5.0 5710 68
03/04/96 8. 1 123 25.0 1,6 3644 280 64 0.14 03/04/96 5.5 5830 72
03/05/96 6.1 156 7.1 1.6 3560 290 97 0.14 0.15 03105/96 5.6 5550 40
03/06/96 6,2 163 24.D 1.6 3404 2368 270 61 0.13 0.14 03/08/96 5.7 5000 24
03/07/98 6.2 160 17.6 1.7 3536 280 81 0.13 0.14 03/07/98 5.6 5080 28
03/08/96 8.2 140 16.6 1.7 3600 290 94 0.12 0.13 03/08/96 5.6 4850 20
03/09/96 6.1 149 14.D 1.7 3572 260 106 0.16 0.14 03/09/98 5.6 6420 26
03/10/98 6.2 121 35.2 1.5 3400 260 106 0.18 o. 14 03/10/98 6.5 7000 20
03/11/96 8.2 119 10.0 1.7 3480 320 94 0.17 0.15 03/11/96 6.3 6700 24
03/12/96 6.1 126 14.1 1.8 3740 320 94 0.16 0.16 03/12/98 5.5 6550 24
03/13/98 8.1 137 15.2 1.8 3524 2368 330 100 0.18 0.17 03/13/98 5.4 6520 24
03/14/98 6. 1 144 28.8 1.8 3900 320 108 0.14 0.16 03/14/98 5.4 6000 16
03/16/98 8.0 148 26.8 1.9 5372 320 121 0.08 0,14 03/ 15/98 6.6 6490 62
03/18/98 8. 1 174 28.8 1 ,6 4000 310 135 0.14 0.14 03/18198 6,7 83-40 60
03/17/98 6.0 164 26.4 1.6 3760 310 121 0.17 0.14 03/17/96· 5.6 7290 46
03/18/96 6.0 146 24.0 1.8 4536 330 106 0.12 0.13 03/18/96 5.2 6250 48
03/19/96 6.0 145 18.8 1.3 4604 310 121 0.09 0.12 03/19/96 5.7 6010 52
03/20/96 6.0 139 40.4 1.7 3912 2688 330 135 0.12 0.13 03/20/96 5.4 5100 12
03/21/96 6.0 149 38.9 1.0 3860 320 106 0.14 0.13 03/21/96 5.3 5880 40
03/22/98 6.1 163 29.7 1.7 3892 310 121 0.13 0.12 03/22/98 5.6 5500 16
03/23/96 6.0 169 30.0 1 ,9 3604 320 121 0.13 0.12 03/23/96 5.7 5450 24
03/24/96 6.0 163 34.9 1 .4 3880 320 106 0.14 0.13 03/24/98 5.7 6100 24
03/25/96 8.0 184 1 ◄.5 1 ,6 4284 320 121 0. 11 0.13 03/25/98 6.0 5200 52
03/28/96 6.0 176 15.9 1.9 4132 330 108 0.12 0.12 03/26/96 5.6 5350 24
03/27/96 6.0 177 17.7 1.7 4624 3148 320 135 0.10 0.12 03/27/98 5.7 5280 46
03/28/96 6.0 165 18.2 1.7 3996 310 106 0.12 0.12 03/28/98 5,4 5610 32
03/29/96 6.1 199 19.6 1.6 4816 320 121 0.10 0.11 03/29/96 5.5 5480 60
03/30/96 6.0 190 18.9 1 ,7 4740 320 135 0.10 0.11 03/30/98 6.3 5310 46
03/31 /96 6.1 161 20.4 1.9 4560 310 121 o. 11 0.11 03/31/96 5.6 5730 56
AVG: 6.1 156 23 2 3922 2843 303 109 0.13 0.13 AVG: 5.7 5764 36
MAX: 6.3 199 40 2 5372 3148 330 135 0.18 0.17 MAX: 6,5 7290 72
MIN: 6.0 119 7 2844 2368 240 61 0.09 0. 11 MIN: 5.2 4850 12
March 1996 Page 3 of 10 March 1996 Page 4 of 10
-- --- ---- -- - - ------
GAOLNJWATEA MONTH. Y MONITOANG: GAOLNJWATEA MONTH.Y MOOITOANG:
SBA EFFLUENT:(OECANI) #4SBAE INi-EATIEA EClUAI.IZATION TANK: ITEOT
PAGEN0.5 PAGEN0.2
MAR.1996 WAS. NH3N PH05. MAR.1996
DATE: FLOW: COD: TSS: TSS ADOED: ADDED: DATE: PH COO: OT WATER ADDED
CHI ppm ppm ppm gal lbs pH ppm gal
03/01/96 2279 244 140 10640 2 03/01/96 7.4 5380
03/02/96 2296 278 120 12000 03/02/96 7.3 5770
03/03/98 2285 208 138 12200 03/03/96 7.4 5540
03/04/96 2228 259 124 11140 2 03/04/98 7.4 5800
03/05/96 2233 280 104 9000 1 4 03/05/96 7.3 4900
03/06/96 2264 270 120 10300 1 1 03/06/96 7.3 5200
03/07/98 2284 255 95 9860 1 1 03/07/96 7.2 5100
03/08/96 1780 235 92 8640 1 03/08/96 7.3 •4700
03/09/96 2280 290 104 9660 1 03/09/96 7.2 5820
03/10/98 2260 300 124 9240 1 1 03/1 0/98 7.2 8500
03/11/98 2281 280 98 1020D 1 1 03/11/96 7.1 7000
03/12/96 2246 285 150 8840 2 2 03/12/96 7.0 8900
03/13/98 2267 275 200 10260 2 3 03/13/96 8.9 7570
03/14/96 2242 250 184 10460 1 03/14/98 7.0 5800
03115198 2287 243 11 2 18600 03/15/96 7. 1 5650
03/18/96 2228 240 120 18100 1 03/18/96 7.0 6970
03/17/96 2285 223 138 16000 1 03117/96 7.1 6970
03/18/96 2218 175 152 12420 1 03/18/96 7.4 7330
03/18/98 2247 191 180 16280 2 03/19/96 7.2 4980
03/20/96 2199 180 88 9620 0 03/20/96 7.3 5300
03/21/96 2190 188 80 13080 0 03/21198 7.2 5900
03/22198 2233 195 48 10580 1 0 03122196 7.3 5500
03/23198 2205 205 80 10280 0 0 03/23/98 7.3 5300
03/24/98 2257 210 108 10460 1 0 03/24/98 7.3 5400
03/25/96 2237 190 80 11700 0 1 03/25/96 7. 1 5150
03/26/96 2271 190 80 11180 0 2 03/26/96 7.5 5400
03/27/96 2247 148 40 13200 0 1 03127198 7.4 5320
03/28/96 2198 182 98 9140 1 2 03/28/96 7.0 5400
03/29/96 2240 185 48 12640 03/29/96 7.1 5610
03/30/96 2273 208 58 12020 03/30/96 7.0 5240
03/31/96 2248 251 58 11680 03/31/96 7. 1 5540
AVG: 2233 227 105 11465 AVG: 7.2 5736 #OIV/01
MAX: 2296 300 200 18800 2 4 MAX: 7.5 7570 0
MIN: 1760 148 40 8640 0 0 MIN: 8.0 4700 0
March 1996 Page 5 of 10 March 1996 Page 6 ol 10
- ---- --- - -- ----- - --
GOOLN>WATEA MONTH_ Y MONITORNG: GAOl.NlWATEA MONTH. Y MONITOAl>IG:
IM'EAT!EACARBONFILTEAEFFLLENT #8 ITEF OUTER TEA CARBON FL TEA EFFLLENT: t7OTEF
PAGE NO. 7 PAGE NO. 3
MAA.1996 MAR.1996
DATE: Pl-t COO: TOC: TSS: DATE: Pit TOC: TSS:
pH ppm ppm ppm pH ppm ppm
03/01/96 03/01/98
03/02/96 03/02/96
03/03/96 03/03/96
03/04/96 03/04/96
03/05/96 03105196
03/06/96 8.4 285 18 48 03/08/98 7.0 3 7
03/07/96 03/07/96
03/08/96 03/08/98
03/09/96 03/09/96
03/10/98 03/10/96
03/11/96 03/11198
03/12/98 03/12/98
03/13/96 8.4 283 50 03/13/96 6.8 3
03/14/96 03/14/96
03/15/98 03/15/98
03/18/98 03/16/98
03/17/96 03/17/96
03/18/96 03/18/96
03/19/98 41 03/19/98 3
03/20/96 8.3 160 03/20/96 6.8
03/21/98 03/21/96
03/22/98 03/22/96
03/23/96 03/23/96
03/24/96 03/24/96
03/25/98 03/25/96
03/26/96 83 03/26/96 7
03/27/96 8.3 141 03/27/96 8.9
03/28/96 03/28/96
03/29/96 03/29/96
03/30/96 03/30/98
03/31/96 03/31/96
AVG: 8.4 217 48 48 AVG: 8,8 4 7
MAX: 8.4 285 83 48 MAX: 7.0 7 7
MIN: 8.3 141 16 48 MIN: 8.6 3 7
March 1996 Page 7 of 10 March 1996 Page 8 ol 10
-------------------
MAINTENANCE ACTIVITIES-GROUNDWATER OPERABLE UNIT #1
INNER TIER SYSTEM
ACTION
DATE LOCATION PROBLEM DATE ACTION
3/1/96 IT-1 LOW FLOW 3/4/96 REPLACED BLADDER CLEANED SCREEN
ADJUSTED FLOW
3/5/96 IT-5 LOW FLOW. 3/5/96 REPLACED BLADDER & SCREEN
3/7/96 IT-9 LOW FLOW 3/12/96 CLEANED PROBES
3/7 /96 IT-4 LOW FLOW 3/13/96 REMOVED REGULATOR, CLEANED SCREEN
ADJUSTED FLOW
3/12/96 IT-5 LOW FLOW 3/12/96 REPLACED BLADDER CLEANED STRAINER
ADJUSTED FLOW
3/16/96 IT-8 LOW FLOW 3/1 8/96 CLEANED STRAINER
3/17/96 IT-4 LOW FLOW 3/18/96 REPLACED BLADDER & CONTROLS
3/20/96 IT-8 NO FLOW 3/22/96 REPLACED PUMP
3/25/96 IT-8 NO FLOW 3/25/96 REPLACED FLOW METER
3/31/96 IT-1 LOW FLOW 4/2/96 ADJUSTED FLOW
-------------------March OTMAINT1 .WK1
MAINTENANCE ACTIVITIES-GROUNDWATER OPERABLE UNIT #1
OUTER TIER SYSTEM
ACTION
DATE LOCATION PROBLEM DATE ACTION MECHANIC
03/12/96 OT-6A WELLCOVER 03/12/96 REPLACED WELL COVER JPPP
03/14/96 OT-1 STRAINER 03/14/96 CLEANED STRAINER JPPP
03/14/96 OT-2 STRAINER 03/14/96 CLEANED STRAINER JPPP
03/21 /96 OT-1 LOW FLOW 03/22/96 CLEANED STRAINER JPPP
03/21 /96 OT-2 LOW FLOW 03/22/96 CLEANED STRAINER JPPP
03/25/96 OT-2 LOW FLOW 03/25/96 CLEANED STRAINER JPPP
Page 1 of 1
-- - - --- - -- - --- -----
GFO.NlWAlEA MONTlt. Y MONITOANJ: GAOUNOWAlEATAEATMENTPI.ANT
l<NEA TEA SYSTEM ( 1 )
RAINFALL DATA
MAA.1996
OAlECHcSOAY
ITEM INFLUENT EFFU.ENT %RED.
03/01/96 0.10
03/02/96 0.00 FLOW -TGO 2.6 2.6
03/03/96 0.00
03/04/96 0.00 coo • mg/I. 6716.2 217.3 98.8%
03/05/96 1.10
03/08/96 1.30 TSS • mg/I. 12. 1 48.0
03/07/96 0.30
03/08/98 0,00 LOW 5.4 6.3
03/09/98 0.00 pH
03/10/98 0.00 HIGH 6.6 6.4
03/11198 0.00
03/12/98 0.00
03/13/98 0.00 GAOUN)WAlEATAEATMENTPI.ANT
03/14/96 0.00 OJIEATEA SYSTEM (2)
03/15/98 0.30
03/18/98 D.20
03/17/96 0.10
03/18/96 0.90 ITEM INFLUENT EFFU.ENT %RED.
03/19/96 0.1 D
03/20/96 0.00 FLOW -TGD 74.9 74.9
03/21198 0.00
03/22/96 0.00 TSS • mg/I. 7.0
03/23/96 0.00
03/24/98 0.00 LOW 5.6 6.6
03/25/96 0.10 pH
03/28/96 0.00 HIGH 6.1 7.0
03/27/96 0.70
03/28/98 0.20
03/29/96 0.00
03/30/96 0.10
03/31/96 1.50
0.23
1.50
0.00
March 1996 Page 9 ol 10 March 1996 Pago 10 of 10
I INNERTIER
I DAILY FLOW:
I APRIL
1996: IT-1 IT-2 IT-3 IT-4 IT-5 IT-6 IT-7 IT-8 IT-9
I 04/01/96 11 5 63 162 189 148 123 171 973 648
04/02/96 187 82 155 138 196 151 213 979 819
I 04/03/96 204 76 129 126 143 149 200 1079 758
04/04/96 196 72 123 116 142 147 176 1 019 679
04/05/96 189 69 11 8 116 120 156 168 1023 646
I 04/06/96 197 73 125 127 107 167 177 1074 672
04/07/96 188 73 131 136 90 135 180 1120 701
04/08/96 220 83 142 167 119 156 216 565 816
I 04/09/96 218 80 133 180 176 154 220 950 833
04/1 0/96 185 69 115 140 227 136 173 1009 674
04/11/96 179 68 113 131 271 141 173 1003 663
I 04/12/96 1 79 65 11 6 126 227 139 172 959 662
04/13/9 6 208 77 133 159 274 150 205 721 788
04/14/96 183 69 11 6 144 236 124 180 948 682
I 04/15/96 206 76 134 156 284 155 205 748 785
04/16/96 206 76 88 147 282 160 207 701 792
04/17/96 187 71 81 137 253 134 190 859 733
I 04/18/96 178 56 65 1 7 225 21 181 981 653
04/19/96 162 69 69 90 225 0 171 949 611
04/20/96 147 62 61 86 235 0 175 980 629
I 04/21 /96 170 70 44 98 308 0 204 396 725
04/22/96 179 72 32 11 0 346 123 234 869 890
04/23/96 167 74 33 105 299 220 208 874 797
I 04/24/96 172 84 36 118 296 220 228 955 884
04/25/96 185 89 126 132 298 227 229 216 908
04/26/96 177 82 140 121 236 199 211 124 877
I 04/27/96 184 79 137 121 233 195 201 361 881
04/28/96 175 75 146 116 249 202 197 194 895
04/29/96 173 78 148 131 308 205 194 1031 891 I 04/30/96 173 78 140 142 349 195 189 1265 871
AVG: 183 74 11 0 127 230 143 195 831 762 I TOT: 5489 2210 3291 3822 6902 4284 5848 24925 22863
I
I
I
I
I OUTERTIER
DAILY FLOW:
I
APRIL
I 1996: OT-1 OT-2 OT-3 OT-4 OT-5 OT-6 OT-6A OT-7 OT-8
04/01/96 16400 19000 2198 1351 2779 6081 6477 2764 18200 I 04/02/96 16200 19200 2194 1353 2823 6156 6550 2783 18300
04/03/96 16300 18600 2190 1349 2748 6404 6368 2754 17800
04/04/96 16400 18600 2192 1360 2439 6447 6420 2769 18100 I 04/05/96 16000 18200 2139 1329 2383 6613 6337 2390 17800
04/06/96 16500 18500 2173 1341 2412 6782 6480 2730 18300
I 04/07 /96 500 29700 2166 1344 3022 8165 7809 2668 22300
04/08/96 14500 17700 2168 1354 2377 6759 6392 2734 18100
04/09/96 16800 17800 2192 1362 2465 7044 6692 2761 18900
I 04/1 0/96 16600 17600 2186 1352 2456 6977 6613 2747 18600
04/11/96 16900 17900 2171 1350 2482 7036 6787 2733 13400
04/12/96 17000 17800 2175 1352 2636 6976 6811 2726 12900
I 04/13/96 17000 17900 2182 1350 2771 7042 6800 2746 13000
04/14/96 12400 18100 2205 893 2834 7165 6882 2773 13200
04/15/96 16700 17400 2179 491 2753 6881 6591 2729 12700
I 04/16/96 17400 18000 2189 1 2912 7150 6794 2736 13100
04/17/96 17400 18000 2187 1 2954 7058 6855 2742 13300
04/18/96 17200 17600 2177 1330 2772 6757 6660 2732 13000
I 04/19/96 16900 17500 2166 1363 2841 6885 6665 2719 13100
04/20/96 17100 17500 2170 1380 2873 6832 6658 2725 13000
04/21 /96 17200 17800 2200 1382 2906 6818 6742 2784 13300
I 04/22/96 17300 17800 2199 1370 2798 6839 6737 2762 13300
04/23/96 16900 17400 2147 1364 2824 6511 6621 2732 13100
04/24/96 17100 17300 2145 1372 2603 6954 5920 2711 15100
I 04/25/96 17300 17900 2206 1404 2558 6966 5804 2777 16000
04/26/96 16700 17300 2130 1361 2447 6850 5649 2694 15500
04/27/96 17700 18300 2.163 1412 2510 6981 5897 2790 16100
I 04/28/96 17600 18000 2194 1402 2278 6895 5808 2778 15800
04/29/96 17400 17800 2202 1407 2030 6825 5771 2787 15600
04/30/96 17100 17400 2173 1401 2245 6683 6424 2749 15000
I
AVG: 16150 18320 2179 1229 2631 6851 6500 2734 15530
I TOT: 484500 549600 65358 36881 78931 205532 195014 82025 465900
I
I
I
I
-- - - - - - - - - - - - - - ----
GROUI-OWATERMONTILYMONITORNG: GROU'IDWATER MONTH. Y MONITORING:
N'ER TIER COMBINED tfll.ENT #2 ITC[ OUTER TIER COMBr-ED tfll.ENT: #10TCI
PAGE l'0.1 PAGEN0.1
APRIL 1996 APRIL 1996
DATE: A.OW: Ptt COO: TSS: TOC: DATE: A.OW: Ptt TOC:
Gt) pH ppm ppm ppm Gt) pH ppm
04/01/96 2592 5.6 5420 10 1333 04/01/96 75250 6.0 3
04/02/96 2920 5.5 5520 4 04/02/96 75559 5.6
04/03/96 2864 5.6 8200 19 04/03/96 78694 5.7
04/04/96 2670 5.5 7850 8 04/04/96 74727 5.6
04/05/96 2805 5.6 6700 5 04/05/96 73491 8.1
04/06/96 2719 5.5 6000 23 04/06/96 75218 8.0
04/07/96 2754 5.5 5400 8 04/07/96 77674 5.9
0◄/08/96 2-184 5.6 5730 16 1309 04/08/96 72084 5.9 5
04/09/96 2944 5.4 6950 11 04/09/96 76018 5.7
04/10196 2728 5.8 5040 9 04/10/96 75131 5.7
04/11/96 2742 5.5 5000 6 04/11196 70759 5.6
0-4/12/96 2645 5.8 5550 8 04/12/96 70378 5.7
0-4/13/96 2715 5.3 6660 8 04/13/96 70791 5.8
0-'114/96 2662 5.4 6310 7 04/14/96 88452 5.7
04/15/96 2749 5.5 5620 9 04/15/96 88424 8.4
04/16/96 2859 5.6 5824 7 1570 04/16/98 70282 8.3 3
04/17/96 2645 5.5 5300 12 04/17/98 70497 6.2
04/18/96 2377 5.8 5810 10 04/18/98 70228 5.6
04/19/96 2346 5.4 5400 5 04/19/96 70139 8.1
04/20/96 2375 5.5 5250 18 0,4/20/96 70238 8.0
04/21/96 2015 5.5 5460 6 04/21/98 71132 8.0
04/22/98 2855 5.4 5750 40 1747 04/22/98 71105 5.8 17
04/23/96 2777 5.5 5350 26 04/23/98 69599 5.9
04/24/96 2993 5.3 6690 45 04/24/96 71205 5.7
04/25/96 2410 5.4 6150 26 04/25/96 72915 6.2
04/26/96 2187 5.3 6990 21 04/26/98 70631 6.0
04127/96 2392 5.4 7890 10 04/27196 73853 5.9
04/28/96 2249 5.5 6570 8 04/28/96 72755 6.0
04/29196 3159 5.4 6320 10 1881 04/29/96 71822 5.7 8
04/30/96 3402 5.5 5560 9 04/30/96 71175 5.9
AVG: 2654 5.5 5970 13 1568 AVG: 72274 5.9 7
MAX: 3402 5.8 7890 45 1681 MAX: 78694 8.4 17
MIN: 2015 5.3 5000 4 1309 MN: 86452 5.6 3
Aprll 1996 Page 1 of 10 April 1996 Page 2 of 10
-- - - - - - - - --- -- - - - --
GAOlJt,()WATER MCMK. V MON!TORt-lG: GOOLNJWATER MONTlU MON!TORJNG:
SBA MIXED LJQUOR: S8fM. AFTER PLATE SEPARATOR BEFORE SBR: SBR
PAGEN0.4 PAGEN0.3
APRIL 1996 SETT. S.UJGE 5/DAV APRIL 1996
DATE: Pt-t NH3N: P04: 00: MLSS: MLVSS: SOLIDS: WASTED F/M: F/M: DATE: PH: coo: TSS:
pH ppm ppm ppm ppm ppm ml/I gal ratio ratio pH ppm ppm
04/01/96 8.0 144 12.9 1. 7 4400 300 135 0.09 04/01/96 5.7 4650 60
04/02/96 8.1 176 28.2 1.8 4000 320 135 0.13 04/02/98 5.5 5820 ..
04/03/96 8.0 172 30,8 1.6 392◄ 2560 310 121 0.12 04/03/98 5.7 5300 18
04104/96 6.1 183 22.6 1.4 3964 300 121 0.12 04/04/98 5.6 6360 72
04/05/96 6. 1 184 50,8 1.6 3812 340 135 0.12 0.12 04/05/96 6.3 5450 26
04/06/96 8.0 164 42.4 1.5 3812 330 121 0.14 0.13 04/06/96 6.5 5800 16
04/07/98 6.0 151 38.8 1.4 3816 310 106 0.13 0.13 04/07/96 6.1 6500 32
04/08/96 6.3 154 20.3 1.6 3840 325 135 0.14 0.13 0'4/08/96 5.4 6100 32
04/09/96 6.1 168 15.6 1.5 4160 370 146 0.12 0.13 04/09/96 6.0 6700 12
04/10/98 6.2 146 19.6 1.7 4140 2772 380 136 0.13 0.13 04/10/96 5.8 5870 48
04/11/88 8.1 158 34,0 1.7 3872 385 135 0.13 0.13 04/11/96 6.8 5760 32
04/12/98 6.0 214 25.4 1.8 2932 340 135 0.16 0.14 04/12/96 5.9 5820 16
04/13/96 6.1 184 16.2 1.7 4880 350 121 0.12 0.13 04/13/96 5.8 6370 32
04/14/96 6.0 174 17.0 1.6 6724 340 136 0.08 0.13 04/14/96 6.6 5730 38
04/15/96 6. 1 160 12.4 1.6 6120 345 160 0.11 0.12 04/15/96 5.7 8190 40
04/16/96 6.2 148 32,3 1.3 2040 370 146 0.22 0.14 04/16/96 5.6 4950 ·32
04/17/96 6.1 153 28.6 1.6 4640 2804 360 121 0.10 0.13 04/17/96 6.2 5150 24
04/18/96 6.0 150 27.0 1.4 4440 340 121 0.11 0.12 04/18/96 5.7 5880 32
04/19/96 7.8 140 27.8 1.6 4172 330 121 0.11 0.13 0 4/19/96 6.2 5200 24
04/20/96 6.0 165 41.8 1.0 4280 330 121 0.11 0. 13 04/20/98 6.1 5480 24
04/21/96 7.8 144 33.4 1. 1 4212 320 106 0.13 0. 11 04/21/96 6.1 5980 32
04/22/96 6.1 171 15.2 1. 1 4180 340 135 0.11 0. 11 04/22/96 5.5 5060 32
0-4/23/96 7.8 128 32.7 1.9 4804 340 175 0.11 0. 11 04/23/98 5.7 5900 32
04/24/96 6.0 131 26.4 1.4 4860 2960 340 162 0.11 0. 11 04/24/96 5.5 5610 36
04/25/98 6.0 154 44.4 1.4 3832 350 162 0.11 o. 11 0-4/25/96 5.7 4950 20
04/26/96 6.1 160 40.0 1.6 5224 340 135 0.10 o. 11 0•126106 5.5 5890 72
04/27/96 7.8 150 •2.0 1.6 4912 330 121 0.11 o. 11 04/27/96 5.1 6080 46
04/28/96 7.6 154 36.0 1.6 4080 340 161 0.13 o. 11 04/28/96 5.4 6090 40
0-4/29/96 7.4 130 3-4.0 1.7 5460 340 121 0.08 0. 11 04/29/96 5.0 5010 48
04/30/96 6.0 ###ti 16.5 1.6 4860 350 135 0.10 0.10 04/30/96 5.7 5440 56
AVG: 6.0 156 28 2 4286 2779 336 134 0.12 0.12 AVG: 5.6 5601 36
MAX: 6.3 214 51 2 5724 2960 380 175 0.22 0.14 MAX: 6.5 8370 72
MIit 7.4 116 12 2040 2580 300 106 0.08 0.10 MN: 5.0 4650 12
April 1996 Page 3 ol 10 Aprll 1996 Page 4 of 10
-- - - - - -- - -- - - - -- ---
GROJr-DWAlER MCMH. Y MONITORNG: GROlHlWAlERMCMH.YMONfTOAING:
SBA EFFLLENT(DECANT) "4S8AE IN!-ERTIEA EQUAI.IZATIONTA1'0<: fTEOT
PAGEN0.5 PAGEN0.2
APRIL 1996 WAS. NH3N PHO& APRIL 1996
DAlE: FLOW: CXlO: TSS: TSS ADDED: ADDED: DATE: Pl-t COO: OTWAlERAODED
GD ppm ppm ppm gal lbs pH ppm gal
04/01/96 2241 183 60 12800 3 04/01/96 7.0 ◄220
04/02/96 2613 181 72 11600 1 04102196 7.1 5810
04/03/96 2253 195 60 12840 1 04/03/96 7.0 5450
04/04/98 2252 181 40 12200 0 04/04/96 7.1 5460
04/05/96 2263 195 66 10200 1 0 04/05/96 7.2 5450
04/06/96 2233 215 84 10460 0 04/06/96 7.2 5900
04/07/96 2241 200 64 9100 0 04/07/96 7.3 5450
04/08/96 2280 203 180 10140 0 04/08/96 7.2 8130
04/09/96 2231 215 78 12800 2 04109196 7.3 8000
04/10/96 2202 213 06 10160 2 0 4/1 0/96 7.1 5920
04/11/98 2207 210 108 10580 0 04/11/96 7.2 5250
04/12/98 2233 198 92 10420 04/12/96 7.1 5930
04/13/98 2275 20◄ 8◄ 10280 04/13/96 7.4 5760
04/14/98 2211 210 72 10400 0 4/14/96 7.1 5610
04/15/96 2262 187 48 9600 3 04/15/96 7.2 5480
04/16/98 2292 1 ◄ 0 92 8820 0 0 4/16/96 7.6 51 ◄ 0
04/17/96 2221 165 120 10020 0 04/17/96 7.3 4850
04/18/86 2270 229 100 10200 04/18/96 7.6 5270
04/19/96 2241 180 56 10020 04/19/96 7.4 5000
04/20/96 2290 200 100 10000 0 04/20/96 7.5 6220
04/21/96 2291 225 80 11640 0 04/21/96 7.4 5390
04/22/96 2303 185 72 10000 0 2 04/22/96 7.4 4750
04/23/96 2288 200 124 8540 1 04/23/96 7.2 5300
04/2-4/96 2226 195 38 10460 04/24/96 7.1 6050
04/25/96 2271 180 60 8080 0 04/25/96 7.2 5300
04/26/96 2277 17 ◄ 100 10840 0 04/26/96 7.3 5610
04/27/96 2262 184 60 11020 0 04/27/96 7.2 6023 400
04/28/96 2139 173 72 10140 04/28/96 7,0 6110 451
04/29/96 2285 1◄1 80 10300 1 0 04/29/96 7.6 5510
04/30/96 2187 192 80 10680 2 2 04/30/96 7.2 5320
AVG: 2261 192 63 10511 AVG: 7.3 5495 428
MAX: 2613 229 180 12840 2 3 MAX: 7,8 6130 451
MIN: 2139 140 36 8080 0 0 MN: 7.0 4220 400
April 1996 Page 5 of 10 Aprtl 1996 Page 6 of 10
-- - - - - - - - --- - -- - - --
GACUl',OWATEA MONllt_Y MONJTOAJNG: GAOLN)WATEA MONTH. Y MONITOAJNG:
NEA TIER CAROON FL TEA EFFU.et/T #SITEF OUIEATIEA CAAB(),I FL TEA EFFLl.Et/T: 17OTEF
PAGE NO. 7 PAGEN0.3
APRIL 1996 APRIL 1996
DATE: PH: COO: TOC: TSS: DATE: PH: TOC: TSS:
pH ppm ppm ppm pH ppm ppm
04/01/98 36 04/01/96
04/02/96 04/02/96
04/03/96 6.3 200 44 04/03/96 7.0 2 4
04/04/96 04/04/96
04/05/96 04/05/96
04/06/86 04/06/96
04/07/98 04/07/96
04/08/98 24 04/08/96
04/09/98 04/09/96 5
04/1 0/96 6.4 207 04/10/96 7.8
04/11/96 04/11/96
04/12/96 04/12/96
04/13/98 04/13/98
04/14/98 04/14/98
04/15/96 04115/96
04/18/96 45 04/16/98 2
04/17/96 6.2 180 04/17/96 6.5
04/18/96 04/18/96
04/19/98 04/19/96
04/20/96 04/20/96
04/21/96 04/21/96
04/22/96 32 04/22/96 3
04/23/96 04/23/98
04/24/96 6.2 164 04/24/96 5.8
04/25/96 04/25/96
04/26/96 0-4/26/98
04/27/96 04/27/96
04/28/96 04/28/96
04/29/96 04/29/96
04/30/96 31 04/30/98 4
AVG: 6.3 193 34 44 AVG: 6.6 3 4
MAX: 6.4 207 45 44 MAX: 7.6 5 4
MIN: 6.2 160 24 44 MN: 5.6 2 4
April 1996 Page 7 ol 10 April 1996 Page 8 of 10
---- - - - ------- -- ---
GACXJtOWATEAMOITH.YMONJTORN3: GAOLNOWAlERTREAlMENTPI.ANT
( 1 ) N-ERTIER SYSlEM
RAINFALL DATA
APRIL 1998
OAlE CHEOOAY
ITEM IIIFLl£NT EFFLLENT %RED.
04/01/96 0.10
04/02/96 0.00 FLOW • TGD 2.8 2.7
04/03/98 0.00
04/04/98 0.00 COD . mg/\. 5983.B 192.8 96.8%
04/05/98 0,00
04/06/96 0.00 TSS mg/I. 13.5 44.0
04/07/98 0.00
0◄108196 0.20 Low· 5.3 8.2
04/09/96 0.00 pH
04/10/96 0.00 HIGH 5.8 8.4
04/11196 0.00
04/12/98 0.00
04/13/98 0.40 GROLNDWAlERTREAlMENTPI.ANT
04/14/98 0.00 ( 2) OUTER TEA SYSTEM
04/15/98 0.10
04/16/96 0.00
04/17/96 0.00
04/18/96 0.00 ITEM IIIFLl£NT EFFLLENT %RED.
04/19/98 0.15
04/20/98 0.45 FLOW • TGD 72.3 72.3
04/21/96 0.00
04/22/98 0.00 TSS mg/I. 4.0
04/23/96 0.00
04/24/96 0.00 LOW 5.8 5.8
04/25/96 0.00 pH
04/26/96 0.50 HIGH 8.4 7.8
04/27/98 0.00
04/28/96 0.00
04/29/96 0.90
04/30/96 0.00
AVG. 0.28
MAX. 0.90
TOTAL 2.80
April 1996 Page 9 of 10 April 1996 Page 10 of 10
-------------------
MAINTENANCE ACTIVITIES-GROUNDWATER OPERABLE UNrT #1
INNER TIER SYSfEM
ACTION
DATE LOCATION PROBLEM DATE ACTION
3/31 /96 IT-5 LOW FLOW 4/9/96 REPLACED BLADDER CLEANED SCREEN
4/9/96 IT-8 LOW FLOW 4/9/96 CLEANED PUMP & SfRAINER
4/16/96 S:R 0.0. PROBE BRACKET 4/16/96 REPLACED HOLDING BRACKET
4/26/96 IT-8 LOW FLOW 4/26/96 REPLACED PUMP & CLEANED SCREEN
4/25/96 IT-3 LOW FLOW 4/29/96 CLEANED STRAINER
4/27/96 IT-8 LOW FLOW 4/29/96 REPLACED PUMP
-------------------
MAINTENANCE ACTIVITIES-GROUNDWATER OPERABLE UNIT #1
OUTER TIER SYSTEM
ACTION
DATE LOCATION PROBLEM DATE ACTION MECHANIC
03/27 /96 OT-1 LEAK AT STRAINER 04/02/96 REPLACED STRAINER JPPP
04/01 /96 OT-1 LOW FLOW 04/01/96 CLEANED STRAINER JPPP
04/07/96 OT-1 LEAK AT STRAINER 04/08/96 REPLACED BUSHING JPPP
04/11/96 OT-1 LOW FLOW 04/11/96 CHECKED FLOW AT 17 GPM JPPP
04/11/96 OT-2 LOW FLOW 04/11/96 CHECKED FLOW AT 18.8 GPM JPPP
04/16/96 OT-1 LOW FLOW 04/16/96 ADJ. FLOW RATE AT 18.5 GPM
04/16/96 OT-4 LOW FLOW 04/18/96 REPLACED CONTROL BOX
04/24/96 OT-6A LEAK AT FLOW METER 04/24/96 TIGHTEN FIJJW METER JPPP
I
I
I INNERTIER
DAILY FLOW:
I MAY
1996: IT-1 IT-2 IT-3 IT-4 IT-5 IT-6 IT-7 IT-8 IT-9
I 05/01 /96 143 65 47 107 259 149 163 995 679
05/02/96 28 1 5 22 17 38 28 28 159 109
05/03/96 122 60 4 73 159 120 140 776 533 I 05/04/96 139 60 35 85 192 133 163 876 612
05/05/96 169 75 4 116 246 170 207 1104 771
I 05/06/96 159 76 30 118 269 159 215 1130 792
05/07/96 159 76 0 116 273 148 215 1139 796
05/08/96 157 74 0 124 28.1 146 206 1092 770
I 05/09/96 153 75 0 120 298 144 199 1063 749
05/1 0/96 142 64 83 108 267 137 184 982 692
05/11 /96 139 59 88 104 229 128 171 919 650
I 05/12/96 144 59 95 108 244 131 183 986 698
05/13/96 152 55 95 111 298 135 185 976 706
05/14/96 148 54 1 01 11 0 299 34 184 959 702
I 05/15/96 146 52 87 111 258 233 180 907 689
05/16/96 159 58 105 127 260 140 1 91 916 738
05/17/96 155 57 102 130 282 145 194 1014 745
I 05/18/96 158 60 99 121 286 143 186 992 737
05/19/96 153 56 95 114 269 144 185 986 732
05/20/96 142 51 61 131 234 135 170 914 670
I 05/21 /96 147 55 70 146 283 144 183 996 721
05/22/96 120 44 61 109 237 108 141 814 556
05/23/96 146 51 65 106 281 124 170 1011 678
I 05/24/96 156 56 72 119 316 127 183 1039 682
05/25/96 159 57 75 120 332 132 191 26 786
05/26/96 1 71 61 82 147 391 144 215 6 855
I 05/27/96 169 61 81 132 363 135 204 0 857
05/28/96 165 61 80 131 369 130 184 1074 853
05/29/96 123 46 60 95 257 98 134 837 635
I 05/30/96 158 57 80 98 276 117 1 71 992 742
05/31/96 166 56 76 187 282 122 189 999 756
I AVG: 147 58 63 114 269 132 178 861 700
I TOT: 4547 1806 1955 3541 8328 4083 5514 26679 21691
I
I
I
I
I
I OLJTERTIER
DAILY FLOW:
MAY
I 1996: OT-1 OT-2 OT-3 OT-4 OT-5 OT-6 OT-SA OT-7 OT-8
05/01 /96 17200 2160 1396 2260 6549 6693 16800 2745 14900
I 05/02/96 400 500 80 96 56 168 1 61 92 300
05/03/96 12500 12800 1322 1001 1658 4841 4924 1886 11100
05/04/96 16000 16400 2033 1438 2172 6511 6475 2791 14400
I 0 5/05/9 6 17300 18000 2224 1424 2363 6923 7079 2855 15700
05/06/96 15000 15600 2204 1409 2087 6096 6232 2808 13500
05/07/96 22500 23400 1060 1391 3017 7595 9021 2733 20400
I 05/08/96 24400 25400 825 1372 3018 8539 9675 2716 21900
05/09/96 20100 21300 1694 1400 2505 7767 8236 2760 18300
05/10/96 23500 24500 873 1377 2791 8486 9516 2696 21700
I 05/11/96 24300 24100 770 1411 2716 8633 9713 2763 21900
05/12/96 23200 23000 768 1373 2477 8325 9410 2683 21100
05/13/96 23000 23200 904 1380 1855 8375 9515 2716 21200
I 05/14/96 22400 22900 750 1374 1814 8214 9383 2665 20800
05/15/96 22400 23300 873 1394 1820 8384 9600 2725 21000
05/16/96 20800 22300 752 1359 1863 8009 9118 2613 19900
I 05/17/96 21500 23300 887 1407 1960 8448 9651 2730 20900
05/18/96 20800 22900 765 1372 1935 8267 9459 2671 20200
05/19/96 20700 23400 900 1405 1998 8379 9592 2724 20500
I 05/20/96 O.T. WELLS OFF TO TIE NEW O.T. # 2
05/21 /96 23200 10400 836 1309 1751 7564 723 2446 18500
0 5/22/9 6 27700 10000 836 1393 2092 2466 2205 2723 21800
I 05/23/96 31100 1000 737 1381 2241 7311 2450 2707 18300
05/24/96 25400 11700 828 1382 2228 8198 2668 2677 19700
05/25/96 24500 12000 720 1382 2240 8243 3018 2701 20200 I 05/26/96 23600 12200 842 1391 2246 8180 2795 2697 20200
05/27 /96 22400 12400 844 1386 2251 8155 2847 2687 20500
05/28/96 21000 12500 737 1375 2225 8077 7880 2686 20000 I 05/29/96 19200 11600 2376 1376 2197 8032 9687 2662 19700
05/30/96 17900 13600 2370 1380 2235 7970 9624 2621 19500
05/31 /96 16500 12800 2369 1375 2257 8074 9760 2661 19800 I AVG: 20003 16790 1178 1330 2144 7359 6904 2588 18597
I TOT: 620100 503700 35339 39909 64328 220779 207110 77640 557900
I
I
---- --- ----- - ------
GAOJl'CIWATEAMCMH.YMONJTOAID: GAOLN)WATEA MONTH. Y MONITORING:
N£ATIEA COMBlllEO N'LlENT #2 ITCI OUTER TIER COMBtED tfllENT: #1 OTCI
PAGEN0.1 PAGE NO. 1
MAY MAY 1996
DATE: FLOW: PH COO: TSS: TOC: DATE: FLOW: PH TOC:
GO pH ppm ppm ppm GO pH ppm
05/01/96 2607 5.4 5100 15 05/01196 70703 6.0
05/02/96 444 5.3 5260 26 05/02/98 1853 5.7
05/03/96 1987 5.5 5430 9 05103/96 52032 5.6
05/04/98 2295 5.5 5900 21 05/04/96 66220 6.2
05/05/96 2662 5.5 4750 12 05/05/96 73868 6.1
05/06/98 2948 5.4 4530 5 1718 05106196 84936 5.9 7
05107/96 2922 5.5 4000 10 05/07/96 91117 5.6
05/08/98 2850 5.7 4650 14 05/08/96 97845 5.9
05/09/98 2601 5.7 5360 15 05109/98 84082 5.9
05/10/98 2859 5.8 5360 14 05/10/96 95439 5.8
05/11/96 2487 5.5 5-410 12 05111198 98308 5.7
05/12/98 2848 5.8 5510 10 05/12/98 92338 5.8
05/13/98 2713 5.7 4970 12 1333 05/13/96 92145 5.6
05/14/98 2591 5.6 5460 24 05/14/98 90300 5.7
05/15/96 2683 5.7 5100 6 05/15/96 91498 5.7
. 05/16/96 2894 5.5 5280 13 05/16/98 88714 5.7
05/17/96 2824 5.7 5200 11 05/17/98 90783 5.9
05/18/98 2782 5.5 4980 11 05/t 8/98 88369 5.9
05/19/98 2734 5.8 4900 10 05/19/96 89598 6.0
05/20/98 2508 5.6 5680 10 05/20/98 0 5.9
05/21 /96 2745 5.5 5890 10 05/21/96 66729
05/22/96 2190 5.6 4310 11 1613 05/22/98 71215 6.0 5
05/23/96 2632 5.7 5840 11 05/23/96 67277 5.7
05/24/96 2750 5.7 4840 11 05/2◄/96 74781 5.6
05/25/96 1678 5.6 6220 10 05/25/96 75004 5.7
05126/96 2072 5.7 5720 20 05/26/96 74151 5.6
05/27/96 2002 5.4 5770 10 05/27/96 73470 5.8
05/28/96 3047 5.3 6520 12 1778 05/28/96 76480 6.0 3
05/29/96 2285 5.6 5050 6 05/29/96 76830 5.8
05/30/96 2891 5.7 6130 18 05/30/96 77200 5.8
05/31/96 2753 5.7 5200 10 05/31/96 75596 5.8
AVG: 2518 5.6 5301 13 1611 AVG: 75060 5.8 4
MAX: 3047 5.7 6520 28 1778 MAX: 97645 6.2 7
MIi'< 444 5.3 4000 5 1333 MN: 0 5.6 3
May 1996 Page 1 ol 10 May 1996 Page 2 ol 10
---- -- - -- ---- --- ---
GROJIOWATEA MCMlt.Y MONITORN3: Gfk)LN)WATER MONTH. Y MONJTOR1"6:
SBRMIXED LJOU)R: --AFTcR PIATE SEPARATOR BEFORE SBA: SBR
PAGEN0.4 PAGEN0.3
MAY 1996 SETT. Sl.1.llGE 5/DAY MAY 1996
DATE: PH: NH3N: ?04: DO MLSS: MLVSS: SQDS: WASTED F/M: F/M: DATE: PH: COO: TSS;
pH ppm ppm ppm ppm ppm ml/I gal ratio ratio pH ppm ppm
05/01/96 8.0 155 49.8 1.6 4080 2784 340 135 0.10 05/01/96 5.8 4600 24
05/02/96 6.0 90 22.4 1.8 4576 345 175 0.11 05/02/96 6.0 5660 40
05/03/96 6.0 168 31.6 1.6 3720 340 165 0.10 05/03/96 5.9 4100 16
05/04/96 8.0 165 48.0 1.6 4740 340 175 0.05 05/04/96 8.0 2900 48
05/05/96 7.9 204 44.0 1.3 4620 300 350 0.07 0,09 05/05/98 6.0 3390 8
06/06/96 8.0 149 48.0 1.0 4578 300 350 0.08 0.08 05/06/98 6.1 3110 18
05107196 6.1 158 40.0 1.8 5084 300 320 0.08 0.07 05/07/98 5.6 3400 16
05/08/96 8.0 200 40.0 1.5 8820 4112 290 335 0.08 0.06 05/08/96 5.6 4310 12
05/09/96 8.0 156 30.6 1.4 3852 290 351 0.10 0.07 05/09/98 . 5.6 4160 18
05/1 0/96 6.1 147 25.3 1.7 5268 280 148 0.08 0.07 05/10/96 5.7 4600 24
05/11 /96 6.0 150 30.D 1.6 5200 275 146 0.08 0.07 05/11/96 5.8 4710 40
05/12/96 6.2 142 28.4 1.6 5204 260 189 0.08 0.08 05/12/96 5.7 4820 32
05/13/96 6.0 165 13. 1 1.4 4880 370 188 0.10 0.09 05/13/96 5.7 5380 24
05/14/98 7.6 137 22.6 1.8 4104 370 160 0. 11 0.08 05/14/96 5.5 6210 12
05/15/98 7.9 164 28.5 1.8 5048 3212 380 188 0.09 0.09 05/15/96 8.3 6000 58
05/16/98 8.0 135 18,0 1.8 4800 410 190 0.10 0.10 05/18/98 5.8 5250 48
05/17/98 8.0 129 17.0 1.8 3880 420 190 0.11 0.10 05/17/98 5.8 4850 36
05/1 8/96 5.9 125 28.0 1. 7 3360 420 202 0.13 0.11 05/18/96 5.9 5020 44
05/19/96 7.9 134 36.0 1.6 3560 350 135 0.12 0.11 05/19/98 5.4 4850 24
05/20/96 6.0 121 14.0 1.9 3724 360 148 0.13 . 0.12 05/20/98 5.9 5400 20
05/21/96 8.0 108 11.0 1.8 3760 340 148 0.12 0.12 05/21/98 5.9 5100 40
05/22/98 7.9 100 12.6 1.8 4720 3200 350 162 0.09 0.12 05/22/98 5.8 5020 58
05/23/96 7.8 118 19.0 1.6 4648 330 162 0.09 0.11 05/23/98 5.9 4620 44
05/24/96 7.9 110 24.8 1.7 5012 320 175 0.09 0.10 05/24/98 5.9 4820 40
05125196 6.0 120 26.0 1.5 4380 340 150 0.10 0.10 05/25/98 5.8 5110 44
05/26/96 8.0 100 22.4 1.8 4524 340 162 0.12 0.10 05/26/98 5.9 8020 40
05/27/96 7.9 77 12.5 1.5 5240 350 180 0.09 0.10 05/27/96 5.8 5380 44
05/26/96 7.9 47 27.3 1.9 3968 350 200 0.13 0. 11 05/28/96 5.7 5710 40
05129/96 7.8 66 26.4 1.7 4800 3124 390 202 0.14 0.12 05/29/96 5.3 7500 28
05/30/96 7.8 97 38.5 1.9 4800 370 180 0.08 0.11 05/30/96 5.4 4190 56
05/31/96 7.8 48 29.6 1.5 3600 350 148 0.12 0.11 05/31/96 5.6 4750 24
AVG: 7.8 129 28 2 4528 3286 341 198 0.10 0.10 AVG: 5.8 4810 33
MAX: 8.2 204 50 2 6620 4112 420 351 0.14 0.12 MAX: 6.3 7500 56
MIN: 5.9 47 11 3360 2784 275 135 0.05 0.06 MN: 5.3 2900 8
May 1996 Paga 3 of 10 May 1996 Page 4 ol 10
------- - --- -- --- - --
GROJ1'0WA TEA MONTH. Y MONITORN3: GFUN)WATER MONT1-L Y MONITORING:
SBR EFFLLEr-IT:(DECANT] #4SBRE INl>ERTIER EQUALIZATION TA>a<: ITEOT
PAGEN0.5 PAGEN0.2
MAY 1996 WAS. NH3N PHOs. MAY 1996
DATE: FLOW: COO: TSS:TSS ADDEO: ADDEO: DATE: Pft COO: OT WATER ADDEO
GFO ppm ppm ppm gal Iba pH ppm gal
05/01/96 2280 140 92 9220 0 05/01 /96 7.3 4700
05/02/96 2145 150 72 11240 3 1 05/02/96 7.3 5880
05/03/96 2364 130 60 9460 0 0 05/03/98 7.3 2450
05/04/96 2244 140 66 9800 1 05/04/96 7.3 2850
05/05/96 2277 146 56 9120 0 0 05/05/98 7.3 3560
05/06/96 2263 180 72 10000 0 0 05/06/96 7.3 3210
05107196 2297 140 84 12900 0 0 05101196 7.2 4300
05/08/98 2273 124 66 12000 0 (i 05108198 7.3 4630
05/09/98 2302 130 98 10440 0 0 05/09/96 7.3 4620
05/10/98 2330 120 92 10800 1 05/10/96 8.4 4860
05/11/98 2211 140 60 10400 1 05/11/98 8.3 4790
05/12/96 2208 145 84 10440 0 0 05/12/96 8.2 4890
05/13/96 2249 150 148 .10620 2 05/13/98 7.3 5450
05114/98 2280 153 40 9120 1 05/1 ◄/96 7.2 6140
05/15/98 2313 135 44 11720 05/15/98 7.8 4900
05/16/96 2258 117 40 SUD 05/18/98 7.7 5310
05/17/96 2273 130 80 BUD 05/17/96 7.0 6500
05/18/96 2273 130 84 9000 05/18/96 7.2 4980
05/19/96 2397 155 80 9420 0 05/19/96 7.2 4910
05/20/96 2387 190 80 10200 1 05/20/96 7.0 5250
05/21/96 2323 188 44 10280 2 2 05/21/96 7.8 5180
05/22/96 2300 183 48 10940 3 3 05/22/96 7.5 5027
05/23/96 2330 190 58 9400 05/23/96 7.6 6480
05/24/96 2297 208 80 6400 05/24/96 7.5 5240
05/25/96 2285 171 78 9600 1 05/25/96 7.6 5150
05/26/96 2296 167 80 10660 3 05/26/96 7.5 5730
05/27/96 2271 160 76 10400 2 05/27/98 7.3 4780 375
05/28/98 2075 190 32 10540 2 1 05/28/96 7.5 5690 558
05/29/96 2242 210 60 9000 5 2 05/29/96 7.6 4750
05/30/96 2277 224 48 10920 2 0 05/30/96 7.3 4850
05/31/96 2252 195 48 12140 5 1 05/31/96 7.0 5100
AVG: 2276 156 89 10154 1 1 AVG: 7.4 4844 468
MAX: 2397 224 148 12900 5 3 MAX: 8.4 6480 556
MIN: 2075 117 32 8140 0 0 MIii: 7.0 2450 375
May 1996 Page 5 of 10 May 1996 Page 6 of 10
--- - - - - - - --- - --- ---
GROJl'OWATEAMONTH...VMONrroRNJ: GAOLff)WATEA MOml-L V MONITORJNG:
NERTIE A CAABON FL TEA EFFLLENT 118 ITEF OUfEA TIER CAABON FL TEA EFfllENT: #70TEF
PAGE NO. 7 PAGEN0.3
MAY 1996 MAY 1996
DATE: PH: COD: TOC: TSS: DATE: PH: TOC: TSS:
pH ppm ppm ppm pH ppm ppm
05/01/96 8.0 140 38 05/01/96 7.1 4
05/02/98 05/02/96
05/03/98 05/03/96
05/04/96 05/04/98
05/05/96 05/05/96
05/06/96 187 05/08/96 8
05/07/96 05/07/96
05/08/96 8.3 100 05/08/98 7.1
05/09/96 05/09/96
05/10/98 05/10/98
05/11/96 D5/11/96
05/12/96 05/12/98
05/13/98 21 05/13/98 3
05/14/98 05/14/98
05/15/98 8.3 130 05/15/96 8.8
05/16/96 05/16/96
05/17/96 05/17/96
05/18/98 05/18/96
05/19/96 05/19/96
05/20/98 05/20/98
05/21 /96 05/21/98
05/22/96 8.2 131 57 05/22/96 8.7 2
05/23/98 05/23/96
05/24/98 05/24/96
05/25/96 05/25/96
05/26/96 05/28/96
05/27/96 05/27/96
05/28/96 32 05/28/96 3
05/29/96 8.2 210 05/29/96 8.5
05/30/96 05/30/96
05/31/96 05/31/96
AVG: 8.2 142 89 38 AVG: 6.8 4 4
MAX: 8.3 210 187 38 MAX: 7.1 6 4
MIN: 8.0 100 21 38 MN: 8.5 2 4
Mey 1996 Pege 7 of 10 May 1996 Page 8 of 10
-- - -- - ------- ---- - --
GFOlWWATEA MONTH. Y Mo.lrTORNG: . GR'.JUtlJWATERTREATMENTPLANT
(1) NERTERSVSTEM
RAINFALL DATA
MAY 1996
DATECHEOOAY
fTEM L'FLLENT EFR.LENT %RED.
05/01/96 0.00
05/02/96 0.00 FLOW • TGD 2.5 2.5
05/03/96 0.00
05/04/96 0.00 COD . mg/L 5275.5 142.2 97.3%
05/05/96 0.00
05/06/96 0.00 TSS • mg/L 12.7 36.0
05/07/96 0,00
05/08/96 0.00 LOW 5.3 6.0
05/09/96 0.00 pH
05/10/96 0.00 HIGH 5.7 8.3
05/11/96 0,20
05/12/96 0.00
05/13/96 0.10
05/14/96 0.00 OOTES
05/15/96 0.00
05/16/98 0.00 OLfTIER TIER waLS OFF 05120/98 TO CONNECT NEW Q.T. 2
05/17/96 0.00 TO HEADER AID TO TIE IN ELECTRICAL
05118/96 0.00
05/19/96 0.00
05/20/96 0.00 GFD..Jt,OWATEA TREATMENT Pl.ANT
05/21/96 0.00 (2) aJTERTERSVSTEM
05/22/96 0.00
05/23/96 0.00
05/24/96 0.90
05/25/96 0.00 fTEM L'FLLENT EFR.LENT %RED.
05/26/96 0.30
05/27/96 0.40 FLOW • TGD 75.0 75.0
05/28/98 0.00
05/29/96 0.20 TSS . mg/L 4.0
05/30/96 0.00
05/31/96 0.00 LOW 5.6 6.5
pH
TOTAL 2.10 HIGH 6.2 7. 1
May 1996 Page 9 of 10 May 1996 Page 10 of 10
-------------------
MAINTENANCE ACTIVITIES-GROUNDWATER OPERABLE UNIT #1
INNER TIER SYSTEM
ACTION
DATE LOCATION PROBLEM DATE
05/06/96 IT-3 LOW FLOW 05/10/96
05/27/96 IT-8 NO FLOW 05/28/96
ACTION
REPLACED BLADDER & EXHAUSTER VALVE
CLEANED OUT SUPPLY LINE FROM PUMP
REPLACED PUMP AND CLEANED STRAINER
MECHANIC
JPPP
JPPP
-------------------
MAINTENANCE ACTIVITIES-GROUNDWATER OPERABLE UNIT #1
OUTER TIER SYSTEM
ACTION
DATE LOCATION PROBLEM DATE ACTION MECHANIC
05/06/96 OT-2 LOW FLOW 05/07 /96 CLEANED STRAINER JPPP
05/07 /96 OT-1 LOW FLOW 05/07 /96 CLEANED STRAINER JPPP
05/07/96 OT-6 LOW FLOW 05/07 /96 REPLACED FLOW METER JPPP
05/22/96 OT·6A LOW FLOW 05/22/96 CLEANED STRAINER ..M
05/23/96 OT-6A LOW FLOW 05/28/96 ADJUSTED FLOW JPPP
05/26/96 OT-2 REPLACEMENT 05/26/96 WELL IN PRODUCTION
I JUNEF55WEU.S
I INNERTIER
DAILY FLOW:
I
I JUNE
1996: IT-1 IT-2 IT-3 IT-4 IT-5 IT-6 IT-7 IT-8 IT-9
I 06/01 /96 164 57 65 100 300 11 9 194 988 766
06/02/96 160 56 61 99 317 115 190 982 741
I 06/03/96 160 54 80 103 345 119 192 910 730
06/04/96 153 55 84 103 375 119 190 979 731
06/05/96 154 57 89 113 402 131 205 1057 742
I 06/06/96 160 56 91 1 1 400 125 193 1004 752
06/07/96 175 61 92 11 0 382 127 191 880 416
06/08/96 167 61 91 91 386 125 178 3534 0
I 06/09/96 151 53 103 71 328 113 168 1469 654
06/1 0/96 164 55 117 63 417 115 193 1099 214
06/11/96 162 55 113 77 409 11 8 176 1067 178
I 06/12/96 163 54 115 77 375 144 174 1052 696
06/13/96 163 51 112 73 374 93 175 1052 491
06/14/96 159 55 107 80 380 114 176 935 614
I 06/15/96 150 53 104 71 383 109 168 986 441
06/16/96 153 56 108 48 397 113 172 1088 0
06/17/96 156 54 118 50 420 117 174 1107 164
I 06/18/96 153 53 113 61 370 112 172 1079 568
06/19/96 139 49 103 72 360 103 159 982 566
06/20/96 146 52 1 1 1 82 360 11 0 164 968 523
I 06/21 /96 13 5 1 0 8 36 10 16 87 21
06/22/96 150 54 117 63 358 109 176 1015 550
06/23/96 165 52 111 93 407 122 214 1116 267
I 06/24/96 162 49 106 81 387 114 204 1059 155
06/25/96 163 50 114 53 396 115 202 1053 646
06/26/96 158 50 109 50 386 115 196 1049 727
I 06/27/96 156 51 111 85 400 118 192 1074 723
06/28/96 151 50 106 93 396 115 164 1065 717
06/29/96 149 50 1 1 1 92 398 112 166 1080 699
I 06/30/96 144 50 108 93 408 111 165 1090 689
I AVG: 152 52 99 76 368 113 177 1097 506
I TOT: 4563 1558 2980 2266 11052 3382 5299 32906 15181
I
I
I JUNEF55WEUS
I OUTERTlER
DAILY FLOW:
I
JUNE
I 1996: OT-1 OT-2 OT-3 OT-4 OT-5 OT-6 OT-GA OT-7 OT-8
06/01 /96 15000 12700 2332 1357 2241 7967 9648 2617 19600
I 06/02/96 14000 13200 2361 1387 2283 8090 9811 2645 19900
06/03/96 12100 13300 2372 1389 2275 7977 9603 2667 19800
06/04/96 6600 11100 2290 1370 1921 6291 7384 2600 16400 I 06/05/96 11700 700 36 1064 1792 5964 7218 1978 16200
06/06/96 18600 10300 0 1407 2232 7246 8639 2694 19200
06/07/96 13400 9100 2554 1400 1881 5101 6022 2735 12600 I 06/08/96 10900 7800 2163 1404 1686 4216 4998 2662 10300
06/09/96 23100 12000 1934 1382 3225 8130 9614 2648 20500
I 06/10/96 22200 12100 2153 1358 3079 8086 9605 2671 19200
06/11/96 21700 12100 2383 1379 2837 7991 9434 2739 20900
06/12/96 21500 12000 2122 1355 2669 7884 9247 2773 19800
I 06/13/96 21700 12200 2375 1377 2638 7996 9413 2800 19900
06/14/96 21600 12300 2124 1361 2524 7908 9350 2773 19800
06/15/96 21700 12200 2361 1371 2480 7902 9351 2789 19800
I 06/16/96 21600 12300 2168 1373 2444 7953 9411 2806 19800
06/17/96 21700 12400 2125 1378 2451 7944 9413 2799 19900
06/18/96 21300 12100 2347 1370 2429 7861 9286 2757 19600
I 06/19/96 21100 12000 2324 1355 2418 7872 9275 2769 19400
06/20/96 18200 10900 2349 1381 2102 6949 8094 2744 16800
06/21 /96 21500 10500 1087 1338 1863 7776 9218 2662 19300
I 06/22/96 21700 11100 1419 1382 1901 7871 9382 2731 19400
06/23/96 21000 12300 1878 1384 1890 7947 9382 2761 19200
06/24/96 22300 12000 2148 1360 1757 7779 9098 2718 18300
I 06/25/96 23500 12400 2372 1379 1800 7866 9221 2774 18500
06/26/96 23500 12500 2324 1356 1673 7793 9135 2738 18200
06/27/96 24000 12600 2280 1366 827 7845 9192 2747 18200
I 06/28/96 24500 12000 2256 1344 851 7648 8956 2699 17700
06/29/96 24800 12100 2297 1363 952 7754 9014 2724 17600
06/30/96 25100 12500 2375 1383 1521 7772 9117 2680 18300
I
AVG: 19720 11427 2044 1362 2088 7513 8884 2697 18470
I TOT: 591600 342800 61309 40873 62642 225379 266531 80900 554100
I
I
I
-- - -- - - - - --- --- - - --
GROUIOWATEA MONlH. V MONfTOANi: GROI.IDWATEA MONTH. V MONITOAW3:
N'EATIEA COMBINED l\FI.LENT #2 ITCI OUIEA TIER COMBtED l\FI.LENT: #1 OTCI
PAGE t-.0.1 PAGEN0.1
JUNE 1896 JUNE 1996
DATE: FLOW: Pit COO: TSS: TOC: DATE: FLOW: Pit TOC:
GO pH ppm ppm ppm GO pH ppm
06/01/96 2753 5,4 4850 10 06/01/96 75596 5.9
06/02/96 2721 5.6 5460 14 06/02/96 73677 5.9
06/03/96 2693 5.8 5100 15 06/03/96 71483 8.2
06/04/96 2769 5.7 6480 30 1337 06/0-4/98 55956 8.1 5
06/05/96 2950 5.7 5750 ,. 06/05/96 -16652 8.0
08/06/96 2892 5.8 5400 26 06/06/98 70318 6.0
06/07/96 2434 5.6 5330 11 08/07/96 64793 5.9
06/08/96 4553 5.7 5360 10 06/08/96 46129 5.8
08/09/98 3110 5.6 5240 9 06/09/96 82533 5.5
08/10/96 2437 5.7 5040 6 06/10/96 80452 5.7
06/11 /96 2355 5.4 6950 3 1378 06/11/96 61◄63 5.9 3
06/12/96 2650 5.6 6890 5 06/12/96 79350 5.8
06/13/98 2584 5.4 6450 5 08/13/96 80399 5.9
08/14/96 2820 5.4 10200 1 06/14/98 79740 8.1
06/1 6/96 2464 5.3 5700 9 06/15/96 7995 .. 5.6
06/16/98 2135 5.4 6500 4 '06/16/96 79855 5.7
08/17/96 2380 5.5 796D 24 06/17/96 80110 5.9
06/18/96 2681 5.6 5500 13 2426 06/18/96 7923-4 5.e 6
06/19/96 2533 5.5 6040 8 06/19/98 79234 5,7
06/20/98 2516 5.8 5720 5 08/20/98 69519 5.6
06/21196 206 5.5 7000 22 06/21/96 75244 6.2
06/22/96 2592 5.6 5620 12 08/22/98 76888 5,9
06/23/98 2547 5.5 6380 9 08/23/96 77742 5.9
06/24/96 2317 5.5 7050 29 08/24/96 77460 6.0
06/25196 2791 5.8 5270 20 06/25/96 79812 6.1
06/26/96 2840 5.5 5190 18 2126 06/26/96 79219 6.0 5
06/27/96 2910 5.4 5270 19 06/27/96 79057 5.3
06126196 2857 5.4 5140 ,. 06/28/96 77954 5.e
06/29/96 2857 5.3 5340 11 08/29/96 78604 5.3
06/30/98 2858 5.3 5200 10 06/30/96 80748 5.7
AVG: 2640 5.5 5913 13 1454 AVG: 74306 5.8 4
MAX: 4553 5.7 10200 30 2428 MAX: 82533 6.2 6
MIN: 206 5.3 4850 3 0 MN: 46129 5.3 0
June 1996 Page 1 of 10 June 1996 Page 2 of 10
-- -- -- - - - - -- - --- ---
GROJrDWATEAMO.ffi-LYMONITO~: GAOlH)WAlEA MON11-t. Y MONITOAJNG:
SBA MIXEO LIQUOR: SRAL AFTER PlAlE SEPARATOR BEFORE SBA:
PAGEN0.4 PAGEN0.3
JUNE 1996 SETT. SI.I.IJGE 5/0AY JUNE 1996
DAlE: Pl-t NH3N: P04: DO: MI.SS: MLVSS: sa.os: WAS'IED F/M: F/M: DAlE: Pl-t COO: TSS:
pH ppm ppm ppm ppm ppm ml/t gal ratio ratio pH ppm ppm
06/01/96 7.6 64 40.4 1.6 3744 260 162 0.11 06/01/96 6.2 4850 16
06/02/96 7.6 74 28.0 1.3 3880 330 135 0.13 06/02/96 8.3 5450 12
08/03/96 7.9 84 21. 1 1.8 3838 280 175 0.15 06/03/96 8.2 8310 24
06/04/96 7.7 4 18.8 1.9 5400 270 175 0.10 06/04/96 5.8 6240 32
06/05/96 7.7 14 13.2 1. 7 4696 280 175 0.10 0.12 06/05/96 5.7 5160 48
06/06/96 7.8 44 14.1 1.5 3552 3200 270 175 0.13 0.12 08/08/96 8,1 5250 20
06101196 7.7 34 9,6 1.8 4800 270 175 0.09 0.11 06/07/96 8.1 6050 24
06/08/96 7.8 40 10.0 1.8 4880 265 175 0.09 0.10 08/08/98 6.7 6110 84
06/09/96 7.8 38 9.0 1.8 4960 275 175 0.09 0.10 08109198 6.9 5090 80
06/10/96 7.7 40 18.0 1. 7 4852 310 182 0.09 0.10 06/10/96 6,8 4490 84
06/11/98 7.7 50 30.0 1.9 3880 340 200 0.11 0.10 06/11/98 5.8 ,USO 40
06/12/96 7.8 65 22.0 1.9 4538 3064 340 202 0. 11 0.10 08/12/96 5.9 5400 36
06/13/96 7.9 107 19.8 1.6 46D0 350 202 0. 11 0.10 06/13/98 6.8 5500 20
08/14/98 7.9 110 16.8 1.6 3560 310 169 0.14 0.11 08/14/98 6.0 5700 36
08/15198 7.9 114 40.0 1.3 3560 300 169 0.12 0.12 06/15/98 6.4 4850 32
06/18/96 7.9 112 38.0 1.6 3384 260 202 0.13 0.12 06/16/96 5.8· 4950 20
06/17/96 6.2 139 34.0 1. 7 4744 290 202 0.09 0.12 06/17/96 5.6 5060 52
06/18/96 6.1 145 24.0 1.5 3672 270 260 0.13 0.12 06/18/96 6.7 5450 16
06/19/98 6.2 110 27.8 1.5 4344 2320 260 200 0.12 0.12 08/19/98 6.6 5750 20
06120196 6.0 189 18.4 1.7 4844 200 180 0.09 0.11 06120196 6,9 4810 40
06/21/96 6.1 141 56.0 1.2 4852 200 80 0.00 0.09 06/21/96
06122196 8,0 130 48.8 1.8 4480 190 202 0.13 0.09 06/22/96 5.6 6350 48
06/23/96 6.1 110 36.4 1. 7 4640 150 250 0.12 0.09 06/23/96 8.0 6100 40
06/24/96 8.1 106 39,4 1.6 3560 160 230 0.13 0.09 06/24/96 5.8 5340 40
06/25/96 8.2 136 27.0 1.9 3260 150 250 0.16 0.11 06/25/96 5.7 5880 72
06/26/96 6.1 154 28.2 1.9 3640 2400 160 189 0.13 0.13 06/26/96 6.0 5490 28
06127196 6,1 106 26.0 1.7 3400 170 189 0.14 0.14 06/27/96 5.6 5310 52
06/28/96 8.2 118 15.6 1.8 3040 170 165 0.14 0.14 06/28/96 5.9 4910 80
06/29/96 6.0 132 22.1 1.8 3012 170 189 0.15 0.14 06/29/96 6.1 4950 140
06/30/96 6.0 120.0 33.6 1.6 3040 150 135 0.14 0.14 06/30/96 6.1 4800 26
AVG: 7.9 94 26 2 4075 2748 247 185 0.12 0.11 AVG: 5.9 5322 44
MAX: 6.2 169 56 2 5400 3200 350 250 0.18 0.1◄ MAX: 8.3 6350 140
MIN: 7.8 4 9 3012 2320 150 80 0.00 0.09 MN: 5.4 4490 12
June 1996 Page 3 of 10 June 1996 Page 4 of 10
-- -- - ---- - -- - --- - -
GAOJl'OWATEAMON!l-l.YMONITORN3: GROLN)WATER MONTH. Y MONITORJNG:
SBREFFLUENT~OECANT] #4 SBRE IWERTIER EQUALIZATION TAAi<: ITEQT
PAGE N0.5 PAGEN0.2
JUNE 1996 WAS. NH3N Pl-06. JUNE 1996
DATE: A.OW: roo. TSS: TSS AOOEO: AOOEO: DATE: PH: COO: OTWATERADOED
cro ppm ppm ppm gal lbs pH ppm gal
06/01/96 2407 205 80 11740 2 06/01/96 7 .1 4850
06/02/96 2317 220 84 10660 2 06/02/96 8.8 5150
06/03/96 2298 181 58 9080 2 08/03/98 7.0 5080
06/04/98 2538 192 148 8800 5 08/04/96 7.1 8310
06/05/96 2536 176 116 13400 3 06/05/96 7.4 5210
06/06/96 2534 210 60 11600 3 1 06/06/96 7.2 5150
06/07198 2548 215 72 8600 3 1 06/07/96 7.6 6140
06/08/96 1911 200 60 10000 4 2 08/08/96 7.6 6210
06/09/96 2827 100 60 10200 6 2 08/09/96 7.7 6180
08/1 D/98 2280 313 116 9060 8 06/10/96 7.0 6060
08/11 /96 22.U 340 144 9740 8 06/11/96 6.6 6350
06/12/96 2168 350 68 10920 6 06/12/96 7.1 6500
06/13/96 1975 360 120 9140 6 1 08/13/96 7.1 620D
08/14/98 2181 405 168 8000 8 3 06/14/96 7.0 6800
06/15/96 2198 430 80 8800 6 3 06/15/96 7.4 4900
06/16/96 1728 400 66 10320 6 0 06/16/96 7.3 5100
06/17196 2194 500 124 11140 • 0 06/17/96 7.2 8450
08/18/96 1817 520 130 11480 4 06/18/96 7.1 5700
06/19/96 2190 683 98 11300 4 06/19/96 7.2 6894
06120196 2229 812 40 14220 2 06/20/96 7.3 4870
06/21 /96 0 580 120 11260 2 0 06/21/96 7.3 4880
06/22/96 2126 620 100 10700 2 0 06/22/96 7.2 6520
06/23/96 2178 663 120 10920 4 0 06/23/96 7.3 6240
06/24/96 2205 665 218 10600 4 0 06/24/96 7.1 5870
06/25/96 2190 628 180 10000 2 06/25/96 7.2 6150
06/26/96 2135 518 204 13800 • 06/26/96 7.1 6281
06127196 2346 519 218 9240 6 1 06/27/96 7.2 5410
06/28/96 2242 536 80 11260 5 2 06/28/96 7.1 5090
06/29/96 2356 617 280 17560 5 2 06/29/96 7.4 5340
06/30/96 2281 580 220 11060 5 06/30/96 7.4 4700
AVG: 2169 426 122 10820 4 1 AVG: 7.2 5446 #DIV/01
MAX: 2627 665 280 17560 8 3 MAX: 7.9 6520 0
MIN: 0 161 40 6000 2 0 MN: 8.8 4650 0
June 1996 Page 5 ol 10 June 1996 Page 6 of 10
--- ---- - - - - - - - -----
GRO.Jt-r)WATER MOOTlt.Y MONITOAN3: GAOlIDWAlER MONTI-LY MONfTORlr-13:
NEATIERCARBONFLlEAEffiUENT #8 ITEF OUTER TIER CARBON FL lER EffiUENT: 17OTEF
PAGE NO. 7 PAGEN0.3
JUNE 1996 JUNE 1996
DATE: PH: COO: TOC: TSS: DAlE: PH: TOC: TSS:
pH ppm ppm ppm pH ppm ppm
06/01/96 06/01 /96
06/02/96 06/02/96
06/03/96 06/03/96
06/04/96 10 08/04/96 3
06/05/96 8.2 170 24 06/05/96 8.4 15
06/06/96 06/06/96
06/07/96 06/07/96
06/08/96 06/08/96
06/09/96 08/09/96
06/10/96 06/10/96
06/11196 48 06/11/96 2
06/12/96 8.0 320 06/12/96 6.8
06/13/96 06/13/96
06/14/96 06/14/96
06/15/96 08/15/96
06/16/96 06/16/96
06/17/96 06/17/96
06/18/96 27 06/18/98 3
06/19/96 6.0 219 06/19/96 7.1
06/20/98 06/20/96
06/21/96 06/21/96
06/22/96 08/22/96
06/23/96 06/23/96
06/24/96 06/24/96
06/25/96 06/25/96
06/26/96 8.1 512 12 08/26/96 7. 1 5
06/27/96 06/27/96
06/28/96 06/28/96
06/29/96 06/29/96
06/30/96 06/30/96
AVG: 7.8 305 24 24 AVG: 8.9 3 15
MAX: 8.2 512 48 24 MAX: 7. 1 5 15
MIN: 8.0 170 10 24 MN: 8.4 2 15
June 1996 Page 7 of 10 June 1996 Page 8 of 10
--- - ----- -
GROJNJWATERMONTH.YMON/TOANG:
RAINFALL DATA
OATECHESDAY
06/01/96 0.00
06102196 0.00
08/03/96 0.00
06/04/96 0.20
06/05/96 0.00
06/06/96 0.00
06/07/96 0.00
06/08/96 2.00
06/09/96 0.10
06/10/96 0.20
06/11/96 0.00
06/12/98 0.20
06/13/96 0.10
06/14/98 0,00
06/15/96 0,00
06/16/96 0.00
06/17/96 0.00
06/18/96 0.00
06/10/96 0.00
06/20/96 0.00
06/21 /98 0.00
06/22/96 0.00
06/23/96 0.00
06/24/96 0.00
06/25/96 0.00
06/26/96 0.00
06/27/96 0.00
06/28/96 0.00
06/29/96 0,00
06/30/96 0,00
lOfAl. 2.00
AVG 0.46
June 1996 Page 9 ol 10
--
JUNE 1996
fTEM
FLOW • TGD
COD • mg/I.
TSS mg/I.
LOW
pH
HIGH
fTEM
FLOW -TGD
TSS mg/I.
LOW
pH
HIGH
June 1996
- --
GAOLNDWATER TREAlMEt,ff PUWT
Ill-ER TEA SYSTEM
l>ELUEM" EFfll.ENT %RED.
2.6 2.6
5937 .2 305,3
13.2 24.0
5.3 6.0
5.7 6.2
GAOLNDWATERTREAlMEt,fff'UWT
OlfTERTER SYSTEM
llfl.lJENT EFFl.LENT %RED.
74. 1 74.1
15.0
5.3 6.4
6.2 7.1
----
94.9%
Page 10 of 10
-------------------
MAINTENANCE ACTIVITIES-GROUNDWATER OPERABLE UNIT #1
INNER TIER SYSTEM
DATE
06/17/96
06/17/96
LOCATION
STRIPPER
IT-9
PROBLEM
DISCHARGE PUMP
NO FLOW
ACTION
DATE ACTION
06/18/96 REPI.ACEDPUMP
06/25/96 CLEANED PROBES AND RESET
MECHANIC
JPPP
JPPP
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MAINTENANCE ACTIVITIES-GROUNDWATER OPERABLE UNIT #1
OUTER TIER SYSTEM
ACTION
DATE LOCATION PROBLEM DATE
06/06/96 OT-1 LOW FLOW 06/06/96
06/06/96 OT-2 LOW FLOW 06/06/96
06/27/96 OT-5 LOW FLOW 06/27/96
ACTION MECHANIC
REPLACED PUMP JPPP
SET FLOW JPPP
ADJUSTED FLOW JPPP
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Attachment 2
QA Summary Report and Analytical Data for the
January 15-16, 1996 Sampllng Event
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SDG Narrative:
PROJECT DATA ASSESSMENT
Hoechst Celanese -Shelby, NC
First Quarter 1996 Sampling Event
This report summarizes the assessment of field and laboratory data generated from the January
1996 sampling event at the Hoechst Celanese -Shelby, North Carolina plant The sampling and
analysis was conducted by Shealy Environmental Services, Inc. (SES!) according to the revised
Sampling and Analysis Plan (document control nos. 026SB-0005a and 026SB-0038). All
analyses were performed according to Test Methods for Evaluating Solid Waste.
Physical/Chemical Methods (including Update I) and EPA 600/4-79-020 Methods for Chemical
Analysis of Water and Wastes. TJSEPA March 1993 for the following parameters:
1. pH by EPA Method 150.1, Temperature by EPA Method 170.1 and Conductivity by EPA
Method 120.1 (field analyzed and documented in the Field Log)
2. Total Organic Carbon (TOC) by EPA Method 415.1
3. Toxic Metals by EPA Methods 6010A and 7470A
4. Toxicity Characteristic Leach Procedure ("Full" TCLP) by EPA Method 1311
5. Volatile Organic Compounds (VOCs) by EPA 8260A
6. Semi-volatile Organic Compounds (SVOCs) by EPA Method 8270B
7. Pesticides/PCBs by EPA Method 8080A
8. Herbicides by EPA Method 8150B
9. Ethylene Glycol by EPA Method 8015A (modified)
Definitions:
Class A Data:
Class B Data:
Class C Data:
Data Qualifier U:
Data Qualifier R:
useable for quantitative purposes
useable for qualitative assessment of absences or presence
unusable data
the analyte was not detected at the reported concentration due to its presence
in the associated method blank
the sample results are rejected due to serious deficiencies in the ability to
analyze the sample and meet quality control criteria.
1
Data Quality Assessment:
Field Sampling and Handling
Ground water samples from the monitoring wells, domestic wells and process points were
collected according to their specific sampling procedures. The pH, temperature and conductivity
measurements were taken by SES! personnel and documented in the Field Log Book. The data
indicates that stability of the parameters were generally achieved after purging three well volumes,
where applicable.
1. All samples were collected according to the Sampling and Analysis Plan matrix. All field
measurements were documented in the Field Log Book.
2. All necessary field QNQC samples were collected at an acceptable frequency with the
exception of TOC duplicates which were not collected (see laboratory section below).
3. All sample related information was documented on the Chain-of-Custody (COC) forms with
the following exceptions:
a. The COC did not contain client's address or the project manager's telephone
number.
b. The specific methods of analysis were not filled in on the COC as required by this
COC's particular format
Note: These deficiencies did not compromise the quality of the analytical data.
Laboratory Analysis
Total Organic Carbon by EPA Method 415,1
Two process point and two monitoring well samples were collected and analyzed for Total Organic
Carbon. All method acceptance criteria were met (Class A).
2
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Laboratory Analysis (cont.)
Toxicity Characteristic Leach Procedure CTCLP) RY EPA Method 1311
Two sludge samples were collected and analyzed for full TCLP analysis. The samples were
processed according to EPA Method 1311 after it was determined that the % solids were at a
concentration high enough that both ZHE (VOCs) and SVOA/Metals extractions were necessary.
The samples were extracted and analyzed within method holding times. All acceptance criteria for
methods 6010A, 7470A, 8260A, 8270B, 8080A and 8150B were met (Class A) with the
following exceptions:
1. The TCLP digested blank for metals determinations contained Barium (Ba) at
0.009 mg/L. This is a common lab contaminant from the TCLP filter. Samples
with Ba results > PQL but less than 0.09 mg/L Ba will be flagged with a U
(Class B).
2. The mercury (Hg) results were obtained without running a daily calibration curve as stated
in the method. Consequently, the Hg results for these two sludge TCLP samples should
be flagged with an R (Class C).
Volatile Organic Compounds RY EPA Method 8260A
Three process point, two domestic wells and thirteen monitoring wells were collected and analyzed
for VOCs. All method acceptance criteria were met (Class A).
Ethylene Glycol by EPA Method 8015A (modified)
Two process point samples were collected and analyzed for ethylene glycol using a modified
version of Method 8015A. All method acceptance criteria were met (Class A).
Discussion:
For the DQOs of this project (level II and level III) to be met, the data was assessed based on the
following overall project criteria:
• holding times • completeness
• blank contamination • transcription accuracy
• report qualifiers • comparability/consistency with historical data
Non-conformances not mentioned above in the method criteria assessments include failure to
establish precision due to the absence of laboratory sample duplicates and/or field sample duplicate
for TCLP and TOC analyses. Although not a method requirement, this information is used to
evaluate precision with these methods of high variability. However, based on the project criteria
mentioned above, thess data were assessed as Class A data.
HCC-Shelby QI 1996 3
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--i/ 1
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I I.
I II.
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I III.
I IV.
I V.
I VI.
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TABLEOFCON1
Master Tracking List
Case Narratives
(By analytical test method)
Sample Results
(By analytical test method)
Quality Control Data
(By analytical test method)
Field Data Summary
Chain of Custody Records
}:::(_,¾ c:,;:;).],J~B-oa'-1-~
-i-;r\r=nr-i~G') ; ~-: ~~~--t.:-.= ... .-:. _:,,:: I
; ,...,,
-------------------
Client Sample
ldcnlilication
ITCI
ITEF
ITIW DUPLICATE
OTCI
OTEF
SBR WASTED SLUDGE
FILTim PRESS SLUDGE
RUNYANS
LAMBERT
C-49
K-28
1'-58
T-35
V-23
AA-54
CC-33
CC-33 IJUl'LICATE
EE-58
FF-34
FF-62
GG-61
HH-48
HH-77
Master Track int'. List
HOECHST CEl,ANESE-Shclhy
First Quai·k,· llJ9(,
SIi EALY Lah I )all'
ID NmnlH.'r CollLTkd
Ground-Water
83003N 01/1(,/9(,
83156 Ul/17/96
83157 01/17/9(,
83001N 01/1 (i/%
83002N 01/16/96
83160 01/17/96
83004N 01/1(,/%
83212 01/18/%
83168 01/17/%
83165 01/17/96
82997N 01/1 (i/96
82998N 01/16/96
83164 01/17/96
82999N 01/1(,/96
83211 01/18/96
83162 01/17/'!6
83163 01/17/'!6
83209 . 01/18/96
83207 01 /18/9(,
83208 01/18/96
83210 0 l /18/96
83167 01/17/96
83166 01/17/96
llak
Rt.Tl'i\'l'd
01/17/96
O l /18/')(,
II 1 /I 8/'!6
Ol/17/')(,
01/17/96
II 1 /I 8/%
111/17/96
111 /18/96
111/18/96
01 /18/96
01/17/96
01/17/96
01/18/96
01/17/<JG
01/18/96
01 /I 8/96
01/18/96
01 /I 8/96
01 /18/96
01/18/96
01/18/96
01/18/96
01/18/96
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I CASE NARRATIVES
I
TCLP Metals
I
I Methods
1311/6010A
I 1311/7470A
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K LLb LJ ~ ~VL-,
CASE NARRATIVE
General Information
~1ethod:
Analysts:
~feta!S-2.J;O ,'l
Preparation G\~.
Sample ID numbers:
'6')00Lj , '63l(c0
Date Received:
Dace Prepared:
Dace Analyzed:
OC (Attach Data For Each Item)
Analysis ~\
Indicate whether or not each item was acceptable for the batch.
l. Blank ·~
2. Duplicates (precision) N fl-
~ Spikes (precision/accuracy)
\ __________
.J .
4. ICV standard ✓
), CCV standard ~
6. LCSS/LCS\V ✓
Problems/Comments:
CASE NARR,\TIVE
General Information
i',,fethod: i',,fetals-1311 / 7:tJ oA
Analysts: Preparation 1=-1 Analysis 1= T
Sample ID numbers:
S-,si leO ~)()DYN , _____ _
Date Received:
Date Prepared:
Date Analyzed:
s,-;,t,,c:, 11,11~1.
2::, "v-11'-l 111711 ~
I I 2-?:-{ '1 (,
OC (Attach Data For Each Item)
Indicate whether or not each item was acceptable for the batch.
1. Blank ~
2. Duplicates (precision) ~
.) . Spikes (precision/accuracy) ~
,1 ICY standard ·~ --r.
5. CCV standard ✓
6. LCSS/LCS\V ✓
Problems/Comments:
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I CASE NARRATIVES
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I TCLP Volatiles
I Method 1311/8260A
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CASE NARR~ TIVE
General Information
Method: Volatiles-/3,i/ o'2-Lcrr
I
Analysts: Preparation -'-&!--'--',---''--Analysis !Z_t3-,)
Sample ID numbers:
>cs/ I Yl/',1Y1~
S->o'-\,.{!V -1/1_7/ 1 (,
Date Received: ,;,c c -!}1f/'l,
Date Prepared: 1 I n,/'i 1,
J / 3 :; ) '; '~ -f] I!,, e,"
Date Analyzed: rl,111, -s--:;r),_:;...iN ,
OC (Attach Data For Each Item)
lndic::ite whether or not e::ich item was acceptable for the batch.
l . B I a n k V----
2. Duplicates (precision)
3. Spikes (precision/accuracy)
4. Instrument Tuning (BFB)
) ICY Star.clarcl
6. CCV StancLlrcl
7. LCSS/LCSW
8. I nteral Standards
9. Surrogates
Problems/Co111111ents:
:•I ;-j
/
__,----
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I CASE NARRATIVES
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I TCLP Semi-Volatiles
I Method 1311/8270B
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CASE NARRATIVE
General ! nformation
Method: Semi volatiles-I?, 1 1 /, 2 7 c 1J I .
Analysts: Preparation
Sample ID numbers:
8100~~._-~?~J~·~~'-
Date Received:
I ! JS j J , ~ ) ~ .. , , ....
i/,7/JG \-l,i
Date Prepared:
Date Analyzed:
OC (Attach Data For Each [tern)
Analysis __ b_e-.:i_,__r:>_
Indicate whether or not each item was acceptable for the batch,
l, B!Jnk ✓
2. Duplicates (precision) '·.i ;~
~ Spikes (precision/accuracy) ~ J.
4 Instrument Tuning (DFTPP) /
). [CV Standard /
6. CCV Standard /
7. LCSS/LCSW / c.---
8. !nteral Standards (./'/
9. Surrogates
Problems/Comments:
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I CASE NARRATIVES
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I TCLP Pesticides
I Method 1311/S0S0A
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CASE NARR>\ TIVE
General Information
iv!ethod: Pesticides!PCBs-/jJ@0 8'0 A
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Analysts: Preparation ('rl1~~fYQ_
Sample ID numbers:
i11b 0 "t.,oo'-fvJ
Date Received: i/1s-I 10
Date Prepared:
Date Analyzed:
I
ll+t--1 /J..4/ q G
drs-l·3b
OC (Attach Data For Each Item)
Ana I ysis __,P,""?...__ __
Indicate whether or not each item was acceptable for the batch.
I. Blank (jk
2. Duplicates (precision) ") IA
~ Spikes (precision/accuracy) /l 1 (I'.. .) .
5. !CV Standard c~iz
6. CCV Standard c:[<
7. LCSS/LCS\V rJ (A--
S. Surrogates N (tr-
Problems/Comments:
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I CASE NARRATIVES
I
I TCLP Herbicides
I Method 1311/8150B
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CASE NARRATIVE
General Information
J\,fethod:
Analysts:
Herbicides-
Preparation l'l1 I~ l,Yrz
I
Sample ID numbers:
~!,tti7
Date Received:
Date Prepared:
Date Analyzed:
I
I l,},).!r;l -1/11-/1l~
I I
1(.li,,f 'fh
OC ( Attach Data For Each Item)
Analysis --FR--=~~--
Indicate whether or not each item was acceptable for the batch.
1. Blank Ok._
2. Duplicates (precision) b.' L6. ' ,
,., Spikes (precision/accuracy) tv /tr .) .
5. ICV Standard ot<. ..
6. CCV Standard Dk
7. LCSS/LCSW f'v' //>r
8. Surrogates vk
Problems/Comments:
CASE NARRATIVE
General Information
r-ifethod: Herbicides-· k:,h4-0J3 _ {LJ!t/ ?1 ,o B)
Analysts: Preparation cn1Str:-Analysis --"Q.,.,,~"----
Sample ID numbers:
~3oot,l\l ~rK ----
Date Received:
Date Prepared:
Date Analyzed:
1!~1jqb; ,/~1/¥,
J-jijql,,
OC ( Attach Data For Each Item)
Indicate whether or not each item was acceptable for the batch.
1. Blank ok
2. Duplicates (precision) N ft+:
~ Spikes (precision/accuracy) c--k .) .
5. ICV Standard ek
6. CCV Standard ck_
7. LCSS/LCSW N If± I
8. Surrogates ol.
Problems/Comments:
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I CASE NARRATIVES
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I TCL Volatiles
I Method 8260A
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CASE NARRATIVE
General Information
Method: Volatiles-'"3-;i_(o o fr .
Analysts: Preparation D,v F /P. 1ZP/24G
Sample ID numbers:
$'. ). "l 'i" S' /0
Date Received:
Date Prepared:
Date Analyzed:
OC (Attach Data For Each Item)
Analysis DN p/~2-V/2,l{g
Indicate whether or not each item was acceptable for the batch.
l . BI a nk ~
2. Duplicates (precision) ✓
e Spikes (precision/accuracy) ✓ J.
4. Instrument Tuning (BFB) ✓
). ICY Standard µA-
6. CCV Standard ✓
7. LCSS/LCS\V IV(}
3. lnteral Standards ✓
9. Surrogates ✓
Problems/Com men ts:
CASE NARRATIVE
General Information
Method: Volatiles-'i 2-I:, 0 A .
Analysts: Preparation Drif'l,,ecV /2il<s'
Sample ID numbers:
S, '.,-"JC/ 7 r\J f ~ ,0(, 1.J
S3te,7 ·37:,Jb~
"332..lf \;'32-12-
Date Received:
Date Prepared:
Date Analyzed:
OC !Attach Data For Each Item)
Indicate whether or not each item was acceptable for the batch.
I . B I a n k ;_,.,-----
2. Duplicates (precision) ./'
3. Spikes (precision/accuracy) ~
4. Instrument Tuning (BFB) ~
5. ICY Standard 104
6. CCV Standard v
7. LCSS/LCSW f!/r
8. Intern! Standards v
9. Surrogates /
Problems/Comments:
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I Ethylene Glycol
I Method 8015A
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CASE NARRATIVE
General Information
i'vfethod: Ethylene Glycol-8015M
Analysts:~ Preparation S:J(., Analysis ~d-t&~---
Sample ID numbers:
8 ?x:c,'S ,iJ , 9 3 I "59 ,\.l ,nJj), ------
8 :?i i 5b cJ , P:3:12 :i,:J
~ 'J,J<S'l t-1
Date Received:
Date Prepar.ed:
Date Analyzed:
OC (Attach Data For Each Item)
Indicate whether or not each item was ac?table for the batch.
1. Blank _..i___ .
2. Duplicates (precision) fer /'
,. ,/,I/"'{)
~ Spikes (precision/accuracy) .) . .
5. !CV Standard ✓
6. CCV Standard rJ (t
7. LCSS/LCS\V tJ{r
CASE NARRATIVE
General Information
Nfethod:
Analysts:
Ethylene Glycol-8015Nf
Preparation }ftG-
Sample ID numbers:
8 ::co.:'.) ,✓
Date Received:
Date Prepar.ed:
Date Analyzed:
OC ( Attach Data For Each Item)
Analysis~-
Indicate whether or not each item was acceptable for the batch.
I. Blank
2. Duplicates (precision) ,IJA
3. Spikes (precision/accuracy) N"1
5. ICV Standard ,/
6. CCV Standard rJ A .,
7. LCSS/LCS\V Ji-\"
Problems/Comments:
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SAMPLE RESULTS
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I TCLP Metals
I Methods
I 1311/6010A
1311/7470A
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-------------------
Client Sample
ldcntifin.1tion
SIIR SLUDGE
Fl' SLUDGE
Client Sample
Identification
SUR WASTEll SLUDGE
FILTER !'RESS SLUDGE
Master Tracking List -TCLP Metals (Except Mercury)
HOECHST CELANESE-Shelby
First Quarter 1996
SHEALY Lab llale llale
II) Numhcr
83160
83004N
Collected Rc(·civcd
01/17/96 01/18/96
01/16/96 01/17/96
Master Tracking List -TCLP Mercury
HOECHST CELANESE-Shelby
First Quarter 1996
SHEALY Lab Dale Date
Ill Numhcr Collected Received
83160 01/17/96 01/18/96
83004N 01/16/96 01/17/96
Prep. Analysis
llale Dale
01/22/96 01/26/96
01/22/96 01/26/96
Prep. Analysis
Dale llate
01/22/96 01/31/96
01/22/96 01/31/96
I SHEALY ENVIRONMENTAL SERVICES, INC.
I 06 VANTAGE POINT DRIVE
CAYCE, SOUTH CAROLINA 29033
I SC DHEC No. 32010
Client:
I
Attention:
I SHEALY Lab No, 83160
Description: SBR WASTED SLUDGE
Date Received: 01/18/96 I Date Reported, 02/02/96
I Parameters
I TCLP METALS
arsenic
barium
cadmium
I chromium
lead
selenium
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silver
Scientists and Consultants
CERTIFICATE OF ANALYSIS
HOECHST CELANESE-SHELBY PLANT P.O. Box 87 Shelby, NC 28151-0087
Kathryn Frank
[phone]
FAX [phone]
NC DEHNR No. 329
Coll. Date, 01/17 /96
Coll. Time: 0830
QA/QC Officer _--l'r--)_~flf~~---~-
V.P. Analytical -~f'l_,!{L,J ____ _
Date Date
Method Reaul t Units PQL Prepared Analyzed Anal.
1311/6010A
1311/6010A
1311/6010A
1311/6010A
1311/6010A
1311/6010A
l311/6010A
ND
0. 0 5 5
ND
ND
ND
ND
ND
mg/1
mg/1
mg/1
mg/1
mg/1
:ng/1
mg/1
Terms and Conditions on Reverse Side ·
0.050 01/22/96 01/26/96 FT
0.010 01/22/96 01/26/96 FT
0.010 01/22/96 01/26/96 FT
0.010 01/22/96 01/26/96 FT
0.020 01/22/96 01/26/96 FT
0.050 01/22/96 01/26/96 FT
0. 02 0 01/22/96 01/26/96 FT
;Q6 VANTAGE POINT DRIVE
CAYCE. SOUTH CAROLINA 29033
SHEALY ENVIRONMENTAL SERVICES, INC.
Scientists and Consultants
CERTIFICATE OF ANALYSIS
[phone]
FAX [phone];;1
I
I
SC DHEC No. 32010 NC DEHNR No. 329 I
Client: HOECHST CELANESE-SHELBY PLANT P .o. Box 87 1 Shelby, NC 28151-0087
Attention: Kathryn Frank
SHEALY Lab No, 8 3 0 04N
Description: FILTER PRESS SLUDGE
Date Received: 01/17/96
Date Reported: 02/02/96
QA/QC
Coll. Date: 01/16/95
Coll. Time: 1510
Officer -h-1AS-:
V.P. Analytical ft'~
I
I
Date Date
Method Result Units PQL Prepared Analyzed Anal. Parameters I ------------
TCLP METALS
arsenic
barium
cadmium
chrom~um
lead
selenium
silver
1311/6010A ND mg/1
1311/6010A 2.87 mg/1
1311/6010A ND mg/1
13ll/6010A ND mg/1
1311/6010A ND mg/1
1311/6010A ND mg/1
1311/6010A ND mg/1
Terms and Conditions on Reverse Side
0.050 01/22/96 01/26/96 FT
0.010 01/22/96 01/26/96 FT
0.010 01/22/96 01/26/96 FT
0.010 01/22/96 01/26/96 FT
0.020 01/22/96 01/26/96 FT
0.050 01/22/96 01/26/96 FT
0.020 01/22/96 01/26/96 FT
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I SHEALY ENVIRONMENTAL SERVICES, INC.
I 7 06 VANTAGE POINT DRIVE
CAYCE, SOUTH CAROLINA 29033
I SC DHEC No. 32010
Client:
I Attention:
I SHEALY Lab No, 83160
Description: SBR WASTED SLUDGE
Date Received: Ol/~S/96 I Date Reported, 02,'02/96
I Parameters
I TCLP METALS
mercury
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Scientists and Consultants
CERTIFICATE OF ANALYSIS
HOECHST CELANESE-SHELBY PLANT
P.O. Box 87
Shelby, NC 28151-0087
Kathryn Frank
Method Result Units PQL
[phone]
FAX [phone]
NC DEHNR No. 329
Coll. Date: 01/17/96
Coll. Time: 0830
QA/QC Officer "mAf ~
V.P. Analytical /;Jf1:/
Date Date
Prepared Analyzed Anal.
1311/7470A ND mg/1 0.001 01/22/96 01/31/96 FT
Terms and Conditions on Reverse Side
SHEALY ENVIRONMENTAL SERVICES, INC. I
106 VANTAGE POINT DRIVE
CAYCE, SOUTH CAROLINA 29033
SC DHEC No. 32010
Client:
Attention:
SHEALY Lab No, 83004N
Description: FILTER PRESS SLUDGE
Date Received: Ol/~7/96
Date Reported: 02/02/96
Parameters
Scientists and Consultants
CERTIFICATE OF ANALYSIS
HOECHST CELANESE-SHELBY PLANT P.O. Box 87 Shelby, NC 28151-0087
Kathryn Frank
Method Result Units PQL
[phone]
FAX [phone]
I
NC DEHNR No. 329 I
Coll. Date: 01/16/95
Coll. Time: 1510
QA/QC Officer _'h:c..,..Jt/r=~✓'--,--
V.P. Analytical -~('1-~ ___ • __
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Date Date I
Prepared Analyzed Anal. ------------
TCLP METALS
mercury 1311/7470A ND mg/1
Terms and Conditions on Reverse Side
0.001 01/22/96 01/31/96 FT I
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I SAMPLE RESULTS
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TCLP Volatiles
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I Method 1311/8260A
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- ------------------
Client Sample
Identification
SBI{ WASTED SLUIJ<;E
FILTEI{ PRESS SLUD<;E
Master Tracking List -TCLP Volatiles
I IOECI 1ST CELANESE-Shelhy
First Quarter 1996
SIIEALY Lah Date Date
II> Numhcr Collected Received
81160 01/17/96 01/18/96
81110'1N 111 /16/96 111/17/96
Prep. Analysis
Date llatc
()J/19/% 01/29/96
0 I /22/96 II 1/25/')6
I SHEALY ENVIRONMENTAL SERVICES, INC.
Scientists and Consultants I 06 VANTAGE POINT DRIVE
CAYCE. SOUTH CAROLINA 29033 CERTIFICATE OF ANALYSIS
[phone]
FAX [phone]iii
I SC DHEC No. 32010 NC DEHNR No. 329
Client:
I Attention:
I SHEALY Lab No, 8 3 16 0
Description: SBR WASTED SLUDGE
Date Received: 01/18/96 I Date Reported, 02/02/96
I Parameters
I TCLP VOLATILES
benzene
carbon tetrachloride
chlorobenzene
I chloroform
1,4-dichlorobenzene
1,2-dichloroethane
1,1-dichloroethen~
-utanone
I :achloroethene
L .... i::::hloroethene
vinyl chloride
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HOECHST CELANESE-SHELBY PLANT P.O. Box 87 Shelby, NC 28151-0087
Kathryn Frank
Coll. Date: 01/17/96
Coll. Time: 0830
QA/QC Officer
V.P. Analytical
Date Date
Method Result Units PQL Prepared Analyzed Anal.
1311/8260A
1311/8260A
1311/8260A
1311/8260A
1311/8260A
1311/ 8 2 6 OA
1311/8260A
1311/8260A
1311/8260A
1311/8260A
1311/8260A
ND
ND
ND
ND
ND
ND
ND
ND
m>
ND
ND
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
Terms and Conditions on Reverse Side
0.100
0.100
0.100
0.100
0.100
0.100
0.100
0.100
0.100
0.100
0.200
01/19/96 01/29/96 RED
06 VANTAGE POINT DRIVE
CAYCE, SOUTH CAROLINA 29033
SHEALY ENVIRONMENTAL SERVICES, INC.
Scientists and Consultants
CERTIFICATE OF ANALYSIS
[phone]
FAX [phone]
I
I
SC DHEC No. 32010 NC DEHNR No. 329 I
Client: HOECHST CELANESE-SHELBY PLANT P .o. Box 87 1 Shelby, NC 28151-0087
Attention: Kathryn Frank
SHEALY Lab No, 83004N
Description: FILTEP. PRESS SLUDGE
Date Received: 01/17/96
Date Reported: 02/02/96
Coll. Date: 01/16/96
Coll. Time: 1510
QA/QC Officer ·h""'cL-c:
v. P. Analytical ,111 ~
I
I
Date Date I
_P_a_r_am_e_te_r_• _______________ M_e_t_h_od _____ •_•_•_u_1_t ___ u_n_i_t_• ____ PQ_L __ P_r_•_P_•_r_e_d_An_a_lY_•_•_d_An_a_1_. ____ _
TCLP VOLATIL;;!S
benzene
carbon tetrachlor~Je
chlorobenzene
chloroform
1,4-dichlorobenzene
1,2-dichloroethane
1,1-dichloroethene
'Utanone
::-achloroethene
1. ... i.chloroethene
vinyl chloride
1311/8260A
1311/8260A
1311/8260A
1311/8260A
1311/8260A
1311/8260A
1311/8260A
1311/8260A
1311/8260A
1311/8260A
1311/8260A
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
Terms and Conaitions on Reverse Side
0.100
0.100
0.100
0.100
0.100
0.100
0.100
0.100
0.100
0.100
0.200
01/22/96 01/25/96 RED I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I SAMPLE RESULTS
I
I TCLP Semi-Volatiles
I Method 1311/8270B
I
I
I
I
I
I
I
I
I
I
I
I
--· - - - - - --- - - - - - - - - -
Client Sample
Identification
SBR WASTED SLUDGE
FILTER PRESS SLUll<;E
M:ister Tracking List -TCLP Semi-Volatiles
HOECHST CELANESE-Shelby
First Quarter 1996
SIIEAL Y Lah Dale Bale
ID Number Collcclcd Received
83160 01/17/96 01/18/96
8300-IN 01/16/96 01/17/96
Prep. Analysis
Dale Bale
01/22/96 01/30/96
01/22/96 01/29/96
I SHEALY ENVIRONMENTAL SERVICES, INC.
I ·05 VANTAGE ?OINT DRIVE
CAYCE. SOUTH CAROLINA 29033
I SC DHEC No. 32010
I
I
Client:
Attention:
SHEALY Lab No, 8 3 16 0
Description: SER WASTED SLUDGE
Date Received: 01/18/96 I Date Reported, 02/02/96
I Parameters
I TCLP SEMIVOLATILES
4-methylphenol
2-methylphenol
2,4-dinitrotoluene
hexachlorobenzene I hexachlorobutadiene
hexachloroethane
nit::-obenzene
,tachlorophenol
I idine
~,4,5-trichlorophenol
2,4,6-trichlorophei:ol
I
I
I
I
I
I
I
I
I
Scientists and Consultants
CERTIFICATE OF ANALYSIS
HOECHST CELANESE-SHELBY PLANT
P.O. Box 87 Shelby, NC 28151-0087
Kathryn Frank
[phone]
FAX [phone]
NC DEHNR No. 329
Coll. Date: 01/17/96
Coll. Time: 0830
QA/QC Officer t)JA£-
v. P. Analytical /}f~
Date Date
Method Result Units PQL Prepared Analyzed Anal.
1311/82708
1311/82708
1311/82708
1311/8270B
1311/82708
1311/82708
1311/8270B
1311/8270B
1311/8270B
1311/82708
1311/82708
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
Terms and Conditions on Reverse Side
0.020
0.010
0.010
0. 010
0.010
o. 010
0.010
0.020
0.010
0.010
0.010
01/22/96 01/30/96 DNP
SHEALY ENVIRONMENTAL SERVICES, INC.
)6 VANTAGE POINT DRIVE
CAYCE, SOUTH CAROLINA 29033
Scientists and Consultants
CERTIFICATE OF ANALYSIS
[phone]
FAX [phone]n 1
I
SC DHEC No. 32010 NC DEHNR No. 329 I
Client: HOECHST CELANESE-SHELBY PLANT P.O. Box 87
Attention:
SHEALY Lab No, 83004N
Description: FILTER PRESS SLUDGE
· Date Received: 01/17/96
Date Reported: 02/02/96
Parameters
Shelby, NC 28151-0087
Kathryn Frank
Method Result Unite PQL
I
Coll. Date: 01/16/95 I
Coll. Time: 1510
QA/QC Officer ~
V. P. Analytical ,11~ I
,I Date Date
Prepared Analyzed Anal. -------------------------
TCLP SEMIVOLATILES
4-methylphenol
2-methylphenol
2,4-dinitrotoluene
hexachlorobenzene
hexac h lor,obu tad i e~e
hexachloroethane
nitrobenzene
tachlorophenol
idine
~.4,5-trichlorophenol
2,4,6-trichlorophenol
1311/8270B ND mg/1
1311/82708 ND mg/1
1311/8270B ND mg/1
1311/82708 ND mg/1
1311/82708 ND mg/1
1311/82708 ND mg/1
1311/8270B ND mg/1
1311/82708 ND mg/1
1311/82708 ND mg/1
1311/82708 ND mg/1
1311/82708 ND mg/1
Terms and Conditions on Reverse Side
0.020
0.010
0.010
0.010
0.010
0.010
0.010
0.020
0.010
0.010
0.010
01/22/96 01/29/96 DNP I
I
I
I
I
I
I
I
I
I
I
I
I
I
I SAMPLE RESULTS
I
I TCLP Pesticides
I Method 1311/S0S0A
I
I
I
I
I
I
I
I
I
I
I
I
-------------------
Client Sample
Identification
SllR WASTED SLUll<;E
FILTER PRESS SLUDGE
Master Tracking List -TCLP Pesticides
HOECHST CELANESE-Shelby
Fourth Quarter 1995
SHEALY Lah llatc Date
II) Numhcr Collected H.ccdvcd
83160 Ol/17/96 01/18/96
8300-lN 01/16/96 01/17/96
Prep. Analysis
llale llale
01/22/96 01/25/96
01/22/96 01/25/96
I
I
SHEALY ENVIRONMENTAL SERVICES, INC.
I
I
06 VANTAGE POINT DRIVE
CAYCE, SOUTH CAROLINA 29033
SC DHEC No. 32010
Client:
Attention:
I SHEALY Lab No, 83160
Description: SBR WASTED SLUDGE
I
Date Received: 01/18/96
Date Reported: 02/02/96
I Parameters
I
I
I
I
I
I
I
I
I
I
TCLP PESTICIDES
chlordane
endrin
heptachlor
heptachlor epoxide
gamma-BHC (lindane)
methoxychlor
toxaphene
Scientists and Consultants
CERTIFICATE OF ANALYSIS
HOECHST CELANESE-SHELBY PLANT P.O. Box 87 Shelby, NC 28151-0087
Kathryn Frank
[phone]
FAX [phone]
NC DEHNR No. 329
Coll. Date: 01/17/96
Coll. Time: 0830
QA/QC Officer _::t:YJ&f_,__'--'~'-"'✓'-----
V.P. Analytical __ /¥1 __ bJ_., ___ _
Date Date
Method Result Units PQL Prepared Analyzed Anal.
1311/8080A
1311/SOSOA
1311/BOSOA
1311/BOBOA
1311/BOBOA
1311/BOBOA
1311/B0S0A
ND
ND
ND
ND
ND
ND
ND
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
Terms and Conditions on Reverse Side
0,030
0.003
0.003
0.003
0.003
0.010
0.250
01/22/96 01/25/96 RZ
06 VANTAGE POINT DRIVE
CAYCE. SOUTH CAROLINA 29033
SHEALY ENVIRONMENTAL SERVICES, INC.
Scientists and Consultants
CERTIFICATE OF ANALYSIS
[phone]
FAX [phone]
I
SC DHEC No. 32010 NC DEHNR No. 329 I
Client: HOECHST CELANESE-SHELBY PLANT
P.O. Box 87 I Shelby, NC 28151-0087 ,
Attention:
SHEALY Lab No, 83004N
Description: FILTER PRESS SLUDGE
Date Received: 01/17/96
Date Reported: 02/02/96
Parameters
Kathryn Frank
Method Result Units
Coll. Date: 01/16/96
Coll. Time: 1510
QA/QC Officer --~m.,_~if,[..,-"='------
V.P. Analytical __ /i1_J->...I ___ _
Date Date
PQL Prepared Analyzed Anal. ------------------------------------------
TCLP PESTICiiJES
chlordane
endrin
heptachlor
heptachlor epoxide
gamma-BHC (lindane)
mee.hoxychlor
toxaphene
1311/8080A ND mg/1
1311/S0S0A ND mg/1
1311/B0B0A ND mg/1
1311/B0B0A ND mg/1
1311/BOSOA ND mg/1
1311/S0S0A ND mg/1
1311/SOSOA ND mg/1
Terms and Conditions on Reverse Side
0.010
0.001
0.001
0.001
0.001
0.004
0.100
01/22/96 01/25/96 RZ
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I SAMPLE RESULTS
I
I TCLP Herbicides
I Method 1311/8150B
I
I
I
I
I
I
'I
I
I
I
I
I
-------------------
Client Sample,
ldcnlificalion
SIIR WASTEll SLIJll(;E
FILTER PRESS SLUD(;E
Master Tracking List -TCLP Herhicides
HOECHST CELANESE-Shelby
First Onarter 1996
SHEALY Lah Date llate
Ill Numhcr Colkclcd Received
83160 01/17/96 01/18/96
83004N 01/16/96 01/17/96
Prep. Analysis
llate llatc
01/22/96 01/26/96
01/22/96 01/26/96
I SHEALY ENVIRONMENTAL SERVICES, INC.
I 06 VANTAGE POINT DRIVE
CAYCE, SOUTH CAROLINA 29033
I SC DHEC No . .32010
Client:
I
Attention:
I SHEALY Lab No, 83160
Description: SBR WASTED SLUDGE
Date Received: 01/18/96 I Date Reported, 02/02/96
I Parameters
I TCLP HERBICIDES
2,4-D
2,4,5-TP
I
I
I
I
I
I
I
I
I
Scientists and Consultants
CERTIFICATE OF ANALYSIS
HOECHST CELANESE-SHELBY PLANT P.O. Box 87
Shelby, NC 28151-0087
Kathryn Frank
Method
1311/81508
1311/81508
Result
NO"
ND
Units
mg/1
mg/1
Terms and Conditions on Reverse Side
PQL
0.100
0.100
[phone]
FAX [phone]
NC DEHNR No. 329
Coll. Date: 01/17/96
Coll. Time: 0830
QA/QC Officer :1Y)A.:_,
V. P. Analytical ;11k"--'
Date Date
Prepared Analyzed Anal.
01/22/96 01/26/96 RZ
SHEALY ENVIRONMENTAL SERVICES, INC. I
06 VANTAGE POINT DRIVE
CAYCE. SOUTH CAROLINA 29033
SC DHEC No. 32010
Client:
Attention:
SHEALY Lab No: 83:)Q4N
Description: FILTEH PRESS SLUDGE
Date Received: 01/17/96
Date Reported: 02/02/96
i?arameters
Scientists and Consultants
CERTIFICATE OF ANALYSIS
HOECHST CELANESE-SHELBY PLANT P.O. Box 87
Shelby, NC 28151-0087
Kathryn Frank
Method Result Units PQL
(8031 791-9700
FAX [phone]i i 1
I
NC DEHNR No. 3291 1
Coll. Date: 01/16/96
Coll. Time: 1510
QA/QC Officer ~~
V.P. Analytical M~
Prepared Analyzed Anal.
I
I
I
Date Date I I
--------------I
TCLP HERBICIDES
2,4-D
2,4,5-TP
1311/8150B
1311/8150B
ND
ND
mg/1
mg/1
Terms and Conditions on Reverse Side
0.100
0.100
01/22/96 01/26/96 RZ I
I
I
I
I
I
I
I
I
I
I
I
I SAMPLE RESULTS
I
I TCL Volatiles
I Method 8260A
I
I
I
I
I
1.
I
I
I
I
I
I
- - - - -- -
Client Sampk SIIEAL\' Lah
I dcntifin1 I ion JI) Numhcr
ITCI 8311111N
ITEF 83156
ITEF l>IJl'LIC,\TE 83157
OTCI 83011 I N
OTEF XllllPN
IWN\'ANS 83212
LAMIIERT 8 l 168
C-49 83165
K-28 82997N
P-58 82998N
T-:15 83164
V-2J 82999N
AA-54 83211
CC-33 83162
CC-33 DUPLICATE 83163
EE-58 832119
FF-34 83207
FF-62 83208
.(;(;.<,1 83210
1111-48 83167
1111-77 83166
- --- -
Masti.:r Track in<> List -TCL VOCs
IHlECIIST CELANESE-Shelby
First ()uar·tcr 1996
Hate Date
Collcckd Received
01/1/,/96 01/17/96
111/17/96 01/18/96
111/17/% 111/18/96
111/16/96 01/17/96
(11/16/9(, 01/17/96
0 I /18/96 01/18/96
111/17/96 ll 1 /18/%
01/17/96 01/18/96
01/16/96 01/17/96
01/16/96 01/17/96
01/17/96 01/18/96
01/16/96 01/17/96
01/18/96 ll I /18/96
01/17/96 01/18/96
lll/1-7/96 01/18/96
lll/18/96 01/18/96
01/18/96 01/18/96
01/18/96 01/18/96
111/18/96 01/18/96
01/17/96 01/18/96
01/17/96 01/18/96
- --- - - -
Prep. Analysis
Date Date
--111/2(,/%
--(I J/26/96
--(I 1/26/%
111/2(,/'!6
--01/)6/96
01/27/'!6
--01/27/'!6
.. 111/26/96
.. O I /26/96
--0 I /76/96
--01/26/96
--01/26/96
--ll 1/27/96
--ll I /26/96
--ll 1/26/96
01/27/96
--01/26/96
--lll/27/96
--0 I /27/96
--01 /27/96
--0 I /27/96
I
I JS VANTAGE POINT DRIVE
CAYCE, SOUTH CAROLINA 29033
I SC DHEC No. 32010
I
I
Client:
Attention:
SHEALY Lab No, 83003N
Description: ITCI
Date Received: 01/17/96 I Date Reported, 02/01/96
I Parameters
I VOLATILE ORG.'lliICS
acetone
benzene
bromodichloromethane
bromoform
I' bra"momethane
2-butanone
carbon disulfide
-~on tetrachloride
I )robenzene
c,,..Loroethane
chlorofor:n
chlaromethane
I dibromochloromethane
1,1-dichloroethane
1,2-dichloroethane
1,1-dichloroethene
cis-1,2-dichloroethene
I trans-1,2-dichloroethene
1,2-dichloropropane
cis-1,3-dichloropropene
ethylbenzene
2-hexanone I methylene chloride
4-methyl-2-pentanc~e
styrene
1,1,2,2-tetrachloroethane
I tetrachloroethene
toluene
1,1,1-trichloroet~~ne
1,1,2-trichloroethene
I crichloroethene
vinyl acetate
vinyl chloride
xylenes
I
I
I
I
SHEALY ENVIRONMENTAL SERVICES, INC.
Scientists and Consultants
CERTIFICATE OF ANALYSIS
HOECHST CELANESE-SHELBY PLANT
P.O. Box 87
Shelby, NC 28151-0087
Kathryn Frank
Method
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8250A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260.A
8260.A
8260.A
8260A
8260.A
8260A
8260A
Result Units
0.3420 mg/1
0.0183 mg/1
ND mg/1
ND mg/1
ND mg/1
0.3520 mg/1
ND mg/1
ND mg/1
0.0088 mg/1
ND mg/1
ND mg/1
ND mg/1
ND mg/1
ND mg/1
ND mg/1
ND mg/1
ND mg/1
ND mg/1
ND mg/1
ND mg/1
ND mg/1
ND mg/1
ND mg/1
ND mg/1
ND mg/1
ND mg/1
ND mg/1
ND mg/1
ND mg/1
ND mg/1
ND mg/1
ND mg/1
ND mg/1
ND mg/1
Terms and Conditions on Reverse Side
PQL
0.0500
0.0050
0.0050
0.0050
0.0100
0.0100
0.0200
0.0050
0.0050
0.0100
0.0050
0.0100
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0100
0.0150
QA/QC
[phone]
FAX [phone] i
NC DEHNR No. 329
Coll. Date: 01/16/96
Co_ll. Time: 1455
Officer r,\AL
V.P. Analytical Mff'J
Date Date
Prepared Analyzed Anal.
01/26/96 RED
06 VANTAGE POINT DRIVE
CAYCE, SOUTH CAROLINA 29033
SC DHEC No. 32010
Client:
Attention:
SHEALY Lab No, 83156
Description: ITEF
Date Received: 01/18/96
Date Reported: 02/01/96
Parameters
SHEALY ENVIRONMENTAL SERVICES, INC.
Scientists and Consultants
CERTIFICATE OF ANALYSIS
HOECHST CELANESE-SHELBY PLANT
P.O. Box 87 Shelby, NC 2a1s·1-0087
Kathryn Frank
QA/QC
(803) i9Hi00
FAX (803) i91-9111
NC DEHNR No. 329
Coll. Date: 01/17/96
Coll. Time: 1050
Officer -fn~ 2
V.P. Analytical ,01/fLV
Date Date
Method Result Units PQL Prepared Analyzed Anal. ----------------------------------------
VOLATILE ORGANICS
acetone
benzene
bromodichloromethar.e
bromoform
bromomethane
2-butanone
carbon disulfide
~on tetrachloride
Jrobenzene
caloroethane
chloroform
chloromethane
dibromochlorome th'-.:e
1,1-dichloroethan,i
1,2-dichloroethane
1,1-dichloroethene
cis-1,2-dichloroethene
~rans-1,2-dichloroethene
1,2-dichloropropane
~is-1,3-dichloropropene
ethylbenzene
2-hexanone
~ethylene chloride
4-methyl-2-pentanone
styrene
l,l,2,2-tetrachloroethane
tetrachloroethene
toluene
1,1,1-trichloroeth~ne
l,1,2-trichloroethane
':.richloroethene
vinyl acetate
vinyl chloride
xylenea
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8250A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
Terms and Conditions on Reverse Side
01/26/96 RED
0.0500
0.0050
0.0050
0.0050
0.0100
0.0100
0.0200
0.0050
0.0050
0.0100
0.0050
0.0100
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0100
0.0150
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
06 VANTAGE POINT DRIVE
CAYCE, SOUTH CAROLINA 29033
SC DHEC No. 32010
Client:
Attention:
SHEALY Lab No, 83157
Description: ITEF Duplicate
Date Received: 01/18/96 I Date Reported: 02/01/96
I Parameters
ORGANICS
acetone I VOLATILE
benzene
bromodichloromethane
I bromoform
bromomethane
2-butanone
carbon disulfide
I Oon tetrachloride
.:,robenzene
cnloroethane
chlorofor:n
chloromethane
I dibromochlorometha1!e
1,1-dichloroethanfl
1,2-dichloroethane
1,1-dichloroethene
cis-1,2-dichloroethene I trans-1,2-dichlor~~thene
1,2-dichloropropane
cis-1,3-d:chloropropene
ethylbenzene
I 2-hexanone
methylene chloride
4-methyl-2-pentanone
styrene
1,1,2,2-tetrachloroethane I tetrac~loroethene
toluene
1,1,1-trichloroeth~ne
1,1,2-trichloroethane
I trichloroethene
vinyl acetate
vinyl chloride
xylenes
I
I
I
I
SHEALY ENVIRONMENTAL SERVICES, INC.
Scientists and Consultants
CERTIFICATE OF ANALYSIS
HOECHST CELANESE-SHELBY PLANT P.O. Box 87 Shelby, NC 28151-0087
Kathryn Frank
Method
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
3260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
Result
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND.
ND
ND
ND
ND
Units
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
:ng/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
Terms and Conditions on Reverse Side
PQL
0.0500
0.0050
0.0050
0.0050
0.0100
0.0100
0.0200
0.0050
0.0050
0.0100
0.0050
0.0100
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0100
0.0150
[phone]
FAX [phone]
NC DEHNR No. 329
Coll. Date: 01/17/96
Coll. Time: 1050
QA/QC Officer :::(YJAf~
V. P. Analytical [h,ti,J
Date Date
Prepared Analyzed Anal.
01/26/96 RED
06 VANTAGE POINT DRIVE
CAYCE, SOUTH CAROLINA 29033
SC DHEC No. 32010
Client:
Attention:
SHEALY Lab No, 83001N
Description: OTCI
Date Received: 01/17/96
Date Reported: 02/01/96
Parameters
VOLATILE ORGANICS
acetone
benzene
bromodichloromethane
bromoform
bromomethane
2-butanone
carbon disulfide
~on tetrachloride
.:>robenzene
c!l.loroethane
chloroform
chloromethane
dibromochloromethane
1,1-dichloroethane
1,2-dichloroethane
1,1-dichloroethene
cis-1,2-dichloroethene
trans-1,2-dichloroethene
1,2-dichloropropane
cis-1,3-dichloropropene
ethylbenzene
2-hexanone
~ethylene chloride
4-methyl-2-pentanone
styrene
1,1,2,2-tetrachloroethane
tetrachloroethene
toluene
1,1,1-trichloroethane
1,1,2-trichloroethane
trichloroethene
vinyl acetate
vinyl chloride
xylenes
SHEALY Et':JVIRONMENTAL SERVICES, INC.
Scientists and Consultants
CERTIFICATE OF ANALYSIS
HOECHST CELANESE-SHELBY PLANT P.O. Box 87 Shelby, NC 28151-0087
Kathryn Frank
QA/QC
(8031 79J.9700
FAX [phone]; 1
NC DEHNR No. 329
I
I
I
I
Coll. Date: 01/16/96 I
Coll. Time: 1430
Officer -trsc,
V.P. Analytical /l1,rv--' I
Method
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
Result
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Units
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
Terms and Canaitians an Reverse Side
PQL
0.0500
0.0050
0.0050
0.0050
0.0100
0.0100
0.0200
0.0050
0.0050
0.0100
0.0050
0.0100
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0100
0.0150
Date Date
Prepared Analyzed Anal. I
01/26/96 RED I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
i6 VANTAGE.POINT DRIVE
CAYCE, SOUTH CAROLINA 29033
SC DHEC No. 32010
Client:
Attention:
I SHEALY Lab No, 83QQ2N
Description: OTEF
I
I
I
I
I
I
Date Received: 01/17/96
Date Reported: 02/01/96
Parameters
VOLATILE ORGANICS
acetone
benzene
bromodichlorome tha:-:e
bromoform
bromomethane
2-butanone
carbon disulfide
~on tetrachloriae
)roben:z:ene
cnloroethane
chloroform
chloromethane
dibromochloromethane
1,1-dichloroethane
1,2-dichloroethane
1,1-dichloroethene
cis-1,2-dichloroethene
I trans-1,2-dichloroethene
1,2-dichloropropane
cis-1,3-dichloropropene
ethylbenzene
12 -hexanone
methylene chloride
4 -methyl -2 -pen tan.-,•1e
styrene
1,1,2,2-tetrachloroethane
I tetrachloroethene
toluene
1,1,1-trichloroethane
1,1,2-trichloroethane
I trichloroethene
vinyl acetate
vinyl chloride
xylenes
I
I
I
I
SHEALY ENVIRONMENTAL SERVICES, INC.
Scientists and Consultants
CERTIFICATE OF ANALYSIS
HOECHST CELANESE-SHELBY PLANT
P.O. Box 87 Shelby, NC 28151-0087
Kathryn Frank
Method
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8250A
8260A
8250A
8250A
8260A
8260A
8260A
8250A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8250A
8260A
8260A
8260A
8260A
8260A
8250A
8260A
8260A
8250A
8260A
Result
lID
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
NC
ND
NC
ND
ND
ND
Units
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/_l
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
Terms and Conditions on Reverse Side
PQL
0.0500
0.0050
0.0050
0.0050
0.0100
0.0100
0.0200
0.0050
0.0050
0.0100
0.0050
0.0100
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0100
0.0150
QA/QC
[phone]
FAX [phone]
NC DEHNR No. 329
Coll. Date: 01/16/96
Coll. Time: 143 5
Officer -~-
V.P. Analytical m,y,,J
Date Date
Prepared Analyzed Anal.
01/26/96 REC
06 VANTAGE POINT DRIVE
CAYCE. SOUTH CAROLINA 29033
SHEALY ENVIRONMENTAL SERVICES, INC.
Scientists and Consultants
CERTIFICATE OF ANALYSIS
[phone]
FAX [phone] ii
I
I
=S=C=D=H=E=C=N=o=·=3=2=0=l=O=======================N=C~D;;;E;;;HNR;;;;;~N:,;,o;,;;;. =3;;;2;;9 I
Client:
Attention:
SHEALY Lab No, 8 3 212
Description: RUNY.k..~S
Date Received: 01/18/96
Date Reported: 02/01/96
Parameters
VOLATILE ORGANICS
acetone
benzene
bromodichloromethane
bromoform
bromomethane
2-butanone
carbon disulfide
·bon tetrachloride
.,robenzene
c:1.loroethane
chloroform
chloromet:hane
dibromochloromethane
1,1-dichloroethane
1,2-dichloroethan"
1,1-dichloroethen~
cis-1,2-dichloroethene
trans-1,2-dichloro~thene
1,2-dichloropropa~~
cis-1,3-dichloropropene
ethylbenzene
2-hexanone
methylene chloride
4-methyl-2-pentanone
styrene
1,1,2,2-tetrachlorcethane
tetrachloroethene
toluene
1,1,1-trichloroethane
1,1,2-trichloroethane
trichloroethene
vinyl acetate
vinyl chloride
xylenes
HOECHST CELANESE-SHELBY PLANT
P.O. Box 87
Shelby, NC 28151-0087
Kathryn Frank
Method
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260,\
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
826011.
8260A
8260A
8260A
8260A
8260A
Result
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Units
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
Terms and Conditions on Reverse Side
PQL
0.0500
0.0050
0.0050
0.0050
0.0100
0.0100
0.0200
0.0050
0.0050
0.0100
0.0050
0.0100
0.0050
0,0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0100
0.0150
QA/QC
I
Coll. Date: 01/18/96 I
Coll. Time: 1445
Officer --row,
V.P. Analytical Mk:'::'::'. I
Date Date
Prepared Analyzed Anal. I
01/27/96 RED I
I
I
I
I
I
I
I
I
I
I
I
I
I 06 VANTAGE POINT DRIVE
CAYCE, SOUTH CAROLINA 29033
I SC DHEC No. 32010
I
I
I
Client:
Attention:
SHEALY Lab No, 8 316 8
Description: LAMBERT
Date Received: 01/18/96
Date Reported: 02/01/96
I Parameters
I VOLATILE ORGANICS
acetone
benzene
bromodichloromethane
I
I
bromoform
bromomethane
2-butanone
carbon disulfide
r"·-rbon tetrachlori.le
)robenzene
.oroethane
chloroform
chloromethane
dibromochloromethane I 1,1-dichloroethane
1,2-dicbloroethane
1,1-dichloroethene
cis-1,2-dichloroetnene
I trans-1,2-dichloroethene
1,2-dichloropropane
cis-1,3-dichloropropene
ethylbenzene
2-hexanone I methylene chloride
4-methyl-2-pentanane
styrene
1,1,2,2-tetrachloroethane
I tetrachloroethene
toluene
1,1,1-trichloroethane
1,1,2-trichloroethane
I
I
I
I
I
trichloroethene
vinyl acetate
·.rinyl chloride
xylene.s
SHEALY ENVIRONMENTAL SERVICES, INC.
Scientists and Consultants
CERTIFICATE OF ANALYSIS
HOECHST CELANESE-SHELBY PLANT
P.O. Box 87 Shelby, NC 28151-0087
Kathryn Frank
Method
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
