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Home My WebLink AboutNCD003446721_19880101_Celeanse Corporation - Shelby Fiber_FRBCERCLA SAP QAPP_Summary of Off-Site Well Sampling 1986 - 1987-OCRI I Celanese Corporation NPL I Site I Shelby, Cleveland County, I NC I NCD 000 608 117 I ' ' I I ~ ! i' I I Summary of Off -Site Well I Sampling I 1986 -1987 I -· I _; I Pat DeRosa I NC Superfund Section ··-- I I I I I I I I I I I NC CERCLA Unit Sampling I February 11, 1986 I I I I I I I I I I I I le I I I I I I I 1• I I I I I I llt I I Well u 1 2 3 4 5 RESIDENTIAL WELLS SAMPLED BY NC CERCLA UNIT FEBRUARY 11, 1986 Name, Description_ McLane Residence, Bored well, 2'diam;, Water level 10.5' Total depth= 35' Graham Residence, Drilled well, Total depth= 50-60' Mobile Estates, Drilled well, Total-depth= 220' Camp Residence, Drilled well, Total depth= 110' Owens Residence, Drilled well, Total depth= 100' Summary of Significant Contamination Inorganics: Not sampled due to steel bucket in well° used to·· retrleve water. Organics: Below detection limits. Inorganics: No contamination. Organics: Below detection limits. Inorganics: Arsenic, 0,10 mg/1. Organics: Below detection limits. Inorganics: No contamination. Organics: Below detection limits. Inorganics: No contamination. Organics: Below detection limits. Leonard Camp Property o ~ NCD9810Zl 702 • '->'D ,:,,\\'\. ··-.. ~ --•. SAMPLE ANALYSES REQUEST Seate Laborarnry of Public Health P. 0. Box 28047 306 N. Wilmington Street Raleigh, 2761 I I Environmental ~ 0roundwacer (I) ___ Surface Water (2) I 11-Soil (3) I___ Other ( 4) Concentrate __ Solid (5) __ Liquid (6) ___ Sludge (7) __ Other (8) Field Sample Number -=2'--_f_-_J,_Q=----------- Sire Loca:ion -----------'M--c<.u',:,,=e:C-1...,•c-LIY.JLJ.(_? __ _ Dare Collected _,,f),.c:,,__-_J,_,{c_. -~£"-C,,._,_ ___ Time /II\ Comments fu ha cq Re.uJJ. I INORGANIC CHEMISTRY Extractables Parameter Arsenic __ Barium I _ Cadmium [-Chromium ___ Lead I ..e:~;~~~: ~~ilvcr Parameter Results mg/ I Results mg/ I Parameter ~Arsenic ->L... Barium ~ Cadmium __ Chloride -.,.L...Chromium __ Copper __ Fluoride __ Iron _.L._Lead __ Manganese -.,L Mercury __ Nitrate. ~Selenium Results mg/ I <,:J,o/ < ,O.oJ ORGANIC CHEMISTRY Parameter Results mg/ I P&T:0C/MS ______ · _EDB II --Acid:B/N Ext. 1 __ TOX ''= __ PCB's __ Petroleum __ Endrin __ Lindane Total Parameter Silver __ Sulfates __ Zinc _Ph __ Conductivity _TDS _TOC Parameter __ Methoxychlor __ T oxaphene _2,4-D __ 2,4,5-TP (silvex) Results mg/ I Results mg/ I I L_ _______ M_1_c_R_o_B_10-Lo __ G_Y_1__.:._. ,_,,,,,,~-;:<..,;;,::,:"'~" ""'£"""os:-.,,-,-------_JR_A_o_1o_c_H_E_M_1_s_T_R_Y ______ _j Parameter --(MF) Coliform Colonies/lOOmls '= (MPN) Coliform Colonies/ IOOmls eccivcd Parameter Results PCi/ I ,-,,., -.-,, : ) __ Gross Alpha r-...•~ -~-~--. ; _,_ Gross &ta _, ...... ;" ( .. ::--· Dar~ ReporreJ __________________ _ le Extracted __________________ _ Reported I3y Da« Analy:cd ---~~--------------- ,_ ....,,,£.:-.: .. ) J .' Lab Number ___________________ _ ~r) :. ~=..:nt of Human Resources siollllllllJalth Services SAMPLE ANALYSES REQUEST State: Laboratory of Public Health P. 0. Box 28047 306 N. Wilmington Street Raleigh, 2 76 i I ' N/1 ti) -· Tf3 ft Field Sample Number __ .;;;?«-'----'>f'---7L..lf _________ _ Ma/I Site Loca:ion __________ _,B=at..,J._c:i;---4_,_/v~'-l.::c.. __ .m; J ,-0.[I) fie, 11«1d Bv A.t=l>e 40L4-lD# -~'3-'-'R'-'-----Date Collected :J. -ff -J'C, Time /J J 0 pc I sample: ::nwonmental _Jl._ Groundwater (I) -.-Surface Water ----Soil (3) (2) __ Other (4)· Concentrate __ Solid (5) __ Liquid (6) __ Sludge (7) . __ · Other (8) Comments t22ob1/e, £:mA, I INORGANIC CHEMISTRY Extractables Total .. .!rzrnecer Resuks mg/ 1 Parameter Results mg/1 Parameter Results mg/ l _Arsenic I ....,.L_ Arsenic ,_-•. /1. ; :.:,, ~Silver -<o,r,r:- =r•rium _L Barium ✓.:::: o~ I __ Sulfates Cadmium . --1.L Cadmium -<. £l. oo:£_ __ Zinc --1,:mium __ Chloride _Ph -..,L..Chromium < i/· DI __ Conductivity =t ercury __ Copper _ms __ Seknium __ Fluoride _TOC __ Silver . __ Iron -- =I __,L_ Lead <. {Y. C/ ·1 -- __ Manganese -- _..,LMercury <a ,00()~ -- -- =I __ Nitrate. -- _LSelenium ,.:. /) ,);:_,.----- ORGANIC CHEMISTRY Parameter __ P& T:GC/MS ¼ Acid:B/N Exe. ----TOX Parameter Results mg/1 MICROBIOLOGY (MF) Coliform Colonies/l00mls __ (MPN) Coliform Colonies/\OOmls Parameter -·EDB __ PCB's __ Petroleum __ Endrin __ Lindane ' I'" Recd ved I ate l:>=rr:.ctcd __________________ _ 11.1":'.'.~'j' ~~-... -, --. _-.o-,-, ----------------- Results mg/1 Parameter Paramcrer __ Mechoxychlor __ T oxaphenc _Z,4-0 __ Z,4,5-TP (silvcx) RADlOCHEMISTR Y Results mg/ 1 Dare Reported __________________ _ Date Analy:ed ----------~-------- , '. ', . I' ,.., :. : ~ 1 / ' ,. ! \ ! . ··-·-Lab Number I 1-:~;· . : D,prnm,nt of H~m~n Resou.rccs sion of Health Services SAMPLE ANALYSES REQUEST Stare Laboratory of Public Health P. 0. Box 28047 306 N. Wilmington Street Raleigh, 276 I I ,'l!t,., N~ b~ ,q- lmc of Site . (_ e D /'I Ax r¥2 t°{J'P ;!;; follected By ,/1 -I= De /2().[4: ID# - .oiSample: ll~nvironment2.l Concentrate ._L Groundwater (!) ___ Solid (5) IL_ Surface Water (2) __ ._Liquid (6) Soil (3) --Sludge(7) Field Sample Number __ d_J_~7_2--________ _ Site Locarion --------~f:r-:.,~i1:~d,~-· ... N~c .... 7 ___ _ Date Collected ~P-~-~L~f_-~if~½~--Time / </ '-f. S::: Comments Cima Res;& . (J l l ___ Other (4)· __ Other (8) INORGANIC CHEMISTRY Extractables Pa!°~metcr Arsenic Barium C2.dmium Chromium Lead Mercury Sdenium· Silver Results mg/1 Parameter _,L_Ar.senic ~Barium __,L_ Cadmium __ Chloride -vL--Chromium __ Copp<r __ Fluoride __ Iron _.L Lead __ Manganese -,.LMercury __ Nitrate . ....:,/_ Selenium Results mg/ I .-; f.• / Total Parameter Silvef __ Sulfates __ Zinc _Ph __ Conductivity _ms _TOC Results mg/ I ORGANIC CHEMISTRY Parameter Results mg/1 P&T:GC/MS MICROBIOLOGY Parameter (t,ff) Coliform Colonies/lOOml;· _ (MPN) Coliform Colonies/lOOmls Parameter _EDB __ PCB's __ Petroleum __ Endrin __ Lindane ••He E){(ractc.::i __________________ _ a Rcporr~.:i Uy H5 _1 I 1>1 I R(,•t,;t·J 7185 J ,;,.1 ,.,,.J ~b:..:1!..J.t?..~~ \V ~~tc-{Rn·ic-" 71S i} Results mg/ l Parameter Parameter __ Methoxychlor __ T oxaphene _2,4-D __ 2,4,5-TP (silvcx) RADIOCHEMISTRY Result< mg/1 Results PCi/1 · Date Reponed __________________ _ Date Analy:cd •-·-'~S·J I I Lab Numl:-cr ___________________ _ . CJli.~;rtmc:nt of Human Re:sources ·i\·j-Hc:altl, Services SAMPLE ANALYSES REQUEST State: Ubor:atory of Public Hc:Jlth P. 0. Box 28047 306 N. Wilmington Street Raleigh, 27611 i,clu'."ber -I-N--'--'t~7 .,_/)..,_-__,__Q_,!'1_,_,__A~-------Field Sample Number Z~J r :5 1aJJ of Site _· __ 6, __ -.,.p~• .,_o.,..,.R~-_._n_,)c..,f_,_fb~,.s'--,AO'-Lo,._,u"'P-"=--r-...,1:;'-+---Site Loca:ion 2~ /J C'.'.. :ollfted By ~<-' £0/d-\D# .3R Date Collected fd.-II -£ C, Time / 'r/ 0 -1".&,f Sample: Environmental --ll--Groundwater (1) ___ Surface Water (2) 1--Soil (J) __ Other (4) Concentrate __ Solid (5) __ Liquid (6) ___ Sludge (7) __ Other (8) Comments DuJPo <; f.e c i cO INORGANIC CHEMISTRY Excracta bles P:1ra1neter __ Arsenic I • Barium /=Jcadmi~m , __ Chro~~1um l~ad ercury _ Sel~nium ___ Silver Resuhs mg/1 Parameter ....LArsenic ....£Barium ~Cadmiu;,, __ Chloride .....,.LChromium __ Copper __ Fluoride __ Iron __._L_Lead __ Manganese ---..LMercury __ Nitrate -----~-· ....:L..Selenium Results mg/1 c,. I <0,0003 Total Parameter Silver __ Sulfates __ Zinc __ Ph __ Conductivity __ ms __ Toe - -R-e~su'-'-lt-"s~m=g-/_l_ '· ,I' -<o~ o __ c;- ORGANIC CHEMISTRY Pa-rameter Parameter Results mg/1 Parameter Re,;ults mg/I ---. ---------------1--------------'-----4--------------::;__ __ Results mg/ I __ P&T:CC/MS -.-!\cid:rl/N Exe. .-TOX Parameter MICROBIOLOGY _EDB __ PCB's __ Petroleum __ Endrin __ Lindane $?, };t:: ~ ··l :.·":: l __ Gross Alpha __ Gross Beta __ Methoxychlor __ T oxaphene __ 2,4-D __ 2,4.S-TP (silvex) RADIOCHEMISTRY Resu !ts PCi/ I Date Rcponed ---------------,------ ,·:: ~-s•:cived -'.i .::,:·r,},~i"r:d ___________________ OJtt" An:ily:ed -----,-~-,-,-~----------- U 1'· •·· ! L:ib Number ____ ~_~_-_--'_,_,_' _'._:· ___ , _,_,_7 ..:.c_,..._ ______ _ ii I I I N. C. Department of Human Resources b_sion of Health Secvices . SA~LE ANALYSES REQUEST .. '9 '$1/0Z.,<...0( ~ State Laboratory of Public Health P. 0. Box 28047 306 N. Wilmington Street Raleigh. 27611 Wire Number -~/Yi_c_slc.:7-L/).,__,_/~()"-L-.:...fr_,_ _______ Field Sample Number -~!)~0:~2 _/~2~---------- 1-lame of Site --L0..f.J,✓<-.d<4-<&.w,[_J2t""'°~L--.l=e._~d;uj'-'-'=>--"--'-·---Site Location ______ _,__£%~,..,,d:_c:_,_/✓i-=...,(3~---- Collected By elLt: 'be lu1 Ur ID# 21 ? Date Collected --=2.=--L/ LI _ _,?'-'6'----Time __..,_/.,__Q,_,-i'-LQ.,___ Jype of Sample: Environmental Concentrate I _L_ Groundwater {I) __ Solid (5) ___ Surface Water (2) __ Liquid (6) Comments /J?c Lac-e ce.J1<2. - I __ Soil (3) __ Sludge (7) ___ Other (4) __ Other (8) INORGANIC CHEMISTRY Extractables Parameter __ Chromium __ Lead _ Mercury _·_Selenium Results mg/ 1 Parameter __ Arsenic __ Barium __ Cadmium __ Chloride __ Chfornium __ Copper __ Fluoride __ Iron __ Lead __ Manganese __ Mercury __ Nitrate. __ Selenium Results mg/1 Total Parameter __ Silver __ Sulfates __ Zinc _Ph __ Conductivity _TDS _TOC Results mg/ 1 ORGANIC CHEMISTRY Parameter Results mg/ 1 Parameter .Results mg/ 1 Parameter Results mg/ 1 P&T:GC/MS _EDB __ Methoxychlor Acid: BIN Ext. __ PCB"s __ T oxaphene TOX __ Petroleum _2,4-D __ Endrin __ 2,4,5-TP (silvex) __ Lindane MICROBIOLOGY RADIOCHEMISTRY Parameter Parameter Results PCi/ 1 __ (MF) Coliform Colonies/lO0mls __ Gross Alpha __ (MPN) Coliform Colonies/lO0mls __ Gross Beta ate Reported __________________ _ 1);1.:e Extracted __________________ _ Date Analyzed ___________________ _ Reported By Lab Number l >HS 31ql (R,:viscd 7185) oli,! ;ind H:i::i.rdous \Vast,: fRcvkw //87) I. ( ( .~. C. Ocp~rtment of Human Resources State Laboratory of Public Health P. 0. Box 28047 306 N. Wilmington Street Raleigh, 27611 Division of Health Services SAMPLE ANALYSES REQUEST .. '18/0"2...'2-0 I< Site Number #11 iJ-7?J/t fame o"t Sire -!J ~f; ~ -~ . Jrrhd7J Collected By ~ /1,/):,; ID# 2J )? I y;:,c of Sample: Environmental I _,L__ Groundwater ( l) ___ Surface Water (2) _. __ Soil (3) • --Other (4) Concentrate __ Solid (5) __ Liquid (6) __ Sludge (7) __ Other (8) Field Sample Number __ .,_2,..._C,-l-'l~3=---------- Sire Location .,.......ec:',=:....ecf'-'/'_,_l....,,...,..,l(..c. _('_==---------- Dare Collected _ _,,2..=--,_!,_/_-_f"-'(,=---Time I/ I) I • • Comments 6r:aham Gt?-,r)<f II INORGANIC CHEMISTRY Extractables Parameter J ,__ Arsenic __ Barium I I __ Cadmium ~ Ch:·omium. __ Lead .Mercury I _Sck~ium ,___ Si!vcr , ____ · _____ · Resu l,s mg/ 1 I.------------- 1 ~ Parameter P&T:GC/MS Acid:B/N Ext. TOX Par2meter Results rng/1 MICROBIOLOGY 1--(\1F) Coliform Colonies/l00mls ,= (MPN) Coliform Colonies/lOOmls - Parameter __ Arsenic __ Barium __ Cadmium __ Chloride __ Chromium __ Copper __ Fluoride __ Iron __ Lead __ Manganese __ Mercury __ Nirrate __ Selenium Results mg/1 ORGANIC CHEMISTRY Parameter _EDB _PCB's __ Petroleum __ Endrin __ Lindane Results mg/ 1 Parameter __ Gross Alpha __ Gross Beta Total Pa~ame::er __ Siin:r __ Sulfates __ Zinc -·· -·· _Ph __ Conductivity _TDS _TOC Parameter __ Methoxychlor __ Toxaphene _2,4-D __ 2,4,5,TP (silvex} RADIOCHEMISTRY Results mg/1 Results mg/1 Results PCi/ 1 .),He fn;:ac(eci ________________ _ Date Ar,sly:ed ___________________ _ Lab Number ___ G_,_' ·_·{_J_,_J_,P_:;_C_j ____________ _ R.1..··r,1rn::J Li\· l ,!·i:=-}l'~i (r-:.,.i,d f:S5J ,,::.: .rn.l ii.i:,1~si0:l~ \\1,15:\· (R.c•,ic.•: 7/87) I. ~-Depar:ment of Human Reso~rces Division of Health Services State Laboratory of Public Health SAMP~ANALYSES REQUEST P. o. Box 28047 ~umber /\ ~ l O-Z..:Z..<.9 1 '::, 306 N. Wilmington Street -, Raleigh, 27611 -~,~11'-'(C""_'-/)""'------'/-L.Cf?:,_,Au._ ______ Field Sample Number __ "2-=._,_C/_,l_,__f_· ________ _ ' ame of Site ollected By ~ Ay_ du~ ;;l-DtizµX#? '? Site Lo=ion _ __.Ac..,,.,..,ca--d-,r-1/J-"-"'t:_"------ ,r ~ ,t:_h, W!±._ _...,,;J~?L--Date Collected _ _,,2.=---,_/ ,_1 _-__,f'--"(:,'----Time -1-/-1-/_.,~1Ql.l.L_ 1-ype of Sample: Environmental Concentrate Comments I ~ Groundwater (1) __ Surface Water (2) __ Soil (3) __ Solid (5) __ Liquid (6) ,m -0 b; Jd £ tfzt>l--g. __ Sludge (7) 1---· Other ( 4 )· __ Other (8) I Extractables Parameter Remits m_g/1 EArsenic __ Barium __ Cadmium !=Chromium Lead . Mercury _ Selenium __ Silver -- F -- t Parameter Results mg/ 1 ~P&T:GC/MS '....I.L Acid:B/N Ext. _TOX I= MICROBIOLOGY Parameter (MF) Coliform Colonies/ IO0mls (MPN) Coliform Colonies/IO0mls INORGANIC CHEMISTRY Parameter Results mg/ 1 __ Arsenic __ Barium __ Cadmium __ Chloride __ Chromium __ Copper __ Fluoride __ lron __ Lead __ Manganese __ Mercury __ Nitrate __ Selenium ORGANIC CHEMISTRY Parameter _EDB __ PCB's __ Petroleum __ Endrin __ Lindane · Results mg/1 Parameter __ Gross Alpha __ Gross Beta ll;i:t: Exr:-:i.::teJ ___________________ Date: Analy::cd R:.:port~d Bv L,b Number .. Total Parameter Results mg/ 1 __ Silver __ Sulfates __ Zinc _Ph __ Conductivity _TDS _TOC -- -- -- ---- -- Parameter Results mg/ 1 _._ Methoxychlor __ Toxaphene _2,4-D __ 2,4,5-TP (silvex) -- RADIOCHEMISTRY Results PCi/1 ' ' l.· Depcrt~en< of Human Resources SAMPLE ANALYSES REQUEST State Laboratory of Public Health )i,,.ision of Health Sen•ices P. 0. Box 28047 h.mber q'lSIO-Z.l 10?_ 306 N. \~lilmington Street LS Raleigh, 276 I I N {!_ /) -Tij_ I-}-Field Sample Number 2fl I Im, df Site t'.£d>Oacrf 14qp /,-0,e--1 Site Location l?e.--f Al<!.. J llccted By _fl,, ;t Z;)e fZo [tr f (, Time / 'f:. ~ ~ ,- ID# )? Date Collected 2--11-I [ of Sample: nvironmental Concentrate Comments C Groundwater (I) __ Solid (5) lJ.~ if<f (l_g°tt ~tfl- .. .. Surface Water (2) __ Liquid (6) __ Soil (3) __ Sludge (7) 1---C,her (4) . C -, __ Other (8) ' ·-·-~;,:.::. -INORGANIC CHEMISTRY Extractables Total .,· Paramt~tcr Resu Its mg/ 1 Parameter Resulcs rog/1 Parameter Results mg/1 FA~ .. ~:· __ Arsenic __ Silver --Barium __ Barium __ Sulfates __ Cadmium __ Cadmium __ Zinc I== Chromium __ Chloride _Ph Lead __ Chromium __ Conductivity ~ercury __ Copper _ms cienium __ Fluoride _TOC ilver __ Iron -- --__ Lead -- F __ Manganese -- __ Mercury -- __ Nitrate -- __ Selenium -- I ORGANIC CHEMISTRY ·-· Parameter Results mg/ l Parameter Results mg/1 Parameter ·-~~--~· Results mg/1 ~P&T:GC/MS _EDB __ Methoxychlor ~ Acid:B/N Ext. __ PCB's __ Toxaphene _TOX __ Petroleum _2,4-D I= __ Endrin ' __ 2,4,5-TP (silvex) __ Lindane -- I MICROBIOLOGY RADlOCHEMlSTR"\'. Parameter Parameter Results PCi/1 ., --(MF) Coliform Colonies/lOOmls __ Gross Alpha '= (MPN) Coliform Colonies/lOOmls __ Gross Beta . -- I ---- , Rect:ived -% d,l-t:_c,q_ /2,; /. · ·,/9,<,;:;.e>(;Z,) Date Rcpomd I ~ I [. Departmc:nt of Human Resources Division of Health Services State Laboratory of Public Health P. 0. Box 2804 7 306 N. Wilmington Street ._ 9'if/0'2. 2-07 ':;2__./ s!Wmber -----'--/._,__/ C~/)_--_,~~&C.L.:t:.-'---~----'-· _ Field Sample Number ~ d Vb rw,e of Site IB1; /Jc.d;il~ >4v,o ~-Site Loca:ion 1-?od, NC Raleigh, 27611 caected By ,f/2, H\-e n1)J k I~ _if'-"''----Date Collected -""2c:...-~l,_,__/_-_,,Y"--'(."'----Time ; 21 (:J Tl of Sample: vironmental ~ Groundwater (I) I=--Surface Water (2) __ Soil (3) 1--Other (4) Concentrate __ Solid (5) __ Liquid (6) __ Sludge (7) __ Other (8) -INORGANIC CHEMISTRY ~ Extractables Parameter Results mg/1 .A_rsenic Barium __ Cadmium .Chromium Lead ~ercury leriium Iver -- :l -- . Parameter Results mg/ 1 r-J"P& T:GC/MS __ Acid:B/N Exe. _TOX :t MICROBIOLOGY Parameter __ (MF) Coliform Colonies/lO0mls =I (MPN) Coliform Colonies/lO0mls . Parameter Results mg/ 1 __ Arsenic __ Baritim __ Cadmium __ Chloride __ -Chromium __ Copper __ Fluoride _._# Iron __ Lead _._Manganese· __ Mercury __ Nitrate __ Selenium ORGANIC CHEMISTRY Parameter _EDB __ PCB's __ Petroleum __ Endrin __ Lindane Results mg/1 Parameter __ Gross Alpha __ Gross Beta· Comments 0 w-ft'1 _f ,rt;./! 'cf . .. Total Parameter Results mg/1 __ Silver __ Sulfates __ Zinc -_· Ph -- __ · Conductivity _TDS _TOC -- -- -- -- -- -- ., Parameter Results mg/ 1 __ Methoxychlor __ Toxaphene _2,4-D __ 2,4,5-TP (silvcx) -- RADIOCHEMISTRY Results PCi/ I .. I PURGEABLE COHPOUNOS COHPOUND loranethane bn:m:xnethane ·chlorodifluoranethane nvl chloride loroethane methvlene chloride ichlorofluoranethane ene. 1. 1-dichloro ethane 1. 1-dichlo!'O" ,-trans-dichloroethene orofonn . ethane. 1.2-dichlo!'O" une. l.Ll trichloro- --hnntetrachloride "fflVfichloranethane r ane 1 2-dichloCO" -trans-di ch lo, ne chloroethvlene libn:m:xnethane , 1 1.2-trichloro- s-dichlo ne 2-<:hloroethvl vinvl ether form STATE LABORATORY Of PUBLIC HEALTH DIVISION Of HEALTH SERVICES, N.C. DEPARTMENT Of HUMAN RESOURCES ·P.O. BOX 28047 -306 N. WILHINGTON, ST., RALEIGH, N.C. 27611 ORGANIC CHEHICAL ANALYSIS LAB NO D./'; 1,i/. (-· J /,,/! C<rV"t· l~/2C, l/,1''; /../!(i-f,Jtf FIELD# .2--C//(, , 4/'i 'Hi/1,1 , 4 /?, TYPE ( I l ( /} t I l ( /) UNITS ,..6/1\un/ka f.n/ 1 \,nfkn &/l ! .. n/ka ,(,n/1 ),on/ka .....,_-, A ~ WI -' ,,,___,,,, .11 I ' ~· , : .. - . ane. 1. 1 2.2-tetrachloro- ethene tetrachloro- luene orobenzene ' , I ethvlbenzene '\ I I / ' I \ I . ! tone I /I I I. I ; utanone . , carbondisulfide 2 exanone 4 thvl z_,,,.ntanone stvrene V 1 acetate . lene \ I \ I I 'I . ,. l K ctual value is known to be less than value given. ~tJ{)' , ..... :,-7 ,2_q '2-- ( ) '-n/ 1 '.• ,n/ka = I A I ~· ·--. I \ I A ' ' I J ijst1mated value. L tual value is known to be greater than value given. U -terial was analyzed for but not detected. The nurber is the Hini1TU11 Detection Limit. Not analyzed. Tentative identification. ~ On NROC List of Priority Pollutants. N.C. Division of Health Services DI 3068-0 (4/86 Laboratory) / / V ) £n/L .. n/ka .. .. BASE/NEUTRAL ANO ACID EXTRACTABLES · CXJMPOUNO \ itrosodimethvlamine 12-chloroethvl)ether hlornnhenol henol 1 -<lichlorobenzene 1 -<lichlorobenzene 1 . 2--<1 i ch 1 oroben zene b" (2-ch loroi 1\ether h ch loroethane N-ni troso-di -n ..nNV'\vlamine n; robenzene ~ hhorone 2 itroohenol 2 4-<limethvlohenol b 2-chloroethoxv)methane 2 i ch l orooheno 1 1 2 4-trichlorobenzene n thalene h ch 1 orobutadi ene 4-c 1 oro--01-creso 1 hex rocvcl(V)pntadiene 2 -richloroohenol 2 loronaohthalene acenaohthvlene d" thvl ohthalate 2 initrotoluene acenaohthene £, Alinitrnnhenol £, .dinitrotoluene 4-troohenol fluorene loroohenvlohenvlether di hvl ohthalate 4,6-<linitro-o-cresol ~amine ne 4 henvlohenvlether hexachlorobenzene ch 1 orooheno 1 0 nthrene anthracene ~vl ohthalate anthene ( ( STATE LABORATORY OF PUBLIC HEALTH DIVISION OF HEALTH SERVICES, N.C. DEPARTMENT OF HUIIAN RESOURCES P.O. BOX 28047 -306 N. WILNINGTON, ST., RALEIGH, N.C. 21611 ORGANIC CHENICAL ANALYSIS LAB NO 1./){yU,r f /.bOllfrc.,t /..-,JI') I '1(:UY, FIELD # ,.J Cf/(,, J <j/,1 J qj(t o1 q /~ TYPE (/ 1 I I l r I) ( I \ UNITS run/ f\1,n/ko un/J ',on/ko un/J).,n/ko 1,,n/ 1 )un/ko ~-I A I /I -I A I • . . / ' l_j t'", k_ / ,1 ,. -- • I I , I I V/ \ I \ I ,! Ir, k IOI< /0 I<. !() I< ;_.,, /// / ,1 I A ( ual value is known to be less than value given. ' /4C' C LJ ,r / )6/; c / l /un/1 ,,n/ko I - ., -· I 1 ' I I\ ',/ i,, l ~stimated value. --ua) value is known to be greater than value given. J -ter1al was analyzed for but not detected. The nurber is the Nini1TUT1 Detection Limit. IA.I Not analyzed. I/ Tentative identification. · (I On NROC list of Priority Pollutants. '. ii V,i_v.u.fon 06 He.a.Uh SVtvic.u 'H-113068-0 (4/86 La.botr.a..to11.y) / / V ) zfn/ 1 .. n/ko ,. ,. , I BASE/NEUTRAL ANO ACID EXTRACTABLES COMPOUND rene nzidine butvl benzvl ·nhthalate nz(alanthracene rvsene 3.3-<!ichlorobenzidine ls(2-ethvlhexvllnhthalate -n-octvl ohthalate benzo(blfluoranthene nzo(k)fluoranthene nzo(a)nvrene deno ( l . 