Result
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
Units
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
Terms and Conditions on Reverse Side
PQL
0.0500
0.0050
0.0050
0.0050
0.0100
0.0100
0.0200
0.0050
0.0050
0.0100
0.0050
0.0100
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0100
0.0150
QA/QC
[phone]
FAX [phone]
NC DEHNR No. 329
Coll. Date: 01/17/96
Coll. Time: 1502
Officer ~G
V.P. Analytical ,'Ylk"::!
Date Date
Prepared Analyzed Anal.
01/27/96 REC
06 VANTAGE POINT DRIVE
CAYCE, SOUTH CAROLINA 29033
SC DHEC No. 32010
Client:
Attention:
SHEALY Lab No, 83165
Description: C-49
Date Received: 01/18/96
Date Reported: 02/02/96
SHEALY ENVIRONMENTAL SERVICES, INC.
Scientists and Consultants
CERTIFICATE OF ANALYSIS
HOECHST CELANESE-SHELBY PLANT P.O. Box 87
Shelby, NC 28151-0087
Kathryn Frank
QA/QC
(803) 791 -9700
FAX [phone]
I
I
NC DEHNR No. 329 I
I
I Coll. Date: 01/17/96
Coll. Time: 1320
Officer '--'frf:G '
V.P. Analytical Md I
Parameters I ---~---------
Date Date
Method Result Units PQL Prepared Analyzed Anal.
VOLATILE ORGANICS
· acetone
benzene
bromodichloromethar.e
bromoform
bromomethane
2-bucanone
carbon disulfide
·bon tetrachloride
)robenzene
c.. •• ..:.oroethane
chloroform
chloromethane
dibromochloromethane
1,1-dichloroethane
1,2-dichloroethane
1,1-dichloroethene
cis-1,2-dichloroethene
trans-1,2-dichloroethene
1,2-dichloropropane
cis-1,3-dichloropropene
ethylbenzene
2-hexanone
:nethylene chlorid,1
4-methyl-2-pentano~e
styrene
1,1,2,2-tetrachlaraethane
tecrachlaraethene
toluene
1,1,1-trichloraethane
1,1,2-trichloroethane
trichloroethene
vinyl acetate
vinyl chloride
xylenes
01/26/96 RED
8260A ND mg/1 0.0500
8260A ND mg/1 0.0050 I 8260A ND mg/1 0.0050
8260A ND mg/1 0.0050
8260A ND mg/1 0.0100
8260A ND mg/1 0.0100
8260A ND mg/1 0.0200 I
8260A ND mg/1 0.0050
8260A ND mg/1 0.0050
8260A ND mg/1 0.0100
8250A ND mg/1 0.0050 I
8260A ND mg/1 0.0100
8260A ND mg/1 0.0050
8250A ND mg/1 0.0050
8260A ND mg/1 0.0050
8260A ND mg/1 0.0050 I
8260A ND mg/1 0.0050
8250A ND mg/1 0.0050
8260A ND mg/1 0.0050
8250A ND mg/1 0.0050 I
8260A ND mg/1 0.0050
8260A ND mg/1 0,0050
8250A ND mg/1 0.0050
8260A ND mg/1 0.0050
8250A ND mg/1 0.0050 I
8260A ND mg/1 0.0050
8260A ND mg/1 0.0050
8260A ND mg/1 0.0050
8260A ND mg/1 0.0050 I
8260A ND mg/1 0.0050
8260A ND mg/1 0.0050
8260A ND mg/1 0.0050
8250A ND mg/1 0.0100
8260A ND mg/1 0.0150 I
I
I
I
Terms and Conditions on Reverse Side I
I
I
I
I
I
I
I
06 VANTAGE POINT DRIVE
~AYCE. SOUTH CAROLINA 29033
SC DHEC No. 32010
Client:
Attention:
SHEALY Lab No: 82997N
Description: K-28
Date Received: 01/17/96
Date Reported: 02/01/96
Parameters
I VOLATILE ORGANICS
acetone
benzene
bromodichloromethane
I bromoform
bromomethane
2-butanone
carbon disulfide
-·· --ban tetrachloride
I ~robenzene
.oroethane
chloroform
chloromethane
I dibromochloromethane
1,1-dichloroethane
1,2-dichloroethane
1,1-dichloroethene
c1s-l,2-dichloroettene I trans-1,2-dichlorcethene
1,2-dichloropropane
c1s-l,3-d1chloropropene
ethylbenzene
12 -hexanone
methylene chloride
4-methyl-2-pentanone
styrene
1,1,2,2-tetrachloroethane I tetrachloroethene
toluene
1,1,1-trichloroethane
1,1,2-trichloroethane
I trichloroethene
vinyl acetate
vinyl chloride
xylenes
I
I
I
I
SHEALY ENVIRONMENTAL SERVICES, INC.
· Scientists and Consultants
CERTIFICATE OF ANALYSIS
HOECHST CELANESE-SHELBY PLANT P.O. Box 87
Shelby, NC 28151-0087
Kathryn Frank
QA/QC
[phone]
FAX [phone]
NC DEHNR No. 329
Coll. Date: 01/16/96
Coll. Time: 1230
Officer -1Y1A::.--
V.P. Analytical /Y/~
Method
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
Result
ND
0.0086
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Units
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
Terms and Conditions on Reverse Side
Date Date
PQL Prepared Analyzed Anal.
01/26/96 RED
0.0500
0,0050
0.0050
0.0050
0.0100
0.0100
0.0200
0.0050
0.0050
0.0100
0.0050
0.0100
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0100
0.0150
06 VANTAGE POINT DRIVE
CAYCE. SOUTH CAROLINA 29033
SC DHEC No. 32010
Client:
Attention:
SHEALY Lab No, 82998N
Description: P-58
Date Received: 01/17/96
Date Reported: 02/01/96
Parameters
VOLATILE ORGANICS
acetone
benzene
bromodichloromethane
bromoform
bromomethane
2-butanone
c«rbon disulfide
·bon tetrachlor~. 1e
orobenzene
~:i.loroethane
chlorofo~
chloromethane
dibromochloromethane
1,1-dichloroethane
1,2-dichloroe~hane
1,1-dichloroethene
cis-1,2-dichloroethene
trans-1,2-dichloroet.hene
1,2-dichloropropane
cis-1,3-dichloropropene
ec.hylbenzene
2-hexanone
methylene chloride
4-methyl-2-pent.anone
styrene
1,1,2,2-tetrachloroethane
t.et.rachloroethene
toluene
1,1,1-trichloroethane
1,1,2-trichloroethane
trichloroethene
vinyl acetate
vinyl chloride
xylenes
SHEALY ENVIRONMENTAL SERVICES, INC. I
Scientists and Consultants
CERTIFICATE OF ANALYSIS
HOECHST CELANESE-SHELBY PLANT
P.O. Box 87 Shelby, NC 28151-0087
Kathryn Frank
Method
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
Result
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Units
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
:ng/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
Terms and Conditions on Reverse Side
PQL
0.0500
0.0050
0.0050
0.0050
0.0100
0.0100
0.0200
0.0050
0.0050
0.0100
0.0050
0.0100
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0100
0.0150
QA/QC
[phone]
FAX (803) 791 ·9111
NC DEHNR No. 329
I
I
I
Coll. Date: 01/16/96 I
Coll. Time: 1330
Officer ~D::'£l-
V.P. Analytical MJ--" I
Date Date
Prepared Analyzed Anal. I
01/26/96 RED I
I
I
I
I
I
I
I
I
I
I
I
I
I 16 VANTAGE POINT DRIVE
~AYCE, SOUTH CAROLINA 29033
I SC DHEC No. 32010
Client:
I
Attention:
•
SHEALY Lab No, 83164
Description: T-35
Date Received: 01/18/96 I Date Reported, 02/01/96
I Para.meters
I VOLATILE ORGANICS
acetone
benzene
bromodichloromethane
I bromoform
bromomethane
2-butanone
ca·.cbon disulfide
)on tetrachloride
I ,robenzene
::::.1oroethane
chloroform
chloromethane
I dibromochloromethane
1,1-dichloroethane
1,2-dichloroethane
1,1-dichloroethene
cis-1,2-dichloroethene
I trana-1, 2 -dichloroethene
1,2-dichloropropane
cis-1,3-dichloropropene
ethylbenzene
12 -hexanone
~et~ylene chloride
4-methyl-2-pentanone
styrene
1,1,2,2-tetrachloroethane
I tetrachloroethene
toluene
l,1,1-trichloroethane
1,1,2-trichloroethane
I trichloroethene
vinyl acetate
vinyl chloride
xylenes
I
I
I
I
SHEALY ENVIRONMENTAL SERVICES, INC.
Scientists and Consultants
CERTIFICATE OF ANALYSIS
HOECHST CELANESE-SHELBY PLANT P.O. Box 87 Shelby, NC 28151-0087
Kathryn Frank
Method Result Units PQL
8260A ND mg/1 0.0500
8260A ND mg/1 0.0050
8260A ND mg/1 0.0050
8260A ND mg/1 0.0050
8260A ND mg/1 0.0100
8260A ND mg/1 0.0100
8260A ND mg/1 0.0200
8260A ND mg/1 0.0050
8260A ND mg/1 0.0050
8260A ND mg/1 0.0100
8260A ND mg/1 0.0050
8260A ND mg/1 0.0100
8260A ND mg/1 0.0050
8260A ND mg/1 0.0050
8260A ND mg/1 0.0050
8260A ND mg/1 0.0050
8260A ND mg/1 0.0050
8260A ND mg/1 0.0050
8260A ND mg/1 0.0050
8260A ND mg/1 0.0050
8260A ND mg/1 0.0050
8260A ND mg/1 0.0050
8260A ND mg/1 0.0050
8260A ND mg/1 0.0050
8260A ND mg/1 0.0050
8260A ND mg/1 0.0050
8260A ND mg/1 0.0050
8260A ND mg/1 0.0050
8260A ND mg/1 0.0050
8260A ND mg/1 0.0050
8260A ND mg/1 0.0050
8260A ND mg/1 0.0050
8260A ND mg/1 0.0100
8260A ND mg/1 0.0150
Terms and Conditions on Reverse Side
QA/QC
[phone]
FAX [phone]
NC DEHNR No. 329
Coll. Date: 01/17/96
Coll. Time: 1240
Officer -~
V.P. Analytical Mil?/
Date Date
Prepared Analyzed Anal.
01/26/96 RED
SHEALY ENVIRONMENTAL SERVICES, INC. I
Scientists and Consultants
106 VANTAGE POINT DRIVE
,;AYCE. SOUTH CAROLINA 29033 CERTIFICATE OF ANALYSIS
SC DHEC No. 32010
Client:
Attention:
SHEALY Lab No, 82999N
Description: V-23
Date Received: 01/17/96
Date Reported: 02/01/96
Parameters
HOECHST CELANESE-SHELBY PLANT
P.O. Box 87 Shelby, NC 28151-0087
Kathryn Frank
Method Result Units PQL
QA/QC
[phone]
FAX [phone]
I
NC DEHNR No. 3291
I
Coll. Date: 01/16/96 I
Coll. Time: 1330
Officer fDei::--:
V.P. Analytical /1;11j-1,<./ I
I Date Date
Prepared Analyzed Anal. ----------------------------------------
VOLATILE ORG..U<ICS
acetone
benzene
bromodichloromethane
bromoform
bromomethane
2 -butanone
carbon disulfide
ca~·bon tetrachloride
~;robenzene
oroethane
c!".loroform
chloromethane
dibromochloromethane
1,1-dichloroethane
1,2-dichloroethane
1,1-dichloroethene
cis-1,2-dichloroethene
trans-1,2-dichloroethene
1,2-dichloropropane
cis-1,3-dichloropropene
ethylbenzene
2-hexanone
~ethylene chloride
4-methyl-2-pentanone
styrene
1,1,2,2-tetrachloroethane
~etrachloroethene
toluene
1,1,1-trichloroethane
1,1,2-trichloroet!_dne
trichloroethene
vinyl acetate
vinyl chloride
xylenes
8260A
8260A
8250A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8250A
8250A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
0.4870
0.0193
ND
ND
ND
3.6000
0.0490
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
0.2820
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
Terms and Conditions on Reverse Side
01/26/96 RED
0.0500
0.0050 I
0.0050
0.0050
0.0100
0.0100
0.0200 I
0.0050
0.0050
0.0100
0.0050 I
0.0100
0.0050
0.0050
0.0050 I 0.0050
0.0050
0.0050
0.0050
0.0050 I
0.0050
0.0050
0.0050
0.0050 I 0.0050
0.0050
0.0050
0.0050
0.0050 I
0.0050
0.0050
0.0050
0.0100 I 0.0150
I
I
I
I
I
I .06 VANTAGE POINT DRIVE
CAYCE, SOUTH CAROLINA 29033
I SC DHEC No. 32010
Client:
I
Attention:
I SHE,.LY Lab No, 83211
Description: AA-54
Date Received: 01/18/96 I Date. Reported, 02/01/96
I Parameters
I VOLATILE ORGANICS
acetone
benzene
bromodichloromethane
I bromoform
bromomethane
2-butanone
cai:·bon disulfide
i1on tetrachlorite
I orobenzene
c:-.1.loroethane
chloroform
chloromethane
I dibromochloromethane
1,1-dichloroethane
1,2-dichloroethane
1,1-dichloroethene
cis-1,2-dichloroethene I trana-1,2-dichloroethene
1,2-dichloropropane
cis-1,3-dichloropropene
ethylbenzene
12 -hexanone
methylene chloride
4-methyl-2-pentanone
styrene
1,1,2,2-tetrachloroethane I tetrachloroethene
toluene
1,1,1-trichloroethane
1,1,2-trichloroethane
I trichloroethene
vinyl acetate
vinyl chloride
xylenes
I
I
I
I
SHEALY ENVIRONMENTAL SERVICES, INC.
Scientists and Consultants
CERTIFICATE OF ANALYSIS
HOECHST CELANESE-SHELBY PLANT
P.O. Box 87 Shelby, NC 28151-0087
Kathryn Frank
Method Result Units PQL
8260A ND mg/1 0.0500
8260A ND mg/1 0.0050
8260A ND mg/1 0.0050
8260A ND mg/1 0.0050
8260A ND mg/1 0.0100
8260A ND mg/1 0.0100
8260A ND mg/1 0.0200
8260A ND mg/1 0.0050
8260A ND mg/1 0.0050
8260A ND mg/1 0.0100
8260A ND mg/1 0.0050
8260A ND mg/1 0.0100
8260A ND mg/1 0.0050
8260A ND mg/1 0.0050
8260A ND mg/1 0.0050
8260A ND mg/1 0.0050
8260A ND mg/1 0.0050
8260A ND mg/1 0.0050
8260A ND mg/1 0.0050
8260A ND mg/1 0.0050
8260A ND mg/1 0.0050
8260A ND mg/1 0.0050
8260A ND mg/1 0.0050
8260A ND mg/1 0.0050
8260A ND mg/1 0.0050
8260A ND mg/1 0.0050
8260A ND mg/1 0.0050
8260A ND mg/1 0.0050
8260A ND mg/1 0.0050
8260A ND mg/1 0.0050
8260A ND mg/1 0.0050
8260A ND mg/1 0.0050
8260A ND mg/1 0.0100
8260A ND mg/1 0.0150
Terms and Conditions on Reverse Side
QA/QC
[phone]
FAX [phone]
NC DEHNR No. 329
Coll. Date: 01/18/96
Coll. Time: 1402
Officer --YY'IGL
V.P. Analytical /ti 1)1_,.....)
Date Date
Prepared Analyzed Anal.
01/27/96 RED
, 06 VANTAGE POINT DRIVE
CAYCE, SOUTH CAROLINA 29033
SHEALY ENVIRONMENTAL SERVICES, INC.
Scientists and Consultants
CERTIFICATE OF ANALYSIS
(803) 79i-9700
FAX [phone]:.
I
I
=S=C=D=H=E=C=N=o=. =3=2=0=1=0=========================N=C=D=E=HNR==N=o=. =3=2=9 •
Client:
Attention:
SHEALY Lab No, 83162
Description: cc-33
Date Received: 01/18/96
Date Reported: 02/01/96
Parameters
HOECHST CELANESE-SHELBY PLANT P.O. Box 87 Shelby, NC 281Sl-0087
Kathryn Frank
Method Result Units PQL
QA/QC
Coll. Date: 01/17/96
Coll. Time: 1205
Officer -07.s.f~
V.P. Analytical IY1~
Date Date
Prepared Analyzed Anal. --------------------------------------------------
VOLATILE ORGANICS
acetone
benzene
bromodichlorome tha~1e
bromoform
bromomethane
2-butanone
carbon disulfide
·:::·ban tetrachloride
·)robenzene
.oroethane
cnloroform
chloromethane
dibromochloromethane
1,1-dichloroethane
1,2-dichloroethane
1,1-dichloroethene
cis-1,2-dichloroethene
trans-1,2-dichloroethene
1,2-dichloropropane
cis-1,3-dichloropropene
ethylbenzene
2-hexanone
methylene chloride
4-methyl-2-pentanone
styrene
1,1,2,2-tetrachloroethane
tetrachloroethene
toluene
1,1,1-trichloroethane
1,1,2-trichloroethane
trichloroethene
vinyl acetate
vinyl chloride
xylenea
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
ND
0.0100
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
Terms and Conditions on Reverse Side
01/26/96 RED
0.0500
0.0050
0.0050
0.0050
0.0100
0.0100
0.0200
0.0050
0.0050
0.0100
0.0050
0.0100
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0100
0.0150
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I 06 VANTAGE POINT DRIVE
CAYCE, SOUTH CAROLINA 29033
I SC DHEC No. 32010
Client:
I
Attention:
I SHEALY Lab No, 83163
Description: CC-33 Duplicate
Date Received: 01/18/96
I Date Reported: 02/01/96
I Parameters
I VOLATILE ORGANICS
acetone
benzene
bromodichloromethane
I bromoform
bromomethane
2-butanone
::.,.,._.·ban disulfide
·,on tetrachloride
I ::irobenzene
cr.loroethane
chloroform
chloromethane
I dibromochloromethane
1,1-dichloroethane
1,2-dichloroethane
1,1-dichloroethene
cis-1,2-dichloroethene I trans-1,2-dichloroethene
1,2-dichloropropane
cis-1,3-dichloropropene
ethylbenzene
12 -hexanone
methylene chloride
4-methyl-2-pentanone
styrene
1,1,2,2-tetrachloroethane
I tetrachloroethene
toluene
1,1,1-trichloroethane
1,1,2-trichloroethane
I trichloroethene
vinyl acetate
vinyl chloride
xylenes
I
I
I
I
SHEALY ENVIRONMENTAL SERVICES, INC.
Scientists and Consultants
CERTIFICATE OF ANALYSIS
HOECHST CELANESE-SHELBY PLANT P.O. Box 87
Shelby, NC 28151-0087
Kathryn Frank
Method
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
Result
mi
0.0125
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Units
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
Terms and Conditions on Reverse Side
PQL
0.0500
0.0050
0.0050
0.0050
0.0100
0.0100
0.0200
0.0050
0.0050
0.0100
0.0050
0.0100
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0100
0.0150
QA/QC
[phone]
FAX [phone]
NC DEHNR No. 329
Coll. Date: 01/17/96
Coll. Time: 1205
Officer -tY1GL
V.P. Analytical ;;,p,-,r
Date Date
Prepared Analyzed Anal.
01/26/96 RED
06 VANTAGE POINT DRIVE
,AYCE, SOUTH CAROLINA 29033
SC DHEC No. 32010
Client:
Attention:
SHEALY Lab No, 83209
Description: EE-58
Date Received: 01/18/96
Date Reported: 02/01/96
Parameters
VOLATILE ORGANICS
acetone
benzene
bromodichloromethane
bromoform
bromomethane
2-butanone
carbon disulfide
C-".:bon tetrachlori,le
'jrobenzene
.:iroethane
cnloroform
chloromethane
dibromochloromethane
1,1-dichloroethane
1,2-dichloroethane
1,1-dichloroethene
cis-1,2-dichloroethene
trans-1,2-dichloroethene
1,2-dichloropropane
cis-1,3-dichloropropene
echylbenzene
2-hexanone
~ethylene chloride
4-methyl-2-pentanone
sty:-ene
1,1,2,2-tetrachloroethane
tetrachloroethene
toluene
l,l,l-trichloroet'.1dne
1,1,2-trichloroethane
trichloroethene
vinyl acetate
vinyl chloride
xylenea
SHEALY ENVIRONMENTAL SERVICES, INC.
Scientists and Consultants
CERTIFICATE OF ANALYSIS
HOECHST CELANESE-SHELBY PLANT
P.O. Box 87 Shelby, NC 28151-0087
Kathryn Frank
Method
8260A.
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
Result
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Units
mg/1
mg/1
mg/1
mg/1 ·
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
:ng/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/l
mg/1
mg/1
Terms and Conditions on Reverse Side
PQL
0.0500
0.0050
0.0050
0.0050
0.0100
0.0100
0.0200
0.0050
0.0050
0.0100
0.0050
0.0100
0.0050
0.0050
· 0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0100
0.0150
[phone]
FAX (803) 79i-91i1
I
NC DEHNR No. 329 I
QA/QC
Coll. Date: 01/18/95
Coll. Time: 1230
Officer '7ll!-§,,
V.P. Analytical /11,r-/
Date Date
Prepared Analyzed Anal.
01/27/96 RED
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I I 06 VANTAGE POINT DRIVE
CAYCE, SOUTH CAROLINA 29033
I SC DHEC No. 32010
Client:
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
Attention:
SHEALY Lab No, 83207
Description: FF-34
Date Received: 01/18/96
Date Reported: 02/01/96
Parameters
VOLATILE ORGANICS
acetone
benzene
bromodichloromethane
bromofonn
bromomethane
2-butanone
carbon disulfide
•tbon tetrachloride
orobenzene
.oroethane
chlorofor::n
chloromethane
dibromochloromethane
1,1-dichloroethane
1,2-dichloroethane
1,1-dichloroethene
cis-1,2-dichloroethene
trans-1,2-dichloroethene
1,2-dichloropropanc
cis-1,3-dichlorop=~pene
ethylbenzene
2-hexanone
methylene chloride
4-methyl-2-pentanone
styrene
1,1,2,2-tetrachloroethane
tetrachloroethene
toluene
1,1,1-trichloroethane
1,1,2-trichloroethane
trichloroethene
vinyl acetate
vinyl chloride
xylenes
SHEALY ENVIRONMENTAL SERVICES, INC.
Scientists and Consultants
CERTIFICATE OF ANALYSIS
HOECHST CELANESE-SHELBY PLANT P.O. Box 87 Shelby, NC 28151-0087
Kathryn Frank
Method
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8250A
8250A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
Result
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Units
mg/1
mg/1
:ng/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
:ng/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
Terms and Conditions on Reverse Side
PQL
0.0500
0.0050
0.0050
0.0050
0.0100
0.0100
0.0200
0.0050
0.0050
0.0100
0.0050
0.0100
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0100
0.0150
QA/QC
[phone]
FAX [phone]
NC DEHNR No. 329
Coll. Date: 01/18/96
Coll. Time: 1128
Officer 4"r",PS°-
V.P. Analytical «' f1:'.1.-'.-:! i
Date Date
Prepared Analyzed Anal.
01/26/96 RED
06 VANTAGE POINT DRIVE
CAYCE, SOUTH CAROLINA 29033
SC DHEC No. 32010
Client:
Attention:
SHEALY Lab No, 83208
Description: FF-62
Date Received: 01/18/96
Date Reported: 02/01/96
Parameters
SHEALY ENVIRONMENTAL SERVICES, INC.
Scientists and Consultants
CERTIFICATE OF ANALYSIS
HOECHST CELANESE-SHELBY PLANT P.O. Box 87
Shelby, NC 28151-0087
Kathryn Frank
QA/QC
[phone]
FAX [phone]
I
I
NC DEHNR No. 329 I
Coll. Date: 01/18/96
Coll. Time: 1151
Officer ':fhe-f <
I
I
V.P. Analytical M J2:'.V". I
I Method
Date Date
Result Units PQL Prepared Analyzed Anal. --------------------------------------------------
VOLATILE ORGANICS
acetone
benzene
bromodichlorometha~e
bromof_orm
bromomethane
2-butanone
ca:::-bon disulfide
·bon tetrachloride
orobenzene
_ .. loroethane
chlorofor:n
chloromethane
dibromochloromethaHe
1,1-dichloroethan~
1,2-dichloroethane
1,1-dichloroethene
cis-1,2-dichloroet~ene
trans-1,2-dichloroethene
1,2-dichloropropan~
cis-1,3-dichloropropene
ethylbenzene
2-hexanone
methylene chloride
4-methyl-2-pentanone
styrene
1,1,2,2-tetrachloroethane
tetrachloroethene
toluene
1,1,1-trichloroethane
1,1,2-trichloroethane
trichloroethene
vinyl acetate
vinyl chloride
xylenes
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8250A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
Terms and Conditions on Reverse Side
01/27/96 RED
0.0500
0.0050 I
0.0050
0.0050
0.0100
0.0100
0.0200 I
0.0050
0.0050
0.0100
0.0050 I
0.0100
0.0050
0.0050
0.0050
o. oofo I
0.0050
0.0050
0.0050
0.0050 I
0.0050
0.0050
0.0050
0.0050
0.0050 I
0.0050
0.0050
0.0050
0.0050 I
0.0050
0.0050
0.0050
0.0100
0.0150 I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
'06 VANTAGE POINT DRIVE
~AYCE. SOUTH CAROLINA 29033
SC DHEC No. 32010
Client:
Attention:
SHEALY Lab No: 83210
Description: GG-61
Date Received: 01/18/96
Date Reported: 02/01/96
Parameters
VOLATILE ORGANICS
acetone
benzene
b romodi ch 1 orome tha;.e
bromoform
bromomethane
2-butanone
carbon disulfide
,..,rbon tetrachloride
:irobenzene
.oroethane
chloroform
chloromethane
dibromochlorometh.l.le
1,1-dichloroethant
1,2-dichloroethane
1,1-dichloroethent
cis-1,2-dichloroec~ene
trans-1,2-dichlorouthene
1,2-dichloroprapane
cis-1,3-dichloroprc.pene
ethylbenzene
2-hexanone
methylene chloride
4 -methyl - 2 -pentanor.e
styrene
1,1,2,2-tetrachloroethane
tetrachloroethene
toluene
1,1,1-trichloroethane
1,1,2-trichloroethane
trichloroethene
vinyl acetate
vinyl chloride
xylenes
SHEALY ENVIRONMENTAL SERVICES, INC.
Scientists and Consultants
CERTIFICATE OF ANALYSIS
HOECHST CELANESE-SHELBY PLANT
P.O. Box 87 Shelby, NC 28151-0087
Kathryn Frank
Method
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
82.60A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
Result
NU
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Onita
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1,
mg/1
mg/1
mg/1
Terms and Conditions on Reverse Side
PQL
0.0500
0.0050
0.0050
0.0050
0.0100
0.0100
0.0200
0.0050
0.0050
0.0100
0.0050
0.0100
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0. 0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0100
0.0150
QA/QC
[phone]
FAX [phone]
NC DEHNR No. 329
Coll. Date: 01/18/96
Coll. Time: 1318
Officer ~mRF ,-'.
V.P. Analytical t1 ,ri.,----
Date Date
Prepared Analyzed Anal.
01/27/96 RED
06 VANTAGE POINT DRIVE
CAYCE, SOUTH CAROLINA 29033
SC DHEC No. 32010
Client:
Attention:
SHEALY Lab No, 8 3167
Description: HH-48
Date Received: 01/18/96
Date Reported: 02/01/96
Parameters
SHEALY ENVIRONMENTAL SERVICES, INC.
Scientists and Consultants
CERTIFICATE OF ANALYSIS
HOECHST CELANESE-SHELBY PLANT P.O. Box 87
Shelby, NC 28151-0087
Kathryn Frank
QA/QC
[phone]
FAX [phone]
NC DEHNR No. 329
I
I
I
I
Coll. Date: 01/17/96 I
Coll. Time: 1438
Officer ~b:::'Af<
V.P. Analytical Mir½! I
I Method
Date Date
Result Units PQL Prepared Analyzed Anal. ----------------------------------------
VOLATILE ORGANICS
acetone
benzene
bromodichloromethane
bromoform
bromomethane
2-butanone
rarbon disulfide
~on tetrachloride
orobenzene
O.::nloroethane
chloroform
chloromethane
dibromochloromethane
1,1-dichloroethane
1,2-dichloroethane
1,1-dichloroethene
cis-1,2-dichloroethene
trans-1,2-dichloroethene
1,2-dichloropropane
cis-1,3-dichloropropene
ethylbenzene
2-hexanone
methylene chloride
4-methyl-2-pentanone
styrene
1,1,2,2-tetrachloroethane
cetrachloroethene
toluene
1,1,1-trichloroethane
1,1,2-trichloroethane
trichloroethene
vinyl acetate
vinyl chloride
xylene a
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
0.1650
ND
ND
ND
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
Terms and Conditions on Reverse Side
01/27 /96 RED
0.0500
0.0050 I
0.0050
0.00S0
0.0100
0.0100 I 0.0200
0.0050
0.0050
0.0100
0.0050 I
0.0100
0.0050
0.0050
0.0050 I
0.0050
0.0050
0.0050
0.0050
0.0050 I
0.0050
0.0050
0.0050
0.0050 I
0.0050
0.0050
0.0050
0.0050
0.0050 I
0.0050
0.0050
0.0050
0.0100 I
0.0150
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
06 VANTAGE POINT DRIVE
CAYCE, SOUTH CAROLINA 29033
SC DHEC No. 32010
Client:
Attention:
SHEALY Lab No: 83166
Description: HH-77
Date Received: 01/18/96
Date Reported: 02/01/96
Parameters
VOLATILE ORGANICS
acetone
benzene
bromodichloromethane
bromoform
bromomethane
2-butanone
carbon disulfide
·bon tetrachloride
:,robenzene
.. .Loroethane
chloroform
chloromethane
dibromochloromethane
1,1-dichloroethane
1,2-dichloroethane
1,1-dichloroethene
cis-1,2-dichloroethene
trans-1,2-dichloroethene
1,2-dichloropropane
cis-1,3-dichloropropene
ethylbenzene
2-hexanone
methylene chloride
4-methyl-2-pentanone
styrene
1,1,2,2-tetrachloroethane
tetrachloroethene
toluene
1,1,l-trichloroethane
1,1,2-trichloroethane
trichloroethene
vinyl acetate
vinyl chloride
xylenes
SHEALY ENVIRONMENTAL SERVICES, INC.
Scientists and Consultants
CERTIFICATE OF ANALYSIS
HOECHST CELANESE-SHELBY PLANT P.O. Box 87
Shelby, NC 28151-0087
Kathryn Frank
Method
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
Result
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
0.1870
ND
ND
ND
Units
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
Terms and Conditions on Reverse Side
PQL
0.0500
0.0050
0.0050
0.0050
0.0100
0.0100
0.0200
0.0050
0.0050
0.0100
0.0050
0.0100
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0100
0.0150
[phone]
FAX [phone]
NC DEHNR No. 329
Coll. Date: 01/17/96
Coll. Time: 1410
QA/QC Officer ~b:Jef___.
V. P. Analytical /)JI rr::iJ
Date Date
Prepared Analyzed Anal.
01/27/96 RED
06 VANTAGE POINT DRIVE
CAYCE. SOUTH CAROLINA 29033
SC DHEC No. 32010
Client:
Attention·:
SHEALY Lab No, 8300QN
Description: Field Blank
Date Received: 01/17/96
Date Reported: 02/01/96
Parameters
SHEALY ENVIRONMENTAL SERVICES, INC.
Scientists and Consultants
CERTIFICATE OF ANALYSIS
HOECHST CELANESE-SHELBY PLANT P.O. Box 87
Shelby, NC 28151-0087
Kathryn Frank
QA/QC
[phone]
FAX [phone]
NC DEHNR No. 329
I
I
I
I
Coll. Date: 01/16/96 I
Coll. Time: 1400
Officer tr:ec
V.P. Analytical Nlr,J I
I Method
Date Date
Result Units PQL Prepared Analyzed Anal. ----------------------------------------
VOLATILE ORGANICS
acetone
benzene
bromodichloromethane
bromoform
bromomethane
2-butanone
carbon disulfide
~on tetrachloride
.:>rcbenzene
:...1loroethane
chloroform
chloromethane
dibromochloromethane
1,1-dichloroethane
1,2-dichloroethane
1,1-dichloroethene
cis-1,2-dichloroethene
trans-1,2-dichloroethene
1,2-dichloropropane
cis-1,3-dichloropropene
ethylbenzene
2-hexanone
~ethylene chloride
4-methyl-2-pentanone
!Jtyrene
1,1,2,2-tetrachloroethane
~etrachloroethene
toluene
1,1,1-trichloroethane
1,1,2-trichloroethane
trichloroethene
vinyl acetate
vinyl chloride
xylenes
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
Terms and Conditions on Reverse Side
01/26/96 RED
0.0500
0.0050 I
0.0050
0.0050
0.0100
0.0100 I 0.0200
0.0050
0.0050
0.0100
0.0050 I
0.0100
0.0050
0.0050
0.0050 I 0.0050
0.0050
0.0050
0.0050
0.0050 I
0.0050
0.0050
0.0050
0.0050 I 0.0050
0.0050
0.0050
0.0050
0.0050 I
0.0050
0.0050
0.0050
0.0100 I 0.0150
I
I
I
I
I
I '06 VANTAGE POINT DRIVE
CAYCE, SOUTH CAROLINA 29033
I SC DHEC No. 32010
Client:
I Attention:
I SHEALY Lab No, 83006N
Description: Trip Blank
Date Received: 01/17/96
Reported: 02/01/96 I Date
I Parameters
I VOLATILE ORGANICS
acetone
benzene
bromodichloromethane
bromofor.n
I bromomethane
2-butanone
carbon disul!ide
~on tetrachlo~ .. de
I ,robenzene
,.,._ .. oroethane
chloroform
chloromethane
dibromochloromethane
11, 1-dichloroethane
1,2-dichloroethan~
1,1-dichloroethen i
cis-1,2-dichloroet~ene
I trans~ 1, 2 -dichloro~thene
1,2-dichloroprop~~:
cis-1,3-dichloropr:,pene
ethylbenzene
2-hexanone
l :11ethylene chloride
4-methyl-2-pentanor.e
styrene
1,1,2,2-tetrachloroethane
I tetrachloroethene
toluene
1,1,1-trichloroethane
1,1,2-trichloroethane
t:richloroethene
•
vinyl acetate
vinyl chloride
xylenes
I
I
I
I
SHEALY ENVIRONMENTAL SERVICES, INC.
Scientists and Consultants
CERTIFICATE OF ANALYSIS
HOECHST CELANESE-SHELBY PLANT P.O. Box 87 Shelby, NC 28151-0087
Kathryn Frank
Method
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8250A
8260A
8250A
8260A
8260A
8260A
8260A
8260A
8260.i\
8260.i\
8260A
8250A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8250A
8260A
Result
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Units
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/l
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
Terms and Conditions on Reverse Side
PQL
0.0500
0.0050
0.0050
0,0050
0.0100
0.0100
0.0200
0.0050
0.0050
0.0100
0.0050
0.0100
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0,0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0100
0.0150
QA/QC
[phone]
FAX [phone]
NC DEHNR No. 329
Coll. Date: 01/16/96
Coll. Time: 0730
Officer M8S-
V.P. Analytical /vi~
Date Date
Prepared Analyzed Anal.
01/27/96 RED
16 VANTAGE POINT DRIVE
;AYCE SOUTH CAROLINA 29033
SHEALY ENVIRONMENTAL SERVICES, INC.
Scientists and Consultants
CERTIFICATE OF ANALYSIS
[phone]
FAX [phone]
I
I
SC DHEC No. 32010 NC DEHNR No. 329 I
Client: HOECHST CELANESE-SHELBY PLANT
Shelby, NC 28151-0087 P.O. Box 87 I
Attention:
SHEALY Lab No, 83161
Description: Trip Blank
Date Received: 01/18/96
Date Reported: 02/01/96
Parameters
VOLATILE ORGANICS
acetone
benzene
bromodichloromethane
bromoform
bromomethane
2-butanone
carbon disulfide
-hon tetrachloride
:irobenzene
.oroechane
chloroforsn
chloromethane
dibromochloromethane
1,1-dichloroethane
1,2-dichloroethane
1,1-dichloroethene
cis-1,2-dichloroechene
trans-1,2-dichloroethene
1,2-dichloropropar.e
cis-1,3-dichloropr~pene
ethylbenzene
2-hexanone
methylene chloride
4-methyl-2-pentanone
styrene
.1,1,2,2-tetrachloroethane
tetrachloroethene
toluene
1,1,1-trichloroethane
1,1,2-trichloroethane
trichloroethene
vinyl acetate
vinyl chloride
xylenes
Kathryn Frank
Method
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
Result
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
NO
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Units
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
Terms and Conditions on Reverse Side
PQL
0.0500
0.0050
0.0050
0.0050
0.0100
0.0100
0.0200
0.0050
0.0050
0.0100
0.0050
0.0100
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0100
0.0150
QA/QC
Coll. Date: 01/16/95 I
Coll. Time: 0730
Officer ·rn0f,_.
V.P. Analytical /Yl,/1,J I
I Date Date
Prepared Analyzed Anal.
01/26/96 RED I
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SHEALY ENVIRONMENTAL SERVICES, INC.
Scientists' and Consultants
106 VANTAGE POINT DRIVE
CAYCE, SOUTH CAROLINA 29033 CERTIFICATE OF ANALYSIS
[phone]
FAX [phone]
SC DHEC No. 32010
Client:
Attention:
SHEALY Lab No: 83213
Description: Trip Blank
Date Received: 01/18/96
Date Reported: 02/01/96
Pa:t"ameters
VOLATILE ORGANICS
acetone
benzene
b=omodichloromethar.e
bromoform
bromomethane
2-butanone
carbon disulfide
·::ion tetrachlori-1e
orobenzene
.• .i.oroethane
chloroform
chloromethane
dibromochloromethane
1,1-dichloroethane
1,2-dichloroethane
1,1-dichloroethene
cie-1,2-dichloroethene
trane-1,2-dichlorcethene
1,2-dichloropropane
cis-1,3-dichloropropene
ethylbenzene
2-hexanone
methylene chloride
4-methyl-2-pentanone
styrene
1,1,2,2-tetrachloroethane
tetrachloroethene
toluene
1, 1, 1-trichloroet.',ane
1,1,2-trichloroethane
trichloroethene
vinyl acetate
vinyl chloride
xylenes
HOECHST CELANESE-SHELBY PLANT P.O. Box 87 Shelby, NC 28151-0087
Kathryn Frank
Method
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8250.i\
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
Result
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Units
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
Terms and Conditions on Reverse Side
PQL
0.0500
0.0050
0.0050
0.0050
0.0100
0.0100
0.0200
0.0050
0.0050
0.0100
0.0050
0.0100
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0100
0.0150
NC DEHNR No. 329
Coll. Date: 01/16/96
Coll. Time: 07 30
QA/QC Officer ~"'
V.P. Analytical /1/1~
Date Date
Prepared Analyzed Anal.
01/27/96 RED
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I SAMPLE RESULTS
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I Ethylene Glycol
I Method 8015A
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Client Sample
ldcnlificalion
ITCI
ITEF
ITEF lllll'LICATE
Maslc:r Track inc>: List -E1hyk11c Glycol
IIOECIIST CELANESE-Shelby
First Quarter 1996
SIi EALY Lah Dale llatc
ID Numhcr Collcdcd Received
831lll3N lll/16/96 01/17/96
83156 01/17/96 01/18/96
83157 01/17/96 01/18/96
Prep. Analysis
llatc llatc
01/19/96 01 /22/96
01/19/96 01/19/96
01/19/96 01/19196
I
I 06 VANTAGE POINT DRIVE
CAYCE. SOUTH CAROLINA 29033
I SC DHEC No. 32010
Client:
I
Attention:
I SHEALY Lab No, 8 3 0 0 3 N
Description: ITCI
Date I Date
Received: 01/17/96
Reported: 02/01/96
I Parameters
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ethylene glycol
SHEALY ENVIRONMENTAL SERVICES, INC.
Scientists and Consultants
CERTIFICATE OF ANALYSIS
HOECHST CELANESE-SHELBY PLANT P.O. Box 87 Shelby, NC 28151-0087
Kathryn Frank
[phone]
FAX [phone]
NC DEHNR No. 329
Coll. Date: 01/16/96
Coll. Time: 1455
QA/QC Officer _"l-'---'C'f:('----";;s,.~--'------
v.P. Analytical _/t/w.,~k"---'c_ __ _
Date Date
Method Result Onita PQL Prepared Analyzed Anal.
8015A 1100 mg/1 6.50 01/19/96 01/22/96 SAG
Terms and Conditions on Reverse Side
.06 VANTAGE POINT DRIVE
CAYCE. SOUTH CAROLINA 29033
SC DHEC No. 32010
Client,
Attention:
SHEALY Lab No, 83156
Description: ITEF
Date Received: 01/18/96
Date Reported: 02/01/96
Parameters
ethylene glycol
SHEALY ENVIRONMENTAL SERVICES, INC. I
Scientists and Consultants
CERTIFICATE OF ANALYSIS
HOECHST CELANESE-SHELBY PLANT P.O. Box 87
Shelby, NC 28151-0087
Kathryn Frank
Method Result Units PQL
[phone]
FAX [phone]
I
NC DEHNR No. 329 I
I
Coll. Date: 01/17/96 I
Coll. Time: 1050
QA/QC Officer ::[()FJL
V. P. Analytical /n fr!.---/
Date Date
Prepared Analyzed Anal.
8015A ND mg/1 6.50 01/19/96 01/19/96 SAG
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I Terms and Conditions on Reverse Side
I
I . 06 VANTAGE POINT DRIVE
CAYCE, SOUTH CAROLINA 29033
I SC DHEC No. 32010
Client:
I Attention:
I SHEALY Lab No, 8 3 15 7
Description: ITEF Duplicate
Date Received: 01/18/96 I Date Reported, 02/01/96
I Parameters
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ethylene glycol
SHEALY ENVIRONMENTAL SERVICES, INC.
Scientists and Consultants
CERTIFICATE OF ANALYSIS
HOECHST CELANESE-SHELBY PLANT
P.O. Box 87
Shelby, NC 28151-0087
Kathryn Frank
Method Result Units PQL
[phone]
FAX [phone]
NC DEHNR No. 329
Coll. Date: 01/17/96
Coll. Time: 1050
QA/QC Officer t:'r:J8E,,
V. P. Analytical /J'/ ~
Date Date
Prepared Analyzed Anal.
8015A ND mg/1 6.50 01/19/96 01/19/96 SAG
Terms and Conditions on Reverse Side
I 06 VANTAGE POINT DRIVE
CAYCE, SOUTH CAROLINA 29033
SC DHEC No. 32010
Client:
Attention:
SHEALY Lab No, 83005N
Description: Field Blank
Date Received: 01/17/96
Date Reported: 0:!22/96
Parameters
SHEALY ENVIRONMENTAL SERVICES, INC. I
Scientists and Consultants
CERTIFICATE OF ANALYSIS
HOECHST CELANESE-SHELBY PLANT P.O. Box 87
Shelby, NC 28151-0087
Kathryn Frank
Method Result Units PQL
[phone]
FAX [phone]
I
NC DEHNR No. 329 I
Coll. Date: 01/16/96
Coll. Time: 1500
QA/QC Officer "l'Y'&fc:'.
V,P. Analytical /11~
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Date Date I
Prepared Analyzed Anal. -------------
ethylene glycol 8015A ND mg/1
Terms and Conditions on Reverse Side
6.50 01/19/96 01/19/96 SAG
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I QUALITY CONTROL
DATA
I TCLP Metals
I Methods
I 1311/6010A
1311/7470A
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INSTIUJMENT QC V AUDATION SUMMARY
FOR EPA METIKJD 6010A
For Samples: lab ID It S5°c'frJ
lab ID# $31 bO
-JabID# __ _
labID# __ _
Jab ID#
CRITERIA
lablD# __ _
lablD# __ _
labID# __ _
labID# __ _
lab ID#
labID# __ _
labID# __ _
labID# __ _
lab ID# labTD# __ _
l).,.J-.,_
P/F mw.IBNTS
( 4'1."'l ''12€
INITIAL CALIBRATION: Date of calibration: , I 21.c I 'l "
AJJ suu,dsnls and solntiom pitj)ih:,:J/lllitiw:I within method p required holding ti.ma
Oil 5irl run i,_ediately after caiilnlioo .,ill> val-wilt.ill
5% of lrue value p
lnterrerenee chock scandJard analy,.ed ii. die beginning ll!ld ~ie
end of the nm (oc every 8 hr-whicht:va: is more frequent) with p resulis within mediod required oonl!Ql limiis
Intr:rfereocc cb,ck s,imple lllllllyz<d lit Ille beguwung and dw: rod
of the ru11 (or ~very 8 hr-..,hidlevais mac frequent) wilh p
resu!ci ;vitmli mctlm reqli.,-00 co.;;mJ li.i'iit!
S<,cood"""""" inirial calloratioo vwficotion and initiRI
calibration hlani< Slllly,ed wnh rcsum within medlod reQuired p
control Lim.its
CONTP.1/UING CALIBRATION
.-\ rontinuing C3!ibralion verifu:3tica "'3ndam and cootinuing
::.ilillro..tion bl;:cl:c ::nal1..ed c·=; lO =ip!e,: 3'Jd ~ ~'ie e::d cf p the aruo.lytical run '"i.th re,nJIS within rnemc.d required control
limits
SAMPLE CRITERIA
Anaiyw:i within linear !3Ilge of :he cur,c p
I hereby certify that all the above information is correct to the best of my knowledge. _.;.JI out--of-
comm! rrx:~'5un:mcnts relating to the me.thcd requirro =q-itaoce crircria trnvr, been dcx:urrenre.:l in
the above table. along with possible effects on the sample analytical data. ·
QA Officer Signarure: '-'f~ ~L,,_,c-c>--::-:{L
INS'TRUMENT QC VALIDATION SUMMARY FOR EPA ME'JHOO 7470/7471
For Samples: lab ID# i'3co'JN
lab ID# <oc, i60 ,,,lab ID # __ _
iabID# __ _
labID#· __ _ lab ID# __ _ labID#· __ _ labJD#, __ _
· lab ID#· __ _ labID#-__ _ labID# __ _ lab ID# __ _
'l)qf-C ei:n.q,1'1
CRlTERIA P/F COMMENTS I
INITIAL CALIBRATION:l&vrw:4 cal blank aod :i Dare of calibration: , I 11 ,a I•
!ca,t 5 <'..and3nl,: with r > 0.995) ):)
AU Slandanls and !clutions ~ "11hin med1od p required holding times
Second source inilw calibruion verification and initial p calibralioo bl.!mk run and in conlrol
CONTINUING CALIBRATION
A continaing calibrnrion wrificacion Slandard and continuing
calibration blank analyttd in ca,11'01 ewry 10 samples and 11 p the end of lhe analytical run
SAMPLE CRITERIA
l. ,\nolyzod w'.:run v.:rlc'-g ""'SI' cf mo cllrV1!( <'tigt..--s: p ~
2. Watet and soil samples no< run under !be .mn,, Cm"l'C
l ·n=tiy certify thal all the at,o,,e mform.ation is correct to the best of my knowledge. All om-Qf-coorrol measurements relating to the metho:i requiml accepuna: criu:ria have been documented in the above table along with possible effects en the sample illlalytical data.
QA Officer Signature: ·~ D~
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Client:
Project Name:
Attention:
HOECHST CELANESE
P.O. Box 87
Shelby, NC 28151-0087
Hoechst Celanese -Shelby Plant
l\ils. Kathryn Frank
Shealy Lab No: TCLP Blank digested 01/24/96 QA/QC Officer .rre:.:,
VP Analytical f/1. tJ---/'
METALS
BLANK RES UL TS FOR BATCH
Date analyzed: 01/26/96
Date digested: 01/24/96
COMPOUND RESULT POL (mg/I)
Arsenic ND 0.050
Barium 0.009 0.005
Cadmium ND 0.010
Chromium ND 0.010
Lead ND 0.020
Selenium ND 0.050
Silver ND 0.020
Client:
Project Name:
Attention:
HOECHST CELANESE
P.O. Box 87
Shelby, NC 28151-0087
Hoechst Celanese -Shelby Plant
Ms. Kathryn Frank
Shealy Lab No: 83160 TCLP Spike QA/QC Officer ::fhRC
VP Analytical fll ir/
METALS
Date analyzed: 01/26/96
TCLP SPIKE RESULTS FOR BATCH Date digested: 01/24/96
COMPOUND % RECOVERY
Arsenic 104
Barium 103
Cadmium 97.0
Chromium 97.0
Lead 103
Selenium 103
Silver 64.0
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Client:
Project Name:
Attention:
HOECHST CELANESE
P.O. Box 87
Shelby, NC 28151-0087
Hoechst Celanese -Shelby Plant
Ms. Kathryn Frank
Shealy Lab No: 83004N TCLP Spike QA/QC Officer ::YYJ&
VP Analytical mir-J
METALS
Date analyzed: 01/26/96
TCLP SPIKE RESULTS FOR BATCH Date digested: 01/24/96
COMPOUND % RECOVERY
Arsenic 95.0
Barium 94.0
Cadmium 87.0
Chromium 89.0
Lead 91.0
Selenium 98.0
Silver 90.0
Client: HOECHST CELANESE
P.O. Box 87
Shelby, NC 28151-0087
Project Name: Hoechst Celanese -Shelby Plant
Attention: Ms. Kathryn Frank
Date Analyzed: 01/31/96 QA/QC Officer -'n6C
Date Digested: 01/30/96 VP Analytical f1 ,,,.,_,...---
TCLP MERCURY
Comoound % Recoverv
Shealv Lab No.: 83160 MS
Mercury 96.0
Comoound % Recoverv
Shealy Lab No.: 83004N MS
Mercury 94.0
L b a oratory C ontro IS amo e
Comoound % Recoverv
Mercury 99.0
TCLP Blank dioested 01/30/96 ·-
Comoound Result POL (me/I)
Mercurv ND 0.001
ND= Not detected
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I QUALITY CONTROL
DATA
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TCLP Volatiles
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I Method 1311/8260A
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INSTitUMENT QC VALIDATION SUMMARY
FOR EPA ME1HOD 8260A
For Samples: lab ID #8 30dft\!' lablD# __ _ labID#-__ _
labID# __ _ labID# __ _ labID#-__ _
labID# __ _ lab ID# ---labIDlt __ _
labID# __ _ IabID# __ _ labID# __ _
CRITERIA P/F COMMENTS
INITIAL CALIBRA TION:(a 1qa s suu will>,-at Date of calibruion: I l,,1p(,
croeaMDL) p
All !l81ldarm and 50iution., ~ ,.,.i,;,, mcdlod p required boldiftg times
BFB Tune Oileria(lable 3) r
SPCCs -criteria me1: in section 7.4.3.1 in method 82(,l)A p
%XSD tor all analytes < 15%(usc avg.~ RF furcalc.) p
%RSD for all anal~ > 15%{cuulall:: C3I curve wilh r >-0.995) i0 A r~o,qCj
CCC, ave RFs %RSD < 30 r'
DAILY OR CONTINUING CALIBRATION Date analyzed: I h,/q(,
(begiming r:J each day ande.....-y 12 hr)
BFB 1\:a,e Crilm:,(11ble 3) p =~)ofo'7'io /;r,<15'
Midpoint calibration Sid run IO verity.
1. SPCC, -criteria met in xctioo 7.4.3. l m meihod 81J50A
2. CCC, %Drift < 20 ? 3. r,_,,,.i Standards R r widrin 30 sec of last ch<cl< !lld(or cal)
4. Ek..7' area for JSs -50% 10 +100% from la.st cbeck(or cal)
5. Surrogate% n:c Wllhin memo<! control limits
SA.\IPLE CRITERIA
I. '>let criteria in stcps 3 • 5 und<r dailykontinoing calibrnlioo ? 2. Run within 12hr of last in~trol tune
3. Analyzed widlin war1dng range of the curve( <:highest Sid)
I hereby certify that all the above information is correct to the best of my knowledge. All out-of•
rontrOI meas=:ments ~laling IO the method requim:1 a.cceptance criteria have been documented in
the above table along with possible efft,;:ts on the sample analytical data.
Name:
INSTIUJMENT QC VALIDATION SUMMARY
FOR EPA METHOD 8260A
For Samples: lab ID # '3 3 I b0
labID# __ _
lab!D# __ _
lab ID# ---
labID#· __ _
labID#. __ _
lab ID# ·---labID#. __ _
lab ID# __ _
labID#. __ _
labID# __ _
labID# __ _
CRITERIA P/F COMME.VI'S
INITIAL CALIBRA TION!(lll l£a>t S "'1s wi1b oae a! -p Date of calibration: I IN J:,G,
ctlle2rMDL)
All 3'alldard3 and :,oJution3 ~ within mcd>od p Jl!qum!d bolding time&
BFB Tune Crileria(lable 3) p
SPCC, -crilt7ia met in section 7.4J.1 in mednl 8260A p
%RSD liJr all. analytes < l5%(U9C avg. relative RF fur calc.) p
%RSD foe all malytes:, 15%{C31culart: c3I curve wilh r >0.995) N It r > D ,q'j
CCCs ave RFs %RSD < 30 p
DAILY OR CONTINUING CALIBRATION Dale analyred: I /z."1 lrC
(begiming cl each day and e-r 12 hr)
BFB Tin, Crileria(tallle 3) p Time(s) of
o1~'J... runing:
Midpoint calilnli{)n Sid run IO 'lfflfy;
l. SPCC, -criteria met in xction 7 .4.3. l -, method 82tiOA
2. CCC. %Drift < 20 p 3. rnttmal Stlllldacds RT within 30 ,ie,:: of l&!t check sul(orcal)
4. Ek..7' """'-for lSs •50% IO+!~ frcm last cbeck(or cal)
5. Surrogmt: % m: within rrw::thod control limits
SAMPLE CRITERJA
L ¼c1 cril<ria in Steps 3 . 5 under daily,,::ontinning calibratioo r 2. Run within 12hr of last in-aJ11trol tune
3. Analyzed within wcrlci.og rang< of the curve( <higoon .ul)
I hereby certify that all the above infonnation is coattt to the best of my knowledge. All out-of•
contr0l measurements relating lo the method required aca:ptance criteria have been documented in
the above t.1ble along with possible effectS Oil the sample analytical data.
Name:
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Analyst :_~D_I-J_._P~/~f!..~eJ)~--C-C/MS 1:D: ,.,,,J 3 Date/Time: l/i..>faG IY,J -~-.1-"'~--'----'---l...-
Daily scd ID: __ w_'1.._1_1~_),,..__ Initial Cal. Dace '-~•~i~, '{_f~'i_.t,~--Heaced pu:::-ge e/N) :
SYSTEM PSR?ORMANCE C-IBC< COMPOUNDS (SPCCs) :
I CCMFOu'ND
I
RF '.,<J · 1 (daily)
MIN RF
I Chlorcmechane I o. {03 0.100 ----------------------------------------------------i -=~ ==:=:~=::::=~~,=---__ ---i __ 0, 3 :l-1 _____ -~~ =~~ _ --_ I B:::-c:moform O, 'f7,) I > 0. 100 ----------------------------------------------------. I l,1,2,2-Tet:-ac:'~lcrcechane I
I C:t--~lor2Cenzer:e v,911
I C)NC. (t.:c;/L)
(C:a.:.2.y)
0.300
0.300
I MAX %-D
======================================---==--==--===--==----=--
/ C,' .CC'~·-; ~~~cc'-c~c l/(0 '{. (:, 20 .0 ---------------------------------------------------------------
i_ ~~'=:::~:~ ______________ i _____ 'i_',~ J ______ i __ }c J ____ i __ ~~ ~ ~ ____ i
i _ ~ ~ = =: ==~= ===~==~~~-= -----i _ ----~( { ------i --{J ~ i_ _ --i _ -= ~ ~ ~ ----i I TcL:e:-,e I ',/. ~ I 5. c) 20. 0 ---------------------------------------------------------------~. ~=~:~·=-~:~'=:~': _ ---------------~~--'='----_ i __ t,_i__ ------~~: ~ -----'. _ ,~-=~-~-=-~~-====~:---------------~-j~,_/_ -------j~ ~ ~ -