2, 3-cd) nvrene dibenzo(a.hlanthracene nzo(a h il=~lene iline zoic add I alcohol roani line ofuran wlnanhthalene 2-methvlnhenol IIthvlohenol troani 1 i ne 3-nitroaniline -itroani 1 ine , .5-tri ch lo'"""henol 1 j ( STATE LABORATORY Of PUBLIC HEALTH DIVISION Of HEALTH SERVICES, N.C. DEPARTMENT Of HUl1AN RESOORCES P.O. BOX 28047 -306 N. WILMINGTON, ST., RALEIGH, N.C. 27611 ORGANIC CHEMICAL ANALYSIS LAB HO l',./,/5 ,(j y f ,,,_ /JO 1/-Y~ ?-no I/..Y5 1-arorr. FIELD# , ell t; -:2AJ.S-,,2.u11/ .;J..'/1, TYPE ( / ) LI) c I j ( / \ UNITS ,.J(; 1 un/ka A,n/1 : .. n/ka Aon/ 1 ',,n/ka Aon/f)un/ka ~;_.., -....-J A ~ IA '--? I 1 . I , , "' ' ' 'I .. I I y .. I {}V . ,_,,., I:' .. .. . I ' I A I ' / , , I \ \ I \I/ \ ,.,, .. 1/1 I " 1/1 ' I I I I / I I \:/ '·I ' I \ I J ~timited value. K .. tual value is known to be less than value given. /_/,(: y:<.-' / 1'1LL ( I\ l,'n/ 1 un/ka ~ l.,~ I · I 0·1✓ I " '. ~ I ' I I /l I ' I . ·-.-:-• L -tual value is known to be greater than value given. u, llaterial was analyzed for but not detected. The nuroer is the Mininun Detection Limit. Not analyzed. l Tentative identification. f -On NRDC List of Priority Pollutants. N •• V.i..v.u.wn 06 ffe.a.Uh Svr.v.i..c.u vta 3068-0 (4/86 Labotw.,tol/.lf) / / y l I /,a/ 1 · un/ka .. .. I I I I I I I . Wells Sampled by I Cleveland County I Health Department I I I I I I I . •• I I WELL NO, , 102 • / 101 e I I I I ( I I \ I OWNER 100 82 • 69 • 38 • 30 • l I I --,1/·· • 5;...--/ ,-:__~--,;,-;::::-,,--- -WELL SURVEY BOUNDARY LEGEND SAMPLED WELL LOCATION FIGURE 2.::10 OFFSITE .,WELL LOCATION MAP CFO / SHELBY, N.C. S&ME JOB NO. 1175-85-0SOA -,·pc of Sample: Environmental _x_ Groundwater (!) L-Surface Water (2) __ Soil (3) 1--Other ( 4 f Concentrate __ Solid (5) __ Liquid (6) __ Sludge (7) __ Other (8) INORGANIC CHEMISTRY Extractable• Parameter Arsenic __ Barium __ Cadmium .._Chromium .._Lead ,•~~~~u: Silver t= Parameter P&T:GC/MS __ Acid:B/N Ext. _TOX Results mg/I Resulu mg/1 =1-· --- . MiCROB!OLOGY Parameter __ (MF) Coliform Colonies/lO0mls =1 (MPN) Coliform Colonies/lOOmls Parameter 1Arsenic .L..Barium ..LCadmium LChloride ...L..Chromium LCoppe, 1Fiuoride -'j-~a~ . 1-Manganese LMercury 1Nicrate ...d....sdcni~ Results mg/1 o. "J <Oc I <LJ,03 -<o. o3 8RO,UHC CHEMISTRY Parameter _EDB __ PCB's __ Petroleum __ Endrin __ Lindane Results mg/1 Parameter __ Gross Alpha __ Gross Beta Total Parameter Silver Sulfates Zinc ...LPh Conductiviry IDS TOC Parameter __ Mechoxychlor _. _. T oxaphene _2,4-D __ 2,4,S-TP (silvcx) RP,PIOCHl.l UEiTlt'L' Results mg/ l Results mg/1 Results PCi/1 :>\a,xrracrcd __________________ · Dare Analyzed Lli I uc: I HOV lC 07 oorrcd By -------------------Lab Number ----~-------------\ IJG! (Rcv1yJ 7185) !"''. iil:.1rdot1' u1~qr(f.'r,•ir"• 7:G-;1 •·: ~--Dspartmcnt of Human Resources lllt1vis1on of Health Services - -JJN✓ SAMPLE ANALYSES REQUEST State Laborato~y of Public Health P. 0. Box 28047 306 N. Wilmington Srreet Raleigh, 2761 I _,2.;'=-'3'-"'D...L.!..o~o.L..>-3..1...4.1..4__,_,.feec...'1..!....kc:.2:.LI _,--_ Field Sample Number _,Q--.L....::=Oc'.....3~1,_;3""-(o=· ----,------ ~:5"-" / 11\ I \ C I .tame of Site ====_!_..:.:;==--1.===:..:6:cc:;Lr:..i,,C-''C...C::-.o....-=2-'----Site Location ~ e\) e.\9-N10,,D\J0\'b-< l:ollccted By ID# -'l~Z. ___ Date Collected // -/ 0 -'ii, 7 Tim~ o< 66 PIY/ alype of Sample: I Environmental -2(_ Groundwater (1) 1---Surface Water (2) Concentrate __ Solid (5) __ Liquid (6) __ Sludge (7) __ Other (8) Comments ::D, ~ "'\s '"'S ~°' k vX \\ ;s 0-lffi ~\ e __ Soil (3) 1--Other (4) I Extractables Parameter Results mg/ 1 l=Arsenic Barium __ Cadmium I== Chromium Lead 1ercury F e_l~niu!"_:__ -Silver _ I= -- I Parameter Results mg/1 tz,P&T:GC/MS ai::Acid:B/N Ext. -I= J.HGRODIOLOO'lt Parameter __ (MF) Coliform Colonies/lO0mls I= (MPN) Coliform Colonies/lO0mls . . .. .. ntoRo · >ac ettEhHsrnu Parameter Results mg/ 1 __ Arsenic __ Barium __ Cadmium __ Chloride __ Chromium __ Copper __fluoride __Iron __ Lead - __ Manganese __ Mercury __ Nitrate __ Selenium ORGANIC CHEMISTRY . Parameter _EDB __ PCB's __ Perroleum __ Endrin __ Lindane Results mg/ 1 Parameter __ Gross Alpha __ Gross Beta Total Parameter Results mg/1 __ Silver __ Sulfates __ Zinc _Ph --Conductiviry _ms _Toe -- -- -- -- . -- -- Parameter Results mg/ 1 __ Methoxychlor -__ -Toxaphene _2,4-D __ 2,4,5-TP (silvex) -- RADlQCHF> US'FR Y Results PCl/ 1 /-;J-f -,f ,?' Date Reported --~-'-----'----...:::.~~---------f'' . -.. . ;r"' v~ l e Exrracted f~'l-·7 cl/fi·'fl _ · Date Analyu,d 0.<<1< 7,-"'-cr' }2/i,/10 ' (/-,;-ri 1/' _/Li"c-(___,i(___ 70309? r 1 1 ortccl By ""'""'.~c/....,.c-"-----'----------Lab Number __________________ _ ' 3191 [R,vi,cd 7185) J and Ha:ardous Wasre (Review 7 /87) I /NEUTRAL AND ACID EXTRACTABLE$ I COMPOUND N-nitrosodimethvlamine s (2-ch loroethyl )ether h l ornnheno l oheno l I r--<li ch lorobenzene 4--<lichlorobenzene 2--<lichlorobenzene bis (2-ch loroi l)ether lxachloroethane nitroso--di-n-""rnnvlamine ni trobenzene ~horone trophenol .. 4--<l imethvl oheno l bis(2-chloroethoxvlmethane 4--<l i ch l orooheno l 2.4-trichlorobenzene nanhthalene xachlorobutadiene hloro-m-cresol 31orocvcl"""ntadiene trichloroohenol .rh l oronanhtha l ene enanhthvlene dimethyl ohthalate 6--<linitrotoluene en.:1r.hthene 2.4--<linit.-nnhenol 4--dinitrotoluene nitrophenol uorene rh l orophenv l ohenvl ether ethvl ohthalate 6--dinitro-o-cresol diohenvlamine obenzene r~henvlohenvlether hexachlorobenzene ntach lor~heno l enanthrene thracene dibutvl ohthalate uoranthene STATE LABORATORY Of PUBLIC HEALTH DIVISION Of HEALTH SERVICES, N.C. DEPARTMENT Of HUMAN RESOURCES P.O. BOX 28047 -306 N. IIILHINGTON, ST., RAIEIGH, N.C. 27611 ORGANIC OIEHICAL ANALYSIS LAB NO '1 t}_) c:J Y ;1 FIELD# ,,/ Yv TYPE ( I l ( ) ( ) ( l UNITS { uol I I mr/lib ua/ I un/ka uo/l uo/ko uo/ l un/ka /fl/;,~ u _ _,, .. - SQI '&.SO /OJ 330 ,01 "A"O J0/"30 "' 501 11'-',() l J,, to/.330 /n/'l~n so/11,,:ro J/11:nn ,, ..,v m l)L -Actual value is known to be less than value given. ,,.- ( l un/ l · un/ka ' -Estimated value. H,_O/SO/ J._ ~ctua~ value is known to be greater than value given. W!1ater1 al was analyzed for but not detected. The nunoer is the Hin inun Detect ion Limit. ;17}) L NA -Not analyzed. I -Tentative identification. -On NROC List of Priority Pollutants. N. C. D-i.v.u.,-i.on oo He.a,Uh Se.1tv-i.cv, 1s 3068-0 I 4 / 86 Labo,ta,to-1u) ( l un/ l un/ko I •• I I I I I I I •• I I I I I I BASE/NEUTRAL ANO ACID EXTRACTAlllES COMPO.IND nvrene benzidioe butvl benzvl ohthalate benz(alanthracene chrvseoe 3 3-<lichlorobenzidine bis(2-<>thvlhexvllnhthalate di-n-octvl nhthalate benzolblfluoranthene benzo(klfluoranthene benzo (a' ""reoe indeno( 1.2 3-<:dlnvrene dibenzo(a h)anthracene benzo(n h. iloervlene aniline benzoic acid benzvl a lcoho 1 4--ch loroani 1 i ne dibenzofuran 2-<rethvl 0 •""tha 1 ene 2-<rethvlnhenol 4-<nethvlohenol 2-ni troani line 3--ni troani line 4-nitroaniline 2 4 5 trichlo-henol STATE LA!lOHATOHY Of PUBLIC HEALlH. DIVISION Of HEALlH SERVICES, N.C. OEPMTMENT Of HUMAN RES()JRCES P.O. BOX 28047 -306 N. \.IILMINGTON, ST., PALEIGH, N.C. 27611 ORGANIC OlEMICAL ANALYSIS LAB 00 '7,1 ,,,.,9 7 FIELD# 3 ·///ct' · TYPE r I l ( ) ( ) ( l UNITS ( .. n/) ""~ko un/) un/ko un/) un/kn .. n/) .. n/ko /0/:,c,,, "'-- _-<;n/th50 10I::i=io J, so/Jt.,;,, 1o/?3n 1/o/.J?o Soi" ·,u ,!/ ✓./ <o lu,,r (A_, • I, tn/=i:,o .. ,, S"o ,,,_<o ,:, ,v I.~ -Estimated value. ~ -Actual value is known L -Actual value is known mDL H:a.0/ So!L to be less than value given. to be greater than value given. I I U -Material was analyzed NA -Not analyzed. for but not detected. The nuroer l/ -Tentative identification. ~I -On NROC List of Priority Pollutantc_;, N. C. D.i..v..i...,;{(111 06 l{c.a..t01 Sellv--lce.,~ DIIS 306 8-Q I 4 I 86 1.a.bu~ato,u;I 1s the Nininun Detection Limit. ; ., ( l ( ) ""II ··"/ko un/1 uo/ko /!12> L STATE LABORATORY Of PUBLIC HEALTH I •• I DIVISION Of HEALTH SERVICES, N.C. DEPAATMENT Of HUMM RESOU~CES P.O. BOX 28047 -306 N. ll!LM!NGION. SI., RALEIGH, N.C. 27611 I I I I I I I I I I I I I PURGEABLE CXl'IPO.RWS CXl'IPOOND chloranethane brcm:rnethane dichlorodifluoranethane vinvl chloride chloroethane methvlene chloride trichlorofluoranethane ethene. l 1-<lichloro ethane l 1-<lichloro- l 2-trans-<lichloroethene chlorofonn ethane. 1.2--dichloro- ethane. l l 1-trichloro- carbontetrachloride brorrodichloranethane DrlY'lane l 2-<lichloro- l 3-trans-<lichlo ne trichloroethvlene chlorodibrararethane nzene ethane l 1.2-trichloro- l 3-c i s-<I i ch l oroc rooene 2-chloroethvl vinvl ether bronofonn ethane. l l 2 2-tetrachloro- ethene tetrach l oro- toluene ch lorobenzene ethvlbenzene acetone 2-butanone carbondi sulfide 2-hexanone 4-irethvl-2-nPntanone stvrene vinvl acetate xvlenes t+d-all J -Est1rnated value. ORGANIC OlEMICAL ANALYSIS LAB NO "1()/t"'-! 7 FIELD I 1'/XC: TYPE ( I l ( ) ( ) ( ) UNITS ruQ/J ua/kq ua/1 un/ko uo/ l uo/kq uo/1 ua/kq / (,' u J{) ~'1_,i) il) JU ', /AJ s • , ' JO s ·I/ /0 ' J I() ', IG JC > I() I > ,J; jV/IL Ii• I 1 / 1/ I K -Actual value is known to be less than value given . • -Actual value is known to be greater than value given. -Platerial was analyzed for but not detected. The nurber is the Minirrun Detection Limit. NA -Not analyzed. I l/ -Tentative identification. ~/ -On NROC List of Priority Pollutants. N.C. Division of llealth Services I DIIS 3068--0 (4/86 Laboratory) ( ) ( ) uo/1 uo/ko ua/ l un/ka L. C. Department of Human Resources Division of Health Services SAMPLE ANALYSES REQUEST State Laborato'ry of Public Health P. 0. Box 28047 306 N. Wilmington Street ~2.;_<=>-3,_,}).:...L!Q~0"'--'-3.L4..l...-'4L4?>e....c't'....2.~j __ Field Sample Number UO 3 2)-c) (_, rame of Site (YL-Wt (~u_, C F6 #Z dr { ' ;,j Site Location c:, \ e 0 e. \Q.AI\ d C10 Ly.\'½:}, Raleigh, 2761 I ) -=ollected By Ba.\:i\a { &I (-P Q ID# ___,_\..=.2.. ___ Date Collected 7 ,Qj P ] Tim~__:_';i_:,c._7/..::.v~J ~ /) ,7 Ll ;v F s b l;r ype of Sample: C.O '7 Environmental Concentrate _.2(_ Groundwater (1) __ Solid (5) I ---Surface Water (2) Comments :D, ~ "'"''"::) \AO.