-
--

-

-
~~ ~ ~ -

-
--

-
Client:
Project Name:
Attention:
HOECHST CELANESE
P.O. Box 87
Shelby, NC 28151-0087
Hoechst Celanese -Shelby Plant
Ms. Kathryn Frank
Shealy Lab No: TCLP Blank 01/29/96
VOLATILES
COMPOUND RESULT PQL
(me:/1)
benzene ND 0.005
carbon tetrachloride ND 0.005
chlorobenzene ND 0.005
1,4-dichlorobenzene. ND 0.005
1,2-dichloroethane ND 0.005
1, 1-dichloroethene ND 0.005
2-butanone ND 0.005
tetrachloroethene ND 0.005
trichloroethene ND 0.005
vinvl chloride ND 0.010
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QA/QC Officer toff.,.,
VP Analytical tl1~ I
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Client:
Project Name:
Attention:
HOECHST CELANESE
P.O. Box 87
Shelby, NC 28151-0087
Hoechst Celanese -Shelby Plant
Ms. Kathryn Frank
Shealy Lab No: 83004N TCLP MS
VOLATILES
TCLP MA TRIX SPIKE
COMPOUND RECOVERY
benzene 96.1
carbon tetrachloride 92.0
chlorobenzene 91.0
1,4-dichlorobenzene 93.1
1,2-<lichloroethane 94.9
l, 1-<lichloroethene 90.0
2-butanone 88.1
tetrachloroethene 88.7
trichloroethene 93.5
vinvl chloride 50.7
Q Al QC Officer ---f'nOC...
VP Analytical lh~
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I QUALITY CONTROL
DATA
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I TCLP Semi-Volatiles
I Method 1311/8270B
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For Samples:
INSTRUMENT QC VALIDATION SUMMARY
FOR EPA MEIBOD 82708
lab rn # 130°y,0
labID# 'l,1(,0
lablD# __ _
CRITERIA
labID# __ _
labID# __ _
lab!D# __ _
lab ID# ---labID# lablDfl __ _
P/F COMMENTS
1NITIAL CALIBRATION:(111 Jea..t 5 .eds wilh ooc a1 p Dale of calibration: 0 I I "'ff 'I
crlle3:"MDL)
All 5laJJdmrls and sollltions prcpar,:dlutili=l wimin nxmcxl f mquin:d balding times
DFTPP Tune Criteria(table 3) t
DDT drg1+lo•••• <20% tJA-
Ben%idine and penlaclljGtµ~ !¥'C:9Cfll al namal l'l'SjXl0'.11'$ NA-with oo p<3k tailing visiblc(chromalllgraphy cha:t S4d)
Compcmcrus of in1£re.,1 with RTs of 0.80-UO relative to one i' of the Internal SlllOdards
SPCCs -minimum avg. RFs = 0.05 e
%.RSD fee :ll. er1.e.ly1..=s-< t5%(use lvg.. r-...1.?tive RF for ~c.) p
'¼RSD for an analytes > I 5%(wcub1e cal curve 111i1h r >-0.995} /J !+-
CCCs ave RF, '¼RSD < 30% p
DAILY OR CONTINUING CALIBRATION
(beginning oi each day and every 12 hr) p Date analyzed; I / z.._q /qt,.
,
DFTI'P Tune Criteria(Lllble 3) p Tirne(s) of I j}, 'f I ·1 .,, ti "7 :;:..
1/_iq['JiE_ It/ l.£.. tuning:
1'fidpoon calibration std ruo to verify:
I. SPCCs -mirummn lvg. RF, = 0.05 p
2. CCC! %Drift in concallratiun < 20% pp 3. lntcrnal Standards RT within 30 sec oi wt check Sld(ot Cll)
4. ElCP area for !Ss -50% to-,. 100% from last chect(or cal) p
5. Surrogate '¼ rec ·,rithin method :omrol limii, F Ha.h1x 1 n ln/t.Kn u.,J
SAMPLE CRITERIA
l. Met criteria in steps 3 -5 under daily/cootinuing calibn.tion p
2. Run within 12hr of las< in-control mne p
3. Analyud wilh,n worl;ing r.1'1ge of the curve( <llighesr std) ?
I hereby certify that all the above information is correct to the best of my knowledge. All out-of-
conrrol rneasuremenis relating to the method n:quired accepcmce criteria have been documented in
the above table along with possible effects on the sample analytical data.
Name: /Jee /JJ11u 7 Date: J /;& I ti I/
(print) '
:'-/rune:._~/)~(~{ __,_/]-'--'-1/1t1=-.fl-'-----
(sign) • R r' 1 J
QA Officer Signalllre: -f'}1A).}2.._ 117-;{.,1.,~
~
DATA VALIDATION CHECKLIST (SAMPLES)
Paramela Group: __ SYOA __ Client Name: Metllod Re.fe=cc: __ 82700 __ Project Number: Prescrvutive: __ ICE __ _ Site Name:
Prepared by: N/ A a noupplicable
Dale: 7 = mmin~ data
LAB ID It f J., l',l',L),. f3/I, 0 COMMENTS DATA
OUAL
HOLDING TIME
(....,.:7<ioy,IO~~ 40 dll,·-· to ) p p
HCUJING TIME
( ,.,;J ~ 14 ... ., """" ~J .. -:g~\
!NlTIALCAL p e (D1'TPP ..... .,.ta1,.J)
(DOT DliG. "'°"')
!5SM!s..-.bl,.....!,IDLI <l!i't,l!SO r~ ,ii ....i,....
lO ~ Rfl to alal1r.c i;oac) ~is,. mo.A doca! ~
(U. (6) RT O.l-1.20)
(-:t. IUl/2)
(Sl'CC • .JI> 0.05)
ICCC_. RP '11,RSl><lCl
DAILY ,CONT. CAL r p _,_:, Ma21l IN ,._a, f!X' ........ gygp.y 11 HOHl:S
l.RFBt1:1m:.JCC:sb.:!
2.. ~ cat no. dlca:
• • Rf>O.CIS -ax~,~
· LS. n-e;.tT-,,/JOsec of
lase CV <'JI" i.oiuaJ cal m.idp.
-EIC:P f~ LS.(-l~ w
•l~...!._~,~CV .s l,11,m:~!,
METI!OD BLANX I) p
LCS(FuJI List/ /\IA-i..JA-n •.. - -[r«Or'l!m.tnJ~l.eo)
MS/SAMPLE D_llf: tJe>v
v;..,, ••'"' -I
(:cconnncnd able }VII MS l}flUJ
TRIP/FIELD BLANK Ntr tJA-
EQUIP BLANK NA NA-
DEIBCTION L!MJT r p
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Client:
Project Name:
Attention:
HOECHST CELANESE
P.O. Box 87
Shelby, NC 28151-0087
Hoechst Celanese -Shelby Plant
Ms. Kathryn Frank
Shealy Lab No: TCLP Blank 01/29/96
SEMI-VOLATILES
COMPOUND RESULT POL /ms,/])
4-methvlohenol ND 0.020
2-methvlohenol ND 0.010
2. 4-<linitrotoluene ND 0.010
hexachlorobenzene ND 0.010
hexachlorobutad iene ND 0.010
hexachloroethane ND 0.010
nitrobenzene ND 0.010
nentachloronhenol ND. 0.020
nvridine ND 0.010
2 4.5-trichloronhenol ND 0.010
2, 4 .6-trichloroohenol ND 0.010
QA/QC Officer 'i'Y\fC
VP Analytical /JI fr,,./
Client:
Project Name:
Attention:
HOECHST CELANESE
P.O. Box 87
Shelby, NC 28151-0087
Hoechst Celanese -Shelby Plant
Ms. Kathryn Frank
Shealy Lab No: 83004N TCLP MS 01/29/96
SEMI-VOLATILES
COMPOUND RECOVERY
4-methvlohenol 59.1
2-methvlohenol 46.7
2. 4-<l initrotoluene 43.7
hexachlorbbenzene 38.0
hexachlorobutadiene 35.0
hexachloroethane 56.2
nitrobenzene 53.0
oentachloroohenol 45.4
nuridine I 7.3
2. 4,5-trichloroohenol 52.0
2, 4,6-trichloronhenol 46.3
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QA/QC Officer :1Y\9,f._,, I
VP Analytical al~ ' I
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Analyst: DNP GC/M.S ID: ill Date/Time: //zq/CJu ;,cl_ -----------'+,--=-'--1,-=---'-'---' ----
Daily std ID/Cone (ug/ml) : __ w:_:· _;_!~5,::,_{;"'-(;-1..d4----""'l)"'-i[J_1,,!C,,:(./4JtL!.m'-'-!-I _
SYSTEM PERFORMANCE C-IBCK COMPOUNDS (SPCCs):
COMPOUND RF
(daily)
Initial Cal,
MIN RRF
=--==---==---==-----===-====-===-=====-===--==-----------------I ).1 I_ N-Nitroso-di-n-propylamine _____________ /, O 7 }._ __ l ___ ~ ~ ~=~ ___ _
,If) I _Hexachlorocyelopentadiene _______________ o },J,1 _I ___ ~~~=~----1 {J q I _ 2, 4 -Dini trophenol ______________________ -~ ~~ q f __ l ___ ~ ~ ~=~ ___ _
I J J I _ 4 -Ni crophenol __________________________ () ,,,; {J 7 ______ ~ ~ ~: ~ ___ _
I
I --------------------====-====-===-====---------=================
::.ead Cone.
(ug/ml) %D
I lj?/101 tfl I --------------------=========-===-===-,,,,~--------================= & ?' l_Ace~,a;ir,chec:e ________________ l __ fjJi f_ ___ l __ Lf_X ___ l __ :~~~----l
JJ{;,f I /3.i, I 20.0 ----------------------------------------------------------------I
I ;./:) ~ -~=~~~~~~~~~:'~~~=~~= ~ -------_ l _ --.J}i_ -Cj ---l _ ~ ;},_ f_ __ l _ -= ~ ~ ~ ---_ l
,;,,;,11-,-Nicrcscci;ir.e!'.ylamine I --ti/ I /71 </ I 20.0 I 1/ ----------------------------------------------------------------
/(1 / :,4-~ic~la~=~enze~e
' -
1~31 Di-:c.-occyl ;ir,atr,alac;c I tpi,1 I ;q,,f I 20,0 I
I ; c;cI: ~~,~~~~~~~~~~::::: ::: ::: :: ::: I:: :ic~:(::: I: :1.: X:: :I::~~~~:::: I 11 ~ & ~ _ ~=~,=~ ~ ~ ~ ~"==~= ______________ l, __ JJ.~ ___ l __ J;., _'-f ___ l __ : ~ ~ ~ ____ l
;_j{jl _ 4-Chloro-3-methyl;ihenol _____ I __ ij?J, 1 ___ I __ 7,,+ ___ I __ 20,0 ____ I
I 3 & ~ _: ~ ~ =:==~=~==~~,=~~~ __________ l __ -~ t ___ l __ I}~-~ ___ l _ -=~ ~ ~ ____ l
1J-l _: =~===~~~=~~=-_________________ fI'L 9 ______ q, ! _____ -=~~~---__ I :_.., j Phe!1ol :f(I 1 7 / 7 J , 0 · V 20,0
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Date: 1/z-<1/91,
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I QUALITY CONTROL
DATA I
I TCLP Pesticides
I Method 1311/8080A
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r.
INSTII.UMENT QC VALIDATION SUMMARY
FOR EPA ME1HOO 8080
For Samples: lab ID# 1:3co'j t,l
lab ID# 1°'>1 ho
...,.l.wID# __ _
lab!D# __ _
CRITERIA
lab ID# __ _
lab ID# __ _
lab ID#. __ _
lab ID#.~--
J]'lj1TIAL CALIBRATION:(m last 5 std! wid! one al
O< near MDL and use of dual column for ccnfirmation}
All SIJllJdmh and solurims pn:pm:dlutiliud wi11m llldhod
reqwed oolding times
fa ternal ruridard calculation u;,ed 11/illl r ::,. OS'l5
DDT and Endrin degradation < ~
DAILY OR CONTINUING CALIBRATION
(begirm,g of oach day and every 12 hr)
Midpoim calitrarion std rui to verify:
l. Run midl)oint cai Sid to check all analytes wirilin 15% oi
true w.Jue
2. DDi and Endrvt degradation < 20%
3. Surrogaa, 9{, rec witltm lab ;;e,,eraled control Jimirs
C' J. ,1nl' r." r1-...-T"T:'0 I~ •.:,"-.rl'lrLC. \_.ftl I C.f\.tt,,,
I' Bracketed by in-mntrol CVs
2. S=1CS in cootrol
• 3. Analyzed will\Jn wcrblg range o! lbe cu;,:( <highelt ,Id)
lab!D# __ _
lablD#. __ _
lab!D# __ _
labID# __ _
P/F COMMENTS
Darr of calibration: 1l,1-2.11K!L. p I
p
p '/':::,0,'(1
hi /A-I I
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p ! Date an.a.lyzed: J(:z.)/"/C
p
~ /P.. I p
'
p
2 p
I hereby cenify that oll the alxwc inforrruuion is com:ct to the t.!st cf my icnowletlge. All om-of-
contro l measurement~ rel acing to the method required acceptance criteria have been documc nred in
the aoove table along '-;th possible eff= on the sample analytical data.
QA Offker Signature:
Client:
Project Name:
Attention:
HOECHST CELANESE
P.O. Box 87
Shelby, NC 28151-0087
Hoechst Celanese -Shelby Plant
Ms. Kathryn Frank
Shealy Lab No: TCLP Blank 01/25/96 QA/QC Officer --4-Y\f,C.
VP Analytical A~
COMPOUND
~amma-BHC (lindane)
chlordane
endrin
heotachlor
heotachlor eooxide
methox vchlor
toxaohene
PESTICIDES :METHOD 8080A
RESULT
ND
ND
ND
ND
ND
ND
ND
Date analyzed: 01/25/96
Date extracted: 01/24/96
POL (mg/])
0.001
0.01
0.001
0.001
0.001
0.004
0. 10
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Client:
Project Name:
Attention:
HOECHST CELANESE
P.O. Box 87
Shelby, NC 281.Sl-0087
Hoechst Celanese -Shelby Plant
Ms. Kathryn Frank
Shealy Lab No: TCLP Blank 01/31/96 QA/QC Officer -t'Y'\8C-
VP Analytical M ,:1-t--/
COMPOUND
nmma-BHC /lindane)
chlordane
endrin
hentachlor
heotachlor eooxide
methoxvchlor
toxaohene
PESTICIDES METHOD 8080A
RESULT
ND
ND
ND
ND
ND
ND
ND
Date analyzed: 01/31/96
Date extracted: 01/31/96
POL (m~/1)
0.001
0.01
0.001
0.001
0.001
0.004
0.10
Client:
Project Name:
Attention:
HOECHST CELANESE
P.O. Box 87
Shelby, NC 28151-0087
Hoechst Celanese -Shelby Plant
Ms. Kathryn Frank
Shealy Lab No: 83004N TCLP MS QA/QC Officer :hJoc
VP Analytical ,tr1/rl---"'
PESTICIDES METHOD 8080A
MA TRIX SPIKE FOR TCLP BATCH
Date analyzed: 01/31/96
Date extracted: 01/31/96
Comoound ' % Recoverv
MS
eamma-BHC (1indane) 70.8
chlordane 105.3
endrin 85.6
heotachlor 76.6
hentachlor epoxide 84.8
methoxvchlor 98.0
toxanhene 101.0
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I 's"!ETc:?-: To{ evy&~ OATS: i p-4' l,f ( .',NAL YST: ~t2~t ____ _ IC #: I DETSCTCR: ·r;;.,co :jj-J._ COL #: __..,K:_,__._(~r .... )_o....!.(...,_) ____ _
STD/C'.JNC. I I I I I I •--~~~~::2~ ____ lL O ------! _____ J_J) _____ 1 __ . _3 ___ CJ ______ , ____ f, 0 _____ 1 _ s. 0 -------~
I I I I I I ,....,,...., I .~ ... :i::-~ I ~Q::'."I . I ;J,:::=-~ I ~=-;.. I :\.: .... ;::-"I I 1-:~----:-------· -·-· ___________ · -·-"' ___________ ·-·-· ______ ' ___ · --· ___________ · "-: _____ .:. __ 11.2~_!.f I ____ Lb 11.C' ___ 1 ___ JJ. ~JJ-___ , ----ts-1>.Yc[ __ 1 --'l r J-! J. ___ 1 __ :t}-df ] _____ ~
[i&.<c':'.~-~----2:J-J)o ----' ____ fJ:?}Sf. __ 1 ____ J_C.:?f..3 ___ 1 ---ff 4-~ L ___ I __ Lo,ig~~----~
r+ilb.::r,_~---..2..C, & 7 (, ___ 1 ____ ~rd-!L __ ' ____ J_7>..f ~I ___ 1 ---LJ-.k.b 6~ __ 1 __ r ~ 1 r 11 ____ ~
I I I I I I ---------------------------------------------------------------------------------
I I I I I I 1----------------------------------------------------------------------------------
! I I I i I -----------------------------------------------------------------------------------
I I I I I I I ·----------------------------------------------------------------------------------
1 i : I I I ·-------------------------------------------------------------------------------1 ________ ~_ I . I I I _ _ __ I
I I I I I .,---------------------------------------------------------------------------------' I i I I I ------------------------------------------------------------------------------------
1 I I I I I 1----------------------------------------------------------------------------------
; I ! , I I
fa:. a::-ea i (;C, q(, (~ o + 1J )_ c, y.,-c .,I. : ; c s.;f 7 : J_ i 6 I )j : ----------------------------------. -----------------------------------------------
("= ; [c~c~G : ;CJ.lt) i L0 /r>Y-i 16>J-f,3 i b])J.;-;l : --------------------------------------------,-------------------------------------
' .. ,.,,-:_GC: ··-, -~~•-+r_/ _},_) .....,• f1----STJ. •JE:0;':.:.".':CN
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HETER: ___,,e,"'-'l....,1--'-irr~~----C.-----DATE '--''+/-"'-;i-'-4~/_1_6 ____ ANALYST: -~R=t ____ _
;c #: __ -'--/ _____ DETECTCR: _ _:;E.=.c(:.../).,__:#_J.. ___ COL #: ps-(J):g izot)
TD/CONC. I
(ug/ml)I O,r O.J. D,S-O.f i,o -----------------------------------------------------------------------------------
AREA ---------------------------------------------------------------------------------r-" C4 S-__ 1 ___ 1_ 4 <j,~ _____ I ____ 4 S ( o ___ l ____ Jlfll-----I ___ J_ o)._f J ___ 1 ---d.§EJ _____ ~
-f~JJ:.L __ 1 ____ 4 ~0-l ____ 1 ----1 ~1 &t ___ ' ____ ~1b?7 ____ , ---lfl~i)h ___ 1 __ J{ 7s J _____ ~
_, i,_~?J-l __ 1 ----Lo y;i----1
_____ 1usl __ 1 ____ & {2?-8'. ___ 1
__ J_L.-3-;;i_f_o ___ 1
__ l°;,J-!,...I J ----~
_L~-P--1 ____ I lh ~----I ----4 JO sv __ I _____ ; L cos.,). --I __ ..1_-f£..µr _ -I __ _,23;.:: n _____ ~
I r I I I I i
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-------i ----~ b )if-S°.0 --I ____ / s,£-0 / ---'. ---,)_ II~ ri ----I ___ J__j_o5 )I--I __ 4 '{-J cf 5.'j---i :: ______ l ____ ~~-s:t~~---l ___ }))_:=~--~---~L2~]}_~ ___ l __ /j_]f~Jj ____ ~ __ 1_t~±!_t ___ ~
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I ."-i"!ET'::?.: ------1J!-"'J'--''{~~-1J.~-'-'h_e::c.:..::fu,:.,......_ ___ DAT'::: --''-1-!/ &.cc±..l.---1,.//:...tu::x· ____ .~.NAL YST: --'-(<_,__t::__ ____ _ / I re #: __ ...J._ _____ DETECTOR:--l..h«:::J;.c.J{.Q_#'"'--'--.I ___ ·COL#: 7.£: (QB6vg)
"TD/CCNC. I I I · I I I ( (ug/ml)I /,0 I J.o I ~,-0 I q,,o I {'",C / ------------------------------------------------------------------------------------
1 I I I I I l-:~ ______ 1 ____ ·"'--"·-==-~------'----A.R.::.~ ______ 1 ____ ·"'-~EA ______ 1 ___ A.REA ______ 1 ____ ·""-~E:..~-----~
.J_ti, _c_':}~ -~----L -2Jj 'f ____ , ___ ) .. 2Nlf ___ , ___ !1:._r,s-s-_____ , __ .1:i. 0 r(!_{' ___ , ___ b 74,") f ---~ ,_~j_, ~✓ I ____ LJ o~ c ---I -

-
").D~~ }J ----I ---q{LG-t ----I ___ bJ:_(_i V ---I ---b _JS){'" ---~ ·-~¾-~lft :----11~~~1~ ---:. ___ {%;:----:---~~~':----:--]_~ol;i --:--~~~~ ---~ ______________________________ j , ______________ fl __________ 1_7cl--------------------, __ 2,4., fsJ-I-----I I ~ ,.;{;' _, ----l.. +(SJ-__ , __d,J q._5'/ ____ I---~/ Jr:,----' ---~ C& f.S --~ I I . I I I I ------------------------------------------------------------------------------------
l I I I I I I ----------------------------------------------------------------------------------
1 I I I I I
I I i I I I l ----------------------------------------------------------------------------------
1 i i i I I
i I : l i I 1----------------------------------------------------------------------------------
: \ l / ! !
I"":. cc:-~\ 71&l I : 1,-i,1.ri-~ .1JS7Yc 11 3:nfs-S-: )~'f-,i.)i : --------------------------------------------------~--------------------------------1"" : 1 Ir> I : l {;,s)5;--: 1 s J 3,0 : S,J Ly') : 7.)J-'>-r : --------------------------------------------------------------~1-------------------
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.:::.. :;-:,? _:.._G 2 ~-=
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I c:::r.c c: s ::::: .
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I >J-!ET:3: _T.._o_:(_~f-f_0z_.,..,.__ ____ DAT!::: _-'+if-'--~-· ~i_f ( ____ ANALYST: ~12......._:c.: _____ _
::;c #: ___ ~/ _____ DET::cToR, __ 'G.-_C~D_=tt-_J.-__ car. #:---->-aK:.._._(-'-r-'-1_0 -'-(..,_) _____ •
STD/CONC. I I I . I I I I ___ ( uq/ml) I ____ LL o _______ I _____ cl.· u _____ I ____ J_~ z::; _____ I ___ f, o _____ I_ S ~-------~
I I RT _;_~:=·:;, l _.;..;.::.;. -~':;_E:A AREA .:;....c.~.; / I
__ J_ 1, /~ + 1 ____ L0 ;j_::;, ---1 ___ 11 ~JJ----' ____ J:t-'>Y§ -' ----; f+1J.----1 __ 2J_ ~]~~~~~~ I _l& c".;70_, ---~J.!,)c ----I ---~ 7}J<f: ---I ____ -i_oor.-3 ---I ---ff 'tel L ___ I _Lo~~~---~
_ _µ,y)"(, _ 1 ---j__~ & 7 b, ---I ____ s:wL ___ I ____ J 3 r~ I ___ 1 ---LJ-lb cj -I --r ~ I L~l----~ I I I I I I -------------------------------------------------------------------------------
-----------------------------------------------------------------------------------
-----------------------------------------------------------------------------------
-----------------------------------------------------------------------------------
-------------------------------------------------------------------------------
:=.:. s.:-e=.'. l~GC?~ (~.:;'+1J J..D/fC). ~os""-17 : ~ ;£1,Jf ·--------------------------------------------~-----------------------------------
;_:-i l"~c:~6 i )CJ-4; i GJ'r;:;1 : 161;J..f,3: b:f)J-;-;l, : --------------------------------------------.-------------------------------------
r.;
_ _,,&'--ff-1_1_,.....;;,_,-+f--S,J. CE'iIX'.'IC,,i
Ccr.c CE Sc:::.
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I C.>.LI32 ... ",':'ICN C.iR1fS C.'.LC'0LlTIGNS
ITD/CONC. I
(ug/ml)I 0,( D.J. 0.) 0./r (o ----------------------------------------------------------------------------------I RT _.:._~-=-~ -~~.::.:; .¾,£A .,;,,?,EA A..~=-; ---------------------------------------------------------------------------------,-r~ ~:~ --:---1-:: G _____ :----~ ~ 1 ; ---:----~1~17 ----:---:
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__ L 1. fS.L-:----111-31----:----4 ~ C SV --: _____ i L coS.). __ :---L-f£.JK ·-: __ J 31-' .rJ _____ :
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I I 1~:=-:~;:~--------------~--------------~---------~----7-------------7-------------7
I ~ b 5'f-8',0 I I s,(;o I : -:2. (I~ ri i 3__&:cj: )t" ! ~ i{--J y 5,'j-I -t: : 3b>'ffC 1
1 ;'r']c0 _;-: Lf,-}).~1? --; -~7(;:,ff 44J-'{-5f ___ _ ------------------------------~----------------------------------------------• -,.-,,, ·c--r--· -~ ---
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-------------)
cor.c c: s::::.
STD.
:;c ;; ' I
3TD/CONC. I
(ug/ml) I 0,'
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------------------------------------------------
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__ 1 o . .1_ c r -i _____ LlfJ_.)_ ----i ____ 3-0{,).. ----I ____ .'5' i~ r -----I ---i 4'>]£ ----i ___ Lbf 5' i ----I I __ I;; 1~ 1 .I ____ ...s:i11 ____ 1 ____ JL 4--f 7 _____ 1 ____ 1 oc;7 ____ 1 __ .rs-bbb _____ 1 ___ &sS'l-t ---~
--Lµ1j __ ~ _____ :J.JJ'f--~--~-----.Ll.!~----~-----l-iJi ____ ~ ___ LW,1.] _____ ~--~orlJ ____ ~ I __ r4:,Llt6° 1 _____ $:b '/3 ___ 1 ____ I 8J.'}8-___ 1 ____ 4-{¥ ___ 1 ___ ffcb] _____ 1 ___ I I~(,~----~ __ lf,-rtb_~ _____ £Lo_i _____ ~----1-1ii::8:----~----1E-lll ____ ~ __ .1ii?..f: ____ ~ ___ JJ_q{ ____ ~
--I ,i..1JJ;, I ---), 05'------I _____ ') 'f-( a --

-
-
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-
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::~_::::l ____ ~~!-~1 ____ l ___ ~J_?J£ ___ l ____ j]~~~---l ___ i}J~~~0-___ : __ ~C}J >ti __ :
~: ______ : ---j + > {1~ ___ l __ i_±3)2~---~----}_:t~!-~~-~ __ lj_:~~-L_fj ___ : --Cf-Cd5 3 :f-___ :
c:::r.c o: s::::::.
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M -608 DAILY STANDARD VERF!CA T/ON
DATE: ,1:,,, 1c:0 ) f COLUMN: -ff:f£ 1 #-J"~TD#: Wt'I 7-r-).)-C.
ANALYST: Rt: STD#: wx1?-S-,),)-MUL Tl-LEV DA TE: r /.i < -c:t:4 l5L I ' PARAMETER I TRUE CONC /READ CONC I PERCENT D!FF I PRIMARY COLUMN
a!drin
a-BHC
b·BHC
d • BHC
!indane
ch!ordane
4,4' · ODD
4,4' · ODE
4,4' · DDT
die!drin
endosu!fan !
endosu!fan I/
endosu!fan su!fate
endrin
endrin a!dehyde
endrin ketone
I (ug/m!) I (ug/ml) I I
0.05
0.05
0.05
0.05
0.05
0.50
0.05
0.05
0.05
0.05
0.05
0.05
0.05
0.05
0.05
0.05
rJ-5tj
0
b,J-
1_08-1701 ~08-608
1_08-1701 / 08-608
1_08-1701 _L□B-608
1_08-1701 ~DB-608
j_DB-1701 / 08-608
L._,L'.'DB-1701 _L._O8-608
1_08-1701 /□8-608
I_ D B-1 701 _LO 8-608
1_08-1701 _LDB-608
1_08-1701 /DB-608
1_08-1701 ___L..O8-608
1_08-1701 ._.LDB-608
L._O8-1701 /"DB-BOS
L_DB-1701 _L_OB-608
L_OB-1701 _.,:::::_DB-608
L_DB-1701 _L_DB-608
_he_c_ta_c._h' __ or _____ o_.o_5 _____ c_"·-'·-~-G~7-~1.& lr::~· _____ o_s-_1_7_0_1_/_0_8-6_-_08
heptach!or epoxide I 0.05 ccs CS JJ· L._O8-1701 / DB-608
kepone 0.05 L_DB-1701 __ 08-608 ··--·········-······-·--····-·----········---··-···------------
1 C. ,µ,..-,f I it, J L_DB-1701 .....,.L'.:O8-608 -·-·-····················--······································t·······
toxaphene 3.00 I · I 1 1 ./DB-1701 __ 08-608 ----------'2~-).L. .. _ _.__I '-+f __ '--_____ _
methoxychlor I 0.20
PCB· 1016 I L._O8-1701 ,L-DB-608
PCB·1221 L_DB-1701 ...,.LD8-608 ----····--·-·-·····
PCB· 1232 __ f L_DB-1701 __.L.DB-608
PCB · 1242 .. ··-··· Q _ '> ~---1 .. C. /if)__ / ... / _ ff. ;). L._08-1701 _M-608
PCB· 1248 I I L._O8-1701 _L._O8-608 ---······················-····--·······--···-···----·---------
PCB -1254 L._O8-1701 ___,LDB-608
PCB· 1260
---·····-·······----------------------,---
L_.O8-1701 _L"os-so8
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I QUALITY CONTROL
DATA
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I TCLP Herbicides
I Method 1311/SlS0B
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INS1RUMENT QC VALIDATION SUMMAR y
FOR EPA METI-IOD 8150B
For S amp I es: lab ID # '{3oo'-{ rJ
lab ID# 'B 11,0
-:ablD# __ _
Lab.ID# __ _
CRITERIA
Jab ID It __ _
labID# __ _
lab ID I# __ _
Jab ID #---'--
lab ID# __ _
lab ID# __ _
Jab ID# __ _
lab ID# __ _
P/F COMMENTS
INITIAL CALIBRATJON:(at least 5 8'ds with one at f Date of calil:rntion-r h LI 'f I"
er tx= MDL 311d """of dual cowmn fer conf:rm:~.icn) I "
External standald calculation used Wlth r > 0.995 p 7o.9'1
'
DAILY OR CONTINUING CALIBRATION p Date analy=l: i/_U, (_9 (.,,
(beginning of ru, and evay l O samples)
Midpoint Qllilncioo sul ruo IO verify:
l. Ran midpoint cal ,Id to check all anillyte:; within l5% of p
true Vllloc
2. Surrogau % rec within tab genuaced cvntrvl \i.,tiits p
SAMPLE CRITERIA
l. Brncketed by in control CV s p
2. S ~ in COO[I'Q] ~ 3. Analy,cd wilhin woning range of :be cunt( <higl,cst ;Id)
l hereby certify that all the above information is correct to the best of my knowledge. All out-of-
control measurements relating to the method rr:quin:rl acceptance critoia have been documented in
the above table along with possible effects on the sample analytical data.
Client:
Project Name:
Attention:
HOECHST CELANESE
P.O. Box 87
Shelby, NC 28151-0087
Hoechst Celanese -Shelby Plant
Ms. Kathryn Frank
Shealy Lab No: TCLP Blank 01/26/96 QNQC Officer 1Y.G(..
VP Analytical t11tt------:' •
TCLP HERBICIDES METHOD 8150B
Date analyzed: 01/26/96
Date extracted: 01/24/96
COMPOUND RESULT POL (m11/I)
2,4-D ND 0. 10
2,4.5-TP ND 0. 10
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Client:
Project Name:
Attention:
HOECHST CELANESE
P.O. Box 87
Shelby, NC 28151-0087
Hoechst Celanese -Shelby Plant
Ms. Kathryn Frank
Shealy Lab No: TCLP Blank 02/01/96 QA/QC Officer ,l'Y)GC.
COMPOUND
2.4-D
2,4,5-TP
VP Analytical 111;t,.--" '
TCLP HERBICIDES METHOD 8150B
RESULT
ND
ND
Date analyzed: 02/01/96
Date extracted: 01/31/96
POL (mg/I)
0.10
0.10
Client:
Project Name:
Attention:
HOECHST CELANESE
P.O. Box 87
Shelby, NC 281~1-0087
Hoechst Celanese -Shelby Plant
Ms. Kathryn Frank
Shealy Lab No: TCLP Blank MS 02/01/96 QA/QC Officer Tn8::::
VP Analytical IYlrJ .
TCLP HERBICIDES METHOD 8150B
BLANK MA TRIX SPIKE FOR TCLP BATCH
Date analyzed: 02/01/96
Date extracted: 01/31/96
Compound % Recoverv
MS
2,4-D 106.8
2,4,5-TP 97.8
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Client:
Project Name:
Attention:
HOECHST CELANESE
P.O. Box 87
Shelby, NC 28151-0087
Hoechst Celanese -Shelby Plant
Ms. Kathryn Frank
Shealy Lab No: 83004N TCLP MS QA/QC Officer -rnw
VP Analytical (nlJ-L/
TCLP HERBICIDES
MA TRIX SPIKE FOR TCLP BATCH
Compound % Recoverv
MS
2,4-D 112.8
2,4,5-TP 101.2
METHOD 8150B
Date analyzed: 02/01/96
Date extracted: 01/31/96
i\-£615 DAILY STA1'v'DARD VERIFICATION
DATE: . d:{1 11 b
MUL Tl-LEV DATE: J./ ( (10
PARAMETER TRUE CONC
(µg/rnl)
2, 4-D 0.05
2, 4, 5-TP (Silvex) 0.05
COLUMN: ;#7t, if-fr STD#:--"':.=_+c,.-_
ANALYST: f<;};-STD#:--"""L..-f---
READ CONC PERCENT DIFF PRIMARY COLUMN
(ug/mJ)
0 . .,--<+r1 ; lg,-/DB-1701 DB-608 -
.
c,cl+-~ r .)__ ,L.DB-1701_0B-608
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M615 DAILY STA.Nl)ARD VERIF1CATION
DATE: ,(JJc(Yb
MULTI-LEVDATE: ilJ-kl'.f~-
!
PARA.i.'vfETER TRUE CONC
(ug/ml)
2, 4-D 0.05
2, 4, 5-TP (Silvex) 0.05
COLUMN: -#]~, -#k.5,-STD#: w.£,:f c_
'
ANALYST: t<f STD#: i;\!S. 0
I
READ CONC PERCENT DIFF PRHviA.RY COLUMN
(µg/ml)
0,cq (-S, ) J. -:,,,..~ i bB-1701 DB-608
C',Cl{'>/ i}-,,).--_LDB-l70l_DB-608
/
M • 608 DAILY STANDARD VERFICATION
DA TE: i (1.r-f:? £, coLUMN: ,:tt lrf r #,f£ STD#: W4-3 { c. i~ s.17-r~c
MULTl·LEV DA TE ,rtjt~r I r/j l-',U.~I ?b ANALYST: ()t: STD#: k'"!P?{' ;Jr?-.,.-c)~ .
PARAMETER / TRUE CONC /READ CONC / PERCENT DIFF / PRIMARY COLUMN I (ug/ml) I (ug/ml) I I
aldrin 0.05
a· BHC 0.05
o.c1t7<{, r . .,;i
O.O'fb,),.. I 7,c.,
L__DB-1701 _Los.sos
L__DB-1701 / DB-608
b • BHC a.as o . .:'i-7~ (.0 L__DB-1701 ./ D8-608
d • BHC a.as
lindane 0.05
Q.L1't-]) <;.* ,,.c~b)._ 7-(,
L._D8•1701 LDB-608
L__DB-1701 ....'.'.'._DB-608
· chlordane a.so L__DB-1701 J_DB-608
4,4' · DOD 0.05 (.) C~b I 7,fr L__OB-1701 __LOB-608
4,4' · DOE 0.05 o.c\/ Jf [,,) L__DB-1701 ~D8-608
4,4' · DDT a.as ,; c'f]d· i.l,4 L__DB-1701 -,.-,;QB-608
dieldrin 0.05 C,C~f~ 4-,, &" L__DB-1701 _,,,.d)B-608
endosulfan I 0.05 ,~; ,('',{J, ~, v ,-I·-3 s: L__DB-1701 _,.LDB-608
endosulfan II 0.05 -·(j_CI t.,...<.. I I I,,') L__OB-1701 ---L:D8-608
endosu/fan sulfate 0.05 C .~-'+~CJ-f,G L__DB-1701 ~D8-608
endrin 0.05 c-c44(;-( 0 J-L__DB-1701 _,LJ)B-608
enorin aldehyde 0.05 ,. C'L? r C. ' r.x L__DB-1701 ~D8·608
endrin ketone 0.05
C ",i&7 b,b L__DB-1701 /DB-608
heptachlor 0.05 --+r< 1, ..:~ (, ,_L I L__DB-1701 ./D8-608
;1eptac.~lor epoxide I 0.05 --------. '-17 l.,'.1. ' ~.J-1_D8·1701 ,/ DB-608
kepone I a.as L__DB-1701 Los-sos ··---···-··-··-········-···-······· ---~~~.~~~~.'.~~ ..••...•• '. ..• ~. 2? ..•........ '. ..• t.(.)i} .... '. ..... }.-.±:: ... ___ L-__ o_s_-1_7...,.o 1 __ ./r"'o_B-_so_a
toxaphene .•. I 3-00 I j). i' I I ; , c.' L__DB-1701 / D8-608
□cs -1o>o y.,u1 .. ,ia., J~'S-~:c.·.::_u._1_.r_1 _ __,~-'-' </-.,__ __ L-__ □_B-_1?_0_1 _ _.....--__ o_s-<>_-o_a
PCB· 1221 I L__DB-1701 _.....--D8•608 --------------------------PCB · 1232 L__DB-1701 ./DB-608 ----------------------------------------
PCB . 12 42 ··········-··· 0 ·.re.····--···· c:..:_ 1-b I:: i_os-1701 Los.cos
PCB·1248 L__DB-1701 ....,::::::::_DB-608 ----···················-·····--···········-·················--·----------
PCB· 1254 I_DB-1701 _.....--D8-608
PCB·1260 i_DB-1701 / D8-608 ,x -d1k, c{ ,;,,Q'···
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I QUALITY CONTROL
DATA
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I TCL Volatiles
I Method 8260A
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INSTIUJMENT QC VALIDA 110N SUMMARY
FOR EPA METHOD 8260A
For Samples: lab ID# 3:J"f"i7N
Jab ID # '! :Hn fl
lab ID# f]'7"flN
Jab ID # 13 CC/ J'l
lab ID # T.:,0o .l.N
lab ID# ',BcoW
lab ID# $31s-'-
lab ID# S3, S::7
CRITERIA
INITIAL CALIBRATION:(• l£ast S stdB will> ,-a1
ctllt2l'MDL)
Allswidardsand~~tthmmctllod
n,quin,,1 holding time,
BFB Tune Oileria(table 3)
SPCC, -criteria met in section 7.4.3.1 in mell,al 8260A
%llSD ror iill analytcs < 15%(in:: avg. relative RF fur calc:.)
%RSI> foe all malytes :, J5%{alculate cal cum: wilh r >0-995)
CCC• ave RFs % RS D < 30
DAILY OR CONTINUING CALIBRATION
(begiming ~~day ande,ery 12 hr)
BFB Tin: Crileria(w,Je 3)
Midpoint C3li1nlion sld run to verify:
1. SPCC, -criu:ria met in xction 7.4.3.l., !Ildhod 82SlA
2. ca:, %Drift < 20
3. rnttrnal Standards RT with:in 30 sec of J&.t chedc ,id( or ct!)
4. ElCP area for !Ss -50% 10 +100% from last cbca(or cal)
5. Surrogm,: % = w:ithin !IIClhod conlrol limie,
I
SA..W'LE CRITERJA
l. ¼t crill:ria in steps 3 -5 unda dailykontinning calibrarioo
2. RUii ..-ithin 12hr of la& in<ontrol tune
3. Analyzed wimin warting range of the curve( <highest ,ud)
P/F
F
f
f
p
p
Np;.
F
p
p
F
lab ID# ~3,1 <.,;z...
lab ID# "il~ll.3
labID#•n141
lab ID # <J'c; I 6
COMMENTS
Date of calibralion: I I IS I"/ l,,
r::. O,"i.'j'
Dale analyzed: 1/2t,/'lC:,
Tmie(s) of j,
tuning; o 7'+& 111 I ,
I hereby certify that all the above information is correct to the best of my knowledge. All out-of-
contn:>I measurements relating lo the method rcq_uiral acceptance criteria have been documented in
the above table along with po~ble effects Oil the sample analytic.al data.
Date:'Z--ffefaC
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QA Officer Si gnanire:
INSTil.UMENT QC VALIDATION SUMMARY
FOR EPA METHOD 8260A
For Samples: lab ID# ~3fb6
lab ID# g:31c,'7
lab!D# g3;Vx
lab ID # "il '> >c"zl
lab ID # 'i5 s .!.dJ
lab ID II °"" .,_, o
Lab ID# '132-1 I
. lab ID# :?J'-1<-
CRITERIA
INITIAL CALIBRA TION:(ar ie.ut 5 su1s wim one at
crr=-MDL)
All 5lal1dard3 and ,o!ution.1 µrc:para1/uriliml rit,;n mc:dlod
required ~ tin>e.
BFB T ur>e Crileria(lable 3)
SPCC, -criteria met in sa:ticm 7.4.J.I in methcd 8260A
%llSD for ;ill analyta < 15%(usc avg. rdative RF for calc.)
%RSD fee .all malytes > 15%{calculau: ~ curve w:ilb r ::-0.995)
CCC• ave RFs %RS D < 30
DAILY OR CONTINUING CALIBRATION
I (begiming ~ each day and every 12 hr)
BFB 1\me Crncrio(able 3)
Mxlpoint C3librllli-On ,ttl run IO verify:
I. SPCC., -criIGri.a mel in xctioo 7.4_J,l a, mdhoo 8261A
2. CCCJ %Drift< 20
3. [ncemal Standards RTwithin30seccrf mtcheck sldl;orCJ.l)
4. EJCP are,. for JSs -50% to +JOO',, from last cbccr(or cal)
5. Stm"Og!IIC % rec within mclhod corurol limits
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SA .. \IPLE CRITER1A
l. ¼::t cri tai.a in steps 3 -5 Linda daily A:on tin rung cali lrratioo
2. R Ull WJ th in 12hr of last in<ontrol tune
3. Analyzed within wcrl:ing range of Ill curve( <highest Sid)
lab ID# __ _
lab ID# lab ID #-:-. ---
lab ID# __ _
P/F COMMENTS
Date of calibration; I f, '< f:I b
I-'
p
p
p
p
NA-,-> 081
p
I
Date an.al.yzed: j/7n/q(,,
f' Tmie(s) of O"f I I tuning:
? I I
p
I hereby cenify that all the above information is correct to the best of my knowledge. All out-of-
control measurements relating IO the method ro:iuircd accepmnce criteria have been documerned in
the above table along with possible effectS on the sample analytical data.
Dare:
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SHEALY Lab
ID Numher
82997N
82998N
82999N
83000N
83001N
83002N
83003N
83006N -83156
83157
83161
83162
83163
83164
83165
83166
83167
83168
83207
83208
83209
83210
83211
83212
83213
TCL VOCs -Surrogate Recoveries
HOECHST CELANESE-Shelby
First Ouarter 1996
J ,2-Dichlorodhane-d4 Toluene-d8
(%) (%)
78.5 I()(}
97.3 101
92.3 101
100 105
99.5 98.0
104 103
109 105
IOI 107
106 105
110 107
80.7 100
112 106
1 11 105
111 106
109 101
88.2 101
107 104
108 104
112 104
80.2 103
110 102
106 103
107 102
106 104
102 101
4-Uromofluorobenzene
(%)
90.3
92.7
9 I. I
93.2
90.3
93.5
94.0
97.8
92.4
98.0
88.4
97.0
93.2
97.0
93.6
99.8
94.7
94.8
97.1
96.3
94.3
93.6
92.2
94.8
103
Client:
Project Name:
Attention:
HOECHST CELANESE
P.O. Box 87
Shelby, NC 28151-0087
Hoechst Celanese -Shelby Plant
Ms. Kathryn Frank
Shealy Lab No: Blank 01/26/96
VOLATILES
COMPOUND RESULT pnL (mg/I)
acetone ND 0.020
benzene ND 0.005
bromodichloromethane ND 0.005
bromoform ND 0.005
bro mo methane ND 0.010
2-butanone ND 0.010
carbon disulfide ND 0.020
carbon tetrachloride ND 0.005
chlorobenzene ND 0.005
chloroethane ND 0.010
chloroform ND 0.005
chloromethane ND 0.010
dibromochloromethane ND 0.005
l. l-dichloroethane ND 0.005
1,2-dichloroethane ND 0.010
l. l-dichloroethene ND 0.005
cis-1.2-dichloroethene 'ND 0.005
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QA/QC Officer 1Yl0,c. I
VP Analytical /tlr-'
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Page 2
VOLATILES -Continued for Blank 01/26/96
COMPOUND RESULT POL (mgn)
trans-1.2-<lichloroethene ND 0.005
1.2-<l ichloroorooane ND 0.005
cis-1 3-<lichloroorooene ND 0.005
ethvlbenzene ND 0.005
ethvl methacrvlate ND 0.005
2-hexanone ND 0.005
·methvlene chloride ND 0.005
4-meth v 1-2-oentanone ND 0.005
stvrene ND 0.005
I, 1,2,2-tetrachloroethane ND 0.010
tetrachloroethene ND 0.005
toluene ND 0.005
I, 1, I-trichloroethane ND 0.005
I, 1,2-trichloroethane ND 0.005
trichloroethene ND 0.005
vinvl acetate ND 0.005
vinvl chloride ND 0.010
xvlenes ND 0.015
ND = Not detected
Client:
Project Name:
Attention:
HOECHST CELANESE
P.O. Box 87
Shelby, NC 28151-0087
Hoechst Celanese -Shelby Plant
Ms. Kathryn Frank
Shealy Lab No: 83002N MS/MSD QA/QC Officer iY)Qc
VP Analytical /ti~
VOLATILES by 8260A
MATRIX SPIKE/MATRIX SPIKE DUPLICATE FOR BATCH Date· 01/27/96
Comnound % Recovery Control Limits
MS MSD RPD Max % Recovery Range
RPO
benzene 112 99.2 12.0 13.9 37-151
chlorobenzene 106 102 3. I 8.7 37-160
I. l-<lichloroethene 102 100 2.2 10.8 59-155
toluene 105 104 1.3 10.1 47-150
trichlorethene 111 98.0 10.0 15.9 71-157
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Client:
Project Name:
Attention:
HOECHST CELAt~E
P.O. Box 87
Shelby, NC 28151-0087
Hoechst Celanese -Shelby Plant
Ms. Kathryn Frank
Shealy Lab No: Blank 01/27/96
VOLATILES
COMPOUND RESULT POL !m!!/1)
acetone ND 0.020
benzene ND 0.005
bromodichloromethane ND 0.005
bromoform ND 0.005
bromomethane ND 0.010
2-butanone ND 0.010
carbon disulfide ND 0,020
carbon tetrachloride ND 0.005
chlorobenzene ND 0,005
chloroethane ND 0.010
chloroform ND 0,005
chloromethane ND 0.010
d ibromochloromethane ND 0,005
1, 1-dichloroethane ND 0.005
1.2-dichloroethane ND 0,010
I. 1-dichloroethene ND 0.005
cis-1,2-dichloroethene ND 0.005
QA/QC Officer :tnB:,,
VP Analytical ~
COMPOUND
trans-1. 2-<lichloroethene
1.2-<lichloroorooane
cis-1.3-<lichloroorooene ·
ethvlbenzene
ethvl methacrvlate
2-hexanone
.methvlene chloride
4-methvl-2-nentanone
stvrene
I .1.2.2-tetrachloroethane
tetrachloroethene
toluene
I. I. I-trichloroethane
I 12-trichloroethane
trichloroethene
vinvl acetate
vinvl chloride
xvlenes
ND = Not detected
Page 2
VOLATILES -Continued for Blank O 1/27 /96
RESULT enL /m11/])
ND 0.005
ND 0.005
ND 0.005
ND 0.005
ND 0.005
ND 0.005
ND 0.005
ND 0.005
ND 0.005
ND 0.010
ND 0.005
ND 0.005
ND 0.005
ND 0.005
ND 0.005
ND 0.005
ND 0.010
ND 0.015
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Client:
Project Name:
Attention:
HOECHST CELANESE
P.O. Box 87
Shelby, NC 28151-0087
Hoechst Celanese -Shelby Plant
Ms. Kathryn Frank
Shealy Lab No: 83001N MS/MSD Q Al QC Officer ::0:::!1%-:
VP Analytical /VI~
VOLATILES by 8260A
MATRIX SPIKE/MATRIX SPIKE DUPLICATE FOR BATCH Date· 01/26/96
Comoound % Recoverv Control Limits
MS MSD RPD Max % Recovery Range
RPD
benzene 105 105 0 13.9 37-151
chlorobenzene 101 99.8 1.2 8.7 37-160
I. 1-d ichloroethene 95.4 96.0 0.6 10.8 59-155
toluene 97.0 96.0 1.0 IO. I 47-150
trichlorethene 102 104 1.9 15.9 71-157
Analysc:_~i)~N_P+,b~/2_f"'D __ GC/MS ID:_~//"~S~J._3 ____ Dace/Tirr:e: //21,,/44 0'17_7
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Daily std ID:_~t~v'--~-1~1/'------Initial Cal. Date: _ _,_,1~6~i~/_q~b~--Heated purse ("!/N) : "'ii
SYSTEM PERFORMANCE CEECK COMPOUNDS (SPCCs):
I COMPOUND
I Chloromethane
I RF ,CO
(daily)
[), I I I
MIN RE'
0.100
i_:~==~~~~::::::~~: ________ i __ Pc!?f ___ i ___ ~~=~~---i i_~::~:::~ _________________ I __ ~.y,;-2 __ I_>_ 0.100 ___ I
i_:~=~=~==::::::~::::::~:-1::·:_i __ o,,Yl ------~~=~~----I Chlorcoenzene
I COM?CUNiJ
I
C'.::UC (ug/c.)
(da.ily)
0.300
%D I MAZ %D
j ·,,,_,,,~'-•~~~c:-·-c-" '/~,l-' <{,0 j 2C•.O ---------------------------------------------------------------
i -:~~=== ==~ --------------i _ -.. !~: ~ ------i _ --(,~ ?_ --i _ -= ~ ~ ~ ----~ I l,2-iJic:o.lor:::,propar.e I '/1,) I ,;,c.,' j 20.0 I ----------------------~----------------------------------------i_::='~:'.': ______________________ ~<f, 'I _____ i ___ //,v _i __ :~~~-----
i_ ~=~:= _ ::~::'.': _ ---------_ i _ --__ if_i )_ _ ---_ i __ _I!~(}_ -_ i _ -=~ ~ ~ ---_ i I Vinyl chloride I 41,'C:: I ~ o I 20. 0 I
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Analyst. : _ ___:::D_,_tv:..cP+/.,_12----'1:.=-(12-'-'------GC/MS ID : ___ l'-1_'5_J_s___ Date/Time : / /-z. 6 /2., f 7?., y
I /rs/2& Heated purge (Y/N) : f----
' l
Daily std ID : __ Cv_?.~J~r~<'----Initial Cal. Date:
SYSTEM PERFORMANCE C-IBCK COMPOUN""DS (SPCCs):
I Chlorcmethar1e I f),fo( 0.100 ----------------------------------------------------
1 1,1-Dichloroethane I O,s'I,; 0.100
I_ Brcmcfom _________________ I __ O, '>31 __ I_>_ O .100 ___ I
I 1,1,2,2-Tetrachlorcethane I o,3'-l<f I 0.300 I ----------------------------------------------------
1 Chlcrccenzene (i, g'{'] O. 300
C'-.LI3?-"'.TICN C-:ECK CQM?OL1IDS ( CCC::s) :
I CCM?OUL'ill I CCriC (us-/L)
(c:a:.ly) I Mi'\.X %0
-----------------------------------=---------------==-====-====
I , , "' -·-, ~~-e-·-c-c I .-. ri 1 · 1 -o o 1 _, ~--~~------·-------)u, I /,'j ~ ·' --------------------------------------------------------------1 c-,lcrcfcrT, I ,;'i, '7 I cp, cJ I 20. o I ______________________________________________ J _______________ _
~ -= ~ = :~~~~~~~~~~~~~~= -----~ ----~t-r _ ---~ -_'.I?_ ---~ --~= ~~ ----~ l _ :~=,~=~'=-________________ l ____ _LI_ L.~-____ l __ l ~ ~-~ __ l __ ~~ ~ ~ ____ l
I :ethyl benzene I 'fu, i I 1, V I 20. 0 I -------------------------------~---________ j __________________ _
j Vinyl chloride / 1./5", L / er,(,, / 20. 0 /
~PA M8260 ,1
Analyst : _0::::...c.N..::.' _P--'-~-'-f2.----"'CT).=:__ GC/MS ID : __ ;....""'~" _l_"3.:::::..___ Oat e/Time : ------'/...,__/4_;:_z;r:...:.h.:..:c.=----'-/-=-0-=--z. .!..-7 __ 1
Daily std ID: __ 1,_c.._· _z._1..:._f--=C,,:____ Initial Cal. Date : _ __,_,4/'---'----'1 g<.1./_q-'-(,"'---Heated purge.(Y/N) : ,J 1
SYSl!:.M PSRFORMANCE C--IBCK COMPOUNDS (SPCCs):
==-------------------------------J-----------------
1
COMPOUND I RE' S< I MIN RF I · (daily)
~ _ :~:':1:':~'.:=~~~'.: ________________ v, 113 ___ I ___ ~ ~ :~~ ___ _
/ l,1-Dichloroethane 0 ,33,z / 0.100
l _ ~=:~':~':~ ____________________ 0,5"7 ; __ ~ _ ~ _~~=~~ ___ I l_:~=~=~===::==~~~=:=~::=~~::_l __ o,1~r ______ ~~~~~---~ l _ =~=:=:~:~=:~'.:-_______________ /,o<, ,z _______ ~ ~ ~ ~~ ___ _
::_;I__;I3?-...~T:i::ON c-~c:-<: CCMPOL1'luS ( CCCs) :
I CCM~CL1'iD
I I C'.JNC(ug/U
(c:ailyl
%C I Mi'-.X %D
--=============-=====--======--==-=====---=-==-====--=--==--=--~ _ ~ ~ ~ = ~ ~ ·=: ~ ~ ~=:: : : : : ___________ I c.~ } ______ l __ i ~ ._ ~-_____ :: ~ ': ____ _ l _ :~·===: ==~ ___________________ r_~-'J ______ l ___ 1 ~1~ ~ ______ : ~ ~ ~ ____ _ I l, 2-0ichloropropa:-.e I fl" I / 1, -3 I 20. 0 I __________________________________ ] ___________________________ _
l _ === ·~:~·'.: _________________ ~ ____ 2f ~ !:,_ _____ l __ l} ~ ~ __ l __ : ~ ~ ~ ____ l l _ ~~~~-= -~:~::~'.:-__________ l ____ 'it~-_____ l __ Ji'"~--~--=~ ~ ~ ____ l l _ ·:=::'~= -=~=~==~:: -_____________ iJ:9 ___________ ~: ? ___ ~ _ -=~ ~ ~ ____ _
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I QUALITY CONTROL
DATA
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Ethylene Glycol
I Method 8015A
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For Samples:
INS1RUMENT QC V ALIDATICN SUMMARY
FOR EPA METHOD 8015A
lab ID# jj"jf)'C,
lab ID# i3i)'.}
..,.!.lb!D# __ _
lab ID# __ _
CRITERIA
labID# __ _
lab ID# __ _
lab ID# __ _
lab!D# __ _
lab ID# __ _
lab ID# __ _
lab ID# __ _
lab ID# __ _
P/F COMMENTS
INITL\L CALIBRATION:(ai lc&t 5 slds with 011e a1 I Date of calibnrion: 1/J.<:;l<i (, er := MDL and 11.9e of dnal ::,,lumn ftc coafinnatioo) \ . --· ..
All stmd:ml aoo sol'1riom ~li7.ed ,.jthin rnedxx! f ~uired holdq times
futemal """'1anl caJailarm ll<ro with f > Q,995 D ,')O,'i q I
DAILY OR CO!l,TTI1,1JING CALIBRATION Date analyzed: I I I "117b (h::ginning of run and '>cry i O sample$) .
Midroint calilnticn std run to verif:·:
I. Rtm midpoint cal .<Id to ch<--....k all a.nalytes within 15% of
1) -p
true V.UIJC i) NA-2. S~ % rec within lab geaaatcd cootrol limits
I SAMPLE CRITERJA
!. Bracketed by in control CV, •) p
-· Surrog,,tc, :., control ~) ['I Pr
J. Analyud within wcning range of lhe curve{ <tligbesl Sid) ,) i'
I hereby c:::tify that all the .trove information is con= to the best of my k;iowlrdge. All our-,,f-ccntrol mea=me:m relating to :he :ne:toc n,quired acceptance cri::eria have been dcx:'Jn=tec in ~'Jt: :il:G~,,: tink: :iloog s.ith possible dfe::ts on :..'ie sarq,le :in:t.1:,-tic;iJ d:iu
Da.te: -Z-1(~ h b t
' -QA Officer Signature: -/0,o . ./Jl.z._£tL ~f----..
INS1RL1MENr QC VALIDATION SUMMARY
FOR EPA METHOD 8015A
Foc Samples: lab ID# ';/~oo3 rJ LablD# __ _ lab ID# __ _ lablD# __ _ labID# __ _ lab ID# __ _
lab ID #'----lab ID# __ _
lab ID# __ _
Lab ID"-'----
lab ID# __ _
lab ID# __ _
CRITERIA P/F I COMMENTI>
INITIAL CALIBRATION:(ar lc3'!I 5 Sall! ..,jib ooc: at f
c.-IJe:U' MDL~ ~ of dnal column for COl!firmation) i p I Dau: of ca.lilntion: I/ /Ci /q /,,
An Sllmdards and ,olntiom ~ within l!lcmai I f required. holding time3
fulmlal undard calcolation used ,.;u, r > 0.995 p r ') O,'t C/
DAILY OR COl'-o,NUING CALIBRATION Date aiwyzed: I h -z.. I,; C. (beginning of n.i and e>ery i O <ample,)
Midpoim <ailnlicn s:d run to verify: ,")P I. Rm, midpoint c.aJ .,Id to c.ha:: . .I: a.II a.nlU)'tc3 -..ithin 15% v<
trueV21ue
2. Sllffllf!ll'e % rec within lab geMJ attd cootral bmicl i\ NA-
SA~PLE CRITERIA
l. Brac:kl,ted !,y in cootrol CV, i) f 1. s~ in control .... .., ('J tr
3. Analyzed within wcrlcing range afche ~~l,af) 7,) p
[ ;1=by certify that all the above information i.s = to the best of my knowledge. All ouH:,f-=t:'Ol meast=l, :-elacin g to :he method :-equired accept:U1Ce cri ceria bve bee,:i docume:i~ :n ~'ie lbove table along ,,,ilh pc:ssible dfe:::s on the sample anal ytic:il data.
Dare:
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Client:
Project Name:
Attention:
HOECHST CELANESE
P.O. Box 87
Shelby, NC 28151-0087
Hoechst Celanese -Shelby Plant
Ms. Kathryn Frank
Shealy Lab No: Blank 0 I/ 19/96 QA/QC Officer ----fYlQl:...
VP Analytical /IJ,r.-/
COMPOUND
ethylene glycol
ETHYLENE GLYCOL METHOD 8015A
RESULT
ND
Date analyzed: 01/19/96
Date extracted: 01/19/96
POL(mg/1)
6.50
Client:
Project Name:
Attention:
HOECHST CELANESE
P.O. Box 87
Shelby, NC 28151-0087
Hoechst Celanese -Shelby Plant
.Ms. Kathryn Frank
Shealy Lab No: 83158 MS/83159MSD QA/QC Officer--fh;[C.
VP Analytical /11~
ETHYLENE GLYCOL METHOD 8015A
Date analyzed: 01/19/96
Date extracted 01/19/96
MATRIX SPIKE/MATRIX SPIKE DUPLICATE FOR BATCH
Comoound % Recovery Control Limits
MS MSD RPO Max % Recovery Range
RPO
ethvlene glycol 101 82.9 19. 7 25.0 50.0-150
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FCB-~~-1-3'~6 14: ,:::s F.i32
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V
TOC RESU!...TS:
DATE OF DATE RESljL-;:"S ?RESEVED ·ACIDIFIED OPERATOR I REMARKS: SAMPLE: ~N: ?PH: ·, I N .. ~ :3PARGED INITIALS
' 1-)t -'((,, /-2J -ft !?If I Ve:;, ye,s U-· I Tc. I
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Hoechst Cel::i.nese-Shelby, NC
Water Level i'vfeasurements
Date: / (J Ja.,n · 94, (exceptions noted in comment field) Page: / of 4 ----
Measured by: n1 fJ {) ~ (. !IV 1-f Measurement Device: E!ec:lront(.. Wokrievcl .lnd,cc, ·
Monitoring Measuring Depth to Water Comments Location Point Water Level
Elevation (ft) Elevation
(ft, ms]) (ft, ms!)
AA-54 782.16 ;3-'}'-10 7'--F) ')(p
CC-33 812.68 .:J.c 05 7q..2_. &3
EE-58 794.48 Jq,:;4 75 '-I 79
FF-34 772.73 (,;,_,'73' 75qqr;
FF-62 772.19 l5w.3 7S&. 5r.,,
GG-61 771. 78 .;).0:35 75 / '-1-3
HH-48 755.44 -37 ·?o 7;77~
HH-77 755.87 ,,13 """'-3 7 !'7 & '-I-
K-28 811.20 (~-DO ]CJC/.2..0
P-58 788.12 ;)3 04 7uSoY
T-35 777.38 /;,,.?S 11P'-/53
V-23 8 I I. 89 /;. ;,J oDD-'7 5
C-49 864.11 13 gg 8'5J-23
OTCI NA -
ITCI NA -
OTEF NA ·-
ITEF NA -
SBR WASTED NA -SLUDGE
FILTER PRESS NA -SLUDGE
LAMBERT NA -
CROTTS NA -
STINE NA -
RUNYANS NA -
ELLIOTT NA -
A-39 823.36 // '7:? 3!l5S
AA-41 783.68 3& :3 5 ·1'-1'7 33
B-34 790.62 13.39
CC-64 811.37 //'}, j 'i
D-35 845.69 I f.p '71.f
D0 56 845.19 I IP l/-f'
D-88 845.52 /&, '70
DD-58 796.10 -3'/ 54
F-55 849.19 Lf3 .;zs
FF-23 772.33 /;z5q
G-50 848.48 d</:55
G-88 848.26 4ooD
GG-25 771.64 It? 8'J7
GG-39 770.44 /90/
H-59 845.25 5150
J-28 825.18 =2.0 ot/.
J-59 825.01 .Jl3/
K-58 811.39 /t/45
M-44 806.71 J_f.35
N-29 803.38 8 .'fc;
N-53 803.82 6-35
0-25 807.54 /..2. l,j
0-59 806.61 /o.q1
T-17 777.90 13 '7·7
T-58 776.03 /=25/o
U-38 826.55 .)JL./5
Y-38 794.52 /,!_ . )~'-/
Y-74 794.87 / .J J../'7 D-27 845.50 /(_., .:,0
H-79 846.53 5"! 2.4 I-57 837.63 Ji) 50
M-28 806.72 ::)C/.{p/
P-3 l 790.00 c)_; j &
Q-33 783.48 d3 D'f
R-17 779.31 /5 3.:/
R-42 778.81 !)19
S-50 826.02 ,)Jq5
W-23 800.91 I 5 'l?
2
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79'/oJ
8J.'2, q5
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1t,;/.5{p
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-7c;r;. 14
,Jof,13
80 8 .J.J.,
75;,7~
1Sl43
7''?3 75
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-f'D3 ')o
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1·7? 31P
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v,Jaf-c!,~ DCft,,.d'c!n C.U.S1,,:1-
11\..-,, .1,, -1-.,.,., /l/!, A n,,1...--
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X-32
Z-78
BB-18
PZ-1
PZ-2
PZ-3
PZ-4
PZ-5A
PZ-5B
PZ-6A
PZ-6B
PZ-7A
PZ-7B
PZ-8
PZ-9
PZ-10
PZ-11
PZ-12
PZ-13
IT-1
IT-2
IT-3
IT-4
IT-5
IT-6
IT-7
IT-8R
IT-9
OT-lR
OT-2
OT-3
OT-4
OT-5
OT-6
OT-6A
OT-7
796.96
797.08
771.75
773.99
795.81
786.62
750.07
788.72
777.59
795.11
796.89
780.46
784.46
767.99
788.96
784.65
805.48
749.41
776.51
814.20
813.85
809.66
809.08
810.64
812.20
813.52
815.60
808.73
NA
774.01
792.88
790.28
784.00
787.45
798.68
782.16
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OT-7A 782.52
OT-8 782.26
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PEW-1 846.85
PEW-2 848.92
PEW-3 849.25
PEW-4 848.14
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-------------------
Monitoring
Location
AA-54
CC-33
EE-58
FF-34
FF-62
GG-61
HH-48
HH-77
K-28
P-58
T-35
V-23
C-49
OTCI
Hoechst Celanese-Shelby, NC
Water Level Measurements
Page: I Of 2
Measured by: CWH, MPO, MCC Measurement Device: Electronic Water Level Indicator
Date Measuring Depth to Water Temperature pH Specific Comments
Point Water Level (OC) (SU) Conductivity
Elevation (ft) Elevation (umhos/cm)
(ft, ms!) (ft, ms!)
01/18/96 782.16 35.89 746.27 15.2 5.02 342
01/17/96 812.68 19.93 792.75 16.4 6.83 382
01/18/96 794.48 40.44 754.04 15.9 7.01 84.5
01/18/96 772.73 12.77 759.96 15.2 9.72 80.3 well dry at 6.0 gallons
01/18/96 772.19 15.72 756.47 15.4 6.77 73.3 well dry at 11.0 gallons
01/18/96 771.78 20.24 751.54 15.3 6.08 134
01/17/96 755.44 38.00 717.44 15.6 6.14 55.0
01/17/96 755.87 38.13 717.74 15.7 7.10 91.6
01/16/96 811.20 12.00 799.20 16.8 6.88 189
01116196 788.12 22.63 765.49 17.0 7.00 708 well dry at 13.0 gallons
01/17196 777.38 13.00 764.38 15.7 6.16 555 well dry at 6.0 gallons
01/16196 811.89 11.37 800.52 16.7 5.70 5070
01117196 864.11 13.64 850.47 16.6 6.26 23.9
01/16196 NIA NIA NIA 20.9 7.26 650
Monitoring Date Measuring Depth to Water Temperature pH Specific Comments
Location Point Water Level (OC) (SU) Conductivity
Elevation (ft) Elevation (umhoslcm)
(ft, msl) (ft, msl)
ITCI 01/16196 NIA NIA NIA 14.7 5.97 1480
OTEF 01116196 NIA NIA NIA 17.3 7.24 438
ITEF 01/17196 NIA NIA NIA 17.4 8.19 875
SBR 01/17196 NIA NIA NIA NIA NIA NIA
WASTED
SLUDGE
FILTER 01/16196 NIA NIA NIA NIA NIA NIA
PRESS
SLUDGE
LAMBERT 01/17196 NIA NIA NIA 15.6 7.14 208
RUNYANS 01/18196 NIA NIA NIA 16.4 7.34 519
2 -------------------
-------------------Field Data Ii. .... ination Sheet For Groundwater Sa.uuiling
Page \ of \ S ----
Shealy Environmental Scrvkt.~, Inc.
106 Vantage Point Drive
Cayce, S.C. 29033
Date (MM-DD-YY) I (o :TA-tJ q \p Casing Diameter:
Field Pcrsmrnel 2. inches Ca.sing Material: PVC~
CWII, MPQ : Guard Pipe: PVC l Metal)-No Locking Cap: ~-N
Facility Name KUBAL -FURR / HOECHST CELANESE, SHELBY Protcclivc Abutmcrn: y -(N Integrity Satisfactory: ()-
Well ID# Y-23 Well Yield: Low -Mod.(-H[gn
Weather Conditions <::ow I ovizfLcA,,-r { 1.,H r-ln'f Air Tempcratu~c <>c. &;marks.;
Total Well Depth (TWD) 2A.0
Depth To Groundwater (DGW) -11-31"
Length Of Water Column (LWC) I <a. fo3
I Casing Volume (OCV) -LWC x O.ll. 3 -2. '1 gal.
3 Casing Volumes e.1 gal. -Standard Evacuation Volume
Total Volume of Water Removed -
Method of Well Evacuation
Meti10d of Sample Collection
fa:acuali!m aud Coll1a;1i1m~
TB -Ti=flon Bailer
SSB -Stainless Steel Bailer
WW -Well Wizard
GP -Grunfos Pump
VOLUME PURGED (GALLONS)
TIME (24 HOUR SYSTEM)
pH (SU)
WATER TEMPERATURE (°C.)
SP. CONDUCTIVITY (UMHOS/CM)
TURBIDITY (SUBJECTIVE)*
ODOR (SUBJECTIVE)**
4i. \
TB SSB (WW) GP Other
TB SSB (WW) GP Other
C.un.ilan.l.SJPr Casing Dian1eters
1.5" -0.1)92
r = 0.163
3" -0.367
4· -0.652
le
I 3l\Co
':)_SL\
\(.,. 9
3CoDD
I
L\
5" -1.02
6ft = 1.47
r = 2.(X}
8" -2.61
'J..."?
1"3S\
s <.oO
\(.,. C,
?,°ISC)
\
'-\
gal.
FIELD ANALYSES
5.4 ""b. \
, --ssA 1'-lO<\
t; S°\ ,; 7t
i C., ·7 IL. 7
:,C\ o" Y'--c;D
\ \
L\ L\
-) '.:'tfTO
• I= CLEAR 2 == SLIGHT 3 = MODERATE 4 111(,11 .. .-.--.-.. I N<>NL 2-IAINI 3 MCH>LllAIL ·1-SIRONC,
.•
WELL SAMPLE TIME:
l'I \':,
8.tmark.s·
F . .,__QJ l::il "~ l'-\'-100
N
Fiel<l 1;;.1ti matjon Sheet For Groun.d..ll:aleLlilllli!lim:
Page ·1, of \ S
Shealy En\'ironmcntal Sen·. ., Inc.
106 Vantage Point Drive
Cayce, S.C. 29033
Dale (MM-DD-YY) \-\ l,.-. '·\ (,, Casing Diameter: '2 inches Casing Material: PVC _(1,,~
Field Personnel C\VII, MI'Q
Facility Name KUBAL -FURR / IIOECIIST CELANESE, SHELBY
Well ID# ?-':)-.l,
Weather Conditions OveI CC''"' '.I.-c0\1 Air Temperature oc.
Total Well Depth (TWD) = '.:/1. L.\ C)
Depth To Groundwater (DGW) = -;,_2, <...--.'.>
Length Of Waler Column (LWC) = :,S, 77
1 Casing Volume (OCV) -LWC x ,\(,,°:) -t='., _<j, ~ gal.
3 Casing Volumes = \1 ,L\C\ gal. = Standard Evacuation Volume
Total Volume of Water Removed =
Method of Well Evacuation
Method of Sample Collection
~uon and Collecuon Methods
TB -Tenon Bailer
SSB -Stainless Steel Bailer
WW -Well Wizard
GP -Grunfos Pump
I':, gal.
TB SSB ' WW) GP Other
TB SSB ~ GP Other
Conmms for Casmg D1illllCkis
1.5" -0.092 5" -1.02
2· -0.163 6" -1.47
3" -0.367 7" -2.00
4• -o.652 s· -2.61
Guard Pipe: PVC -@Ji-No Locking Cap: (y_}.
Protective Abutment: y -Q::J; Integrity Satisfactory:
Well Yield:( Low) Mod. -High -
R~marks:
wei\ ,\,~ r_J \ --z., ocJ.\ =•• 5 -' ,.)
FIELD ANALYSES c,, ,, 1 ,.._, c•, <.. ~
VOLUME PURGED (GALLONS)
TIME (24 HOUR SYSTEM)
pH (SU)
WATER TEMPERATURE (°C.)
SP. CONDUCTIVITY (UMHOS/CM)
TURBIDITY (SUBJECTIVE)•
ODOR (SUBJECTIVE)••
0
n,-z,
·7.~1
lt-3
'JO(), 0
I
I
• I -CLEAR 2 -SLIGI ff 3 a MODERATE 4 I IIGII
c, 4.::,
i:1':i"
7 :>" ' .J
\7.0
Ll'SO
I
I
••
\\,C..<.., ,...:;,-~1c:;.i WELL SAMPLE TIME:
' I • -, \
i31'l \7::,2S Btmarks·
1, O \ 7.GO
1<.,,:1 17.<..J
""i':5 0 G,CC) = 1;7D'2
\ \
l \
' ' .. ' .. .. I -NONL 2 -IAIN I 3 -MODI.RA IE 4 -.SI RONG
N
co-N
lS:,0
-------------------
--- - - - -- -- - -- -- - - - -Field Data In,. oation Sheet For Groundwater Sampling
Page __3__ of \ S
Date (MM-DD-YY) !I. TA>i9 la
Ficir Perstm11cl CWII, MP~
Facility Name KUBAL -FURR / HOECHST CELANESE, SHELBY
Well ID# K-:i.e,
Weather Conditions 0-./€11..~f½, / c <,Lo)/., t ,-, ')'( Air Temperature oc.
Total Well Depth (TWD) = 28.(.)
Depth To Groundwater (DGW) 1~-0
Length Of Water Column (LWC) -11.,0
I Casing Volume (OCV) = LWC x L,ltc3 = 2 I., gal.
3 Casing Volumes -?. 1:~ gal. = Standard Evacuation Volume
Total Volume of Water Removed =
Method of Well Evacuation
Method of Sample Collection
Evacuatmn and Collecuoo Methods
TB -Teflon Bailer
SSB -Stainless Steel Bailer
WW -Well Wizard
GP -Grunfos Pump
7."t:i
TB SSB <.'!!.'!V GP
TB SSB ~ GP
Conscaa1s for Casmg Diameters
1 .5" = 0.092 5" = 1.02
2" =0.163
3" = 0.367
4" = 0.652
. ..,_ I -
6" = 1.47
7" = 2.00
8" = 2.61
-J..'i
gal.
Other
Other
FIELD ANALYSES
5".'
Shealy Environmental ScrviCl.,, -nc.
106 Vantage Point Urive
Cayce, S.C. 29033
Casing Diameter: -z_. inches Casing Material: ,P_VC) Metal
Guard Pipe: PVC -<t!etali Ne Locking Cap: y N •., ' Protective Abutment: '.Y ! N __ j Integrity Satisfactory: .~ -N
Well Yield: Low -Mod. -~
Remarks·
o rl (,.0 . ~ ... '\ Cc-.c~ c;,. \ -,·le \,cc " \l\ '-?. ,;:"'.{" '.J__
,( ·. -~ .co r,,. ,\ \', ~ C: ·. c/
\D. iO. \C:, ,·/c.r. ' ,<-\ 0 / 0. --rt '--)L'
T:: i/,Ci ' l °i 7 , n. c.. 0 ()_\ J,,_.
I< ., . C\(..~. c~ I , (.YC) 0 .: <\ G.-~-'--l ~.,('._•
7,C'""~ --,,. 7, iD, co--.> '\(t;;(:}c, L\ le,,
-·
7. t~ WELL SAMPLE JIME: /23 VOLUME PURGED (GALLONS)
TIME (24 HOUR SYSTEM) i"1. ti 111 'ei IL 'L') /l,J. 9 R~marks·
pH (SU)
WATER TEMPERATURE (°C.)
SP. CONDUCTIVITY (UMHOS/CM)
TURBIDITY (SUBJECTIVE)*
ODOR (SUBJECTIVE)**
~ .. 3'-1
It.. q
ii-JD,()
'
I
' 1 = CLEAR 2 = SLJGJIT 3 = MOD ERA TE 4 -IIIGH
0.·)'-1
,~.7
jlG.Q
3
1 ..
L, 7,1 (~.9'8
I<. ., /l,. q
ISo.n /1~0. t.) -=7/YCi
2, I
'J, {
.. . . . .. !=NONE 2=FA1Nl 3=MOlllcRAlE 4=SlRONG
Field Data h. _ mation Sheet E'or Groundwater Sampling
Page___tLof _\__2_
Dale (MM-DD-YY) I -I 7 -c-(. Casing Diameter: J_
Shealy Environmental Scrvil:..:..,, Inc.
I 06 Vantage Point Drive
Cayce, S.C. 29033
-inches Casing Material: PVC -a-te1al> -. Field Personnel CWII, MPQ ·: Guard Pipe: PVC -,MctaP No Locking Cap: lcf_ I-N -Facilily Name KUBAL -FURR / HOECHST CELANESE, SHELBY Protective Abutment: y -(_N) ln1egri1y Satisfactory: (Y) -N
Well ID# r·c. -3, 3 Well Yield: Low -Modc__l&v
Weather Conditions C /4v(/v o/J Air Tempcralurc oc. Remarks; -' To1al Well Depth (TWD) = ~J. ao
Depth To Groundwater (DOW) = lf?J
Lenglh Of Water Column (!..WC) = i 3. 0 ')
I Casing Volume (OCV) = !..WC x . ( 6 :J = ,;,:;_ (J gal.
3 Casing Volumes = C, _]j? gal. = Standard Evacua1ion Volume
Total Volume of Water Removed =
Method of Well Evacuation
Method of Sample Collec1ion
Evacua1mo and Collecuon Methods
TB -Teflon Bailer
SSU -Stainless Steel Bailer
WW -Well Wizard
GP -Grunfos Pump
VOLUME PURGED (GALLONS)
TIME (24 HOUR SYSTEM)
pH (SU)
WATER TEMPERATURE (°C.)
SP. CONDUCTIVITY (UMHOS/CM)
TURBIDITY (SUBJECTIVE)*
ODOR (SUBJECTIVE)**
G,. 3°\
TB SSB C'._" GP Other
TB SSB (WV}) GP Other
Q.n1s1ants..for Casmg Diamerers
I .5" -0.092 5" -1.02 /2) -0.163 6" -1.47 '-J = 0.367 7-= 2.00
4• = 0.652 s· = 2.61
0 Yj.31
1 / : 'i9 ;,:;;,i
. ( ~, G. L f -
I 5,~ I l. J...
2, 1'1 <; :J..[(.)
;)_ '.)
;} ~
gal.
,f,',CC--, ' / FIELD ANAi.. YSE , (,) ·
Kt,.':i --v/.,_37
I I;< { i ,l .·t· o
C, , 7 f ,._. r J
Ii:, -J I{:; .i..(
31 <; ~JG --
I I
}. ,i
":'738J
• I = CLEAR 2 = SLIGHT 3 = MODERATE 4 -IIIGII .. ' ,. ' I -NONE 2 -I AINI 3 -MODI.RAIL 4 -SI RONC,
-------