¼ v,K, \\ 6Cl® ~E' __ Soil (3) I __ Other (4) __ Liquid (6) __ Sludge (7) __ Other (8) lti0RO:t\N'1C EllElwHSTRY I Extractables Parameter Results mg/1 Parameter Results mg/ 1 1--Arsenic __ Arsenic __ Barium __ Barium __ Cadmium __ Cadmium I __ Chromium __ Chloride __ Lead __ Chromium .Mercury __ Copper I _ Selenium __ Fluoride __ Silver __ Iron __ Lead ----__ Manganese I --__ Mercury --· __ Nitrate __ Selenium -- I ORGANIC CHEMISTRY Parameter Results mg/ 1 Parameter Results mg/ 1 I v&T:GC/MS EDB ~~B/NExt. __ PCB's __ Petroleum I ----· Endrin --__ Lindane I l,HeiR8B18f:::8Bri.~ Parameter Parameter __ (MF) Coliform Colonies/l00mls __ Gross Alpha I __ (MPN) Coliform Colonies/lO0mls __ Gross Beta -------- I I ?:: Total Parameter Results mg/1 __ Silver __ Sulfates __ Zinc _Ph --Conductivity _ms _TOC -- -- ---- -- -- Parameter Results mg/ 1 Methoxychlor __ . Toxaphene _2,4-D __ 2,4,5-TP (silvex) -- ~ .. glQCWIII H6..R1£ Results PCi/ 1 a_ Ci - IN. C. Depanment of Human Resources Division of Health Services SAMPLE ANALYSES REQUEST State Laborato\-y of Public Health P. 0. Box 28047 306 N. Wilmington Street • • Raleigh, 2761 I Site Number ----"4=--3'--'1)"'--"...,,0""-'-0~3.-c..'-t..,_4.,__,l,,"'-'t'-"'2.c:...Lj ___ Field Sample Number Cx:J .3 Jc'.) 7 • Name of Site Yv10 fu..i): .. 0 GJg_,~9:--, ~-Fo id--::> d fl lbdsite Location Q,\ eu e.l°="'J C,,01,JJAh Collected By Ba.bb { r-'.J f / dt) ID# __,_1..:::2..:c__ __ Date Collected ·7 -.:2 ]-8 7 Tim~--'9-~--"-1-7_ • Type of Sample: Environmental I _x_ Groundwater (1) ___ Surface Water (2) __ Soil (3) I __ Other (4) Concentrate __ Solid (5) __ Liquid (6) __ Sludge (7) __ Other (8) Comments :n--~~'':) IA°'-¼ v.x.\\ 6<l®£\e lfli~REh•t~He @ttet,ffS~Y I I I I I I I Extractables Parameter Results mg/1 __ Arsenic __ Barium __ Cadmium __ Chromium __ Lead ... Mercury ~.Sce_l~l}ill!TI. '.. __ .silver -- --.. -- -- -- Parameter Results mg/1 I ~P&T:GC/MS cid:B/N Ext. 1~lOX J,HGRODIOLOOi'ii Parameter __ (MF) Coliform Colonies/lOOmls __ (MPN) Coliform Colonies/lOOmls Parameter Results mg/ 1 __ Arsenic __ Barium __ Cadmium __ Chloride __ Chromium __ Copper __ Fluoride __ lron __ · Lead __ Manganese __ Mercury __ Nitrate __ Selenium ORGANIC CHEMISTRY Parameter _EDB __ PCB's __ Petroleum __ Endrin __ Lindane Results mg/ 1 Parameter --Gross Alpha __ Gross Beta Total Parameter Results mg/ 1 __ Silver __ Sulfates __ Zinc _Ph __ Conductivity _ms _TOC -- ---- -- ---- Parameter Results mg/1 __ Methoxychlor _· _. Toxaphene _2,4-D __ 2,4,5-TP (silvex) -- R...t\..lJIOCHFl HST-IW Results PCi/ 1 e Received __ / __ -_,_U""---"2'--·--"-J-_·_,7,.c..~--'-;:;--=' _______ Date Reported--~--------------tate Extracted---------------'---- Reported By Date Analyzed _________________ _ Lab Number 7 () / '.7& ~ llitts 3191 (Revised 7185) ~lid and Huardous Waste (Review 7187) VO.fl I N.' ~-,Depa;tmcnt of Human Resources Division of Health Services SAMPLE ANALYSES REQUEST_ State Laboratol'y of Public Health P. 0. Box 28047 306 N. Wilmington Street Raleigh, 2761 I I Type of Sample: Environmental I _L Groundwater (1) __ Surface Water (2) __ Soil (3) I __ Other (4) Concentrate __ Solid (5) __ Liquid (6) __ Sludge (7) __ Other (8) Comments :n--~ v,1/i \~ V::,Q. ~ W:t \\ 60..w, ¢ e Hig1R8!ltfiife @ttet,HS=rRY Extractable& Total Parameter Re&ults mg/1 Parameter Re&ults mg/ 1 Parameter Results mg/1 __ Arsenic __ Arsenic __ Silver __ Barium __ Barium __ Sulfates __ Cadmium __ Cadmium __ Zinc __ Chromium __ Chloride _Ph __ Lead __ Chromium -__ Conductivity· -=Mercury __ Copper _ms Selenium __ Fluoride _TOC __ Silver __ Iron -- --_Lead -- --__ Manganese --__ Mercury ---- --__ Nitrate -- --__ Selenium -- I I I I I I I ORGANIC CHEMISTRY I I I Parameter Re&ults mg/1 ~P&T:GC/MS ~~B/NExt. -- -- J,HGRODJOL007J.T Parameter . __ (MF) Coliform Colonies/lOOmls __ (MPN) Coliform Colonies/lO0mls -- -- Parameter _EDB __ PCB's __ Petroleum __ Endrin __ Lindane Re&ults mg/ 1 Parameter Results mg/ 1 __ Methoxychlor __ . Toxaphene _2,4-D __ 2,4,5-TP (silvex) -- &i'.aJ;.llOCHFl flS::.A: Y Parameter Results PCi/ 1 __ Gross Alpha __ Gross Beta .. ·- -- -- •• Received __ ..::./_------"'c).:::...._L...7_-"'-S--_),"--'e<';e:::.....:'-~,'-'---Date Reported _____________ _ .Date Extracted _________________ _ Reported By Date Analyzed ---::::--------------- Lab Number 7 0 / 9 02 s:= IOHS 3191 (ReviS<d 7185) Solid and Hazardous Waste (Review 7/87) !Vo» IN: C. Depa,:tment of Human Resources Di";sion of Health Services SAMPLE ANALYSES REQUEST State LaboratoTy of Public Health P. 0. Box 28047 306 N. Wilmington Street Raleigh, 27611 •• /]• ,14 0 . .,,;-9110 S, re Number -<=h=-3·0-'J)"--'-_,,,0""-""0~3_,_:r_.__._,(p"'--'t'-"'2=-'-I ___ Field Sample Number -~'-"D"-""._)'--__j.;:->,lf,:._1-1 _______ _ • Name of Site .,,n_,_1'-"c-"bJ='sc:JL==.·---"'~""--"'ks.;,'-'aacik"'' ,..4,"'-'r'-"-5'"",,_:.l=\-'-'-'3'--'l-~;,;~· r~e.wrl_ Site Location C., \ e \) e. \Q-','\ J C;o \.,/0\h B l I > 1\ \" '/-13-0~ (S Collected By -'""'-=°'-"Xc..>'O""-'i'--"""-"--l1l_sl.o"'-.. '--(),_ __ ID//-'--'--,<.. ___ Dare Collected "' • O I Time • Type of Sample: Environmental Concentrate --.X_ Groundwater (!) . __ Solid (5) I --Surface Water (2) __ Liquid (6) Comments '1), ~ Xl½'':) ~o. ¼ ~ \\ 6 0--ffi ~ f --Soil (3) __ Sludge (7) I --Other (4) __ Other (8) Hi~R8.li:?He en~bffSTRJ. I Extractable• Total Parameter Results rng/1 Parameter Results mg/1 Parameter Results mg/1 I __ Arsenic ' __ Arsenic __ Silver __ Barium __ Barium __ Sulfates __ Cadmium __ Cadmium __ Zinc I __ Chromium __ Chloride _Ph __ Lead __ Chromium __ Conductivity .Mercury __ Copper _ms I _ .. $eJel)iurn_'. _ __ Fluoride _TOC __ ··Silver __ Iron --__ Lead ---- --__ Manganese --I -·-__ Mercury ----__ Nitrate -- --__ Selenium -- I ORGANIC CHEMISTRY Parameter Results mg/ l Parameter Results mg/ l Parameter Results mg/1 I ~P&T:GC/MS _EDB __ Methoxychlor :::;?Ac,d:B/N Ext. __ PCB's __ . Toxaphene 'fOX __ Perroleum _2,4-D I= __ Endrin __ 2,4,5-TP (silvcx) __ Lindane -- I J,116iR:SBIBf::88'1~ ~ .. g1gcwa1 !IS.RY Parameter Parameter Results PCi/ l , __ (MF) Coliform Colonies/lOOmls __ Gross Alpha I= (MPN) Coliform Colonies/lO0mls __ Gross Beta '. ------ .K.eceived ---?'-<} 7-5 ?~If Date Reported 1 ,., •• ' f.,.. 13 ' h/i::J ' ,-., ,,. -i·:\ , . 1-h --, r- ' ate Extracted , ·; .\ -,, I ' I Date Analyzed _ _.&''-•.,..2,._Y''-, r;,-9:;,ti,4.,i~.§<=;;i~.,_•,-~~--"-S'-·.i.l.i.'1_-._r..,7"'1.,_'1All,,.· '-- eportcd By -------------------Lab Number __________________ _ a,is 3191 (R,v;..,d 7185) .iiJ and Ha:11rdous Waste (Review 7 /87) {l~ cle /1-?ov//_ IN:. C Department of Human Resources Division of Health Services SAMPLE ANALYSES REQUEST State Laborato\-y of Public Health P. 0. Box 28047 306 N. Wilmington Street •• Sire Number .Name of Site Collected By • Type of Sample: Environmental _x_ Groundwater (I) I ---Surface Water (2) __ Soil (3) I --Other (4) Concentrate __ Solid (5) __ Liquid (6) __ Sludge (7) __ Other (8) Raleigh, 2761 I Comments :::D, ~ "'\; '"':) v::,o_ ~ '-'-X \\ 6 °=® ~ e Hi~RB,~"ne @tt~!,ffS=rR:V I Extractables Total Parameter Results mg/ 1 Parameter Results mg/ 1 Parameter Results mg/1 I __ Arsenic __ Arsenic __ Silver __ Barium __ Barium __ Sulfates __ Cadmium __ Cadmium __ Zinc I __ Chromium __ Chloride _Ph __ Lead __ Chromium --Conductivity __ Copper _ms .MercurY __ Fluoride _Toe 1 .. _$~1,niu,n_'. .. --. · -Silver . __ ·· Iron ---__ Lead ----. __ Manganese I ----__ Mercury ' -·-----__ Nitrate -- --__ Selenium -- I ORGANIC CHEMISTRY Parameter Results mg/1 Parameter Results mg/1 Parameter Results mg/1 I ~& '.:GC/MS _EDB __ Methoxychlor ±Tcta:B/N Ext. __ PCB's __ . Toxaphene OX __ Petroleum _2,4-D II= __ Endrin __ 2,4.S-TP (silvex) __ · Lindane -- 1----~--~1~,(~l§G~R~O~B'.!l§O~L~O~O~\~' __ _: _____ ,-______ _.:!R~.1~A,~J;)~l~G~C~H~F~'~l~JS!J:a~~l'.::' :_ ______ ~ Parameter Parameter Results PCi/ 1 __ (MF) Coliform Colonies/lOOmls E (MPN) Coliform Colonies/lO0mls __ Gross Alpha __ Gross Beta Date Reported------,--------------- "" Extracted __________________ Date Analyu:d ~----------------- !eportcd By _________________ Lab Number -'--7i_0_ .. 4L_'zL..J.%'.;__,,,,-"-;;-"6""----------- i.;s 3191 (Revised 7185) lliJ .ind Ha:nrdous Waste (Review 7/87) /j/{J // IC. De;artment of Human Resources Division of Health Services SAMPLE ANALYSES REQUEST State Laboratory of Public Health P. 0. Box 28047 306 N. Wilmington Street Raleigh, 27611 ~of Sample: ~nvironmental ..----2(_ Groundwater (I) L_ Surface Water (2) Concentrate __ Solid (5) __ Liquid (6) __ Sludge (7) __ Other (8) Comments »'" ~ n¼ )~ t,ao_ ~ V-.,'-<_ \\ 6 OJffi ~ f Soil (3) C Other (4) Extractables Parameter ercury _____ ;i~l~Di~ro _ _:. __ _ · -Silver .__,,_~T:GC/MS id:B/N Ext. ox Results mg/1 Results mg/ 1 J.HGRODlOL001l Ui0ROAl'tlC CflE!tHSTRY Parameter __ Arsenic __ Barium __ Cadmium __ Chloride __ Chromium __ Copper __ Fluoride __Iron _Lead __ Manganese __ Mercury __ Nitrate. __ Selenium Results mg/ 1 ORGANIC CHEMISTRY Parameter _EDB __ PCB's __ Petroleum __ Endrin __ Lindane Results mg/ 1 Total Parameter __ Silver __ Sulfates __ Zinc _Ph __ Conductivity _ms _TOC Parameter __ Methoxychlor __ Toxaphene _2,4-D __ 2,4,5-TP (silvex) RAPlOCHFl fISTRY Results mg/1 Results mg/ 1 Parameter Parameter Results PCi/ 1 I= (MF) Coliform Colonies/lO0mls (MPN) Coliform Colonies/JO0mls eceived --~:2,___---'d;-"--"-)_-J+·~/'--=A'--1.~'""----- __ Gross Alpha __ Gross Beta Date Reported _________________ _ -,L I lte Extracted---------------'----Date Analyzed _________________ _ Reported By Lab Number ---·_,,L/-"Oc:::_L/---L9_._al::._Jy.,-,/:::: ______ _ IS 3191 fRcvi,cd 7185) fl /1 ,/i -J and Hazardous Waste (Review 7 /87) I [I {_/ // I .. BASE/NEUTRAL AND ACID EXTRACTABLES COIIPOOND I nitrosodirrethvlamine is(2-chloroethvllether -chlornnheool heool I · .3-<tichlorobenzene 4-dichlorobenzene 1.2-dich lorobenzene is(2-chloroi llether xachloroethane NCnitroso-di-n~nnnvlamine ciitrobenzene 1-<nnhorone •-nitropheool 2.4-dirrethvloheool is(2-chloroethoxv)rrethane 4-dichlonnnheool 1 2 4-trichlorobenzene hthalene exachlorobutadiene STATE LABORATORY OF PUBLIC HEALTH DIVISION OF HEALTH SERVICES, N.C. DEPARTl'IENT OF HUl1AN RESOURCES P.O. BOX 28047 -306 N. WILHINGTON, ST., RALEIGH, N.C. 27611 ORGANIC CHEHICAL ANALYSIS LAB NO )Dl'·/r~<-. '/? !