-
-

-
-

-

-

-

-
WELL SAMPLE TIME: i,) .. -,. j
Remack.s:
--

-
--
- -- - -- -- -l'icld Data-11.. _,mli2aSbcct For Grouud.l!'.alcr...Samlllilli:
Page '°) of \ '::>
Date (MM-DD-YY) I-I 7 -"1 (.,;.
- - -- -
Casing Diameter: -, ·-
- - - - -Shc,,ly Environmcnlal Scrvk---.,, Inc.
106 Vantage Point Drive
Cayce, S. C. 29033
inches Casing Material: (PVC!-Metal ,, Field Personnel C\VII, Ml'Q ,u.. " ( Guard Pipe: PVC ~-et3)1 -No Locking Cap: ( y1 -N ' -facility Name KUBAL -FURR / HOECHST CELANESE, SHELBY Protective Abutment: y -, N• Integrity Satisfactory: ( Y) -N
' Well ID /I i -?,'::, Well Yield(l:°w__::)Mod. -High
Weather Conditions c:,,~ <:C ,•~ \-, Cc~ Air Tcmpcranire oc. Rrnmk.s.;
Total Well Depth (TWD) =
Depth To Groundwater (DGW) =
Length Of Water Column (LWC) =
I Casing Volume (OCV) = LWC x
3 Casing Volumes = //,
Total Volume of Water Removed =
Method of Well Evacuation
Method of Sample Collection
f.vacuaooo a1xl Collec1tC10 Metlmds
TR -Tenon Bailer
SSB -Stainless Steel Bailer
WW -Well Wizard
GP -Grunfos Pump
VOLUME PURGED (GALLONS)
TIME (24 HOUR SYSTEM)
pH (SU)
WATER TEMPERATURE (°C.)
SP. CONDUCTIVITY (UMHOS/CM)
TURBIDITY (SUBJECTIVE)•
ODOR (SUllJECTIVE)••
7J.7. DC) i) f'v
, ·? I , • G .:, I
, . .-'~. {; i)
i (_, ·) = 7 ,') ,/ gal. .,
/-
') y gal. = Standard Evacuation Volume
(, ()
Tll SSll ·WW) (-~, GP Other
Tll SSll ( WV'!,) GP Other
Coustarns_for Casmg Diameters
I .5" -0.1)92 5" -1.02
2" -0.163
J" -0.367
4" -0.652
0
I) ,/ v
(., I (.I
. I :>' ,.,_(
l/ )';/
I
r
6" = 1.47
r = 2.00
8" -2.61
~ C _;,, i I
I). '.Ji
(_, J1
I (, . I
Lt 10
I
(
gal.
FIELD ANALYSES
~ ' J/.'J ,;/
I J . ](.. I
G, tG
I~-l I
l/ (;,O -?S15G -
I I
I
1\_ \-
• I =CLEAR 2=SLIGIIT ]=MODERATE 4=1IIGII .. ., , " ,,, I = N<>NI: 2 = l·AINJ 3 = l\10Dl:RA 11: 4 =SI RON(,
L 0 i'C...., I ,
,_
-
WELL SAMPLE TIME:/ :J: y L'
Remarks·
Field Data In ,talion Sheet For Groundwater Samp_Jiug
Page & of I':>
Shealy Environmental Ser\'k .... _, Inc.
I 06 Vantage Point Urive
Cayce, S.C. 29033
.. Date (MM-DD-YY) 1-1 7. p(:, Casing Diameter: 2 _ inches Casing Malcrial: &-Mela)
Field Personnel C\VII, MPQ, /1/c.· C ·,
Facility Name KUBAL -FURR / HOECHST CELANESE, SHELBY
Well ID# /' y.,;' -
Weather Conditions c./4:,.~ cc.I/ .
Air Tempcra1ure oc. -
Total Well Depth (TWD) -e;:-r,,O
Depth To Groundwater (DGW) = / ?,_ G't"
Length Of Water Column (LWC) = .JG . .J' C
I Casing Volume (OCV) = LWC x ,tGJ = s-y'_:7 gal.
3 Casing Volumes = I 7. 7;>-gal. = Standard Evacuation Volume
Total Volume of Water Removed =
Method of Well Evacuation
Method of Sample Collection
Evacuauon and Collecuon Methods
TB -Tenon Bailer
SSB -Stainless Steel Bailer
WW -Well Wizard
GP -Grunfos Pump
I 7-t gal.
TB SSB C!!.'JV GP Other
TB SSB rWY GP Other
Omstants for Casmg P1ameiers
I .5" -0.092 5" -1.02
2" -0.163 6" -1.47
3" -0,367 7" -2.00
4" -0.652 8" -2.61
FIELD ANALYSES
Guard Pipe: PVC -~staV-No Locking Cap: C,.," -N
Protective Abutment: y -~) In1cgri1y Satisfactory:( y.,' --
Well Yield: Low -<Mil<.!. -High
Rl.anarks.;
0 _s. ~' J I I. 9 / 7 .. r-WELL SAMPLE TIME: i] • ;;J VOLUME PURGED (GALLONS)
TIME (24 HOUR SYSTEM)
pH (SU)
WATER TEMPERATURE (°C.)
SP. CONDUCTIVITY (UMHOS/CM)
TURBIDITY (SUBJECTIVE)•
ODOR (SUBJECTIVE)••
IJ.':;s ,
7,0'1
15,c.,
Jo
i
I
' !=CLEAR 2=S1.1Glff 3=MODERATE 4 IIIGII -
/!.,.'0/
(;, 7 /
IL. L
Jo
(
I ..
13-'at; i ], : (j Remarks·
6 3 p, (., ;? (;
I b. ri /6. (.,
) (:) ;;:,() =;t .q
I (
I I
-' , .. I-NONI, 2-l·AINl 3-MODLRAlE 4-SIRONG
N
()
- ---

-
-

-
-

-
-

-

-

-

-
-

-
-

-

-
- - - - - - -- - - - - - -l'icld Vala Ir· . 1rnlion Sheet f'.!!L{;IJll!illl.ll'all:r...fuuul!lini:
Page l of \ '::>
Dale (MM-DD-YY) 1 I; 7 /f'(, Casing Diameter: ~;) -
- - - - -Shealy Environmental Scrvk ... ..,, Inc.
106 Vantage Point l>.-ivc
Cayce, S.C. 29033
inches Ca.sing Material: PVC (Mc~aj)
Field Personnel CWII, Ml'Q /J1 V'L. Guard Pipe: PVC (_Mc1'11_;,.No Locking Cap: (_ '{' -N
/
Facility Name KUBAL -FURR / IIOECIIST CELANESE, SHELBY Protective Abutment: y -(N) Imcgrity Satisfactory:(__)'~ -
Well ID# ,.1/ A/ -7 ? Well Yield: Low -(1\1<><1',-High
Weather Cofl<litions c/4_,a{,_ c,-/c( Air Temperature oc. &'.mar.ks.;.
Total Well Depth (TWD) = ~ 77. 9
Depth To Groundwater (DGW) = z.P./:?
Length Of Water Column (LWC) -J 9 -7 )
I Casing Volume (OCV) = LWC x I(, 7 = C <-r gal.
> • /<
3 Casing Volumes -/ f". ~<-gal. = Standard Evacuation Volume
Total Volume of Water Removed =
Method of Well Evacuation
Method of Sample Collection
Evacuauoo and Colkc11on Merhcxls
TB -Tenon Bailer
SSB -Stainless S1eel Bailer
WW -Well Wizard
GP -Grunfos Pump
VOLUME PURGED (GALLONS)
TIME (24 HOUR SYSTEM)
pH (SU)
WATER TEMPERATURE (°C.)
SP. CONDUCTIVITY (UMHOS/CM)
TURBIDITY (SUBJECTIVE)*
ODOR (SUBJECTIVE)••
/ 9. s:--s-
TB SSB 01/JV GP Other --TB SSB CfilY,) GP Other
C!mstanu....fur Casmg Diameters
1.5" ~ 0.092 5" ~ l.02 r = 0.163 6w = 1.47
3" ~ 0.367 7" ~ 2.tXJ
4" = 0.652 gw = 2.61
b G,yr
I): Jr I g ' ~ f . f
'· t p, 7. 5~J
I:::,-. .).._ I '>, (,
70 7v
( (
( I
gal.
FIELD ANALYSES
/,;J ,9(; /7'-yJ~
t 1: ~1 1~1:0'{'
7' ~ J 7, / ~
i ~. l ( ~. ·,
70 7 ~-:;:;:-
I I
I I
qi&
• I= CLEAR 2 = SLIGIIT 3 = MODERATE 4 IIIGII -.. -' -. -' ... 1 NONL 2 I AINI 3 MOl>UlAIE 4 ~SIRON(,
---
WELL SAMPLE TIME:/ 'r: 1 ()
Remarks·
N
Field DalalnL .illli2n Sheet for Groundwatcr...SamulinJ:
Page ii of \ ':) ----
Shealy Environmental ServicLJ, inc.
106 Vuntagc Point l>rh·e
Cayce, S.C. 29033
Date (MM-DD-YY) ( -/1 -f C Casing Diameter: d-inches Casing Material: PVC('Meial
_/ Field Personnel CWH MPQ ;,r,:,,,c. Guard Pipe: PVC -(!'~al'-No Locking Cap: ()? -N , r
Facility Name KUBAL -FURR / HOECHST CELANESE, SHELBY Protective Abutment: y (!::!, Integrity Satisfactory:(_)? -

N

Well ID# i--lH-<r,P Well Yield: (!::o~i:~-lligh
Weather Conditions C /~•c,,_/7 c4/c/ Air Temperature oc_ Remarks· -
Total Well Depth (TWO) = <;.-fl no
Depth To Groundwater (DGW) -2Y.oo
Length Of Water Column (LWC) -/t?' /]
I Casing Volume (OCV) = LWC x /0 J = G"< gal. ' /,
3 Casing Volumes = y. ,I-9 gal. = Standard Evacuation Volume
Total Volume of Water Removed =
Method of Well Evacuation
Method of Sample Collection
E.vacuaoon and Collecrmn MelbO(fs
TB -Tenon Bailer
SSU -Stainless Steel Bailer
WW -Well Wizard
GP -Grunfos Pump
VOLUME PURGED (GALLONS)
TIME (24 HOUR SYSTEM)
pll (SU)
WATER TEMPERATURE (°C.)
SP. CONDUCTIVITY (UMHOS/CM)
TURBIDITY (SUBJECTIVE)*
ODOR (SUBJECTIVE)**
y. /-9
TB SSB (ti_~ GP Other
TB SSB ~ GP Other
C<1ns1aots fuL.C.a.s.1D.2...D1.a.llll:.1'il
I .5' = 0.092 5" = 1.02
2" = 0. 163 6" = 1.47
]" = 0.367 7" = 2.00
4" = 0.652 8" = 2.61
(;; ; G s
1·1 '.jj,"' /'--1'.(f
<o ~✓s, 12 0)
1.:::-) ----IS'. "t
(,,; '-I< , ,
, I
gal.
FIELD ANALYSES
3 ' ;;2 (;, '/.Pf
/•/~)/;, I L,_ ? L
6 -c? o Co I~(
r S', 6 f ,:;-' (,
<; c;: 4.; --
I I
I I
L',._.;,t-1, \-~ 7 -'·ll...,,.
7fi8~D
' I = Cl.EAR 2 = SLIGIIT 3 = MODERATE 4 -IIIGII -.. ' -' . ., 1-NONL 2-J·AINI 3-M(H>LRAIE 4-Sll<<>NG - --

-

-
-

-
-

-
--

-
-

-
WELL SAMPLE TIME:;7 ; :J p
Rtmacks:
----

-
- -- - - - - - -Field Data In Jation Sheet For Groundwater Sampling
Page Ci; of I':)
Date (MM-DD-YY) I . I 7 9-C
- - -- -
Casing Diameter:
- - - - -Shealy Environmental ServkL .. , Inc.
106 Vantage Point Drive
Cayce, S.C. 29033
inches Casing Material: PVC -Metal
Field Personnel CWII, MPQ / fr'<-(_. Guard Pipe: PVC -Metal -No Locking Cap: y -N
Facility Name KUllAL -FURR / HOECHST CELANESE, SHELBY
Well ID# .i ,,._,,,.._ he ✓-T
Weather Conditions
C /.• V ~
Total Well Depth (TWD) -
Deptl1 To Groundwater (DGW) -
Lcngtl1 Of Water Column (LWC) -
1 Casing Volume (OCV) -LWC x
3 Casing Volumes =
Total Volume of Water Removed =
Method of Well Evacuation
Method of Sample Collection
EY..ru;u.aUQn..aad Colh::c1i1m Mi:1bods
TB -Tenon Bailer
SSB -Stainless Steel Bailer
WW -Well Wizard
GP -Grunfos Pump
-C -<,let" Air Temperature "C.
-gal.
gal. = Standard Evacuation Volume
/ ';,--_ () gal.
TB SSB WW GP Other
TB SSB WW GP Other
Cun.s.tants for Casing Dia,m;rers
IS = 0.092
2" =0.163
J" = 0.367
4" = 0.652
5" = 1.02
6" = 1.47
T' = 2.(kJ
8" = 2.61
FIELD ANALYSES
Prolcctive Abutment: y -N Integrity Satisfactory: y -N
Well Yield: Low -Mod. -lligh
Rcnrntks·
1 . f /""YI,,..."...._ C:: 1,.J c / f
--
VOLUME PURGED (GALLONS)
TIME (24 HOUR SYSTEM)
CJ ~.o /c). 0 / .,,:, () WELL SAMPLE TIME: i :;_-_. 0,l
pH (SU)
WATER TEMPERATURE (°C.)
SP. CONDUCTIVITY (UMHOS/CM)
TURBIDITY (SUBJECTIVE)•
ODOR (SUBJECTIVE)*•
I 'l; 'I:.,-
7. J I
l
i '-(. )
110
~
d-
• I= CLEAR 2 = SLIGHT 3 = MODERATE 4 IIIGII
t"r:s·o
·7. J-f
t.:> {
{ .. , 0
I
J. ..
/~/ .5 ~~ I;;-· {i J Remarks·
·7.JJ t, IY
i :::-. (_ I ,;, &
I 76 i 7 {\ -'?do~ -
I Jl. I
I /}
' --' ... I NONL 2 IAIN I 3 MODI.RA IL 4 ~ SI RONG
Field Dara lni .ation Sheet For Groundwater Samu.liug
Page ID of I'::,
Dale (MM-DD-YY) 1//p-/.f'c
Field Personnel C\VII, MPQ, "'1.-,--c_ :
Facili1y Name KUBAL -FURR / HOECHST CELANESE, SHELBY
Well ID# £/~ -~?'
Weather Conditions c.. /4 C, /4,,, Air Temperature oc.
Total Well Deptl1 (TWO) = .
I':.. I. q
Depth To Groundwa1er (DGW) = Y-6. y-V
Length Of Water Column (LWC) = ,:Jr.<...-' I Casing Volume (OCV) = LWC x /65 = < ~ gal.
3 Casing Volumes = / I'> < gal. = Standard Evacuation Volume
Total Volume of Water Removed =
Method of Well Evacuation
Method of Sample Collection
Evacuat10n and Collectrnn ~
TB -Tenon Bailer
SSB -Scainless Steel Bailer
WW · Well Wizard
GP · Grunfos Pump
/6. s-
TB SSB ,WW,,, GP -
TB SSB (!!yj) GP
Dm.~1an1s for Casing D1ame1ers
1.5" -0.092 5· -l.02
2" -0.163
3" -0.367
4" = 0.652
6--l.47
7" -2.<Xl
8" -2.6}
Other
Other
6 3. <
gal.
FIELD ANALYSES
7_ c)
Casing Diameter: ~
Shealy En,·ironmcntal Servic,..._, rnc.
106 Vantage Point Drive
Cayce, S.C. 29033
inches Casing Material: PVC -(f.1etal'
Guard Pipe: PVC ('!vle1al) No Locking Cap: (D-N
Protective Almlmcnl: Ye! h11cgri1y Sa1isfac1ory: er.:'.) N
Well Yield: Low@ -High
lktuarks.;
/o.S:-WELL SAMPLE TIME: / ~ ,' __? o VOLUME PURGED (GALLONS)
TIME (24 HOUR SYSTEM) /@," C Jl-' /cJ.'/'? /,;JJJ../ I J: ;Jf Remarks·
pH (SU)
WATER TEMPERATURE (°C.)
SP. CONDUCTIVITY (UMHOS/CM)
TURBIDITY (SUBJECTIVE)*
ODOR (SUBJECTIVE)••
C:,.P-~
(5,C/
70
{
(
• I= CLEAR 2 = SLIGlff 3 = MODERATE 4 = IIIGII
-------
I [. 9</ 7. DI Ci}O[)°'" ., w 7.01
-. -, s.Y I&, CJ / (' 9 -t-✓-'.J _, -(..) l . ,
71\ 7f'\ 70 -t,,34,S
I I I
( ( I .. I =NONI: 2=1·AJNI 3=MOIH:RAIE 4=SIRON(1
--------

-
--

-
-- - - -- -Field Data In ... _ rntion Sheet Foe GnrnndwatlT Sa111pling
Page _\\_of I '=1
Date (MM-DD-YY) I . //l"-p {,
- -- - -- -
Casing Diameler:
- - - - -Shealy Environmental Ser\'ic, -, inc.
106 Vantage Point Drive
Cayce, S.C. 29033
inches Casing Material: PVC -Metal
Field Personnel CWII, MPQ ;uvC-· Guard Pipe: PVC -Metal -No Locking Cap: y -N ,,
Facility Name KUBAL -FURR / HOECHST CELANESE, SHELBY
Well ID N {{_<,7/'l ,/n/1
Weather Conditions .,. /4 ttoY Air Temperature nc.
Total Well Depth (TWD) -
Depth To Groundwater (DGW) -
Length Of Water Column (LWC) =
I Casing Volume (OCV) = LWC x
3 Casing Volumes -
Total Volume of Waler Removed =
Method of Well Evacuation
· Method of Sample Collection
.f.Yacua11on and Collecuon Methods
TB -Teflon Bailer
SSB -Stainless Steel Bailer
WW -Well Wizard
GP -Grunfos Pump
/
=
gal.
/ c-; n
TD SSD WW GP
TD SSD WW GP
Cons1arus for Casmr Dmneters
1.5" -0.092 5" -1.02 r = 0.163
J" -0.367
4" -0.652
6~ = 1.47
r =2.ex>
8" = 2.61
gal.
= Starn.lard Evacuation Volume
gal.
Other
Other
FIELD ANALYSES
Protective Abutmcnl: y -N Integrity Satisfactory: y -N
Well Yield: Low -Mod. -High
Rtmiuks:
Pr ,· ,, -/../-, /..)P.,,.-1(
VOLUME PURGED (GALLONS)
TIME (24 HOUR SYSTEM)
0 S-,D ;o.o r~o WELL SAMPLE TIME: t'('; y_s.'
pH (SU)
WATER TEMPERATURE (°C.)
SP. CONDUCTIVITY (UMHOS/CM)
TURBIDITY (SUBJECTIVE)*
ODOR (SUBJECTIVE)**
/'-(!JJ.-
7. ob
q.(::,
3() <
I
(
' I = CLEAR 2 -SLIGI rr J -MODERATE 4 IIIGII -
/<f:.3(, {<(:1.1' l'-1-''-lo Remarks·
l. 3 C. 7. -1, 1 7. Jy
/'-(.J. I <: • .1. /6,C...(
y ,.J 6 '-, .J 5 Y.~S" =--;,c:;;q
( 1 J
{ J !) .. -' -' ... I NONL 2 -l·AIN I 3 -MODLRA IL 4 -SI RON(,
Field DataJ..1t\ Jation Shed For Groundwater Samu.ling
Page I J.. of \ '.J
Date (MM-DD-YY) /. / ~ . f? ,,,..-Casing Diameter: d-
Shealy E1n:i,·onmental Scrvic ... __ , inc.
I 06 Vantage Point Drive
Cayce, S.C. 29033
·~
inches Casing Material: PVC -~1e<a_J,,
Pield Personnel CWII, MPQ/ µ.c:---c... Guard Pipe: PVC (Jvic,a1)-No Locking Cap: (.:!)~-N
Facility Name KUBAL -FURR / IIOECIIST CELANESE, SHELBY Pru1ectivc Abutment: y {N__; lnlegrily Salisfacwry: ~-N
Well ID# /-l/7-rs---Well Yield: Low (M~ -High
Weather Conditions c./4 {/ _/ Air Temperature oc. R!.'..tlllllis.;
Total Well Depth (TWO) -cv_ '7
Depth To Groundwater (DOW) -<..S-M
Length Of Water Column (I.WC) -I R-, Jr I
I Casing Volume (OCV) -I.WC x . / r ? = s. 0 b
3 Casing Volumes -p -2-o gal.
Total Volume of Water Removed =
Method of Well Evacuation
·Method of Sample Collection
f.y__ruratkm aod Collc!;;tioa M1:1lmds
TR -Tenon Bailer
SSB -Stainless Steel Bailer
WW -Well Wizard
GP • Grunfos Pump
VOLUME PURGED (GALLONS)
TIME (24 HOUR SYSTEM)
pH (SU)
WATER TEMPERATURE (°C.)
SP. CONDUCTIVITY (UMHOS/CM)
TURBIDITY (SUBJECTIVE)*
9_ c2_
TB SSB (w..J!_ GP
TB SSB ?w5Jl GP
Constants for Casing Diametrrs.
1.5" ~ 0.(!92
2" -0.163
3" -0.367
4" ~ 0.652
5" -1.02
6" -1.47
7" -2.1)()
8" -2.61
gal.
-Standard Evacuation Volume
gal.
Other
Other
FIELD ANALYSES
9.8-c.J WELL SAMPLE TIME: / <001_
Remarks·
ODOR (SUBJECTIVE)** I • I = Cl.EAR 2 = SLIGI l"I" 3 = MODERATE 4 '=-711"'1(~;171 -----'----,;,.,---;-, -=--\:N"O;;-N;cE,---,2'a::7"FA;-;l~N,;,T-'--,3,-ac,,c;Hcc)l;c>lc;'.R;-;Ac;.l,;,.E--'-4;-;a:-.;:,S,lc;.R,:-0;-:-N;,,G,--lL------------_J
- --