/ "f , .. , p FIELD# 3531",, 3'.:,o't TYPE ( 'i ' I l ( ) ( ) UNITS r,,n/] \,n/ko l/4n/] 1,n/ko un/1 un/ko .. n/1 un/ko 10 . _, '-""', , hlo'."°"vcl~ntadiene loro-<n--ereso 1 -tr1chlor01>heool · · oron•nhtha 1 ene .. acenanhthvlene irrethvl ohthalate 6-dinitrotoluene , I acenaohthene 4-dinitrnnhenol sv i 4-dinitrotoluene ID , I ~ nitnnnheool C,7J fluorene /0 -chlornnhenvlohenvlether D iethvl ohthalate I I) 4.6-dinitro-o-eresol ,v iohenvlamine 'tJ zobenzene LJ) 4-brarophenvlohenvlether 0 I 1exachlorobenzene I iJ I ~ntachlorex>heool t;,?J i henanthrene / /1 r anthracene /tJ ! ibutvl ohthalate /v 1/ ;; luoranthene I() VI 'J mf}L .. Estimated value. ,UJ-/J ( \ .. n/1 un/ko Actual value is known to 6eqess than value given. Actual value is known to be greater than value given. u -Haterial was analyzed for but not detected. The nUTDer is the_!!!nillU1I Detection~mit. ·:rmOt-.. -Not analyzed. -Tentative identification. _ -On NRDC List of Priority Pollutants. I . C. V-i.v-</2-i.on on HeaLth SVtv-i.c.u HS 3068-0 (4/86 Labof<iLto~y) ( ) un/1 ""/kn .. FE/NEUTRAL ANO ACID EXTRACT ABLES COHPOJNO ene benzidine '"l benzvl ohthalate z Cal anthracene sene · 3 3-<lichlcrobenzidine 2-,,thvlhexvl 1nhtha late n-octvl ohthalate benzolblfluoranthene zo!klfluoranthene zo(a'n=ene indeno(l 2 3-cdlnvrene 'nzo(a h)anthracene o(n h i'=rvlene line zoic acid ~~l ni 1 i ne ran -n-eth Jn•""thalene 2-n-ethvJnhnnnj fthvl"""""l 1troani line 3-nitroaniline litroani line 5-t rich l orooheno 1 di? ,"'.,3 ff?tl/.;f 5 I I STATE LABORATORY OF PUBLIC HEALTH OIVISIOII OF HEALTH SERVICES, N.C. DEPARTMENT Of HUMAN RESCXJRCES P.O. BOX 28041 -306 N. WILHINGTOII, ST., RALEIGH, N.C. 21611 ORGANIC OlEHICAL ANALYSIS LAB NO If J/'f(,J ') 7/)/9,f, C, FIELD# 3Sc,l, .3 S?•i TYPE ( /) LI) ( ) ( l UNITS r.,n/1 .l,n/ko f.n/1 J,~fko ""' l .. n/ko un/1 un/ko i<> IA /A 1....--P ii) ,J ,~ ,;-o //J iJ Jf7) , I, ~/ ~ /J t., ,,-fl / io 6<l I ' I ! \I/ 'I 11,1 -.t-/-6'//174,,T /-) WWL ,, ,UV ' V ~~stimated value. K -ctual value is known to be less than value given. l -Actual value is known to be greater than value given. ( ) un/ l un/ko ' Material was analyzed for but not detected. The nUTber is the Hininun Oetection__0mit. ::;;-rrJ£)t- -Not .ma l yzed. ·---Tentative identification. '{ -On NROC List of Priority Pollutants. \ · D.i.v-0.,.i.on 06 /lea.lth SVtv.i.cv., ' 3068-0 14/86 I.nhonntoni,) ( l · ·~/ l ""/ko I .. f'UlGEABLE COl1PCXJNOS I C01POOID 1oronethaoe brmonethdne lchlorodi floorarethane nvl chloride ch l oroethane lthvlene chloride 1 ch lorofl oorarethane hene. 1.1-dichloro ethane 1.1--<lichloro- 12-trans--<lichloroethene lorofono · ethane 1 2--<lichloro-I ch.>..... l.1. 1-trlchloro- rbootetrachloride "i ch loranethane -,-,u,.... 1. 2--<I i ch 1 oro- 3--trans--<I I ch 1 i ch loroe+hvJ ene ~brmonethane .:LL2-trichloro- J.-c1 s-'<11 ch r STATE L-IOOY Of PU8LIC HEALTH D!V!S!OH Of HEALTH SERVICES, N.C. DEPAAIMEHI Of ffJIWI RESOJRCES P.O. BOX 28047 -306 N. W!LMINGIOH, SI., RALEIGH, H.C. 27611 ORGANIC <¼cMICAL AHALYS IS LAB NO 70JCilo"i 70/Qf,r, FIELD I "?',7,;{, '~c:>'7 TYPE ( ) ( I l ( ) ( ) UNITS r.;;;.; 11 .. n/ko ,;;;:,/1 l,n/ko ua/1 ua/ko .. n/1 .. n/ka ,o -I, iJ- iO _:µJ JO ill s µ ..,- . . ·' ·. -·-·.••·· , .· ' ',-chloroe+hvl vinvl ether ID ~"";:1.2 ·2-tetrachloro- .,~ ethene .. tetrachloro-. 11-. •· 1 orobenzene I ethvlbenzene \ ' ,, l~ /D IA I.A-- /0 &!sulfide ', none /u 1-2 ~tanone JD stvrene s Ii 1 acetate /0 I 1 enes .lM-aJ) , I ~ / I IJ1/}f__. ,.LCIJ Estunated value. I I tual value is known .ctual value· is known to be less than value given . ( ) .. n/ 1 .. n/kQ to be greater than value given. u -Material was analyzed for but not detected. The nt.nt>er Is the !!.!.!'•l!UII Detection Limit. ':=.,?,/?L-I -Not analyzed. -Tentative identification. -On HROC List of Priority Pollutants. N1.C. Division of S 3068--0 (4/86 Health Services Laboratory) ( ) ua/1 .. n/ko .. . .. . . N,. Department of Human Resources I If State Laboratory of Publlc Health Division of Health Services SAMPLE AN AL YSES REQUEST P. 0. Box 2804 7 .. 306 N. Wilmington Street t.,~_,;/ Raleigh, 27611 Site Number 23 D00344 t, 12= I c~ Field Sample Number oo 2 Is= s- ~e:::S~t: g1r1 :tUc ~ C ~:: 2 I tr' I~ cl D~::ec:::;-C,=7.:...s 1 e'-"~""-'-"\ 3~~'-5:,--7=<1,.,=o_,.,u.,="...!.;"'),i~,-e ---,,9,_.mJ-(tM.- Tt of Sample: nvironmental r-Groundwater (I) __ Surface Water (2) .-Soil (3) IL__ Other (4) Concentrate __ Solid (5) __ Liquid ( 6) __ Sludge (7) __ Other (8) Comments '.Dtlr--b,~ ~ we\\ :S~l~ INORGANIC CHEMISTRY Extractables Parameter Arsenic __ Barium =-=Cadmium Chromium __ Lead .. e:rcury £ lcnium Silver :t Parameter P&T:GC/MS __ Acid:B/N Ext. Results mg/1 Results mg/1 - I= T_o_x_. __________ _ -luHCil:ODIOLOOY Parameter • (MF) Coliform Colonics/!OOmls --(MPN) Coliform Colonics/lOOmls Parameter 1Arsenic 1Barium ~Cadmium Chloride _L_chromium ~Copper Fluoride Iron Lead Manganese Mercury Nitrate, Selenium Results mg/ 1 !},£(} ,::::, ,:, , I .,,_ 0. !){I;::-- Lz;,C,/ <.o,o ~- ,1 2.3 0.07- :5; 0,(;_>3 -<.o,o3 Total Parameter Silver Sulfates Zinc _L_ph Conductivity TDS TOC <O ,ODC:C:Z <1,= < O, oa s, '·, ... -✓ ---esults mg/1 '7.7 0ROtd'HG GIIE!,EISTRY Parameter _EDB __ PCB's __ Petroleum __ Endrin __ Lindane Results mg/1 Parameter __ Gross Alpha __ Gross Beta Parameter __ Methoxychlor __ . Toxaphene _2,4-D Results mg/1 __ 2,4,5-TP (silvcx) ______ _ Results PCi/1 Date eceived _________________ Date Reported __ __,J'-1--/-'-J-t/i'--J'"---.:..7 _________ _ .JI / / i.ae Extracted Date Analyzed -,-,-.,--,-,.,..,.,-,.,-------------- Reported By Lab Number _L_'_i_1 °T_' _j_G_'O_-_J_L_•_~_2_C_, _L_J ________ _ rl.~ 3191 (Rcvis.c.-d 7185) ~ and Hnardous Wasre (Ri:view 7/87) I N. C. Department of Human Resources State Laboratory of Public Health livision of Health Services SAMPLE ANAL YS.E,& REQUEST P. o. Box 28047 ~->' 306 N. Wilmington Street Raleigh, 2 761 I le Number _]7 -,-~._;_•;..·c.· -'-----"•:,:...·_.~·-·.,_.'_,~'--~-~.,.--Field Sample Number __ '7_..._·cc.·.c/_ce::,_··-;-;: ___________ _ me of Site _,tY!c_..::;o_,bew..,Juf.._._[=-....5c,jc,:?.:...l,_,.'f~S,__.,,C,_F'__..(?_,.#u._3...,_ ___ Site Location---,-·~--·-"~· ·c.· -"L.<C'--'-~-------, I -..(") 11 / • , .-I --, · , .· ~ -, · .,-_ .,. Collected By 1 ' · <>• '· ·., · ,7 c; • r1D# -~-~..2~--Date Collected _~_~•~-~-c..'~~----Time -L'-' ·_· ___ _ lpe ,of Sample: Environmental ~ Groundwater (I) ___ Surface Water (2) I-Soil (3) I____ Other ( 4) Extractable& Concentrate __ Solid (5) __ Liquid (6) __ Sludge (7) __ Other (8) INORGANIC CHEMISTRY Parameter Results mg/ I Parameter Results mg/ I Arsenic ..£Arsenic <a.,o/ __ Barium =iBarium o,R Cadmium Cadmium -'() c-t== Chromium -1LChloride s:1y· __ Lead _L Chromium <: CJ.Of __ {ercury ~Opper <.<:J,O.S 1=~lenium luoride /J' 7';r_. _ Silver ✓ Iron <o,o.S- Total Parameter Results mg/ I Silver 01.0S Sulfates L-3 ..Lzinc 0,d.0 _Ph 4'·J L Conductivity GI ms 3;;9 ✓Toe q _L_ Lead ~ I= ~Manganese ' 7._Mercury G_ &>;.u Nitrate ....Lseienium :S:: iQ. D:) S: ORGANIC CHEMISTRY rt= Parameter Results mg/ I P&T:GC/MS __ Acid:B/N Ext. FTOX MICROBIOLOGY Parameter (MF) Coliform Colonies/ IOOmls =F (MPN) Coliform Colonies/lOOmls Parameter _EDB __ PCB's __ Petroleum __ Endrin __ Lindane Date.eived __________________ _ 01 Extracred _________________ _ Reported By DflJ I 91 (Revised 7185) So and H:uardous Waste (Review 7187) Results mg/I Parameter __ Gross Alpha __ Gross Beta Lab Number Parameter Results mg/I __ Methoxychlor __ Toxaphene _2,4-0 __ 2,4,5-TP (silvex) -- RADIOCHEMISTRY Results PCi/ I · ~of Sample: Environmental ~ Groundwater (I) __ Surface Water (2) ---Soil ( 3) ■~--Other (4) Concentrate __ Solid (5) __ Liquid (6) __ Sludge (7) __ Other (8) INORGANIC CHEMISTRY Extractables Parameter Parameter P&T:GC/MS __ Acid:B/N Ext. TOX Results mg/ 1 Results mg/ 1 -MISRODIOLOOY Parameter (MF) Coliform Colonics/lOOmls (MPN) Coliform Colonies/lOOmls Parameter LArscnic LBarium LCadmium ..£chloride LChromium _Leoppcr L Fluoride Iron Lead Manganese Mercury Nitrate. Selenium Results mg/ I < (. .. 0,/7 f), /0 81tOMHG GlIEl,HGTRY Parameter _EDB __ PCB's __ Perroleum __ Endrin __ Lindane Results mg/1 Parameter __ Gross Alpha __ Gross Beta Total Parameter Silver Sulfates Zinc LPh Conductivity TDS TOC Parameter --Methoxychlor __ . Toxaphene _2,4-D __ 2,4,5-TP (silvex) Results mg/ 1 t l'.{(1~~ ..) Results mg/1 R.,A.vL'IOCWtil HBffl :t Results PCil 1 Date Received __________________ Date Reported _________________ _ late Extracted Date Analyzed _________________ _ Reported By • HS Jl91 (Rcvis<d 7185) ~l;,J ,.,,l H~:ardou<; Wasre (Review 7/87) Lab Number u 1300? .1111 1c 87 v"0-· -· ._,_._ I"_.· __ ·,· ,1/_,,,,,. __ ,1.__/.,,_''--~ _•1/r~~--r1/1(--~-=-J--· __ I'/ --,, --·L,.,.t. , • 1, ,. ,-, ' -, ,_ -))' --• , /' , . , rJ ~ 7 fi, •. ',-<{,:,,,,,,;,· --/· --- . ,. J(, .,_ ·"" " -. , . . ;;;1 ~v:, -~-.,C(,:€¥' ,_ • /<' C . ,/;J' N. C. Deportment of Human Resources /-',:., i. {~ '. State laboratory of Public Health o;-·n of Health Services :: w•'<:' ·.·.• · SAMPLE ANALYSES REQUEST P. o. Box 28047 / ,.,,,,_ 306 N. Wilmington Stre<et c)J" C-_,,,,.,,,-. . c/ Raleigh, 27611 SilNumbcr 23 Do~ 1 2. I/ --field Sample Numbcr--.:0=.=0_2---:--=15::___,_ _____ _ N e of Site # 3 ~ __ ,,,:'J-0_,(l, s;:J_eu\__ Site Location _C,=.,l"'e-""'-'-"""':'-'=-"-'~~~------- ujccted By BJib { A ( k <1 ID# I/ ~ Date Collected 7 -/ 5 -'}{7 T ii, of Sample: ~ Environmental ~ Groundwater (1) __ Surface Water (2) 1--Soil (3) __ Other (4) Concentrate __ Solid (5) __ Liquid (6) __ Sludge (7) __ Other (8) INORGANIC CHEMISTRY Extractables Parameter __ Arsenic Barium =-=Cadmium __ Chromium __ ad ~-... ercury Lse1enium __ Silver I= Results mg/ 1 i=---- . Parameter _P&T:GC/MS ---Acid:B/N Ext. .-TOX Resulta mg/ 1 Parameter LArscnic LBarium ..:L.eadmium L Chloride ...L... Chromium ....L_Coppcr _LF!uoride Iron Lead Manganese Mercury Nitrate. Selenium Results mg/ 1 <O.Ot < o,o / 81t0/dil:G Gil:El,HGTR?.it Parameter _EDB __ PCB's __ Petroleum __ Endrin __ Lindane Reaulu mg/1 Total ,., Parameter Silver Sulfates Zinc UL LPh Conductivity TDS TOC Parameter __ Methoxychlor __ . Toxaphene _2,4-D __ 2,4,5-TP (silvex) Resulumg/1 s-- Reaulumg/1 . MICROBIOLOOY Parameter Parameter R.AOIOCWFl HB'FH:Y • Resulu PCi/1 · (MF) Coliform Colonies/lOOmls __ (MPN) Coliform Colonics/lOOmls __ Gross Alpha __ Gross Beta '-------'------l e Received e Extracted _________________ Date Analyzed -~~~---~--------- . 1 J o 1 1· 'I 1,---e Lab Number l.J t, 1 ,.u,. J . / ----------------Date Reported J / :2 q/ tr7 ( State Laboratory of PubUc Health P. 0. Box 28047 306 N. Wilmington Street Raleigh, 2761 I Concentrate __ Solid (S) __ Liquid (6) __ Sludge. (7) __ Other (8) Comments :J),~v,\,,"'s ~o..\;; W:t\\ 6o.rm~\e __ Soil (3) 1--Other (4) Extractables Parameter Results mg/1 Results mg/1 ihHGRODIOLOOl-f Parameter (MF) Coliform Colonies/lOOmls (MPN) Coliform Colonies/ IOOmls ltl0RO2•rPHC SHEftHGTilY Parameter __ Arsenic __ Barium Results mg/ 1 ORGANIC CHEMISTRY Parameter _EDB __ PCB's __ Petroleum __ Endrin __ Lindane Results mg/ 1 Parameter __ Gross Alpha __ Gross Beta Total Parameter __ Silver __ Sulfates __ Zinc _Ph __ Conductivity _TDS _TOC Parameter __ Methoxychlor _· _. Toxaphene _2,4-D __ 2,4,5-TP (silvex) ll:ATJIOCHFl US.RY Results mg/1 Results mg/1 Results PCl/ 1 . Da, eceived.,~-, 1.!,--_,_Is"--,,_8.,_?,.,.,,,,;1.J:..,f\~----------Date Reported -6-,-,J-,-,,f,-c--_,f~--'· fc._O_--'-.F--'-~--,.--------lte Exrracte~!~¼~~-,:-..,R_ Date Analyzed _7'--'-;-'7'---"y'--'7'-'d::c."-C:D'-,,-?0-1-~"'"D-'--f=-s--n:....:.._7_1.,(,I,_,.... __ _ Reported By ~~ g /Li? Lab Number ------------------- Rs 3191 (R,vised 7185) ■lid and Hazardous Waste (Review 7187) I. C. Department of Human Resources Division of Health Services ~-( SAMPLE ANALYSES REQUEST State Laborato'ry of Public Health P. 0. Box 28047 L · O J -. "~/306 N. Wilmington Street .. _ '-' ~ Raleigh, 27611 Site Number 2,3 ~ 0 3 4 4 /e. '12. I Field Sample Number () '.) t me of Site :f.t-3 &..-1~; 5:-,J, <:>cJ-Q__ Site Location C, \ el) e. \Q-"\ J C,p V:-/A,h llected By Ba.\>b { f\ \ \e. t0 ID# __,_\...::;2. ___ Date Collected ·7-/JJ3 --8 7 Tim~ ,?3S Pv1] lype of Sample: Environmental I _x_ Groundwater (I) ___ Surface Water (2) __ Soil (3) Concentrate __ Solid (5) __ Liquid (6) __ Sludge (7) __ Other (8) Comments -n--~"'"''"'5 v:io..¼ v-.H.\\ 6°=®~f 1--Other (4) Hi8ft8MHe @Hffi¥HS'FR-Y Extractables Parameter Arsenic Chromium Lead Mercury _Selenium Silver Results mg/1 Parameter __ Arsenic __ Barium __ Cadmium __________ Chloride __ Chromium __ Copper __ Fluoride __ Iron _Lead __ Manganese __ Mercury __ Nitrate __ Selenium Results mg/1 ORGANIC CHEMISTRY ~arameter Results mg/1 Parameter Results mg/ 1 I P&T:GC/MS _EDB .. -~. -__ PCB's l~TOX .,e;1::n3 __ Petroleum __ Endrin __ Lindane ·~ 1-11ea001e1:::ear1l Parameter Parameter I== (MF) Coliform Colonies/lOOmls __ Gross Alpha (MPN) Coliform Colonies/lO0mls __ Gross Beta -------- Received 1-15-~7 -J'M Date Reported Total Parameter __ Silver __ Sulfates __ Zinc _Ph __ Conductivity _ms _TOC Parameter __ Methoxychlor __ . Toxaphene _2,4-D __ 2,4,5-TP (silvex) -- &r:~.10IQCWlil HS.R¥ Results mg/1 Results mg/1 Results PCi/ 1 .. Date Analyzed _________________ _ late Extracted------------------ Reported By __________________ Lab Number ____ 7 ....... 0~l 9_,.1_5~---------- IHS 3191 (Revi~d 7185) lid and Ha:ardous \X'aste (Review 7187) I . r r . C. Department of Human Resources State Laboratoi'y of Public Health Division of Health Services SAMPLE ANALYSES REQUEST P. o. Box 28047 306 N. Wilmington Street Raleigh, 27611 S umber ~ D ~ 3 4 4 '2 '12 l Field Sample Number 00 3 5 OS- 1,mc of Site~ 3 Q,,yy,..od:-->--c:, S:c:..Rni'>)--f. Site Location C.,\e\)e.\Q--"l,J C,,ou,>,\h ~llccted By Ba..\:ib { -f,,_ ( Le0 ID: I Z. Date Collected 7-/ 3 -8 7 Tim~ J 3S r-i)J l pc of Sample: Environmental I _x_ Groundwater (I) ___ Surface Water (2) __ Soil (3) 1--Other (4) Concentrate __ Solid (5) __ Liquid (6) __ Sludge (7) __ Other (8) Comments ::D,~-n½,"';:) LCo..~ \,,..H_\\ 6°=® ~\e Extractables Parameter Arsenic Chromium Lead MercurV . Selenium_· ... -Silver liarameter P&T:GC/MS . -t:'Tox· -- J Parameter Results mg/1 Results mg/1 :i t;i 11 1,HGRODIOL087l I== (MF) Coliform Colonies/!O0mls (MPN) Coliform Colonies/!O0mls -- -- Os eceived 1-i5-37 :.IM UiOR.Oi!iPUC @tlE!tHSTRY Parameter __ Arsenic __ Barium __ Cadmium __ Chloride __ Chromium __ Copper __ fluoride __ Iron __ Lead __ Manganese __ Mercury __ Nitrate. __ Selenium Results mg/ 1 ORGANIC CHEMISTRY Parameter Results mg/1 _EDB __ PCB's __ Petroleum __ Endrin __ Lindane Parameter , __ Gross Alpha __ Gross Beta -- -- Date Reported Total Parameter __ Silver __ Sulfates __ Zinc _Ph __ Conductivity _ms _TOC Parameter __ Methoxychlor __ . Toxaphene _2,4-D __ 2,4,5-TP (silvex) -- R.t\DIOCHF} cs.a y Results mg/ 1 Results mg/ 1 Results PCi/1 late Extracted------------------Date Analyzed __________________ _ Lab Number __ __,J---'0'-'--/ 9,__/c...,'5"----------Reported By' _________________ _ ■us 3191 (Revised 7185) .,id and Ha!ardous Waste (Review 7187) I lat I PURGEABLE COIIPOUNDS COIIPOIJND I chlororethane braranethane dichlorodifluorcxnethane I vinvl chloride chloroethane rrethvlene chloride 1 trichlorofluorcxnethane ethene 1 1-dichloro ethane. l. l-dlchloro- 1 2-trans-dichloroethene I ch 1 orofonn ethane 1 2-dichloro- ethane 1. 1. 1-trichloro-I carbontetrachloride brorodichlororrethane or~ane. 1.2-dichloro- 1. 3 trans-di ch lo ne I trichloroethvlene chlorodibrarorethane Ilene ne. 1 1.2 trichloro- -cis-dichlo ne 2-chloroethvl vinvl ether STATE LABORATORY Of PUBLIC HEALTH DIVISION Of HEALTH SERVICES, N.C. DEPARTMENT Of HUl1AN RESOURCES P.O. BOX 28047 -306 N. WILMINGTON, ST., RALEIGH, N.C. 27611 ORGANIC CHEMICAL ANALYSIS LAB NO ,r,;q;s FIELD # 75.,:i TYPE ( I l ( ) ( ) ( ) UNITS un/ Vun/kQ ua/1 ua/kq ua/1 un/ka un/ I ua/ka /d ; , /0 ' <) jr.) /t? ,- Z-v ;,- v /6 r I brorofonn ethane. L 1-2.2-tetrachloro- ethene tetrachloro- toluene I ch 1 orobenzene ethvlbenzene ' / ' I acetone /~ . 2-butanone lo carbondi sulfide ,- 1 2--hexanone /<) 4-mathvl-2 =ntanone /v stvrene < vinvl acetate /() I xvlenes tl-d-ai) ' -/ I fr!/)/_ ,u/J J -Estimated value. , " ( ) un/1 un/ka Actual value is known to be less than value given. Actual value is known to be greater than value given. Material was analyzed for but not detected. The nurber is the Mini1TU11 Detection Limit. =01.iJL--Not analyzed. I 1/ -Tentative identification. fl -On NROC List of Priority Pollutants. N.C. Division of Health Services I DHS 3068-0 (4/86 Laboratory) ( ) un/ I un/ka I SE/NEUTRAL AND ACID EXTRACTABLES I (X)HPOUND N-nitrosodimethvlamine I •is(Z-chloroethvl)ether -chlor-henol ohenol 1 3-dichlorobenzene 1-4--dichlorobenzene l 2--dichlorobenzene bis(Z-chloroi llether exachloroethane -nitroso--di-n ~~··lamine nitrobenzene isnnhorone nit'"""henol 4-dimethvlnhenol bis(Z-chloroethoxv)methane 2 4-dichlo-henol 1-2-4-trlchlorobenzene n·-hthalene hexachlorobutadiene 4-ch loro.an-cresol hP achlorocvcl-~ntadiene 6-trichlo'"""henol 2 chloron·-hthalene acenanhthvlene dimethvl 0 hthalate 2 6-dinitrotoluene cenanhthene 2 4-dinitroohenol 2 4-dinitrotoluene 4-oit-henol fluorene 4-chlo-henvlnhenvlether diethvl ohthalate 4 6-dinitro-o-cresol diohenvlamine azobenzene 4-bramohenvlnhenvlether hexachlorobenzene ntachlornnhenol henanthrene anthracene dibutvl nhthalate fl uoranthene ( ·,rATE LABORATORY Of PUBLIC HEALTH DIVISION Of HEALTH SERVICES, N.C. OEPARTHENT Of HUMAN RESOURCES P.O. BOX 28047 -306 N. WILHINGTON, ST., RALEIGH, N.C. 27611 ORGANIC rnEHICAL ANALYSIS LAB NO 'toT7i/<r FIELD # 35,d] TYPE ( /l ( l ( ) ( l UNITS /411 lun/kn un/1 un/ka un/1 un/ka un/ 1 un/kn /a '-...---,·. 1 I I I I I I I I I ' V <7 /0 LO JO Jo /I) <ti .C"ZJ I £?! /iJ I() 'c! 1<> i lo i / () i / /V 'V M/)l- J -Estimated value. ,,«,§(..( ( l un/1 un/ka ., Actual value is known to be less than value given. Actual value is known to be greater than value given. Haterial was analyzed for but not detected. The nurber is the Hinirrun Detection Limit. c=;->?L)L. -Not analyzed. ··1/ -Tentative identification. fl -On NROC List of Priority Pollutants. N. C. V.i.v,u.,.i.on 06 He.a.Uh Se.1tv.i.c.v.. 'HS 3068-0 l4/86 Labo~a,to~y) ( ) un/1 ua/ka I la BASE/NEUTRAL AND AC ID EXTRACTABLES COMPOOND ~~ine butvl benzvl ohthalate 1•)anthracene ene 3 "dichlorobenzidine bis(2--,,thvlhexvllnhthalate di tvl ohthalate be bl fl uoranthene benzo(klfluoranthene ~a\nvrene ( 1 . 2. 3--<:dl nvrene d1 nzo(a h)anthracene =lo(Q.h. il"".rvlene ani 1i ne ~ic acid 1 alcohol i!f';~ ran o>nhtha 1 ene lnhenol 4--<rethvl oheno 1 2 troani 1 ine 3-troani 1 ine 4-nitroaniTine 2 -trichlo=henol =t ( STATE LABORATOOY OF PUBLIC HEALTH DIVISION OF HEALTH SERVICES, N.C. DEPMTMENT Of HUMAN RESOURCES P.O. BOX 28047 -306 N. WILMINGTON, SI., RALEIGH, N.C. 27611 ORGANIC CHEMICAL ANALYSIS LAS NO </1)/41~- FIELD # ·,,,:;J TYPE ( /) ( ) ( ) ( ) UNITS k/ I) .. n/ka .. n/ I ua/kq ua/1 un/l(n .. n/ I .. n/ko iv .._'-::""I ,;7) /o lo /o n /tJ /o P' i , ,i; \1/ ~-z, ~I 5"7 /;J /t) /c} /tl I,; I ,J ,:;--~ ,1 ' I 111/)L u•II I ,, K ual value is known to be less than value given. ( ) .. n/ I uo/kq J ~stirt'dted value. L -ual value ls known to be greater than value given. U -terial was analyzed for but not detected. The nl.lTOer 1s the Hininun Detection Limit. :=.n?/}L-NAI Not analyzed. 