-

-
-

-
-

-
-

-

-

-

-
-

-
-

-

-
-------- - - - -- -- - - - -l'icld Data Infl J.t.i.o.n..Shect For Groundwatrr Sampling
Page 13 of i':J
Dale (MM-DD-YY) 1 . I y. 9l Casing DiamcLcr: :}
Shealy Environmental Servin:.,, .uc.
106 Vantage Point I>rivc
Cayce, S.C. 29033
--
inches Casing Material: PVC Ak1al J
Field Personnel CWH, MPQ J1( v <:. Guard Pipe: . / PVC (Mela')-No Locking Cap: (__!) -N
facility Name KUBAL -FURR / HOECHST CELANESE, SHELBY Protective Abutment: "'y ( N_ l11tcgri1y Satisfactory: ( .:J -N
Well ID# r:.. G, -(; ( Well Yield: Low~-lligh
Weather Conditions c/ouc/. Air Temperature oc. Rruliirki:
Total Well Depth (TWD) = I r.:. (. (J
Depth To Groundwater (DGW) = ...? 0.,:) y
Length Of Water Column (LWC) = 1/0· 7<:.
I Casing Volume (OCV) = LWC x . /6.? = r~.(.,,s----gal.
3 Casing Volumes = / 9. 9 gal. = S1andard Evacuation Volume
Total Volume of Water Removed -
Method of Well Evacuation
Method of Sample Collection
Evacualmn and Collecuon Methods
TB -Teflon Bailer
SSB -Stainless Sceel Bailer
WW -Well Wizard
GP -Grunfos Pump
VOLUME PURGED (GALLONS)
TIME (24 HOUR SYSTEM)
pH (SU)
WATER TEMPERATURE (°C.)
SP. CONDUCTIVITY (UM HOS/CM)
TURBIDITY (SUBJECTIVE)*
ODOR (SUBJECTIVE)**
/9.9
TB SSB (WYf.} GP Other
TB SSB (!!Y GP Other
C.00s1a01s for C asmg Dla.Ill.t..te.I.
I .5" = 0.092 5" = 1.02
2· = 0.163
J" = 0.367
4" = 0.652
0
6ft = 1.47
r = 2.(X)
8" = 2.61
e, ,G y
( ~: S-1 Ir}: ~'i
(, ~( ln. I q , c;, { -IS".!::,
I 35 I t c>
1 I
I (
gal.
f-IELD ANALYSES
I j,JfY I 9. 'ii
I 3 · Of I 3:/<:,
r,, . I c1 (:, .C) ~
If" 3 I~ ,J
If f\ I I f,
I ' r (
·--~ !;if
• I = CLEAR 2 = SLIGHT 3 = MODERATE 4 IIIGH -.. = ' -' -... I NONE 2 I AINf 3 MOl>LRAIL 4 SIRON(,
·--
·-
WELL SAMPLE TIME: 13: rr
Remarks·
Fidd 1Ja1a J11..__ . talion Sheet For GcQ.l.llllllralcr Sam,~lim:
Page l'i_ of J..2_
Date (MM-DD-YY) /-l~·PC.
Field Personnel CWII, MPQ, #f c.-c_ Pacili1y Name KUB'½:-:':,,~R / IIOECIIST CELANESE, SHELBY _,
Well ID II 1--1--~ -,,;:-..J.
Weather Conditions c./ou /y Air Temperature oc. Total Well Depth (TWD) = r~ :i 7 Depth To Groundwater (DGW) = I\, ;:l
Length Of Water Column (I.. WC) = YG.Pr I Casing Volume (OCV) = !..WC x . /(;,J = 7. 6 C, gal. 3 Casing Volumes = c? ;J, '77 gal. = Standard Evacuation Volume Total Volume of Water Removed =
McU10d of Well Evacuation
MeU1od of Sample Collection
-Evacuauon and Co/lec11on Methods TB -Teflon Bailer
SSB • Stainless S1cel Bailer
WW -Well Wizard
GP -Grunfos Pump
VOLUME PURGED (GALLONS)
TIME (24 HOUR SYSTEM)
pll (SU)
WATER TEMPERATURE (°C.)
SP. CONDUCTIVITY (UMHOS/CM)
TURBIDITY (SUBJECTIVE)•
ODOR (SUBJECTIVE)++
//. 0
TB SSB <::!!.Ji> GP OU1er
TB SSB {'!!Jf} GP OU1er
Cnos1ants for Casing D1amc:1crs
1.5' = 0.092
2· = 0.163
3• = 0.367
4• =0.652
0
7, {)
5" = 1.02
6" = 1.47
7" = 2.00 s· = 2.61
7_ (,
ti: Y{)
. 0 7
r ~.
(
(
gal.
I : .ro
~ 7 ...,
~ ::, .
(, 0
I
I
Shealy Enl'ironmcntal Scrl'icc....;, Inc.
106 Vantage Point I>rive
Cayce, S.C. 29033
-Ca.sing Diameter: e,.;;2 inches Ca.sing Material: PVC -°'1ctal
Guard Pipe: PVC-~ No Locking Cap: Q -N
Protective Abutment: y -Qi.:: Integrity Satisfactory: CO -N
Well Yield:~-Mod. -High
Rtnrntk.s· ,, .-/ ,, ./--I I.(!) /?~ / I '
7 WELL SAMPLE TIME: / I : s (
Rtwatks·
• I = CLEAR 2 = SLIGIIT 3 ~MODERATE 4=111GII .. I =NONE 2 = FAINT J = MOIJEIUTE 4 =STRONG -------------------
- - - - -- -Field Data lnh -. .illQIL.'ihcct For Groundwater Samuling
Page \ '5 of IS ----
Date (MM-DD-YY) I·//>'· 9<,.
-------
Casing Diameter: .d-
- - - - -Shealy EnYironmcntal Servic{:_,, .uc.
106 Vu11h1gc Point Uri\rc
Cayce S C 2'1033 • @ -inches Casing Material: ~-f'1ctal/
Field Personnel CWH, MPQ1 />1 t/G Guard Pipe: PVC-~-No Locking Cap: (:)-N
/Sl Facility Name KU~,, -FURR / HOECHST CELANESE, SHELBY Protective Ahutmcnt: y0 Integrity Satisfactory: ~-N -Well ID# 1-·1---:hie~ Y Well Yield:( Low 3 Mod. -High
Weather Conditions c/40clv Air Temperature oc. Rema[k.s·
Total Well Depth (TWD) -'s '(, ~--,~ r\ /
DepU1 To Groundwater (DGW) -/c9. 7 7 ,
Length Of Water Column (LWC) -,2 (. 7?
I Casing Volume (OCV) = LWC x ./1..'r = 'J :;-c,,, gal.
3 Casing Volumes -/ o. b '3 gal. = Standard Evacuation Volume
Total Volume of Water Removed -
Method of Well Evacuation
Method o( Sample Collection
Evacuation and Collec11on Methods
TB -Tenon Bailer
SSB -Stainless Steel Bailer
WW -Well Wizard
GP -Grunfos Pump
VOLUME PURGED (GALLONS)
TIME (24 HOUR SYSTEM)
pH (SU)
WATER TEMPERATURE (°C.)
SP. CONDUCTIVITY (UMHOS/CM)
TURBIDITY (SUBJECTIVE)*
ODOR (SUBJECTIVE)**
I' CJ -TB ~SB f;'.: K GP Other
TB SSB 0'J) GP Other
Ulll!iliilll.S..fur C asmg Diame11:1.s
IS -0.092 5" -1.02
2" -0.163 6" -1.47
3~ = 0.367 r = 'l.<XI
4" -0.652 g~ = 1,61
D ? sy
ll'./J.-I l '.IS
q_r,1 'f. ( <;{
. { '}, J. I 5",;J-
?C> 0)
I I
I I
gal.
FIELD ANA'"" iS)
~__p -
..,,
. ,,-/f) _(; :J ,,.. ,,:..:>.:) I
q. 7;;.. I
I ~.:l I (_ <--:-;-~ .)/
I I
( I
/I ,+-
• I =CLEAR 2 = SLIGlff 3 = MODERATE 4 IIIGII -.. -' -. .. --.. I NONL 2 -IAIN I J MODLKA IE 4 -SI RON(,
(.. 0 ,,-, ~ I ,,
WELL SAMPLE TIME://. ·;i jY
Remarks;
Field Uata lnfora.,•,lion Sheet For Groundwater Sampli1.ig
Page _!__ of -1
Date (MM-DD-YY) Ot)l&Jc;r;,
Field Personnel .
CW ft 1171Pa
Facility Name KUBAL -FURR/ HOECHST CELANESE, SHELBY
Well ID# OTC,I
Weather Conditions Air Temperature
Total Well Depth (TWD) = . \ • Depth To Groundwater (DGW) = \"I r-
Length Of Water Column (LWC) -
I Casing Volume (OCV) = LWC x =
oc_
gal.
3 Casing Volumes = gal. = Standard Evacuation Volume
Total Volume of Water Removed =
Method of Well Evacuation
Method of Sample Collection
.E__yaQliluon and Collectum Melhods
TB -Teflon Bailer
SSB -Stainless Steel Bailer
WW -Well Wizard
GP -Grunfos Pump
VOLUME PURGED (GALLONS)
TIME (24 HOUR SYSTEM)
pH (SU)
WATER TEMPERATURE (°C.)
SP. CONDUCTIVITY (UMHOS/CM)
TURBIDITY (SUBJECTIVE)*
ODOR (SUBJECTIVE)**
TB SSB WW GP
TB SSB WW GP
Crn1s1ants for Casmg Diameters
1.5" = 0.092 5" -l.02
2" =0.t63
3" = 0.367
4" = 0.652
/L/-30
11. 2({)
c2D-1
6~ = I.47
7" = 2.00
8" = 2.61
Other
Other
(_pc,o = '7'" ~ fiO
gal.
FIELD ANALYSES
Casing Diameter:
Shealy E1n·iro11111cntal Services, ... ..:.
106 Vantage Point Drive
Cayce, S.C. 2903.l
inches Casing Material: PVC -Metal
Guard Pipe: PVC -Metal: No Locking Cap: y -N
Protective Abutment: y -N Integrity Satisfactory: y -N
Well Yield: Low -Mod. -lligh
Remarks·
WELL SAMPLE TIME:
Remarks·
• !=CLEAR 2=SLIGIIT )=MODERATE 4 111(,11 I -NONL 2 IAIN I 3 -MUDLRA IL 4 -SI RON(, .. -. . .
- - - - - - -- - - -- - -- -- - -
--- ----ful.!lJJa tlLinfm:,
Page :J. of _!i_
Date (MM DD-YY)
Field Personnel
-,n Sheet For GroIB!!lWiiffi·--5.ill!u~Hng
01 II& Io 1.
C rv ;/, ;-npo
- ---
Facility Name KUBAL -FURR/ HOECHST CELANESli'., SHELBY
Well ID# () I El-
Weather Conditions
Total Well Depth (TWO)
Depth To Groundwater (DGW)
Length Of Water Column (LWC)
I Casing Volume (OCV) LWC x
3 Casing Volumes
Total Volume of Water Removed
Method of Well Evacuation
Method of Sample Collection
~QJ;Hkin and_C'ollection Me..lhuds In -Teflon Bailer
SSB -Stainless Steel Bailer
WW -Well Wizard
GP -Gruufos Pump
VOLUME PURGED (GALLONS)
TIME (24 HOUR SYSTEM)
pH (SU)
WATER TEMPERATURE (oC.)
SP. CONDUCTIVITY (UMHOS/CM)
TURBIDITY (SUBJECTIVE)*
ODOR (SUBJECTIVE)**
Air Tcmpcr.iturc oc_
. I A
I \l II
gal.
gal. Sta11d.1rd Evacuation Volume
gal.
TB SSB WW GP Other
TB SSB WW GP Other
.C.Ons.tams_for Casioe Dffitm-1trs
1.5" ~ 0.002 r =0.163
3" = 0.367
4ft = 0.652
!43S
1.;u-/
/1,J
5.ft = I .Ill
6ft = 1.47
7ft = 2.{XJ
8ft = 2.61
J'7'5-V -<./j8
---Flf'LD ANAi YSES
--
C;1si11g. l)i;11m;tL-r:
---- -
Shealy E11\'iro11mc11lal SlT,·iccs, ... ..:.
106 \'anbq!,l' Point lki,·c
Cayce, S.C. 290.B
inches Casing M;i!cri:d: l'VC -Metal
Ciu;1rd Pipe: PVC -(\.-kt;tl ~ Nu Locking Cap: y N
J>rotccli\'C Ahulllll'lll: y -N Integrity SatisL1ctory: y -N
Well Yield: Low -rvlod. -lligh
!(emark_,_;
--
WELL SAMPLE TIME:
R~marks;
• I : CLEAR 2 :,,: SLIGI IT 3 = MODERATE 4 -111u11 .. t NUNE 2 I' I -A NI J MUDl.l{A IL 4 SI RUNt,
-
ful.1Ul.atw1rQ[,,.".illl!!lil1cct For Gr:i.mmlwa_tc1:lia1_up!i11g
Page -3 of _1._
Date (MM-DD-YY) O!/!{JJ/((&
Field Personnel t:!.w If, /71/J [?
Facility Name KUBAL -FURR/ IIOECIIST Cl•:LANESE, SIIELBY
Well ID# TTc.I.
Weather Conclitions Air Tcmpcr.111uc
Total Well Depth (TWO) -I\\ (\
Depth To Groundwater (DGW) -,~ t1
Length Of Water Column (LWC) -
I Casing Volume (OCV) -LWC, -
oc.
p.al.
3 Casing Volumes -gal. = St;md;ud Evacu;i1io11 Vol11111c
Total Volume of Water Removed =
Method of Well Evacuation
Method of Sample Collection
Ev a _acJ.1 _ _1mn...and...Collt..e..11un..Mt..1hOOs
Tn -Teflon Bailer
SSD -Stainless Steel Railer
WW -Well Wizard
GP -Grnnfos Pump
VOLUME PURGED (GALLONS)
TIME (24 HOUR SYSTEM)
pl! (SU)
WATER TEMPERATURE (°C.)
SP. CONDUCTIVITY (UMIIOS/CM)
TURBIDITY (SUBJECTIVE)*
ODOR (SUBJECTIVE)**
gal.
TB SSB WW GI• Other
TB SSIJ WW GP Other
l:.ousta nts Jo 1-..Cas.iu2..U 1a111(: te, s
1.5" = 0.1)92 5" = 1.02
2" = 0.U,3 6" = 1.47
3" = 0.367 7" = 2.IX)
4" = 0.652 8" = 2.61
FIELD ANAI.YSFS -
/J-/55
SC/')
IL/. r;
/,20D __:_ ;,-I '-I-'3 3
Shealy l-'.ll\'.iro11111c11l:il St.T,·ke.'-, >11c.
106 \':ml:1gc Poi11( l>rin~
Cayce, S.C. 2911.B
C:isi11g Dia111clcr: inches Casing l\.btcrlal: PVC -[\.k1al
..
t_;11;11d l'ipc: PVC -/'vlc!a! ~ No Locking Cap: y N
l'rnlLTlivc 1\hul11H.:11l: y N l111egrity S:itisL1clc1ry: y -N
Well Yield: I.ow-J\·lod. -lligh
Hc111;11 ks:
-~-
WELL SAMPLE TIME:
J!..@li!lliS.:
• I = CLE/\R 2 = SLIGHT 3 = MODER/\TE 4 111<.ill .. I NUNL 2 I /\IN I .I r,.111J)J Ill\ 11. •I SI llllN<..1 - - - -- - - - - ---- ---- - -
---------- -
Ei_cldJl;!l'LlnfliL,. ,\lULS!!l:.C_LEllL<.i!mmdKa(~!:liampliui:
Page _.L}_ of 4
Dale (MM-IJIJ-YY) 01/ ;,iJq /_
Field Per sonnet J Ctu!I-I )J7VG
Facility Name KUfiAL -FURR/ IIOECIIST CELANl•:SE, SHELBY
Well ID ff I 11::f-
Weather Conditions
Total Well Depth (TWO) -
Depth To Groundwater (DGW) -
Length Of Water Column (LWC)
l Casing Volume (OCV) -LWC x
3 Casing Volumes
Total Volume of Water Removed
Method of Well Evacuation
Method of Sample Collection
~CU~liOfland~lion.Mt..Ulihls
l n -1 t:non JJailn
SSA -S1ainlcs~ S1eel Oailer
WW -Well Wj7_ard
GP -Gn111fos Pump
VOLUME PURGED (GALLONS)
TIME (24 HOUR SYSTEM)
pl! (SU)
WATER TEMPERATURE (oC.)
SP. CONDUCTIVITY (UMIIOS/CM)
TURIJIDITY (SUBJECTIVE)•
ODOR (SUBJECTIVE)•*
Air Tc111pc1;11111c ll(.'_
" \ ,,
I '0 r,
=
gal.
TB SS8 WW GP
TB SSB WW GP
!:.oos..taJJlS...foLCas.in ia1 1e e &Jl I 1 IS
5" = I.Ill
6" = I .47 r = 2.00
8" = 2.61
1.5" = 0.091
2" ~0.16.1
J" ~ tl.367
4" = 0.652
/oc;o
f.;q
!'71-
gal.
-Sta1Hl.ud Evacu:11io11 Vol11111c
gal.
Other
Other ----
. --· Fll'l D ANAi YSFS
75D --> ?7s
-------Shealy E11l'iro11111e111:il Serrin·s, .,u.:.
106 V:111l:1ge Poiut D1·i\'e
Caye", S.C. 29113.l
C:isi11g I >ia111clcr: inches ( ·;,si1ig l'vl;11crial: l1V<.: -Mcl;il -~---
(i11;11d l1ipr: l'VC -Ml'i:tl -No Locking Cap: y N
1'1oll'clivc /\li111111c11l: y N l11tcg1ity S:uisl"actory: y N
Well Yield: I .ow -1'\'llld. -II igli
l{i:111;irks;
-
WELL SAMPLE TIME:
&:Ju,11.ks:
' I~ CLEAR 2 = SLIGIIT J = MODERATE 4 -IIIGII .. I,~ NONE 2 FAIN I" J .. tdl IJH·ll /\IL 4 SIRON(,
-
----- - - -- - - -- -- -- -USE BAU POINT PEN ON' · ...,RESS HARD SHEALY ENVIRONMENT·. SERVICES, INC.
106 Vantage i--Drive _ol -
CHAIN OF CUSTODY # 2 3 7 6 Q
Client Name 1-/ {}_ / --------~-------
Re po rt in g Address ______________ _
Cayce, South Caruuna 29033
Telephone No. [phone] Fax No. [phone]
CHAIN OF CUSTODY RECORD
SAMPLE ANALYSIS REQUIRED
County ___________ _
Receiving Stream----------~----·--------
Outfall No. ____ ---------~-------
c:si , .• _, l,y tJ c.. f" +-PRESERVATION (CODE) LAB USE ONLY .
Attention __iJ& '1 r Ve,0,,h c CODE: A= None Program .A.!Jfl_(Circle)_· __ ,. j B = HNO3 ~ ?; § , C = H2SO4 DW ( ,· WNNf'DES · \ Telephone No. P.O. No. ~ 8. { c i f1CHA . SPISOL __ --00 r~ 1 D: NaOH i 00 ' ~ . .. SP1L10 Other: ' i! i 00 I E = ICE ~ X ! 00 f.; 0 ' . F= Y,.!3.3.._w J Q 0 w " ~ ~ X ~8 " ~ ' " Sample ID (Location) TIME J , < 0 H 8 l • ~ a b u
DATE w i5 0 oc r 0 w ~ 8< 6 z ~ u § ' REMARKS SESI • 00 " " 0 w ,. , c w ,, w ;. LAB I.D. Star1 ··-;-,~
\\, Jl:l t--1 '23'--'
Finish l_i '.\·Jq · / '/-;V I<-'.IS ✓ • .:.
Star1
11.:YA t--1 1330 'I P-s2.,
Finish ,/ " ·i•f;,<·:,A I • .. (_\ (_, ' ( ,..;
Star1 ---·
1'-Jf\>-1 \ Li \ 'l,
F1rnsh ,,. I -I \ '}}'/' / 1\ /. '-1-Js I) (,,, ' I / _,,
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Start -----
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Start
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Start
r. :", -<oL u. OG r \(.,. -..-I\ L), '",\ 0
\(~ ~ 6 :~,( (// t,,\ \' Finish ' . ... , "'' 1. ;;, .r,
SAMPLER Date/Time Received by (Sig.) Date/Time Hazards Associated wilh Sample Custody Seal ln1ac1 (C1rcia) t-'1 1LI\..),-! ~PITTLEl~v""'
' '"
YES NO NONE
Pri'\1,am~ ~9,b, ........... r.... " ,.,,_ . . ' fhJCaipt TAC __ _ _rno·1 Signature: 111:,.) ·:.-~. (._ __ l..-\. I" \,.-{;,._ ----·-.-. \ <,;Th.,_\<\ "" i: '
Aeli-is_hed bye-) Q_ (. 'ln \-Date/Time --4 Received by (Sig.) Date/Time
Roca~! p!I ____ ____ su
c,J V (_' • \__: I!©_ 1 l..(I I O',) ~ I Roceip1 TelllJ._~---__ ·c \. ----__ L,, /
Relinquished by (Sig.) I Date/Time .• Lab ~ycei~~Sig.) () ~-~ I/ Late/Time AoceNed on lee (Cude)
I 4--, . r , , f J.l .1] /i ' I ( I,\ '·) rYEs) NO ICE PACK -. . Whl1i r.Oflv· . mri1 .. ,·--. --.. I "•"-~ •··-'. " "---------------· ---. ---. -· -· -·-
USE BALL POINT PEN 0 1'lRESS HARD
CHAIN OF CUSTODY # 2 417 5
ClientNamo I\ (.-J ""',\ ... J\,c,
R rt" Adde epo mg ' ss
•-,\, ,J\, I ,-.:; (.
Attention \(, :-\\.. ' . <'I.'-r ,, \, ' '.,,.. ~
Telephone No. P.O. No.
Yr.--1L.. Sample ID (Location) TIME DATE
j a a m g , ~ ~ 0 u ~
SHEALY ENVIRONME~•--'... SERVICES, INC.
106 Vantage , J Drive
Cayce, South Carolina 29033
Telephone No. [phone] Fax No. [phone]
CHAIN OF CUSfODY RECORD
SAMP LEA NALYS SR I EQUIRED
--
1 ,
>
, ~ ,
! i ~ € C ~ ~ ~ c~ ~ .! ~ ' ~ ~ 0 ,;, 1\ !• ~ ' • f?" J ~8 s . i ' , . u < t: ' l ~ ~ ' g r a jg " 8 w 8i t u 0 w " z ~ ~ ·, a m ,. , " m ,, m u us ,,_ -. ( I S1art ~ £-ti rt. 15,'.. i)
' . ( ... P, : ;_l_ ~-~,[', • \ ' ,. ,,,
,_}, . \' Finish ' 50/J
·-----s, ..
. I/ ) \{,,;,·-y1,)L.l r13::i \ 'I \ ,' _,\,:_,, \, Fm1sh t'
' '
Start
Finish
Slart ·-
Finish
Start
Ftmsh
s,art
Fini$h .
5...,
,_
. ' .....
Finish
SAMPLE~ . . Date/Time Received by (Sig.) Date/Time ~A"''·" ~p.-rn .. en{>-<J~
P.rint_Name: p QJl--
'.11' ,,
-('.fl., -I . Sign~e: .__ J:} \1._t,j~ ·'.-{(:. I ,Uo ,;,: '----' .kn,_ 1...-: ,. .~• I '(!_
/\inqui~hed by (Sig~~/
1 U _ /qate/Time
1
/ _ Received by {Sig.) Date/Time
~f'Ol/1('•. ')i,;1 I 'lo l;-,/_L <, I
'Relinquished by (SiQ.) I Date/ 1 ime ..__.. -it-~•c~1by (Sig~ // .. t~teffi";e, : 1 / • ·---.. . ( 'f'L, ,, I'\.-' / I'/' rl ' , " -._, ------· --'-~ .. ·--•------·' -. -
NPDES # __________ _
County ____________ _
Receivi~g Stream ___________ .
Outfall No
+-PRESERVATION (CODE) LAB USE ONLY
CODE: A= None Program Are!'I fCTrCle}-, B = HNO3 OW ~ CWNNPDES C = H2S04
D = NaOH RCRA ·SP/SOL ... ---·--
SP/LIO Other· E = ICE -·-
)
F-~ \. \
SESI REMARKS LAB 1.0.
,-'J.,,. ,-;\/ , , Lr . 1) .. .. ! ...}
,·,, ') ,· ((' /'-J ~·) ., J( -
., -
--·
Hazards Associated with Sample Custody Seal ln!ac1 (Circl11)
YES NO NONE
RacePt me _.,,.,
R,o::;e{)t pll_. ____ '" -
Recep1 lelf1l. ____ -·c
Rocervecl on Ice (Cuc.ill!
/ Yf.S J,m ICE rACK - - - --
-- - - - ------ - - - - - -- -
\Nr PEN a ,PRESS HARD
,,\USTODY # 2 3 8 j_ 7
'St' \ \, \
SHEALY ENVIRONME~--'... SERVICES, INC.
106 Vantage a Drive
Cayce, South Carolina 29033
Telephone No. [phone] Fax No. (803) 791-91 t 1
.CHAIN OF CUSfODY RECORD
___ ol
NPDES # _______ _
County___ _ ___ _
Receiviny Stream _____ _
Reporting Address _______________ _ SAMPLE ANALYSIS REQUIRED
-,\, C ~ \,. ~, )j(_ ----I \ I\ <-PRESERVATION (CODE) LAB USE ONLY
\'c,<l\\ . ·6": ;\c.._,1..\c.. CODE: A::,: None Prog!am Ar·e;··(ci~Cre1--:-..._ Attention ;--B" HN03 , DW (-CWAINl'l)l:S _) " ~ i , C "H2S04 ' £ , i . RCnA -··sr,srn. -~--Telephone No. P.O. No. a ~ ,, !. j D "NaOH lj ~ ~ ' ' d ~ E" ICE SPILIO Ottier: ~ 0 1 ~ ' ,,
Vr_C\t,..,,, i~ '.'l ' I. i iC . Fa '·• I J a " m u < t· < ~, Sample JD (Location) TIME J a , < a ,. e 0 w • ~ g • e . . .. -DATE • a ~ r 0 ~ 8 e 8-6 z ] ~~ ; SESI ~ u " " m ,. m ,, m u e '. REMARKS LAG LO Star1 ,, ...
l. ' i I· 17 l(;~A.) V. '5 V ... t --, ·:;: / (" \-( Fm1sh
/\ '_) ,J I , . .
OullaU No
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i' .. Start, --:r "'i \" \· 17 \ ':._)":J._".• V . I ' -·1 I, : /
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I· \ I,. c··n·~.: y I ~ C ' :.J IC I \JJ \c,, \, ' Finish u ·-)
S<art
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C C --,, "2.i Start ,, 1-:l. ""7 ~ '.)_ )<. •' I. \'•,,:..-:, ) (r ' ()..._"\,,Je Finish /
(_ I ) ) ,_. -·
SAMPLER Date/Time Received by (Sig.) Date/Time Hazards Associa1cd with Sample --Cuslody Seal lniacl (Ci1cl11)
P,intName:~,-,, ~•-<'~O•' YES NO NONF.
\. '1.<f\J . I' _J Recef)t me ___ _lfl{l-'I Signature: ( ' /tf:~ c-5 C\ro::, -'1 •\ (., c..r.>cu•\• \ ,-1 ' ''I(,, RoceJ)I pH __ -----'" Relinquished by (Sig.) . Date/Time Received by (Sig.) Date/Time 0-c,...~ A.~" 1·9-'rb I IU3U I Roceipt TeJll). _____ '(;
Relinquished by (Sig.)' . Date/Time Lab Roceipl by {Sig.) Date/Time ~ --R&;;orvod un lc11 ;Cuclu) I -\. ~-( ' ·, I I' ) -;; It.' --; r:) (
..
YES' rl<1 ICE PA.CK ------. .. ..
USE BAU. POINT PEN m; ~ESS HARD
CHAIN OF CUSTODY # 2 3 818
Ghent Name ~.J_ ':)\, E ,Q._ \.J )i
SHEALY ENVIRONMEN-. SERVICES, INC.
106 Vantage~ Drive
Cayce, South Carolina 29033
Telephone No. [phone] Fax No. [phone]
CHAIN OF CUSfODY RECORD
__ 01 __
NPOES II _____________ _
County ___________ _
Receiving Stream __________ _
Reporting Address ______________ -~~~_;S~A~M~P~L::!E~A~N~A~L;_Y!:S~IS~R~E~Q~U;"'IR~E:'D~~-~~~------0::'.:ut_::la::'.ll~N::_:o:.=_===::;::=======.::.·..:.·_, -S\,d)\,,3 we. 1·
Attention _________________ _
Telephone No. ________ _
Sample ID (Location)
c z
i 2 ' Q P.O. No. ~ m m ; ] ' i4' ~ 0
y,.~ J 0 • m 0 < t: TIME :; , ~ l1 c u DATE • 0 0 -i 0 w 8 Q m ,
t • c
,!"~ i i! m
' ~ ~ ~, ~ e C c z 0 m
c , i j m
' ; ~ ' %! e
+-PRESERVATION (CODE)
CODE: A = None
Ba HN03
Ca H2S04
D a NaOH
E.a ICE
F"" I\ f. \
LAB USE ONLY
Prog,an} Afeatein:t!!)·---
OW '~CWNNPOf:S
ncRA SPisor-sr1uo Other ______ _ i s ~I § m u C) m m "' s,.., REMARKS SESI r-----------ta=---+--+-+--+--t-+-+-+-t--,-t-·1--1--l---Jf---l-t--t--l--l--t--,f--t-4-+--------------l-----"LA"-"'B.,_l.e,Dc_. ___ _
I· 17 t'.MO t.' '-\ \( Finish
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1-1 l 1"3'l..O X '-\ Fimsh
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I· I 7 ·,.,, (.I, 'i Finish
s,..,
finish
Start ,_
s,.,,
Finish
SAMPLER ·
Print Nam//?!' Ir ~ i·' , ~ 0 ·. ~ \ \ .J \ ·'--.) ,\.
Signature:/ /, /r'c< ,. =1 (.~ .;~ \. 11
Date/Time Received by (Sig.) Date/Time Hazards AssociaIed with Sample Cuslody Seal lnlacl {Ct1dt1)
YES NO NONE
1 \ Date/Time
I !i \"fl, I IO 30
Received by (Sig.) Date/Time
I
RocePt pH _____ ,,.
flocaJ)t lurrp. _________ ·c
Relinquished by (Sig.) Date/Time _Lab Receipt by (Sig}
I t·' ;., . _ 1 ·c ._ ----------·--~---- --Auetir,ed on lc,i (Circle)
,~ •• YF.S ) /Kl ICf' PACK - - -
--- -- ---·-- --- -- -
USE BALL POINT PEN , PRESS HARD SHEALY ENVIRONMF'. ,L SERVICES, INC.
CHAIN OF CUSTODY # 2 3 Li :2 Q
Client Name I-\· Ce.Q. -S\,j\,_._ _,
106 Vantag( 1te Drive
Cayce, South Carolina 29033
Telephone No, [phone] Fax No. [phone]
,,, __ ot ___ _
County _____________ _
CHAIN OF CUSTODY RECORD Receiving Slream_~---
Reporting Address______________ SAMPLE ANALYSIS REQUIRED Oullall No ----------~ \ \' \ ,-,--,---,--,,--,-,-::-[:"-,-,-,--,,-,---,-,,-,--,----------,,----------J '· <.• '\) ~ ),_) (. +-PRESERVA110N (COOE) LAB USE ONLY
\( '\,(. CODE: A= None Program Area (Circle) ~c~., \c. Attention · '·' . ·' -~ B, HN03 DW CW/vNl'llES
C = H2S04 11CRA SP1SOL
.. ,. k i ~
Sample ID (Location)
" P.O. No. ~ w ~
' ' 0 6 C !' '.'l '°I (,, ~ 0 " m 0 ~ t: ,Yr. ~ :, , ~ u 0 u TIME DATE w 0 0 w
Telephone No. ________ _
,.
<j ~ g
w !. C ' ~? " X ~ ~ e w c 8< z
g
w
' • ? e C ~ . ' 0
D, NaOH
E, ICE F - . \( I
SPtllO 01her
5l t it 2 ~ u • u " m , m ,, c m ' ,.
Star1
REMARKS SESI ;;---+---+-+-+='+-+-+-t-+-++-l-+-++---lf-+-+-+-f-l-+-+-+-++----------------1----"LA<;S>B_,_l."Dc_. _____ ...
\-I"\ I\ 'l'\
F)nist,
X ;). \
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I. \~ \\':,\ l'.
F1n1sh
Start .
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Finish
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Fm,sh (. l •' I /( ' / . I) I , ' '
Slart ----· -.
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I ' I I I \ / , . (\ '
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SAMPLER Date/Time Received by (Sig.) Date/Time I lazards Associated with Sample
Print Name:(L·.\, :, ,"') \ \, "-,0 ~
Signature: (/ ,,1:/. I · .tI~~._...__
Date/Time Received by (Sig.)
1-/'/Srll/6l n ,.
Reilnquished by (Sig.) ' l Dale/Time La6peceipl by (Sig.) -·~1
...,_~~-~~-,--,---~..L...-. -. ~.--11~.--__ .L-J,1~" \J-,, -~ C 1 , Wh,,. ,-;.,..,. "-"R••"''"'
Date/Tirne
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Cuslody S11al ln1ac1 (Cn;le)
YES NO NONE
Roceipt pH__ ____ _ ~u
Rec11Pt lorfll. ___ . ·C
Roct1iv11d on Ice (Cuc.Ju)
YES NO !CE PACK
JRIIOU.l'ONTPI LY.PReaatw.:t
:; •· .· .: . ::. ' . ;·.·_,:.-' • · •..• ·-1 .:j ..
CHAIN OF CUSTODY •i:<:23816' ;; .
i·· L: -.;County ___ ,"-.-'----~------
;:tnt:IU.T t:NVIHUNMl:1 'L :;1::H~K;~, IN\;.
· · , · ,. 108 Vantage .... lie Drive " : · .: .
. . ·. · ·· ·: cayce, South Cerolna 29033 ·1 ,: · : .
. 'Telephone No, [phone] :'Fu HD. [phone] . ' . . .. •.. ,•. ..,_.. .
NPOESI_....,.. ________ _
~-· 1-t.: c~~~\e.' ·~ :s, .. ~~~·
~~~ .. . , .. 'i,. CHAIN::oF CUSTODY RECORD.:-. .-;;.:':Aeo,M,gS-____ _
SAMPLE ANALYSIS REQUIRED , '·. · Outfall No. _________ _
u: '-;3\,.e,0\;__ . • uC .
1nen11on . le.J4~:.. ,~, F,,{.. \i ; : · :
r~l'IO .. ___ · _·_· ....,. __ P.o.~:f<"''. f (:;I J ( · f ;
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.....
.....
.....
.. PRESERVATION !C()nA
REMARKS
'•/
LAB USE ONLY
Proyfani Aru (Cirde)
' .·r:1# _ CWWPUES
: ACRA . . SP,Sct. (D
·5p,i_,o ·°"'"''--
~cSI
l)\81.D.
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~ _________ J __ ~L-Dal.LlefflmeL.J._J_.LJ,....Receivecl.L.L_--1.b_yLfSig~.L.I_J·LJLJ_J_J_J__J_,L-L--,°""""1meL..1=-LJLJ--,----:--:--_..--:-:.-;;.,--:-••l-=.,,-;; . .,:cs;:m=n-::plo~--'--,--;:o:::-=..,.=.._,=;;:,c:::.,..~l-j
.--t YES NO NONE
K,w; ::~.: ~: .. ~,-J.\-}_'.''>O,_': . ·. I • • . / / . . , . . .
---·--· (_j{..._ _..J.-.. _ \-\°J'lol ,ioo •...__e. · if ·· · -· · · ,-,,.9.., 1100
IL by ) Dv,to'Tlme by {Sig) . / I · DolorTime · 0, .• J., 'f'9:--f 11-wt. I /11,:-•--,._\ r; /fil• •· 1-n.'n.J i11<':
/~ by (Sig.) Detefrome Lob -i,,, (Sig.) -Dal&'Tlme
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_,.., ____ ... _, ____ -c
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VE:9 NO ICI: PACK
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er: J· L> ,-
--------------------
- --- -- - -------- -- - -
~INOFCUSTC.-i # 23757
• Name ll C~l 0i h<lln 7':j.1-----
-irtnu~-------------
0
LL
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;s ho 'i ~ IJ c..,
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--.No. P.O."°·
v,. IS_'l_l_.. i J ~ a Sample 10 (l.ocation) DATE TIME 8"' ....
l\.::TT\N 1nv
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K
s,.., , .. = .... llJv
}~ F""inilto ,, .,_,
/ lr..J:i. I / '}:;-if -re I ,~ .. .)(
S1"1
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flniah -...... ....
......
1'IPLER Da141/Time
J~ATT LEP.,A.....,._
tl ~--• v.-~ ......... .;Ji:,,-l'lJ , :,i):,
OatafT-.me
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~ •
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•,qulshod by (SliJ.) Date'Time
I .--. . .. . ·• .
1 uu v am age t"01n1e unve .
Cayea, South Ca 1 29033 NPOESI _______ _
Telephone No, [phone] , ax No. [phone] County _ __:c_ _________ _
CHAIN OF CUSTODY RECORD Receiving Strewn ____ _
SAMPLE ANALYSIS REQUIRED -
Outfall No. ___ _
<!-.. PRESERVATION (CODE) LAB USE ONLY --------·-. -. . ---------·-·----COOE: A • Nona < Program Araa iCircle)
~ J B • HN03 ow CWMIPOES ~ j ~ C •H2S04 SP1SQ I l j i l 0-NaOH RCRA (j· .~ p ? ! SJ.'ILIO umer: ' ., E·-1ce ----
X Ji I ' h
., l I { ll ' 1 f F• t ~ h ---· ~ ·• • -I SESI i ~ t; ~, {! .ll REMARKS , 6 LAB I.U. . ..
,..
f
¥-
-
.
----~-
.
--------·----· -.
•
----
-eiwdby(Sig.) Oate/Tme Harards Anociatad WWI Sample CUIIOCIJ,-.lnYatC~1191
' YES NO NONE
~--l::., __ / '1~ -TRC _____ .~_"91
r, • .;_c;;.( . 1>--u) -... " -r ~co,,,v' Oateffime ---__ -c
/_/(...<;~ J'J/', ~1.,,..,._
I.ab Rauo;p< by ('-9.) DatafTlme Rilolh-ed on Ice (Cl,c!e,I
I YES NO ICI::: PACII: ----------·---.. . . .. --_, --111k ' "" P Cop)' po.,
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Attachment 3
QA Summary Report and Analytical Data for the
April 15-16, 1995 Sampling Event
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SDG Narrative:
PROJECT DAT A ASSESSMENT
Hoechst Celanese -Shelby, NC
Second Ouaner 1996 Sampling Event
This report summarizes the assessment of field and laboratory data generated from the April 1996
sampling event at the Hoechst Celanese -Shelby, North Carolina plant The sampling and analysis
was conducted by Shealy Environmental Services, Inc. (SESI) according to the revised Samplin~
and Analysis Plan (document control nos. 026SB-0005a and 026SB-0038). All analyses were
performed according to Test MethQds for Evaluating Solid Waste, Physical/Chemical Methods
(including Updates I, IIA and IIB) and EPA 600/4-79-020 Methajs for Chemical Analysis of
Water and Wastes. USEPA March 1993 for the following parameters:
1. pH by EPA Method 150.1, Temperature by EPA Method 170.1 and Conductivity by EPA
Method 120.1 (field analyzed and documented in the Field Log)
2. Total Organic Carbon (fOC) by EPA Method 415.1
3. Volatile Organic Compounds (VOCs) by EPA 8260A
4. Ethylene Glycol by EPA Method 8015A (modified)
Definitions:
□as-sAData:
C)ass B Data:
QassCData:
Data QnaUfiey U:
Data Qualifier R;
useable for quantitative purposes
useable for qualitative assessrnen• of absences or presence
unusable data
the analyte was not detected at the reported ,.;oncentration due ID its presence
in the associated method blank
the sample results are rejected due ID serious deficiencies in the ability to
analyze the sample and meet quality control criteria.
1
Data Quality Assessment:
Pan One: Field Sampling and Handling:
Ground water samples from the monitoring wells, domestic wells and process points were
collected according to their specific sampling procedures. The pH, temperature and conductivity
measurements were taken by SESI personnel and documented in the Field Log Book. The data
indicates that stability of the parameters were generally achieved after purging three well volumes,
where applicable.
• All samples were collected according to the Sampling and Analysis Plan matrix. All field
measurements were documented in the Field Log Book.
• All necessary field QNQC samples were collected at an acceptable frequency with the
exception of TOC duplicates which were not collected. Although not a method requirement,
field duplicates are recommended due to the project DQOs.
• All sample related information was documented on the Chain-of-Custody (COC) forms with
the following exceptions:
1. The COC did not contain client's address or the project manager's telephone
number.
Note: This deficiency did not evmprnmise the quality of the analytical data.
Pan Two: T abora1Pty Analysis;
Total Organic Carbon by EPA Method 41S.1
Two process point and two monitoring well samples were collected and analyzed for Total Organic
Carbon. All method acceptance criteria were met (Class A).
Volatile Organic Compounds by EPA Method 8260A
Two process points and one domestic supply well were collected and analyzed for VOCs. All
method acceptance criteria were met (Class A) with the following exception:
• Acetone was detected at 46.6 µg/L and 2-butanone at 13.2 µg/L in the Field Blank. However,
the associated samples did not require data nags based on their reponed
concentrations for these compounds.
HCC-Shelby Q2 1996 2
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....
Pan Two; Laboratory Analysjs<cont};
Ethylene Glycol by EPA Method 8015A (modified)
Two process points were collected and analyzed for ethylene glycol using a modified version of
Method 8015A. All method acceptance criteria were met (Oass A).
Discussion:
For the DQOs of this project (level m to be met, the data was assessed based on XCl)Orted method
non-conformances and the following overall project criteria:
• holding times
• blank cnntaminarion
• completeness
• transcription accuracy
• repon qualifiers • comparability/consistency with historical data
Based on this model, all the data associated with the samples in this data package were assessed as
Class A data.
HCC-Shelby Q2 1996 3
D
HOECHST CELANESE
Shelby, NC
ANALYTICAL DATA PACKAGE
Second Quarter 1996
Data package provided by:
SHEALY ENVIRONMENTAL SERVICES, INC.
106 Vantage Point Drive
Overlook Business Center
Cayce, SC 29033
[phone]
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TABLE OF CONTENTS
I. Master Tracking List
II. _Sample Results
(By analytical test method)
m. Method Conformance Summary
IV. Field Data Summary
V. Chain of Custody Records
-------------------
Client Sample
Identification
ITCI
ITEF
RUNYANS
K-28
V-23
Master Tracking List
HOECHST CELANESE-Shelby
Second Quarter 1996
SHEALY Lab Date
ID Number Collected
Ground-Water
87618N 04/15/96
87619N 04/15/96
87622N 04/15/96
87620N 04/15/96
87621N 04/15/96
Date
Received
04/16/96
04/16/96
04/16/96
04/16/96
04/16/96
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I SAMPLE RESULTS
I · Total Organic Carbon (TOC)
I Method 415.1
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-------------------
Client Sample
Identification
ITCI
ITEF
K-28
V-23
Master Tracking List -roe
HOECHST CELANESE-Shelby
Second Quarter 1996
SHEALY Lab Date Date
ID Number Collected Received
87618N 04/15/96 04/16/96
87619N 04/15/96 04/16/96
87620N 04/15/96 04/16/96
87621N 04/15/96 04/16/96
Analysis
Date
04/24/96
04/24/96
04/24/96
04/24/96
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I 106 VANTAGE POINT DRIVE
;AYCE, SOUTH CAROLINA 29033
I SC DHEC No. 32010
Client:
I Attention:
I SHEALY Lab No, 87618N
Description: ITCI
Date Received: 04/16/96 I Date Reported, 04/29/96
I Parameters
INORGANICS I total organic carbon
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SHEALY ENVIRONMENTAL SERVICES, INC.
Scientists and Consultants
CERTIFICATE OF ANALYSIS
HOECHST CELANESE-SHELBY PLANT P.O. Box 87 Shelby, NC 28151-0087
Kathryn Frank
[phone]
FAX [phone]
NC DEHNR No. 329
Coll. Date: 04/15/96
Coll. Time: 1035
QA/QC Officer
V.P. Analytical
Date Date
Method Result Units POL Prepared Analyzed Anal.
415,1 1600 mg/l 1.0 04/24/96 JYR
Terms and Conditions on Reverse Side
106 VANTAGE POINT DRIVE
;AYCE, SOUTH CAROLINA 29033
SC DHEC No. 32010
Client:
A'ttention:
SHEALY Lab No, 87619N
Description: ITBP
Date Received: 04/16/96
Date Reported: 04/26/96
Parameters
SHEALY ENVIRONMENTAL SERVICES, INC. I
Scientists and Consultants
CERTIFICATE OF ANALYSIS
HOECHST CELANESE-SHELBY PLANT P.O. Box 87
Shelby, NC 28151-0087
Kathryn Frank
[phone]
FAX [phone]
I
NC DEHNR No. 3291
I
Coll. Date: 04/15/96 I
Coll. Time: 1040
QA/QC Officer ~qet/ I
V.P. Analytical-"!..!!"-"~----
Date Date
Method Result Units PQL Prepared Analyzed Anal. I ----------------------------------------INORGANICS
total organic carbon 415 .1 31 mg/1
Terms and Conditions on Reverse Side
1.0 04/24/96 JYR I
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106 VANTAGE POINT DRIVE
;AYCE, SOUTH CAROLINA 29033
SC DHEC No. 32010
Client:
Attention:
I SHEALY Lab No, 87620N
Description: K-28
Date Received: 04/16/96 I Dato Reported, 04/25/96
I Parameters
INORGANICS I total organic carbon
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SHEALY ENVIRONMENTAL SERVICES, INC.
Scientists and Consultants
[phone]
CERTIFICATE OF ANALYSIS FAX [phone]
HOECHST CELANESE-SHELBY PLANT P.O. Box 87 Shelby, NC 28151-0087
Kathryn Frank
Method Result Units PQL
415.1 40 mg/1 1.0
Terms and Conditions on Reverse Side
NC DEHNR No. 329
Coll. Date: 04/15/96
Coll. Time: 1620
QA/QC Officer
V.P. Analytical
Date Date
Prepared Analyzed Anal.
04/24/96 JYR
106 VANTAGE POINT DRIVE
:AYCE. SOUTH CAROLINA 29033
SC DHEC No. 32010
Client:
Attention:
SHEALY Lab No, 87621N
Description: V-23
Date Received: 04/16/96
Date Reported: 04/25/96
Parameters
SHEALY ENVIRONMENTAL SERVICES, INC. I
Scientists and Consultants
CERTIFICATE OF ANALYSIS
HOECHST CELANESE-SHELBY PLANT P.O. Box 87 Shelby, NC 28151-0087
Kathryn Frank
Method Result Units PQL
[phone]
FAX [phone]
I
NC DEHNR No. 329 I
I
Coll. Date: 04/15/96 I
Coll. Time: 1645
QA/QC Officer f}~&c--:
V.P. Analytical /,1 I
Date Date
Prepared Analyzed Anal. --------------------------------------------------I
INORGANICS
total organic carbon 415.1 6100
Terms and Conditions on Reverse Side
l.O 04/24/96 JYR I
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I 106 VANTAGE POINT DRIVE
:AYCE. SOUTH CAROLINA 29033
I SC DHEC No. 32 010
Client:
I Attention:
I SHEALY Lab No, 87623N
Description: Field Blank (e)
Date Received: 04/16/96 I Date Reported, 04/26/96
I Parameters
INORGANICS I total organic carbon
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SHEALY ENVIRONMENTAL SERVICES, INC.
Scientists and Consultants
CERTIFICATE OF ANALYSIS
HOECHST CELANESE-SHELBY PLANT P.O. Box 87 Shelby, NC 28151-0087
Kathryn Frank
(803) 791 ·9700
FAX (803) 791·9111
NC DEHNR No. 329
Coll.
Coll,
QA/QC Officer
V. P. Analytical
Date Date
Date: 04/15/96
Time: 1600
~;rlr
Method Result Units PQL Prepared Analyzed Anal.
415.l 1.0 mg/1 1.0 04/24/96 JYR
Terms and Conditions on Reverse Side
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I SAMPLE RESULTS
I
-I Ethylene Glycol
I Method 8015A
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-------------------
Client Sample
Identification
ITCI
ITEF
Master Tracking List -Ethylene Glycol
HOECllST CELANESE-Shelby
Second Quarter 1996
SHEALY Lab Date· Date
ID Number Collected Received
87618N 04/15/96 04/16/96
87619N 04/15/96 04/16/96
Prep. Analysis
Date Date
04/22/96 04/22/96
04/22/96 04/22/96
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106 VANTAGE.POINT DRIVE
CAYCE, SOUTH CAROLINA 29033
SC DHEC No. 32010
Client:
Attention:
SHEALY Lab No, 87618N
Description: ITCI
Date Received: 04/16/96
Date Reported: 04/29/95
Parameters
ethylene glycol
SHEALY ENVIRONMENTAL SERVICES, INC.
Scientists and Consultants
CERTIFICATE OF ANALYSIS
HOECHST CELANESE-SHELBY PLANT
P.O. Box 87
Shelby, NC 28151-0087
Kathryn Frank
[phone]
FAX [phone]
NC DEHNR No. 329
Coll. Date: 04/15/96
Coll. Time: 1035
9rAD/JOJ/
V.P. Analytical _..J/Y\c:..,,:~:._ __ _
QA/QC Officer
Date Date
Method Result Units POL Prepared Analyzed Anal.
8015A 1070 mg/1 6.5 04/22/96 04/22/96 SAG
Terms and Conditions on Reverse Side
. 06 VANTAGE POINT DRIVE
,AYCE. SOUTH CAROLINA 29033
SC DHEC No. 32010
Client:
Attention:
SHEALY Lab No, 87619N
Description: ITEF
Date Received: 04/16/96
Date Reported: 04/26/96
Parameters
ethylene glycol
SHEALY ENVIRONMENTAL SERVICES, INC. I
Scientists and Consultants
CERTIFICATE OF ANALYSIS
HOECHST CELANESE-SHELBY PLANT P.O. Box 87
Shelby, NC 28151-0087
Kathryn Frank
[phone]
FAX [phone]
I
NC DEHNR No. 329 I
I
Coll. Date: 04/15/96 I
Coll. Time: 1040
QA/QC Officer ~d QV
V.P. Analytical Mp I
Date Date
Method Result Units PQL Prepared Analyzed Anal. I
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8015A ND mg/1 6.5 04/22/96 04/22/96 SAG
Terms and Conditions on Reverse Side
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106 VANTAGE POINT DRIVE
CAYCE. SOUTH CAROLINA 29033
SC DHEC No. 32010
Client:
Attention:
SHEALY Lab No, 87623N
Description: Field Blank (e)
Date Received: 04/16/96
Date Reported: 04/26/96
Parameters
ethylene glycol
SHEALY ENVIRONMENTAL SERVICES, INC.
Scientists and Consultants
CERTIFICATE OF ANALYSIS
HOECHST CELANESE-SHELBY PLANT
P.O. Box 87
Shelby, NC 28151-0087
Kathryn Frank
[phone]
FAX [phone]
NC DEHNR No. 329
Coll. Date: 04/15/96
Coll. Time: 1600
fJl1J. )oA,;
V. p. Analytical _.,rn"-'.,!P..:_ __ _
QA/QC Officer
Date Date
Method Result Units PQL Prepared Analyzed Anal.
8015A ND mg/1 6,5 04/22/96 04/22/96 SAG
Terms and Conditions on Reverse Side
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I SAMPLE RESULTS
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I TCL Volatiles
I Method 8260A
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- - - - - - - - - - - - - - --· - - -
Client Sample
I dent ificat ion
ITCI
ITEF
RUNYANS
Master Tracking List -TCL VOCs
lIOECHST CELANESE-Shelby
Second Quarter 1996
SHEALY Lab Date Date
ID Number Collected Received
87618N 04/15/96 04/16/96
87619N 04/ 15/96 04/16/96
87622N 04/15/96 04/16/96
Analysis
Date
04/27/96
04/16/96
04/27/96
I
I I 06 VANTAGE POINT DRIVE
;AYCE. SOUTH CAROLINA 29033
I SC DHEC No. 32010
Client:
I Attention:
I SHEALY Lab No, 87618N
Description: ITCI
Date Received: 04/16/96 I Date Reported, 04/29/96
I Parameters
I VOLATILE ORGANICS
acetone
benzene
bromodichlorometh~ne
bromoform. I bromomethane
2-butanone
carbon disulfide
carbon tetrachloride
I ·orobenzene
Jroethane
-... .. .:.oroform
chloromethane
I dibromochlorometha.ne
1,1-dichloroethane
1,2-dichloroethane
1,1-dichloroethene
cia-1,2-dichloroethene
I ~rans-1,2-dichloroethene
1,2-dichloropropane
cis-1,3-dichloropropene
trans-1,3-dichloropropene
ethylbenzene 12 • hexanone