1/ Tentative identification. ~/ On NROC List of Priority Pollutants. V. II D-i.v.u.,-i.on o 6 fiwUli Se;iv-i.c.e~ ~H.3068-0 14/86 Labonatony) ( ) uo/1 ua/ko ,. ,., : I 18 I ( ( STATE LABORATORY OF PUBLIC HEALTH DIVISION OF HEALTH SERVICES -· ·--N. C. DEPARTMENT OF HUMAN RESOURCES ,, ·fit1!V[d,,,_ P.O, BOX 28047 -306 N. WILMINGTON ST., RALEIGH 2761 )-,-~ ---,'i:,--...::---,. INORGANIC CHEMICAL ANALYSES-PRIVATE-W~-TE ~iiM: ::,, Complete All Items Above Heavy Line (l'?u. ~J '---.. -:'' ·:·T;'· (See Instructions on Reverse Side) ~..)1·,'.,<·-c,'. :/._;,\" .;,· I 1/2 "~~~~.;:,;.-.,,-.~·. ( V \..__../" nesium·· .. ,,'._'-•:· ,mg/I --;._ ':'dn..::e..::ss:,cc,,-a-=c:::oc'-3-:('::Ca;...,-:M-:- 9-:-1--'--,,-,-,-''4-'-,,-"C:..C,.,,.:.~t,;.'½~SP."'m:e:g/:cl.c'. --P-----,-----~-~;...;...--t-7',;-.;,.""'c,-,--,----'--,'-'~~...,.c..:.f.i~ Alkalinity.CaC03 mg/I mg/I units NTU units 0, 2 mg/I le Analyzed ---------Laboratory Number-· -------~D~0..._S~?_],...,.,J.....,M,.AttR-alH6+-tJ647----- OHS Form. 1441 Rev. 10/79 FILE Mildred A. Kerbau.;,h 0·1rector L -1r-r 1{? t(} ~ ::;_ ~ STAT~l~~~g~~~OHREYA~~:~~~~l~:;LTH ;~:_;:"{,~-Ci:IV,:O'•~,\ t!U ~.,, N.C. DEPARTMENT OF HUMAN RESOURCES /'; i_.,.~.R l ,· !'.:,:· ·;r\ It P.0.BOX28047-306N.WILMINGTONST.,RALEIGH 27611 \\;,, r'•, I INORGANIC CHEMICAL ANALYSES -PUBLIC WATER SYSTEM0~~~~lL:f?~·· Complete All Items Above Heavy Line (See Instructions on Reverse Side) I Type of System: ~,:;,t ~ 0CN r/fJ?-~ Community ' Non-Community A ss:C c( ;:;?9:'&t1Cs' /fD Source of Water: C ~-_,, t.., (~ Ground Both -~v~''-'-'"-C'-'q'-"'-7',L'-------ZIP~"-'--=--=-----1 ( I Surface Purchased i, ,.<_;;I:> --S-o-ur_c_e_o_f-Sa_m_p_l_e:-.--------------- ( I Distribution Tap ( ) House Tap R1 T '7D, )/ l--l,J:;LJ (..-J -well Tap rt o: -4"4-.!...::LL,""-<"---=--'---=-.:::.,_---==---------1 ______________________ _ .-? .,,,,rr-. /'l) r" Type of Sample: Address: t:' '-</A'-Ce> . I '_,/ ( ) Raw Treated 3 I s-~-0;/Uc?(. S<Pz1p ___ ____,----------------s &-i.J,iji ~ Type of_Jteatment: I / (U,-None Lime ( ) ( l Chlorinated Soda Ash ( ) Fluoridated Polyphosphate ( ) Filtered Water Softener T]l hone Number: C cted By:--------------~----! ~ AM -z 5 2,.''30 ( l Alum Other Da cted: Z. -u..)=( T=: _'/J__c_:•_:_ __ _:Pc.:M::..i----------------------- -. Type of Sample: Location of Sampling Point: ( ) . Regular Private {Address where sample was collected) I ) Check Special Re.rks: (l~ -C /( q ,,tj',#.(56 Results A ium mg/I mg/I mg/I mg/I mg/I mg/I mg/I mg I units mg/I mg/I 2 WATER SYSTEM I.D. NUMBER (COPY FROM MAILING LABEL) □□-□□-□□□ Optional Parameters (List as needed) Results Date .ived ___________ Date Reported ____ 3~/_f _,/ f~'J_1 ___ Reported By __________ _ I 0042/ 4 MAR 3 87 D Analyzed ___________ Laboratory Number _______________ :...__.:_ ______ _ DIForm 2B87 La •torv 7/79 FILE Mildred A. Kerbaugt, Director ./ .,~<-CEl\11:2) ( _J, ( "',\ C. Ocp;1~cnt of Human Resources 1 ~ ,.,..., ~ \ State Laboratory of Public Health vi,ionofHcalthServtces SAMPLEANALYSESRE E$'.f24 J.9.,, :1 P.O.Box28047 .. I ; 5 <,,,. ';; ·"" i 306 N. Wilmington Sttect !1_,e V" ~c;>, i/'/ Raleigh, 27611 ,.::;:: ~;;Ot!,lt~/' F>dd5:r::: ~~.;~ ~llcctcd Byah N/_ _ ID# / 'l-. Date Collected -S--8 I 336 tpc of Sample: nvironmental ---X-Groundwater (1) I__ Surface Water (2) Concentrate Comments __ Solid (5) ::::Odr,\,,,~ ~k we\\ ;S~\~. __ Liquid (6) ~c:m, '("e.s,J.~\ Y\€.a..\"° --Soil (3) ~ Other ( 4) __ Sludge (7) C,e.\9.:nese. t;::~'ners ~\OJ\v-\" __ Other (8) Per CequeJ-aJ Bd: :l:d:co½ Df:JS So I tti 1 He.~ l.Jas.)e. INORGANIC CHEMISTRY I Extractables Total Parameter Resulumg/1 Parameter Results mg/1 Parameter Resulumg/1 l=Arscnic LArscruc <(2.0I ~Silver ,<'6,Cb __ Barium £Barium <Qr/ Sulfates '-~ __ Cadmium ~Cadmium s£ ,l)tJ < Zinc -< ('), 0 .5 '=Chromium Chloride ~ -lLPh 7,/ Lead -lL.. Chromium ~ '2.' 0/ ~Conductivity Lr.O •4 1,:1!,.a.1: ~V.crcury ~Copper -<.o,o5 TDS //,?8 :denium Fluoride <. {), IC TOC < ~ Silver lron <o.oS-----Lead <tJ,Oii -- I= Manganese -<.o.o -- Mercury ~,';9$?2?--- Nitrate ---- Selenium ::5 I), PO!:. --I ... 8ft8:MHS 611BHSm1.'- s:=Paramctcr Result. mg/1 Parameter Results mg/1 Parameter Results mg/1 P&T:GC/MS _EDB __ Methoxychlor __ Acid:B/N Ext. _PCB's _· _. Toxaphene FTO):( __ Petroleum _2,4-D __ Endrin __ 2,4,5-TP (silvcx) __ Lindane -- I -t,HGR:OBIOLOOY R..'\CIOC:Uti:J HO:fft i • Parameter Parameter Results PCi/ 1 I= (MF) Coliform Colonics/lOOmls __ Gross Alpha (MPN) Coliform Colonics/lOOmls __ Gross Beta -------- Dat Received Date Reported /20/g-7 ' t te Exrracted _________________ Date Analyzed -----,--,,r--,-,-,--rrn--1-1--1•..-' ,·. ____ _ U I ~)(~J; ~CG l~ t.: Reported By < Lab Number I S 3191 (Rcv;,.,,d 71B5) J and Haurdous Waste (Review 7/87) I. C. Department of Human Resources Division of Health Services ( SAMPLE ANALYSES REQUEST State laborato'ry of Public Health . P. 0. Box 28047 306 N. Wilmington Street .. ,-, ~ , I 4 ;i'1 {) () .-, < J,::;;;r7 Site Number L,2,}) 0 0 .3 '-t r 2 I Field Sample Number ,:> KlJ lame of Site --'n-"OL.!..1..lO.c,it';.......,:-..,1-'-c:0'-,-\;~q...L..t:ul f_, ___ c ....... : =-..,c•..c..flc.:Q.:c.a5<...J...f____ Site Location c., \ e0 e lQ.M, ~ C,,o y..M.'b, B Ii -Ori/I @-S-c;;J <SJ? Raleigh, 2761 I Collected Bya.'Ob { bl 1£ o ID# _\!....:CZ.-'---Date Collected _____ .:c:0_1----Time-~"'---:),,_,,.()'--tpe of Sample: Environmental I --2(_ Groundwater ( 1) . ___ Surface Water (2) Concentrate __ Solid (5) __ Liquid ( 6) __ Sludge (7) __ Other (8) Comments :::D,~~'"'S \Ao..¼ \,>-X,\\ 60Jffi¢f 1--Soil (3) __ Other (4) Extractables Parameter Results mg/1 Results mg/ 1 ,_,.,,.- J.HGROBIOLOOil'f Parameter (MF) Coliform Colonies/l00mls (MPN) Coliform Colonies/lO0mls HiiOROi\?HC @ttE!uftSTRY Parameter __ Arsenic __ Barium __ Cadmium __ Chloride __ Chromium __ Copper __ Fluoride __ Iron __ Lead __ Manganese __ Mercury __ Nitrate. __ Selenium Results mg/ 1 ORGANIC CHEMISTRY Parameter _EDB __ PCB's __ Petroleum __ Endrin __ Lindane Results mg/1 Parameter __ Gross Alpha __ Gross Beta Total Parameter __ Silver __ Sulfates __ Zinc _Ph __ Conductivity _TDS _TOC Parameter --Methoxychlor __ . Toxaphene _2,4-D __ 2,4,5-TP (silvex) R..:AaDIQCWFl CS'irRY Results mg/1 Results mg/ 1 Results PCi/ 1 ( ,. C. Department of Human Resources I State Laborato~y of Public Health Division of Health Services SAMPLE ANALYSES REQUEST> P. o. Box 28047 .. , .. ·, 306 N. Wilmington Street Site Number ...,,2;~3'-'D"'--" ... o-"->-a«-->."2,_,_4_,_4..,__,l,,=-'1-'-"'2.~l ___ Field Sample Number '<@cl 3 </ t<J . Raleigh, 2761 I !::::.:s~: -B--'-~-"-'-c,-'-'nb_,__()W~.C:(:,"--;{;;c;lc,...·~-'. 1/µ~...J.-r_,_,~(-',b.}~l-D-#-=--=-,-=-2.-=--=--=--=--=--D~::e::::; C, t=0s~,~-: ,Cp~;) J_:0 tpe of Sample: Environmental I _x_ Groundwater (I) . ___ Surface Water (2) 1--Soil (3) __ Other (4) Concentrate --Solid (5) __ Liquid ( 6) __ Sludge (7) __ Other (8) Comments :)),~"'"''~ ~o.¼ 1.>.x.\\ 60-lffi~\f HiOROAlHC CttEl,HSTRY Extractables Parameter Mercury ____ _!?~l~~i~!Yl~-- . •Silver P&T:GC/MS .X-:::;/'i.cii"d:Btl'sExt:- Parameter Results mg/1 Results mg/ 1 1,HGRODIOLOO¥ (MF) Coliform Colonies/lO0mls (MPN) Coliform Colonies/lO0mls Parameter Results mg/ 1 Total Parameter __ silver __ Sulfates __ Zinc _Ph Results mg/1 __ Arsenic __ Barium __ Cadmium __ Chloride __ Chromium · __ Copper __ Fluoride __ Iron _Lead _______ ... __ Conductivity __ Manganese __ Mercury __ Nitrate _ __ Selenium ORGANIC CHEMISTRY Parameter _EDB __ PCB's __ Perroleum __ Endrin __ Lindane Results mg/ 1 Parameter __ Gross Alpha __ Gross Beta _TDS _TOC Parameter __ Methoxychlor _· _. Toxaphene _2,4-D __ 2,4,5-TP (silvex) RADIOCHFl US.RY Results mg/ 1 Results PCi/ 1 Date Received 8/ 10\ 8 7 JM Date Reported _________________ _ lte Exrracted __________________ Date Analyzed _________________ _ Reported By Lab Number ____ 7-'-D""l'-'Oc..,c~-1-7----------- 11S 3191 (Rc-viS(:d 7185) id :in'1 H:>:Hdnu~ W11~t~ rR~vit":W 7 /87' I N. C. Department of Human Resources State Laboratol'y of Public Health Divi,ion of Health Services SAMPLE ANALYSES REQUEST P. o. Box 28047 I-306 N. Wilmington Street .. . /\/\ // Q 5_ ,', Raleigh, 27611 Site Number -'=4,,,...,3,._,:J)"--'-..,.0"'--'-0"-"3...._'-t...__4,_,,l,."'-''7-'--"'2=-i...l ___ Field Sample Number U-.J 3 I {) · ·· ' fneofSite Aoc1i<-, /Y-/J[I.P/.Y SiteLocation Q\e0e.\Q-A,\J C,,o~ Collected By Ba.\,lo < N-//,t_;,) !D#_,_l_c.2.. ___ Date Collected "i{-.5-i7 Tim~ .33o .of Sample: Environmental tx-Groundwater (I) . ___ Surface Water (2) a--Soil ( 3) Concentrate __ Solid (5) __ Liquid (6) __ Sludge (7) __ Other (8) Comments ::D, ~ "'½'':) 1..Co..¼ Y-X \\ 6<1/ffi ~ e L_ Other ( 4) Extractables Parameter Arsenic __ Barium a-Cadmium a-Chromium __ Lead A1ercur)' ---~-s~J~r:,.iu!O_:, __ -~-· ·Silver . I= Parameter P&T:GC/MS F-~ Parameter Results mg/ 1 Results mg/1 1,HGRODIOL001J.t -a---(MF) Coliform Colonies/lO0mls -----(MPN) Coliform Colonies/lO0mls UiOROt\?HC @IIElvHSTRY Parameter __ Arsenic __ Barium __ Cadmium __ Chloride __ Chromium __ Copper __Fluoride __ Iron __ Lead __ Manganese __ Mercury __ Nitrate. __ Selenium Results mg/ 1 ORGANIC CHEMISTRY Parameter _EDB __ PCB's __ Petroleum __ Endrin __ Lindane Results mg/1 Parameter __ Gross Alpha __ Gross Beta Total Parameter __ Silver __ Sulfates __ Zinc _Ph __ Conductivity _ms _TOC Parameter __ Methoxychlor _· _. T oxaphene _2,4-D __ 2,4,5-TP (silvex) R.J t'IOCWE} usmY Results mg/1 Results mg/1 Results PCi/ 1 D:ite Received ~f>'l-)~/07/_'i~J~~J:~M ____________ Date Reported--~---------------..JI I . LJle Extracted Date Analr..ed _________________ _ Reported By Lab Number ---~J_/J~J_~r;~, ~8~7 _________ _ I ;:~IJ_R~:::d. ~:,~~!. (Q.,, • ., 7/,07' I le • f'U<G€ABLE CXJIIPWiDS l Q;\'<!'O.JIIQ crone th.:me br<m::methdne h lorodi flvorcmethane 1 chloride ch loroethdne thvlene chloride 1ch lorofl uororethdoe hPoe 1.1-dichloro •thdoe 1 1-<lichloro- -trans-<lichloroetheoe oroform •thdoe 1 2-<lichloro- I. I. 1-trichloro- tetrachloride tirorooichlorarethdne I I 2-<lichloro- trans-<llchlo chloroethvleoe i!i brcm::methane --1. I 2-trichloro- I .kis-<l!chlo 0"11 ( STATE LABOOATORY Of P\JBLIC HEAL IH DIVISION Of HEALIH SERVICES, N.C. OEPAATMENT Of ffJIWI RESOORCES P.O. BOX 28047 -306 N. WILMINGTON, ST., RALEIGH, N.C. 21611 ORGANIC ~NICAL I\HALYSIS LAB NO 70;u)'?,_"I FIELD I . i i./,J'f-3'/f - TYPE ( I ) ( ) ( ) ( ) UNITS uq/ 1) un/kq .. n/1 un/kq ua/1 ua/ka .. n/1 ua/kq Jo IA in 2-t) /j) 10 ':, 2--0 < ·v C ,< . .V_• IV I I i .! / 'xi lo s-Eoroethvl vinyl ether 1.1 2 2 tetrachloro- ethene. tetrachloro- uene orobenzeoe I ethvlbenzeoe " V ,M~ /u I l /0 &isulfide ,:::-- none /0 1-2~ntanooe lo st ~ • 1 acetate /v 1 enes l'M-al I ~ , :r r,J/JJ.