~ethylene chloride
4-methyl-2-pentanone
styrene
11, 1, 2, 2-tet::-achloroethane
tetrachlo::-oethene
coluene
1, 1,1-trichloroethane
11, 1, 2 -trichlor~ethane
t.richloroethene
vinyl acetate
vinyl chloride I xylenes
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SHEALY ENVIRONMENTAL SERVICES, INC.
Scientists and Consultants
CERTIFICATE OF ANALYSIS
HOECHST CELANESE-SHELBY PLANT P.O. Box 87 Shelby, NC 28151-0087
Kathryn Frank
[phone]
FAX [phone]
NC DEHNR No. 329
Coll. Date: 04/15/96
Coll. Time: 1035
9ttJJ/ky
V.P. Analytical -~/\1~~~'----
QA/QC Officer
Date Date
Method Result Units PQL Prepared Analyzed Anal.
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
0.6450
0.0585
ND
ND
ND
0. 5370
0.0121
ND
0. 0411
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
0.1930
ND
ND
ND
ND
ND
ND
ND
ND
. ND
ND
ND
ND
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1.
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
Terms and Conditions on Reverse Siae
04/27/96 SAG
0.0200
0.0050
0.0050
0.0050
0.0100
0.0050
0.0050
0.0050
0.0050
0.0100
0.0050
0.0100
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0. 0050
0.0050
C.0050
0.0050
0.0100
0.0150
I 06 VANTAGE POINT DRIVE
~AYCE, SOUTH CAROLINA 29033
SC DHEC No. 32010
Client:
Attention:
SHEALY Lab No, 87619N
Description: ITEF
Date Received: 04/16/96
Date Reported: 04/26/96
Parameters
VOLATILE ORGANICS
acetone
benzene
bromodichloromethane
bromoform
bromomethane
2-butanone
carbon disulfide
carbon tetrachloride
orobenzene
;,roe thane
-.. .. .Lorofor:n
chloromethane
dibromochloromethane
1,1-dichloroethane
1,2-dichloroethane
1,1-dichloroethene
cia-1,2-dichloroethene
~rans-1,2-dichloroethene
~,2-dichloropropane
~ia-1,3-dichloropropene
:rana-1,3-dichloropropene
-!thylbenzene
2-hexanone
-:i.ethylene chloride
t-~ethyl-2-pentanone
.J -:yrene
~,1,2,2-tetrachloroethane
:etrachloroethene
c.oluene
1,1,1-trichloroethane
1,1,2-trichloroethane
trichloroethene
vinyl acetate
vinyl chloride
xylenes
SHEALY ENVIRONMENTAL SERVICES, INC. I
Scientists and Consultants
CERTIFICATE OF ANALYSIS
HOECHST CELANESE-SHELBY PLANT P.O. Box 87
Shelby, NC 28151-0087
Kathryn Frank
Method Result Units PQL
8260A ND mg/1 0.0200
8260A ND mg/1 0.0050
8260A ND mg/1 0.0050
8260A ND mg/1 0.0050
8260A ND mg/1 0.0100
8260A ND mg/1 0.0050
8260A ND mg/1 0.0050
8260A ND mg/1 o.o·oso
8260A ND mg/1 0.0050
8260A ND :ng/1 0.0100
8260A ND mg/1 0.0050
8260.i\ ND mg/1 0.0100
8260.i\ ND mg/1 0.0050
8260A ND mg/1 0.0050
8260A ND mg/1 0.0050
8260A ND mg/1 0.0050
8260.i\ ND mg/1 0.0050
8260A ND mg/1 0.0050
8260A ND mg/1 0.0050
8260A ND mg/1 0.0050
8260A ND mg/1 0.0050
8260.i\ ND mg/1 0.0050
8260A ND mg/1 0.0050
8260A ND mg/1 0.0050
8260A ND mg/1 0.0050
8260A ND mg/1 0.0050
8260A ND mg/1 0.0050
8260A ND mg/1 0.0050
8260A ND mg/1 0.0050
8260A ND mg/1 0.0050
8260A ND mg/1 0.0050
8260A ND mg/1 C.0050
8260A ND mg/1 0.0050
8260A ND mg/1 0.0100
8260A ND mg/1 0.0150
Terms and Conditions on Reverse Side
[phone]
FAX [phone]
NC DEHNR No. 329
Coll. Date: 04/15/96
Coll. Time: 1040
I
I
I
I
'9,2(D acv 1.
V.P. Analytical _ _,,1,1=~'-----
QA/QC Officer
Date Date
Prepared Analyzed Anal. I
04/16/96 SAG I
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106 VANTAGE POINT DRIVE
CAYCE. SOUTH CAROLIN1\ 29033
SC DHEC No. 32010
Client:
Attention:
I SHEALY Lab No, 87622N
Description: Runyans
Date Received:
I Date Reported:
04/16/96
04/29/96
I Para:neters
I
I
VOLATILE ORGANICS
acetone
benzene
bromodichloromethane
bromoform
bromomethane
2-butanone
carbon disulfide
carbon tetrachloride
I · lorobenzene
oroethane
... loroform
chloromethane
I dibromochloromethane
l,l-dichloroethane
1,2-dichloroethane
l,l-dichloroethene
cis-1,2-dichloroethene
I trans-1,2-dichloroethene
1,2-dichloropropane
cis-1,J-dichloropropene
trana-1,3-dichloropropene
I ethylbenzene
2-hexanone
~ec~ylene chloride
4-methyl-2-pentanone
sty=-ene
I 1,1,2,2-tet=-achloroethane
tet::-achloroethene
toluene
I
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I
I
I
1,1,1-t::-ichloroethane
1,1,2-t=-ichloroethane
t::-ichloroethene
•✓inyl acetate
vinyl chloride
xylenes
SHEALY ENVIRONMENTAL SERVICES, INC.
Scientists and Consultants
CERTIFICATE OF ANALYSIS
HOECHST CELANESE-SHELBY PLANT
P.O. Box 87
Shelby, NC 28151-0087
Kathryn Frank
(803) 79i-9700
FAX [phone]
NC DEHNR No. 329
Coll. Date: 04/15/96
Coll. Time: 1728
QA/QC Officer CMD :£CL
'./ --}i,i V.P. Analytical __ &~1P_....-___ _
Date Date
Method Result Units PQL Prepared Analyzed Anal.
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8250A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
Terms ana Conditions on Reverse Side
04/27/96 SAG
0.0200
0.0050
0.0050
0.0050
0.0100
0.0050
0.0050
0.0050
0.0050
0.0100
0.0050
0.0100
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
C.0050
0.0050
0.0100
0.0150
· 06 VANTAGE POINT DRIVE
;AYCE, SOUTH CAROLINA 29033
SHEALY ENVIRONMENTAL SERVICES, INC.
Scientists and Consultants
CERTIFICATE OF ANALYSIS
[phone]
FAX (803) 79i-911i
I
I
SC DHEC No. 32010 NC DEHNR No. 329 I
Client:
Attention:
SHEALY Lab No, 87623N
Description: Field Blank (e)
Date Received: 04/16/96
Dace Reported: 04/26/96
Parameters
VOLATILE ORGANICS
acetone
benzene
bromodichloromethane
bromoform
bromomethane
2-butanone
carbon disulfide
carbon tetrachloride
,robenzene
Jroethane
cnlorofor:n
chloromethane
dibromochloromethane
1,1-dichloroethanc
1,2-dichloroethane
1,1-dichloroethene
cis-1,2-dichloroethene
~rans-1,2-dichloroethene
l,2-dichloropropane
cis-1,3-dichloropropene
t=ans-1, 3-dichloropropene
ethylbenzene
2-hexanone
methylene chloride
4-methyl-2-pentanone
scyrene
l, 1,2,2-tetrachloroethane
~etrachloroethene
~oluene
1, 1,1-trichloroethane
1,1,2-trichloroethane
trichloroethene
vinyl acetate
vinyl chloride
xylenes
HOECHST CELANESE-SHELBY PLAN'I' P.O. Box 87
Shelby, NC 28151-0087
Kathryn Frank
Method
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
Result
0.0465
ND
ND
ND
ND
0.0132
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Units
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
Terms and Conditions on Reverse Side
PQL
0.0200
0.0050
0.0050
0.0050
0.0100
0.0050
0.0050
0.0050
0.0050
0.0100
0.0050
0.0100
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0100
0.0150
I
Coll. Date: 04/15/96 I
Coll. Time: 1600
QA/QC Officer
V.P. Analytical
Date Date
Prepared Analyzed
04/16/96
Anal. I
SAG
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.06 VANTAGE POINT DRIVE
~AYCE. SOUTH CAROLINA 29033
SC DHEC No. 32010
Client:
Attention:
I SHEALY Lab No, 87624NTB
Description: Trip Blank (c)
Date Received: 04/16/96 I Date Reported, 04/26/96
I Parameters
I VOLATILE ORGANICS
acetone
benzene
bromodichloromethane
I bromoform
bromomethane
2-butanone
carbon disulfide
carbon tetrachloride
I -"-lorobenzene
:::-roe thane
. .:.oroform
chloromethane
I dibromochloromethane
1,1-dichloroethane
1,2-dichloroethane
l,l-dichloroethene
cis-1,2-dichloroet~ene
I trans-1,2-dichloroethene
1,2-dichloropropane
cis-1,3-dichloropropene
trans-1,3-dichloropropene
I ethylbenzene
2-hexanone
~ethylene chloride
4-methyl-2-pentanone
styrene
I 1,1,2,2-tetrachloroethane
tetrachloroethene
toluene
l,l,1-trichloroethane
I l,_ 1,2-trichloroethane
':::-ichloroethene
"✓1.nyl acetate
vi:1yl chloride I xylenes
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SHEALY ENVIRONMENTAL SERVICES, INC.
Scientists and Consultants
CERTIFICATE OF ANALYSIS
HOECHST CELANESE-SHELBY PLANT
P.O. Box 87
Shelby, NC 28151-0087
Kathryn Frank
Method
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
8260A
Result
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Units
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
Terms and Conditions on Reverse Side
PQL
0.0200
0.0050
0.0050
0.0050
0.0100
0.0050
0.0050
0.0050
0.0050
0.0100
0.0050
0.0100
0.0050
0.0050
0.0050
0.0050
0.0050
0,0050
0.0050
0,0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0,0050
0.0050
0.0050
0.0050
0.0100
0,0150
QA/QC
(803} 791 ·9i'0,J
FAX [phone]'
NC DEHNR No. 329
Coll. Date: 04/15/%
Coll. Time: 1330
Officer O~o I ov
V.P. Analytical </ frlp
Date Date
Prepared Analyzed Anal.
04/16/96 SAG
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Method Conformance Summary
"6'7bliN -rhr='.iL, &'7(,J'-l NTG
Criteria Volatiles Semi, ol,~tiles IF-tt-r (~ ( ~,. ·, r
Sample Holding Time -~ ✓
Standards Preparation ✓ ✓
Instrument Tuning ./ N f\
Instrument Calibration / ,/
Calibration Verification ✓ ✓
Degradation Check rJ Pr tJA
Interference Sample/Standard tJA tJ ('t
Blank Results ✓ ✓
Method Accuracy ✓ /
Method Precision ✓ ✓
Surrogate Recovery ✓ NA
PDS/SD/MSA + ++-
TCLP Prep NA NA
Key: ✓ = Method Criteria Met
NI A = Not Applicable
* = Method Criteria Not Met -see footnote(s)
~'lt
PDS = Post Digestion Spike
SD = Serial Dilution
MSA = Method of Standard Additions
--r 0 (_
~7G1'i,'N I . I '1 cl
~ 7· L: i cl N I ', 1
~7 L,20 N I . 'i
"-57G'21N I :qc,9
<;;ll,L2,i~ No ci', \v+·,o.,
+
+ -t-
Metals
rJ It
tJ /t
f'IA
A.JA
NA-
N/r
NI+
Nit
rJA
tJA
NA
NA
HA
Vu/,../-, I~_,
1'71,,1::;rJ
E+L1 le • .,_
1'1 6/Z N
Inorganics
✓
✓
NI\
✓
✓
NA
NA
✓
✓
✓
NA
*·~
NA
I: 9 D./,/-,c,
117 (o I
I ; '1 f).l.f,v;._
-------------------
Monitoring
Location
ITCI
ITEF
K-28
V-23
Runyans
Hoechst Celanese-Shelby, NC
Water Level Measurements
Page: lJ!Ll.
Measured by: CWH. MPO. MVC, SWC
Date Measuring Depth to Water Temperature
Point Water Level (OC)
Elevation (ft) Elevation
(ft, msl} (ft, msl)
04/15196 NIA NIA NIA 24.6
04/15196 NIA NIA NIA 24.2
04115196 811.20 11.09 800.11 17.5
04/15196 8 I 1.89 10.20 801.69 17.6 .
04/15196 NIA NIA NIA 16.8
Measurement Device: Electronic Water Level Indicator
pH Specific Comments
(SU) Conductivity
(umhoslcm)
5.37 1720 Flow rate at sampling = 1/2 L
per minute
8.14 3260 voe collected, but sample was
saturated with air.
6.71 175
5.24 3500
7.81 472 Private well I Purge 0ow rate
= 2 GPM
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(',;,c,· Date: 1 J (-1 " 1 le
floechst Celanese -Shelby, NC
\Vater Level J\'Ieasurements
Page:_!_ of_±
l\,leasured by: MPQ, N\v'C., Cc0L+ ,, s,0'--Measurement Device: Electronic Water Level Indicator
lHonitoring Measuring Depth to \Vater Level Comments
Location Point \Vater Elevation
Elevation (ft) (ft,msl)
(Wms!)
A-39 823.36 9. 5lo S\'-\. c, l•JQ...IJ_ w ~ 26 ,-j__
B-34 790.62 I) 9-") "l't '}. i. 9 WLll . z.c I l.AJ• -,.,-....,1
C-49 864.11 I). I ). SS'I .9'1 , .. ,lQ. u.,; zc, ni
D-27 845.50 15.c9 3 7-:, c:. • L.\ \ (;Jt..\.\ cc.· u.,J
D-35 845.69 15.lt8 8~C:-:LI . Lc,Ll~ I l _-Z..Ctrt.l
D-56 845.19 \·5'.\0 'o "3~. c9 ,.., l1 ,
W~7.r•.("-'1
D-88 845.52 15'.50 s·.s·v .0 2 L...l<L~l (...)iz_c,,J
F-55 849. 19 Sl. C'-1 -:+91 i'5 Cs0n~k~I.-Pvf'l",e
G-50 848.48 -,sq. oe. coo:,, -4L) ·7-:,c.: lo...-
G-88 848.26 t..1c,c13 So"' 'SS ( Lll . ··o ,..-J
H-59 845.25 -42. cw 7 ', \,_, "3 ':;, oc.: Iv·
H-79 846.53 -, ,, ci '"?l .'i -:ic;.,-·'i '-/ Be.. \u
I-57 837 .63 A.30 ect::. ·3·.; t3c.Jo1,
J-29 825.18 1'3, 1'3 E,ct=.C~ t,c.,lo.s
J-59 825.01 i9.1-0 so;; 3 i 7:>oc.., IH
K-28 811.20 11.0s 80Cc.ll us<!..\( uJ' z_, ... ~
K-58 811.39 l~ -z_q '?9S.10 c;c,Ji .._.-:,: z...c~c!
M-28 806.72 29. '-!S 117· 24 --, \ I/""..,._: 'L(
M-44 806.71 }c.D ?-'78. '71,, -~ '-'-'•·u,.-& '-'L
N-29 803.38 (c."l-1 '1'°1G l;,'+ Da.J,c,j-,_J r5c, \._r
N-53 803.82 q l4 ?-9'f. IP, '-'-'' II w; z_a.,-~ .
0-25 807.54 i ,"I ,.,,, L . .)<._; 195. 2'-f wJ.l v,.)~l.C,(j
0-59 806.61 IC.c0 1'157-5 -.;..1·....,U W' i,c,rfl
P-31 790.0C 72 1<; +.(p1"c( !?,c.:l~,-
P-58 788.12 2-~ s-3 1G'i-2'i c.oo 0-. \ ~, 2-C-r-v
Date: 15 ;::\ c,,· 9 G
Monitoring Measuring
Location Point
Elevation
(ft/msl}
Q-33 783.48
R-17 779.31
R-42 778.81
S-50 826.02
T-17 777.90
T-35 777.38
T-58 716.03
U-38 826.55
V-23 811.89
W-23 800.91
X-32 796.96
Y-38 794.52
Y-74 794.87
Z-78 797.08
AA-41 783.68
AA-54 782.16
BB-1-6"12; 771.75
CC-33 812.68
CC-64 811.37
D0-58 796. 10
EE-58 794.48
FF-23 772.33
FF-34 772.73
FF-62 772.19
Hoechst Celanese -Shelby, NC
Water Level Measurements
Page:_L of _A
Measurement Device: Electronic Water Level Indicator
Depth to Water Level Comments
Water Elevation
(ft) (ft,msl)
'l1.. IS 76/. 29 fu: \it,
\5.<-10 ';Z le ·3 . q / f3c.: kr
1"3. 2~ 7,_.,. ,-2, ?:.c. ·. I"..-
· 22. C So<t-02 (.,.> 4:.-ll Lo.): z.r.:. ,-v\
13 3q 1!.ai./. 51 c>o.j,, c... h1 ?:i , .. 1(1.c
I Z.91.. 7-lo 1-/. 4 ta <->'L \I w~ 2-c.1~
\'-1 -~ I "./-lo/. "7-'2 LACQ \l w,L.:-r.._l.
20. l/, o.c, . 19 '-'• Lt l...u :--,,._i::,,...S::..
iC, 20 '2,ut.G9 / -,.._\...,l '-..N,-;:!.(..<(._Q__
/(,, fl '784 52 'r?ic..1(!.,
,,-. >{(, '?-S /. 0-0 t?c:kr
I I. ,4 t8"3.15 'Do \,u..h.& 6r--l'-,
IC.'i4 1-'2,"f ~s "'ill \..).J; l<-r J.
,, .~ C' -~ L. L-'. ,._._, ··:n "' . t'i "7.,c,: 1....-
34-10 •:J<-j \:-. 9\::, \;CJ>..l\ W,2.Ml
33-S"G '14S. e,1..., '-'" o._\l \.4: 2.(\ ·( 3.
"i.49 1Gl> 2l., 6v: \'\.,
2 u. If '1-'7).. 5 I '·ill w,-)J,,.j
I 1 7-3 7'1~.L,'t ..,_;t.,11 c.,.j: Z.,J --'I
<,",. <. ;;i. 7G:Z. ·1,2. t.-.o._U.. w, 2,.c.,j. .,a ;-1 '?-5591-WLU Wl2....:..rj
10.l, 0 71,1Fs L'-1,Jl vJ ~ -i..,,\-J.
\c. e .. •-5 ?\c !t3S uA .. Ll vi: 2,_i;Ai-J
14 S1-7-'>7-. 3 2.. w,.JJ . .\ i.._,J,-z._c,rv
II
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11
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Hoechst Celanese -Shelby, NC
Water Level Measurements
Date: 15 A P/2. 9(,, Page:_L of .....1
Measured by: r,u,VS--, rv-('f, 5..~c_, cul+ Measurement Device: Electronic Water Level Indicator
~lonitoring ~Ieasuring Depth to Water Level Co=ents
Location Point Water Elevation
Elevation (ft) (ft,msl)
(ft/ms!)
GG-25 771.64 11 O'i ·,-:, i . 55 , ,,c U, , ·,, ·u,,J
GG-39 770.44 \l,. 4'5 753.99 \,\I u .. ,i2,,.-J '
GG-61 771.78 li\.C:'+ 753 ?4 "\I \ \ w.:L.:.....rJ
HH-48 755.44 ::,1,,7,::) 7 t 8. ,.f ' "iO , . ; -z_,;_,,j
HH-77 755.87 3'1.45' 718. '/1 I '"' u ' ·.,--z._L~f~
PZ..l 773.99 \"f. l+ 75&.S.2 6c.: 1._,
PZ..2 795.81 3-1.c,c, 7(. I 42. 'rs~; \._r
PZ..3 786.62 Well destroyed/Paved over betWeen 8/95
and 11/95
PZ-4 750.07 I +-5 74 e 3 2. ''isc-. I t.,
PZ..5A 788.72 '31. "55 75l, 11 ~; \1..r
PZ..5B 777.59 }3.'o'5 753 7''-/ ~.,._<
PZ..6A 795.11 4 C), "LO 7',-lf '1 I 73e,.. 10..r
PZ-68 796.89 -'ii.L\J ,..,;·5_4 7 t)cc: \u·
PZ..7A 780.46 2-i. s" 75·2. tc ·s 3~: I .. ,
PZ-7B 784.46 (,._ 1-:::, 7T1. C,,:; {S.:.: \ IL(
PZ..8 767.99 (,,_'SJ_ 7GI. 4+ 0c.; \ <L<
PZ-9 788.96 ?,i 3c1 ·7·)f ?-7 f:, .. ' lQ,
PZ.10 784.65 '?,f .. ·5 '", T'4G. 06 &,.·l .. ,,
PZ..11 805.48 5 '-I 8't '15(), Co't &o,: h.,
PZ-12 749.41 O.OG tL/C,.t.j / 6":k.1
PZ..13 776.51 191'1. 7-·,·'?' 2 "'I ~". l!L,
OT-IR 771.44 1;:;ic10 7 5c. 5'-f Cc, .. ., h,. ~-\-p" .-.... ('
OT-2 774.01 \). \ C) +bl c;, Co,1~-\-c..,f"'--\-p._, 0-p
OT-3 792.88 lo'-1. I 5 ·,2c_7-3 c~.--~ ~ ~"" P"'-<"
Monitoring 1Weasuring
Location Point
Elevation
(ftlmsl)
OT-4 790.28
OT-5 784.00
OT-6 787.45
OT-6A 798.68
OT-7 782. 16
OT-7A 782.52
OT-8 782.26
OT-10 804.08
IT-1 814.20
IT-2 813.85
IT-3 809,66
IT-4 809,08'
IT-5 810.64
IT-6 812.20
IT-7 813.52
IT-8R 813.04
IT-9 808.73
PEW-! 846.85
PEW-2 848.92
PEW-3 849.25
-PEW-4 848.14
Hoechst Celanese -Shelby, NC
Water Level Measurements
Page:....!_ of _i
Measuremen,t Device: Electronic Water Level Indicator
Depth to Water Level Comments
Water Elevation
(ft) (ft,msl)
t..\"2_14 8 '+'-l1·. 1:,0 c..o,,., \-....--\-C.1rv-('
J.\s-.95" t:,13. 05 ~0,1-:,'tc-f'.\ (?..,,"\'\()
1.\ '2 . 4-5 rs9oo C (!(',6:,h,,.J, p" co."
to "3. Cl S" "C/"-3',. 0 s C:.-:-,., tc. ,, -I 0 \ u,:-...('
i::::-1 I 'o -:fso.9'2:: ('"'""k.-·I 0 1 L.' t'•--¥
'?, s '-t ,'?3,GI::. CI.)",, h... ,-+ :-) I v.-r
11-2 3 -;zi,,s. o·~ <2..~nc,h.,-\-\J..,,-(
21-\.'f~ +7'?. <.> 0 r3~: I Li
)'(;. 1-'c 755, 4 2 c~ 1l'l-h_.,...,._\ '7 l J !.,.._ (l
,). t:)_ ·;•5 7B5.:50 Cc,,,k .-+ p__,c-~
:;i_-c:," .., . ,_, ,_/ 783.-~8 C.-:::.n-....\..__ .... \. "") \-,...) f""Y-'P
,:,14-'2, c; ·-r 'c!."f. I 'r (,;,n S \.c .• -\-()
'(1..Jrh(')
\ la. -=I-I -:/93. q 3 c,,,),.,,. ~ ;-;
\-\jf"-; {'
r, -cw\c.."'-1. '7 ·,i_ Cl. ,_ "2. ,1e1 q•2, \-._;,..._y
J+. '.\: '.> +S<cG'°i G:.,.,\... .. -1-
') .
\ v,~{7
.;:r:i,. ,c:i cS'i"i'--1 C:'-:.,,)\..,-.\ ()" '" ,'7
> .;,'-\ . "I B --:;,13~_.+S I 1-,~ ·.\.-r.,_;,,J-i..:ar"\ '" uJ'Lu
80 Ci-=!--=? l, 5. S'2.. Co.,, .. ~-* p__, ~/l
12. 0'5 1-+ t_, t,.·7-'-u, .\.,,_ t P._,-p
o,1.. u'-l -;,c.,s.21 C-~,~~-\-() (· ..... -./)
so.Ci+ 7-L,+. I+-C _,.,..,.i..... • .\ '7 r v,--\
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-- - - - - - - - - -Field Pata ,:imllion Shed For <!r.!lu111ht.il!~ .. L__S_atnuling
Page .J._ of ~
Date (MM-DD-YY) APRIL 15, 1996
Fie!J r..-r'-vll!lCl C\\'ll(MPQ, MVC,);\VC
Facility Name KUBAL -FURR / HOECHST CELANESE, SHELBY
Well ID# 1-rc.1
V..'eathcr Conditions .-\A Air Tempcratun; oc.
Total Well Depth (TWD) = DIA
Depth To Groundwater (DGW) =
I \A
Length Of Water Column (LWC) = t--t\A
1 Casing Volume (OCV) = LWC x ~(A = '-.J ( P\ gal.
3 Casing Volumes -NlP. gal. -Standard Evacuation Volume
Total Volume of Water Removed -
Method of Well Evacuation
Method of Sample Collection
Fva~u;i1in□ aml C!1!k1,;ti1,11 M1:1h(1:d:i
TB -Tdlon Bailc:r
SSB -Stainless Stt:c::I Bailer
WW -Wdl WiLard
GP -Grunfos P.ump
~\~
(\.)\0-
VOLUME PURGED (GALLONS)
TIME (24 HOUR SYSTEM)
pH (SU)
WATER TEMPERATURE (°C.)
SP. CONDUCTIVITY (UMHOS/CM)
TURBIDITY (SUBJECTIVE)*
ODOR (SUBJECTIVE)**
.. \\J::\
TU SSB WW GP Other
TB SSB WW GP Other
[O!l:i!illl!:i [1>[ Ci1:ii[lf.l2iillll!:l!:r:i
1.5" = 0.092
2" -tl.t63
3" = 0.367
4" = 0.652
lDo-5
5",' '.}
}'l, I.,
\"'i 00
l
.Lf
5" = 1.02
6" = 1.47
7" = 2.00
8" = 2.61
= > JIJ!&
gal.
FIELD ANALYSES
---
Casing Diameter:
--- -Shealy Environmental Scr\'i ........ , Inc.
106 Vantage Point l>rive
Cayce, S.C. 29033
inch ·s CMg Material: PVC -Metal
Guard Pipe: PVC -Me ~-0 . >ckl 1g Cap: y -N
Protective Abutment: , \_ N I Hegnty Satisfactory: y -N
Well Yield: Low -Mod. -High
Btarnrks·
,J, f 1--'
WELL SAMPLE TIME:
,<.::>"'!>'?
B~rna[k:r
F" LC\u) fZA-'TTZ ;,..--.
;1p,rr,_Pt J ._i.., ~ '/].. L per
N\.;t'\J~«.,
• I = CLl:AK 2 = SLJ(i!IT J :cc MODUlATE --1 111(,11 •• ' ' --... I NONI. ~ IAIN I J MOIJERA IL ➔ SI RON(,
-
fichlllilil :, ma! ilm1iw.:l.'.Lb1r...!.inrn1!.ill\'il lCLlil! l! 111 i !!l:
--Page L of _j
Dale (MM-DD-YY) APRIL 15, 1996
FiclJ Personnel CWII,@l'QXI\IV(), SWC
Facilily Name KUBAL -FURR/ HOECHST CELANESE, SHELBY
Well ID# IT E!=°
V..'cather Conditions µIA Air Temperature "C.
TOlal Well Dcplh (TWO) -,...:ilA
Dcplh To Groundwa1er (DGW) =
t-J ll='I
Length Of Water Column (LWC) = NICI
I Casing Volume (OCV) = LWC x i-1l F>-= gal.
3 Casing Volumes = NI p, gal. = Starn.Jard Evacuation Volume
Total Volume of Water Removed = ,-..)\µ._ . gal.
Method of Well Evacualion w I\ TB SSB WW GP 01hcr
Method of Sample Collection· ~ j\ TB SSB WW GP 01hcr
fa·arnauon and ( olkc11on Mi:1hods
TB -Tdlun Bailer
SSH • Stainless S1eel Bailer
WW -Well Wizard
GP -Grunfos Pump
VOLUME PURGED (GALLONS)
TlME (24 HOUR SYSTEM)
pll (SU)
WATER TEMPERATURE (°C.)
SP. CONDUCTIVITY (UMHOS/CM)
TURBIDITY (SUBJECTIVE)*
ODOR (SUBJECTIVE)**
Ci!J illilll1U1J.Il....asllll:.. Jl.iaJru:.lt I.S
1.5" = 0.092 5" = 1.01
r = o.1<iJ 6" = 1.-11
3" = 0.367 7" = 2.00
4" = 0.652 8" ~ 2.61
I ~'-\0
c;,_14
24-L
Voe. --D-?;; ;)_f.o ;)__
I
3
FIELD ANALYSES
Shealy Environmental Ser
106 Vantage Point I>rh'c
Ca)'cc, S.C. 29033
Casing Diameter: inches Casing Material: PVC -Mela!
Guard Pipe: PVC -Mc ·1I N ,_, eking Cap: y -N
Protective Abutment: "' 7ll ~grily Sa1isfaelory: y -N
Well Yield: Low -MoJ. -Iii I
lli:rnark
J \A
\JOC',. co\ "1,J" ~ l-:,0\-~ .~ol~
v-><--> ~ lv,~-h.J c,.,; .\.L l'X t,... r.
WELL SAMPLE TIME:
ID'1" ''~'3 0 ,.,._,,c, ,,~ff!<!"
Remarks·
• I = CLEAR 2 = SLIGI IT 3 = r,..10DERATE 4 -111(,1 I --.. .. -I-NONI: 2--"l·AINI J=MODl:RAII; 4=.SIJU)N(,
-- - - - - -- - - -- - - - --- -
-- - --- - -- --fir)tl_l!aJa_ nllillili1L:ilii:.l:Ll'l.tu1rnu!! Ul!"illtLSamvli11i:
Page,-.:; of ~
Date (MM-DD-YY) APIUL 15, 1996
Field Personnel CWII, MPQ, MVC, SWC
Facility Namc KUBAL -t,'lJl{I{ / IIOECIIST cm,ANESE, SHELBY
Well ID// I<-J8
- - - --- - -Shcal}' Eu\'ironnu•nfal Sen .J, Inc.
106 Vantage Poinl Drh'c
Cayce, S.C. 29033
-Casi11g Dia111ctcr: 2 incl1cs Casing Material: ~-~ktal
Guard Pipe: PVC ;(Mct'-1)..) No Locking Cap: !!)· N
Prntcclivc Ahut111c11t: .:V-N Integrity Satisfactory: .f!_,,f N
Well Yield: Low -lf':Y -High
Weather Conditions CNQl?.CA':.T /w1>JO'/ Air Temperature oc_ lkrnarks.;
Total Well Depth (TIVD) -~6.~
Depth To Groundwater (DGW) -I\. QC\
Length Of Water Column (LWC) -11,,, C1 /
I Casing Volume (OCV) -LWC x rf,. I l '.s -;::>. 8 gal.
3 Casing Volumes 8.L, gal. -Standard Evacuation Volume
Total Volume of Water Removed -
Method of Well Evacuation
Method of Sample Collection
.. E,~_hl<llli.!ill
TD -Teflon Bailer
SSD -S1ainkss S1ed Daikr
WW -Well Wizard
UP -Grunfos Pump
VOLUME PURGED (GALLONS)
TIME (24 HOUR SYSTEM)
pll (SU)
WATER TEMPERATURE (0C.)
SP. CONDUCTIVITY (UMIIOS/CM)
TURBIDITY (SUBJECTIVE)*
ODOR (SUBJECTIVE)••
·.; '6' -
TB SSB ;ww\ GP Other
TB SSB \ ww_,.,; GP Other
. . Clm:ili1111i...l.1..1r--1.:..allilJ!.lli.a11Kt1,;:r :i
1.5~ = 0,091 5" = 1.01
r = 0.163
]" = 0.3li7
4" =0.652
~r ,-
1ss·1
I 5"1
17. I
I 10
I
3
6" = 1.47
r = ·2.00
8" = 2.&l
7 ?
/(.03
(,,,5"3
I l8, I
</o
.3
I
• I = Cl.EAi{ 2 = SI.ICil IT 3 = MODERATE. 4 111<.,II ..
gal.
FIELD ANALYSES
!i. / ~ -I
f i,1!)9 /I.I'/
I~. 70 /;.. 71
17.3 i7, <;
I </ D ,~o = ::;>-1.,S
7 2.
I I
' ") -; .. --' I NONI. ~ IAIN I 3 MODLR,\I L 4 S 1/U lN(,
WELL SAMPLE TIME:
l~O
Remarks·
ficld Ilata .rm;tf ion Shed _Eu_r__G.Oillll.llifi!l!.T .. .!iamu.lll!g
Page_i±_of :S-
Shealy Environmental Sen
I06 Vantage Poi11t Drive
Cayce, S.C. 29033
, Inc.
Date (MM-DLJ-YY) APRIL 15, 1996 Casing Dia111ctt.T: 2.__ inches Casing tvlatcrial: PVC .. A.1 .. 1:1\ J
Fit:IJ Pasunnel CWH, MPQ, MVC, SWC Guar<l Pipe: PVC ~ N" Locking Cap: !..V-
Facility Name KUBAL -FURR/ HOECHST CELANESE, SIIELBY Protective Abu1n1cnt: y -N c.c/ Integrity Satisfactory:
Well ID# \/-2 3 Well Yield: Low -e_y. -High
Weather Conditions 0'\1EelA-,,Y-/ w1a,:.,1J'1 Air Temperature <le. Rrumk.s.;.
Total Well Depth (TWD) =
Depth To Groundwater (DGW) =
Length Of Water Column (LWC) =
I Casing Volume (OCV) = LWC x
3 Casing Volumes =
Total Volume of Water Removed =
Method of Well Evacuation
Method of Sample Collccliou
furua11on and Col~llillillm
TB -Tenon Baikr
SSB -S1ainless Sted Bailer
WW -Well Wi1.ard
GP -Gnmfus Pump
VOLUME PURGED (GALLONS)
TIME (24 HOUR SYSTEM)
pH (SU)
WATER TEMPERATURE (°C.)
SP. CONDUCTIVITY (UMIIOS/CM)
TURBIDITY (SUBJECTIVE)*
ODOR (SUI3JECTIVE)**
? 3 </0
/D.J..o
I "3 20
l'l./6? = 2, 15' gal.
C,,.'{5 gal. = Standard Evacuation Volume
C:.i'S-gal.
TB SSB f'W \GP Other
TB SSB (:!!!!/GP Other
-L.llima111:iJm ( asmg PuUt~LUS
. 1.5" = 0.091 5" = 1.02
2"; = 0.163 6" = 1.47
3· = o.367 r = 2.00
4" = 0.652 8" = 2.61
FIELD ANALYSES ,~ 7, 15' "{, 3 0 /__ <I'S
/G,?9 I(;, ,'1 ~ //4J1? /(,,y,<
5'. 0 ·2 S.10 S. 17 s-. 1 <{
17..3 17, I /(,,. 9 t 7;'(.,
3S:oo --~000 3000 .'?ooo =
.z 2 2 7
4 ,j 4 4
?3501
• I = CLEAR 2 = SLIGI IT 3 = t-.10DERATE 4 -111(,1 I ---... -. .. .. I -NONI: 2 -h\lN I 3 -MOI H:RA 11: 4 -SI RON( 1
-- -- -- --- - - - - -
·•
WELL SAMPLE TIME:
Remarks:
- --
N
(!_) N
/1'..</K
- -
---- --- --- - ---- --- -
l'kWJlal;L
Page .<of~
Da1c (MM DD-YY) ?____.:\ l'R IL 15, 1996
Ficl<l Personnel ~WIJ/ Ml'Q, MVC, t"VC)
Facility Name KUBAL -FURR/ IIOECIIST CELANESE, SHELBY
Well JO#
R_LX_,\J....\Q.,1,"--"5
Weather Conditions (_q, <CC.•::,·\. Air Tcmpcralurc oc_
Total Well Depth (TWD)
Depth To Groundwalcr (DGW) (\
Length Of Water Column (LWC) I\
I Casing Volume (OCV) LWC x ' gal.
3 Casing Volumes gal. -Standard Evacmuiun Volume
Total Volume of Water Removed gal.
Method of Well Evacuation TB SSB WW GP O1her
Method of Sample Collection TB SSIJ WW GP Other
E.Yacuatioo aml Collection Methods .G.!.filw11t.s..fu.L.C.a~l2liilll.lli 1.S
TB -Tenon Bailer
SSB -Stainless Steel llailer
WW -Well Wizard
GP -Grunfos Pump
VOLUME PURGED (GALLONS)
TIME (24 HOUR SYSTEM)
pH (SU)
WATER TEMPERATURE (°C.)
SP. CONDUCTIVITY (UMIIOS/CM)
TURBIDITY (SUBJECTIVE)•
ODOR (SUBJECTIVE)++
1.5~ = (U)IJ2
2" = 0.16)
r = 0.367
4" = 0.652
0
\ -1 \0
·1.~0
\7. 7
<....\()C::,
\
]_
5" ~ 1.02
6~ = 1.47
7" -2.tK>
8" ~ 2.61
----FIFI D ANAi YSFS
10 2_D
\7 \':, \7 '1.0
7. t,L\ 7. C\ \
17. 1... \ \.,,, 4i
'-\ 'SO 1..\0~
\ \
:;i__ L
Shc<tl)' En,·inmmcntal Sen, _.,, Inc.
106 Vantage Point lki\'c
Cayce, S.C. 290.B
Casing Dia1rn.:tcr: in ·hes Casi11g Material: PVC· Mc1al . ~
Guard Pipe: PY\" r-v ~ta! . N' Locking Cap: y . N
Protective Ahutm nt\ y . Integrity Satisfactory: y . N
Well Yield: Low · Mud. -High
R~m,.ubs·
\\·, ucJ·e. w.z.~\.
'0cu·-c:. F\~,._u ?.a}e --:L. G-'?M.
J
"30 WELL SAMPLE TIME:
\7?.. -i
\7'2..S Remarks;
7. -i,
\ \.,, . """6
L\Q() ~ 7q72_
\
::L
• I =Cl.EAR 2 = SLICillT 3 = MODERATE 4 111<,II .. -0 I NONI. ~ -

I

,\IN I 3 -MOIJLRA IL -l -SI RON(,
- - -- -- -- --·--- -- - - - -USE BALL POINT PEN f\1-JL Y. PRESS HARD SHEALY ENVIRONME~'~AL SERVICES, INC.
CHAIN OF CUSTODY # 2 4 2 7 5
106 Vant&{; :nta Drive
Cayce, South ""'olina 29033
Telephone No. [phone] Fax No. (803)'791-9111
CHAIN OF CUSTODY RECORD
,.. __ .. _
,,.,,
NPDES ··----~-,,-,-,--.,,,--,--,-,--~i'-..
County ______ -,-_._. 'c.:i-~'ci: 'c---:--~1~ ~ -· . :-,1:·
Receiving Stream ___ -',----'-c''-----,---
Reporting Address SAMPLE ANAL vsis REQUIRED , ,· ., .. Outfall No
-. i:O-.\ I", 1--I C. ' •· +-PRESERVATION (CODE) LAB USE ONLY ,
Ii. ltr". fc, ... \'..' -~ CODE: A = None Program Are&·tcirclel Attention ~ ~ l B= HN03 · ' ,. { ~ { C • H2S04 ow \ If,. 1 -RCRA .. "" ' l ' ' -· Telephone No. P.O. No.· t "' "' • 1 i .:! D = NaOH SPlt.10 · Other: , ' ' 11 l E "' E=ICE 0 J ' .. •--.-8 i~ "' • ' ! ' ~ '<, F= v,./"N1.., ~ 3 " m ~ • ·~ ~ " " ~ ' ! Sample 10 (Location) TIME , ~ 0 w • ~ ~ ~ • DATE ~ :;: ,' 0 d " ~I i 0 6 z ~ . ·; 0 ,, REMARKS SESI 8 " " m , m r " m t ~-" ', LAB I.D. s,an 4 ,oc LjlS I · r;; 1/J'(/llll lj)., \C:,1'1 )
F1n1sh ,.
✓ ,/ • Vol 02/.oDI~ Gil,,r,,I <l7&/8/J I ~1 \.. f S· [, I ) /\--
s,an
j ''JI) ,;j It. (ii,,_ ,.; ~,. I l.)L\0 ) Toe, '-l IS I 1:· 11,,.i1we L:;I .1,·
. ' .
/~ rf~F Finish /. ,/ v "~7/oflN )--. ' ' . ~ uG S 21.n)A io ,':i 1\
Start
,r;,. ,, l<..7-..> fol'.. '11 S. I '37 /;2{)/\1 i<-2 ~ FI01Sh ✓ ' ;
-S1a11
j )II_,.,,. ll,~"'> TL;~ -\ 1-; I ~1&21JJ· 1/-2 -) f11l1Sh ' , ✓ ·---
S<a,
a~,-· 1'"·· '>
J .; A.,,.,r 172V ,1 \' '.-(. J;/..1.t. ,A !J1022N Fwoh /. .,. '· -.
'·
j;,\o _(, s .. , r;. iJ ". -, ''-~ '" ) ,,·· ' >-. \ r:e/i 0 /IC11{ (\1-//
·
1?1&J3N
,_
)( ,/ " :·~· v..:~•v'·
' .. e ,; I'S A ,I . Sw1
T. \ 6\~-"-mi.,., r:zr.--:~?vv't
,
[Ii ✓ ..,.,. .. JvC ~1/tJJ1Nl;> -
S""1
Fio1sh
SAMPLER Date/Time Received by (Sig.) O~te/Time Hazards Associated with Sample ~ sear 10,ac, rc,a,1 M~.!J.\r1tl <~t.JATT/.£ flAUIY
6i-1,;.l'-fl, I :;,JiY.).:; -9v I '.Rn-,
NO NONE
-I;!., ii·· 10!. 1/ i,.v ,>c -Aeceipl TRC flll>"1 ign lure. ·; 11 (0 , r J A. _,
'"" Aeceipl pH ' . '" R-e7quished by (Sig.y, 0
Date/Time Received by (Sig.) _ Date/Time
\J.(/.('_..e.,I.__}) () -1 /;-1/'/ k>J.:J1 1/b\ll.VO : I ReceJ)1 Terff). -c
Relinquished by (Sig'.) . Date/Time i,.Y_"'-"'!J_i,y (Sig.J // .. l(p_,4aD le/Time ~ed 001co (Cifde) I r,YJ A (/ /) './l, '16IA1/(') NO CEPACK -• , .. . -. -. .. " -I••· I ('
-------------------Inner Tier Combined Influent TOC Data
ITCI TOC Data
4000 ~-----------------------------------~
3500
3000
i 2500
E -C
0 'lii 2000
~ -C B
C 0 1500---------------------------------------------------------------------------------------------
0
1000 - ---------------------------------------------------------------------------------------------------
500 - ---------------------------------------------------------------------------------------------------
0+-------------j------------+----------------+-----'
1/1/93 1/1/94 1/1/95 1/1/96
Date
-------------------
ITCI Ethylene Glycol Data
LQCaliQ □ llatll. .'Lal.u.e. lln.i.t ITCI Ethylene Glycol Data
rTCI 11 /29/94 2330 mg/I J 2500
rTCI 3/7 /95 1800 mg/I rrc, 5/1 8/95 1000 mg/I JL
rTCI 8/22/95 209 mg/I 2000 -... rTCI 11 /29/95 52 mg/L z -"' rrc, 1 /16/96 1100 mg/L E
; 1500 rTCI 4/15/96 1070 mg/I 0 ..,
I!! \j 1000
" C 0 u
500
0+-----------------''F------'
11 /29/94 11 /29/95
Date
-------------------Monitor Well V-23 TOC Data
V-23 TOC Data
10000-r------------------------------------~
8000
7000 -o:! ~ 6000 -C
0 .:: 5000 ------------------------------------------jg
C
B
C 0
0
3000 - -- - ----- ------- -- ------ -------- ------ ----- -- -- ----- --- - - --- -- ----- --- --- ---- ---- -- ---
2000 -· ----------- -- ----- - -------------------------------
1 000 - --- --- --------- --- -- ------ -----------------------------------------· ------------------- --- -- --- --
0-1-------+-------i------+------~------+-----l
1/1/85 1 /1/87 12/31/88 12/31/90
Date
1 2/30/92 12/30/94
-------------------
Monitor Well V-23 2-Butanone Data (MEK)
l.QCaliQ□ D.alf! ~ J.!ni1
V-23 8/3/89 1 .1 mg/L
V-23 11/9/89 0.45 mg/L V-23 2-Butanone (MEK)
V-23 1 /5 /9 0 0.37 mg/L
V-23 2/23/90 0.038 mg/L 4
V-23 8/8/9 0 0.56 mg/L
V-23 11/7/90 0.01 mg/L u 3.5 ------------------------------------------------
V-23 2/5/91 0.66 mg/L
V-23 5/3/91 0.46 mg/L -3 -------------------------------------------------
...I V-23 8/9/91 0.04 mg/L u -"' V-23 11/4/91 0.05 mg/L u .§. 2.5 -----------------------------------------------.
V-23 2/4/92 0.2 mg/L C 0
V-23 5/5/92 0.2 mg/L u = 2 . ·-------------------------------------------------
i V-23 8/7/92 0.8 mg/L
V-23 11/6/92 0.1 mg/L u t 1.5 ----------------------------------------------..
C
V-23 2/3/93 0.05 mg/L u 0 (J 1 -·-------------------------------------------------V-23 5/5/93 0.25 mg/L u
V-23 8/6/93 0.044 mg/L 0.5 V-23 11 /3/93 0.01 mg/L u
V-23 2/2/94 0.25 mg/L u 0 V-23 8/5/94 0.52 mg/L 6/1 /89 6/1/91 5/31 /93 5/31/95 V-23 3/8/95 0.01 mg/I <
V-23 8/24/95 0.767 mg/I Date >
V-23 1/16/96 3.6 mg/L
-------------------
Monitor Well V-23 Acetone Data
LQC.aliQD .lla1e .'ia.l.u.fl llni1
V-23 8/3/89 0 .1 mg/L u
V-23 11/9/89 0.295 mg/L
V-23 1/5/90 0.3 mg/L
V-23 2/23/90 0.34 mg/L V-23 Acetone Data V-23 8/8/90 0.31 mg/L
V-23 11/7/90 0.01 mg/L u
V-23 2/5/91 0.52 mg/L 1.2
V-23 5/3/91 0.53 mg/L
V-23 8/9/91 0.48 mg/L 1 ------------- - ------------ - ----------------------
V-23 11/4/91 0.53 mg/L -.J
V-23 -2/4/92 0.08 mg/L B DI E 0.8 -- - ------- - ---------------- --------------------
V-23 5/5/92 0.2 mg/L u -C V-23 8/7 /92 1.1 mg/L E 0 til 0.6 --------------------------V-23 11 /6/92 0.14 mg/L ~ ..
V-23 2/3/93 0.05 mg/L u C ..
V-23 5/5/93 1 mg/L B g 0.4 · -------------------- - -
0
V-23 8/6/93 0.025 mg/L u
V-23 11/3/93 0.01 mg/L u 0.2 --
V-23 2/2/94 0.36 mg/L
V-23 8/5/94 0.52 mg/L 0
V-23 3/8/95 0.01 mg/I 6/ 1/89 6/1/91 5/31/93 5/31 /95
V-23 8/24/95 0.648 mg/I J Date V-23 1/16/96 0.487 mg/L
V-23 7/11/96 1.15 mg/I
-------------------
Monitor Well CC-33 Benzene Data
l.acalii;rn .lla1e Yalu.e. J.!nit
CC-33 8/4/8 9 0.085 mg/L
CC-33 11/8/89 0.08 mg/L CC-33 Benzene Data CC-33 2/1 4/90 0.081 mg/L
CC-33 5/4/90 0.079 mg/L 0.14
CC-33 8/9/90 0.096 mg/L
CC-33 11 /6/90 0.073 mg/L 0.12 ------------------------ - - - --------- - ------ - - ------
CC-33 2/6/91 0.095 mg/L
CC-33 5/2/91 0.089 mg/L
CC-33 8/8/91 0.08 mg/L ::J' 0.1 ----------------------------------- --- - ------- - - ---CC-33 11/4/91 0.14 mg/L Cl)
E CC-33 2/4/92 0.11 mg/L -C 0.08 --------------- ------ ---------- - - -
CC-33 5/4/92 o. 11 mg/L 0 .. CC-33 8/7 /92 0.1 mg/L I!
CC-33 11/5/92 0.086 mg/L c o.os CD u CC-33 2/3/93 0.052 mg/L C 0 CC-33 5/5/93 0.055 mg/L O 0.04 ---- - -----------------------------------------------.
CC-33 8/5/93 0.059 mg/L
CC-33 11 /2/93 0.055 mg/L
CC-33 2/2/94 0.045 mg/L 0.02
CC-33 8/4/94 0.026 mg/L
CC-33 3/9/95 0.014 mg/I 0
CC-33 8/24/95 0.0176 mg/I 6/1/89 6/1/91 5/31 /93 5/31 /95
CC-33 1/17/96 0.01 mg/L Date
CC-33 Dupe 1/17/96 0.0125 mg/L
---- - - - - -- -- - --- ---Monitor Well CC-33 Chlorobenzene Data
Localioa D..ale. .llawe. l.!ni1
CC-33 8/4/89 0.024 mg/L
CC-33 11 /8/89 0.027 mg/L
CC-33 2/14/90 0.021 mg/L CC-33 Chlorobenzene Data
CC-33 5/4/90 0.019 mg/L
CC-33 8/9/90 0.02 mg/L 0.03
CC-33 11 /6/90 0.019 mg/L
CC-33 2/6/91 0.018 mg/L
CC-33 5/2/91 0.019 mg/L 0.025 ----------- ----------------------------
CC-33 8/8/91 0.015 mg/L :::r CC-33 11 /4/91 0.024 mg/L -DI 0.02
CC-33 2/4/92 0.017 mg/L E -
CC-33 5/4/92 0.017 mg/L C 0
CC-33 8/7 /92 0.016 mg/L I 0.015 -------------- ------------------- - ----
CC-33 11/5/92 0.012 mg/L C ..
CC-33 2/3/93 0.01 mg/L u C 0.01 ---- - - ---------- ---- -
CC-33 5/5/93 0.01 mg/L J 8
CC-33 8/5/93 0.011 mg/L
CC-33 11 /2/93 0.008 mg/L J 0.005 · ·--------- ------------- - ------
CC-33 2/2/94 0.006 mg/L J
CC-33 8/4/94 0.004 mg/L J 0 -
CC-33 3/9/95 0.005 mg/I < 6/1 /89 6/1/91 5/31 /93 5/31/95 CC-33 8/24/95 0.005 mg/I <
CC-33 1/17/96 0.005 mg/L Date <
CC-33 7 /12/96 0.005 mg/I <
CC-33 Dupe 1/17/96 0.005 mg/L <
-------------------Monitor Well K-28 TOC Data
K-28 TOC Data
8000.00 -r------------------------------------,
7000.00 - ------------- ------- ---------------------------------------------------------------------------
6000.00
~ 5000.00
E -c.
0 f 4000.00 -C B C o 3000.00
0
2000.00 - ----- ------ --- --------------------------------------------------------------------------
1000.00 - ---- --- ----------------------------------------------------------------
0.00 +4~ .... --!--------'l-------1-----+-----+-----+----'"""' .........
9/1/81 9/1/83 8/31/85 8/31/87 8/30/89
Date
8/30/91 8/29/93 8/29/95
-------------------Monitor Well K-28 2-Butanone Data (MEK)
LQ1<aliQ □ ~ :'ial.u.e. lJ.n.il
K-28 8/4/8 9 0.19 mg/L
K-28 11/9/89 0.074 mg/L
K-28 1 /4/90 0.099 mg/L K-28 2-Butanone Data (MEK)
K-28 2/1 9/90 0.28 mg/L
K-28 5/4/90 0.24 mg/L 0.3
K-28 8/8/90 0.12 mg/L
K-28 11 /6/90 0.24 mg/L
K-28 2/6/91 0.04 mg/L 0.25 ------------------------------------------------
K-28 5/3/91 0.05 mg/L u :J' K-28 8/8/91 0.031 mg/L -0.2 · 0) . ----------------------------------------------
K-28 11/4/91 0.046 mg/L J E -K-28 2/4/92 0.094 mg/L C 0
K-28 5/5/92 0.05 mg/L u i 0.15 --------------------------------------------------
K-28 8/7 /92 0.071 mg/L C ..
K-28 11/6/92 0.026 mg/L u C 0.1 --------------------0 K-28 2/3/93 0.01 mg/L u 0
K-28 5/5/93 0.01 mg/L u
K-28 8/6/93 0.056 mg/L 0.05 --------------
K-28 11 /3/93 0.13 mg/L
K-28 2/2/94 0.034 mg/L 0
K-28 8/8/94 0.011 mg/L 6/1/89 6/1 /91 5/31/93 5/31 /95 K-28 3/9/95 0.01 mg/I <
K-28 8/23/95 0.01 mg/I Date <
K-28 1/16/96 0.01 mg/L <
-------------------Monitor Well K-28 Acetone Data
LQ!.aliQ□ .llalll. ~ J.J.ni1
K-28 8/4/89 0.43 mg/L
K-28 11/9/89 □.159 mg/L u
K-28 1 /4/90 0.074 mg/L K-28 Acetone Data K-28 2/1 9/90 0.39 mg/L B
K-28 5/4/90 0.24 mg/L
K-28 8/8/90 0.074 mg/L 3
K-28 11 /6/90 0.39 mg/L
K-28 2/6/91 2.6 mg/L E 2.5 --------------------------------------------------------
K-28 5/3/91 0.25 mg/L -K-28 8/8/91 0.082 mg/L ..J -"' 2 . -------------------------------------------------------K-28 11/4/91 1.1 mg/L .§.
K-28 2/4/92 0.13 mg/L C 0 K-28 5/5/92 0.05 mg/L u ~ 1.5 -------------------------------------------------------
K-28 8/7 /92 0.2 mg/L -C
K-28 11 /6/92 0.029 mg/L
., u 1 C ·----------------- - - - ---- -------- ------ - - - ----------- - -
K-28 2/3/93 0.068 mg/L 0 0
K-28 5/5/93 0.068 mg/L
K-28 8/6/93 0.057 mg/L 0.5 · -----------. - -... . . -----------------------------------
K-28 11 /3/93 0.14 mg/L
K-28 2/2/94 0.034 mg/L 0
K-28 8/8/94 0.02 mg/L 6/1/89 6/1/91 5/31 /93 5/31 /95 K-28 3 /9 /9 5 0.01 mg/I <
K-28 8/23/95 0.01 mg/I Date <
K-28 1 /1 6/96 0.05 mg/L <
K-28 7/11/96 0.02 mg/I <
-------------------
Monitor Well K-28 Benzene Data
LQi.aliQ□ .!late. .llal.u.e. Unit
K-28 8/4/89 0.022 mg/L
K-28 11/9/89 0.005 mg/L u
K-28 1 /4/90 0.015 mg/L
K-28 2/19/90 0.025 mg/L u K-28 Benzene Data
K-28 5/4/90 0.018 mg/L
K-28 8/8/90 0.03 mg/L 0.03
K-28 11 /6/90 0.015 mg/L
K-28 2/6/91 0.019 mg/L
K-28 5/3/91 0.014 mg/L J 0.025 - ------------------ ------------------------ --- -
K-28 8/8/91 0.017 mg/L
K-28 11/4/91 0.03 mg/L J :J" K-28 2/4/92 0.017 mg/L -0.02 ------. -------- ------------------------------"' K-28 5/5/92 0.017 mg/L J E -K-28 8/7/92 0.019 mg/L C 0
K-28 11/6/92 0.009 mg/L J '; 0.015 .. K-28 2/3/93 0.009 mg/L J -C .,
K-28 5/5/93 0.014 mg/L " C K-28 8/6/93 0.015 mg/L 0 0.01 · - ------ ----- -------------- - -0
K-28 11 /3/93 0.011 mg/L
K-28 2/2/94 0.014 mg/L
K-28 8/8/94 0.018 mg/L 0.005 ------------------ - - ----------------- ---------- - - - -
K-28 3/9/95 0.006 mg/I
K-28 8/23/95 0.0205 mg/I
K-28 1/16/96 0.0086 mg/L 0
K-28 7/11/96 0.0149 mg/I 6/1 /89 6/1 /91 5/31/93 5/31/95
Date
-------------------
HH-48 TCE Data
l.ocatio □ .!2a1e. ~ .L!nit
HH-48 8/3/8 9 0.16 mg/L
HH-48 11/7/89 0.14 mg/L
HH-48 2/5/90 0.005 mg/L u
HH-48 5/1/90 0.17 mg/L
HH-48 8/2/90 0.15 mg/L HH-48 TCE Data HH-48 11/2/90 0.15 mg/L
HH-48 2/1/91 0.15 mg/L
HH-48 5/2/91 0.12 mg/L 0.25
HH-48 8 /2/91 0.01 mg/L u
HH-48 11/1/91 0.16 mg/L 0.2
HH-48 2/3/92 0.16 mg/L -... -HH-48 4/30/92 0.15 mg/L "' E
HH-48 8/3/92 0.18 mg/L ;0.15 -- ----
HH-48 11/3/92 0.22 mg/L E 0
HH-48 2/1 /93 0.15 mg/L I -HH-48 5/3/93 0.18 mg/L C 0.1 - - - ---------- ------------------------- ----------.. u
HH-48 8/2/93 0.2 mg/L C
HH-48 11/1/93 0.22 mg/L E 8
0.05 -. -------------- -----------------------------------HH-48 1/31/94 0.2 mg/L
HH-48 8/1 /94 0.16 mg/L
HH-48 8/1/94 0.01 mg/L 0 -
HH-48 3/8/95 0.17 mg/I 6/30/89 6/30/91 6/29/93 6/2 9/95
HH-48 8/23/95 0.222 mg/I Date HH-48 1/17/96 0.165 mg/L
HH-48 DUPE 11 /3/92 0.2 mg/L D
-------------------
L2i:iali!l □ Q.ata ~ JJ.o.i.l
HH-77 8/3/89 0.008 mg/L
HH-77 8/2/90 0.04 mg/L
HH-77 8/2/91 0.13 mg/L
HH-77 8/3/92 0.067 mg/L
HH-77 8/2/93 0.12 mg/L
HH-77 8/1 /94 0.12 mg/L
HH-77 8/23/95 0.332 mg/I
HH-77 1/17/96 0.187 mg/L
HH-77 TCE Data
HH-77 TCE Data
0.35
0.3
::J'
ai0.25 E -C 0.2 0 ;,
~ 0.15 .. u C 0.1 8
0.05
o+zc-------,f------J.------+--...1
6/1 /89 6/1/91 5/31/93
Date
5/31 /95