-- ,,;,) 0 Est1mate-d value. I a, l -twl value is known to be less th.an value given. l -tu.al value· is known to be greater than value given. ( ) ua/ 1 uq/kq U -11.!terial was analyzed for but not detected. 3 Not •nalyzed. The numer is the Nininun Oetect100 L1m1t. =rJJ/Jt.----Tentative identification. . _ Oo HROC list of Priority Pol lut•nts. 5:_/ /1"'-"''>. "- N •• Division of Health Services !ll 3O&/l-0 (t, /86 Laborau,ry) ( ) un/ 1 .. n/ka I ,. BASE/NEUTRAL AND ACID EXTRACTABLES COMPOUND I ri trosodiirethvlami ne sf2---<:h loroethvl )ether ---<:h 1 or~heoo 1 heool I 3---<lichlorobenzene 4---<lichlorobenzene 1 2---<lichlorobenzene ls(2---<:hloroi llether xachloroethane N---nitroso-di-n~~vlamine ~robenzene horone -nit-heool 2-4---<liirethvlnheool Ii s 12---<:h loroethox"'irethane 4---<lichloroaheool 1-2 4-trichlorobenzene hthalene xachlorobutadiene -ro~resol lorocvcl~ntadiene trichlo-heool c.chloronanhthalene acen,nhthvlene irethvl ohthalate 6---<linitrotoluene acen'nhthene I 4---<linitrnnheool 4---<l\nitrotoluene -nitrooheool lfrene hloroahenvlohenvlether ethvl nhthalate 4 6-dinitro---o--cresol thenvlamine obenzene 4-br"Nr<>nhenvlnhenvlether xachlorobenzene ntachlornnheool enanthrene anthracene butvl nhthalate uoranthene ( STATE LABORATORY OF PUBLIC HEALTH DIVISION OF HEALTH SERVICES, N.C. DEPARTl1ENT OF HUMAN RESOORCES P.O. BOX 28047 -306 N. WILMINGTON, ST., RALEIGH, N.C. 27611 ORGANIC CHEMICAL ANALYSIS LAB NO •')O;;/IH'7 FIELD I '-'l41v, TYPE r /l ( J ( J ( l UNITS /4n/1 ;\n/ko un/1 un/ko un/1 .. n/ka .. n/1 .. n/ko /0 ~ iA I i I I I ,i/ • :;u io Ft) /0 / /) ,o ;o ,t,?) :fiV lo JD ,; ti /t' /cl /v '• ! i /,: V mOl- stimated value. ;,t,i;f.x_ ctual value is known to be less than value given. ( J un/ J .. n/kn L Actual value is known to be greater than value given. U -Material was analyzed for but not detected. The nuriier is the Hininun Detection Limit. ,:c,;J-70L I -Not analyzed. -Tentative identification. _ -On NRDC List of Priority Pollutants. I C. V-i.v.0..-i.on 06 He.aLth Sviv-i.cv., S 3068-0 (4/86 LaboJuLi:o~y) ( J .. n/J un/ko I •• • E/NEUTRAL ANO ACIO EXTRACTABLES J;ne aJNPOUNO benzidine 11 benzvl ohthalate •fa l anthracene ch-·sene ;!, -"ichlorobenzidine !!_! 2-ethvlhexvl'"hthalate d !.-octvl ohthalate benzofblfluoranthene olkl fl uoranthene ofa\nvrene indeno(l 2 3-<:dlnvrene znzo(a hlanthracene ofn h i'=rvlene a ine oic acid ben lcohol coani 1 i ne d nzofuran 2-methvln•""thalene lthvlnhenol thvlolienol 2 1 troani 1 ine 3-nitroani 1 ine troaniline 2 5-trichlo-henol 1 J lma.ted value. K -tual valu e ls known ( ( STATE LABORATORY Of PUBLIC HEALTH OIVISION Of HEALTH SERVICES, N.C. OEPMTIIENT Of HUMAN RESOURCES P.O. BOX 28041 -306 N. WILMINGTON, ST., RALEIGH, N.C. 21611 ORGANIC ~EMICAL ANALYSIS LAB NO . uoo y I FIELO # 3Y:R3 TYPE I I l ( l { ) { J UNITS /iin/1 un/ko ··"/1 '""/kn un/ 1 un/ko un/ 1 uo/ko IO -IA ,:.,7) /iJ /0 JD ~;.71 j() /0 .., ) I I Ir iJ \I <;).) /. "'6' /{) I So II ·, !/ 1//(/t- /1/21 I I - to 1 them value be ess g iven. to be greater than value given. ---•-..• ,. . { l ( l .. n/ 1 uo/ko ""/1 '""/ko L Actu.al value is known U ■ Katerial was analyzed 4 Not c1nalyzed. for but not detected. The nurt>er is the Minicn..m Detection Limit.--.:::::-,,..,..-?70c._ --- 1/ -Tentative identification. 21 -On NROC List of Priority Pollutants. ; I. o;_v-i..J.,;_o,; o 6 Ilea Uh SVtv-tC.<'.,~ ...... ',.. -~ . -., . ' ' -. I I- I I I I I Lake Murray Plastics CFO # 1 I I I I I I I I I I I I le. Dep,rtment of Human Resources ( r· State Laboratory of Public Health Division ofHeolth Services SAMPLE ANALYSES REQUEST P. o. Box 28047 L / (l.t1 e, S c 306 N. Wilmington Street .. ('. e; r"'\,r--.. R.leigh, 2761 I SiteNumbcr 23Doo~~4t,r;;✓ FieldSampleNumbcr L,L) 2IS8 .eofSite [..Aw /lluen 1/,i1c\ Ct=b#-1 Site location C.,leug\~J (ov,)\¾ Collected By BM:> f -Pi!kn ID# I 'l-Date Collected 8 -3-81 . Ti~e I a 3 d ~ Comments t ofSample: nvironmental ...x_ Groundwater (I) L_ Surface Water (2) Concentrate __ Solid (5) J:2r:r,\sh~ ~ we.l\ s9I~~~"-. .---Soil (3) 11---Other (4) __ Liquid (6) __ Sludge (7) __ Other (8) INORGANIC CHEMISTRY Extractablea Total Parameter Results mg/1 Parameter Results mg/ 1 Parameter Arsenic ..LArsenic .C?_,Q~ =iSilver __ Barium ..LBarium ·:..:::.o I Sulfates Cadmium ~Cadmium <0,0~ Zinc J=chromium Chloride LPh Lchrornium <(J,iJ/ ~ Conductivity __ Lead i'!ercury ~Copper O.~I TDS lenium Fluoride a. Z3 TOC Iver Iron <:.o.oS--- Lead < tl,O"J. t= Manganese ~o.o3 Mercury -lJ,oo'lJoZ Nitrate .. < {,_ .,?,d) Selenium ~ tJ,ODS:- 0ROldilG GIIBEISTB?l Parameter Reaults mg/1 Parameter Results mg/1 Parameter :t P&T:GC/MS _EDB __ Methoxychlor .--Acid:B/N Ext. __ PCB's _. _. Toxaphene :1=TO~ __ Petroleu.m . _2,4-D __ Endrin __ 2,4,5-TP (silvcx) • __ Lindane ---- . MiSR:9Bl0tB8Y ~ 010CHm AB flt t~ .. Results mg/1 ::< ~os // 0.0.5". 7,C> ry~Y/4"-. << Results mg/1 ◄; ,I Parameter Parameter Results PCi/ 1 ;=I= (MF) Coliform Colonies/lOOmls __ Gross Alpha 1 (MPN) Coliform Colonies/lOOmls __ Gross Beta ----~ -- Date .eived -----------------Date Reported __ .:.~..i/,__,_/_7'---'/4'-Q_""· c....<----------°' Extracted-----------------Date Analyzed ________________ _ Reported By Lab Number LJ / '.j(J,'; J Al /1~ ., '' I , I m 191 (R,-vi,ed 7185) Sn nd Hu■rdow Waste (Review 7187) t . .. ;?:;'\j)J) . ( HAZARDOUS WASTE BRANCH ~; N. C. Departm~nt of Human Resources BATH BLDG. State Laboratory of Public Health lion of Heal.t~ Servi, ·ces SAMPLE ANALYSES REQUEST P. o. Box 28047 . 306 N. Wilmington Street .!. [ / C ,, "',; <"-Raleigh, 27611 .. te Number 2.3 D 00 3 4 4 '2 '12 I Field Sample Number _o.::_o_3_<-(...:..,....e0 ________ _ lime of Site Llftk;E" tf/lr.,{l':/+'j CT_ASTIC S C Foti( Site Location C.,\e0e.\°="'J C1ou,&~~ Collected By BC\.t>b { /tj-/ /er1 ID# I 2. Date Collected ' -3-'67 -*=~ /0 3~71{ ~ of Sample: /';·"> SEP l 7 JS37 :~"'~ Environmental Concentrate ¼Comments_ .~ :::, V I ,':9-~ I_.A_ Groundwater (!) __ Solid (5) t", v::>o.. . S · (\ '\ -l. .§Te~---Surface Water (2) __ Liquid (6) 3:S:Qfu "<' es.1(\g ,n,\ N 0-<" a-Soil (3) __ Sludge (7) C,e.\ Q..M..&S!, °\="iW,'('5, (-)\o,.;1- --Other (4) __ Other (8) Extractables Parameter Results mg/1 Results mg/ 1 P&T:GC/MS bHGRODIOLOO'l Parameter L (MF) Coliform Colonies/lO0mls L (MPN) Coliform Colonies/lO0mls Ire Received 'K · 5-'x 1 FO · 1: ,1 -r1 ~,, te Extract~d ,J ~;r ,,,, p ;; l/2' .o,,.,_,:al MiOR0.1z~HC CflEffHSTRY Parameter __ Arsenic __ Barium __ Cadmium __ Chloride __ Chromium __ Copper __ Fluoride __ Iron __ Lead __ Manganese __ Mercury __ Nitrate. __ Selenium Results mg/ 1 Total Parameter __ Silver __ Sulfates __ Zinc _Ph __ Conductivity _TDS _Toe Results mg/I ORGANIC CHEMISTRY Parameter _EDB __ PCB's __ Petroleum __ Endrin __ Lindane Results mg/ 1 Parameter __ Gross Alpha __ Gross Beta Parameter --Methoxychlor _· _. Toxaphene _2,4-D __ 2,4,5,TP (silvex) R.l tnOCWEl US.RY Results mg/1 Results PCi/ 1 0 -/(J -f 7 Date Reported . ' · < DateAnalr..ed B/Jft<J-X7 i.3J.Y 1'~8'-f-?7 70ZO,i Lab Number __________________ _ I .11 C. Department of Human Resources ( Division of Health Services SAMPLE ANALYSES REQUEST State Laboratory of Public Health P. 0. Box 28047 306 N. Wilmington Street Raleigh, 2761 I la umber 2.31) Q O 3 4 4 G, '12 I Field Sample Number O C 3 <j 8 / l meofSite LA1c£(/,/,,e£il-Y, /~f15T/(S cFo.;:l,_1 Sitel.ocation Q\e0e_ J o llected By 80..\,b { A / /-{jll ID# _,_\-=2..=-----Date Collected 83-3 7-jl3ft rofSample: IE:nvironmental _x_ Groundwater ( 1) .___ Surface Water (2) Concentrate __ Solid (5) __ Liquid (6) __ Sludge (7) __ Other (8) I SEP \ Comments 1 _$;/ u.::,o._~ ~ ':':' Soil (3) I--Other (4) I Extractables Parameter Results mg/1 IFArsenic __ Barium __ Cadmium I Chromium Lead ~~;~~~:~- ilver . -- F f .... Parameter Results mg/ 1 ~P&T:GC/MS 7 Acid:B/N Ext. • TOX l= J.U GRODIOLOO'It Parameter (MF) Coliform Colonies/l00mls F (MPN) Coliform Colonies/lO0mls Ui~RB!~~ue ettef,ffS~Y Parameter Results mg/ 1 __ Arsenic __ Barium __ Cadmium __ Chloride __ Chromium __ Copper __ Fluoride __ Iron __ Lead __ Manganese __ Mercury __ Nitrate __ Selenium ORGANIC CHEMISTRY ', Parameter _EDB __ PCB's __ Petroleum __ Endrin __ Lindane Results mg/1 Parameter __ Gross Alpha __ Gross Beta Total Parameter Results mg/1 __ Silver __ Sulfates __ Zinc _Ph __ Conducriviry _ms _TOC ,. -- -- -- -- -- -- Parameter Results mg/1 __ Methoxychlor __ . Toxaphene _2,4-D __ 2,4,5-TP (silvex) -- -RP :OlQCHFl HS+RY Results PCi/ 1 • 0 ,.-"',.., r-/1. D:it ceived ___ _,,,('L_-~,.,_,-.,,;r:'---'r _ _.,0_,,,c_;'"· '--------Date Reported--~---------------- rile Exrractcd ---------------'-----Date AnalY"..ed _________________ _ U ---:,CJ 2L,LJ'f Reported By·-------------------Lab Number ______ , __ , __ ~ __________ _ rll; 3191 (Re-vised 7185)· 5ll3 and Ha:nrdous Waste (Re-view 7187) ·2 . ,·tt . : /N. C. Dep:l~tment of Human Resources State Laborato?y of Public Health · ·,ion of Health Services SAMPLE ANALYSES REQUEST P. 0. Box 28047 306 N. Wilmington Street Raleigh, 27611 Site Number 2.3 D Q O 3 4 4 {p '12. I Field Sample Number 00 3 <-/ 8 Z fneofSiteLArc117ue,O✓-l( t21JISTICS C(o,rl,( SiteLocation -c~~ Collected By Bo..\:>ki < 4-✓L:a !Off 1 2.. Date Collected ;;'? Time lo& fltv{ .of Sample: Environmental f-2(-Groundwater (I) - ___ Surface Water (2) a-Soil (3) ■~-Other (4) Concentrate __ Solid (5) __ Liquid (6) __ Sludge (7) __ Other (8) ' \\ \ Comments t.,.::\O..~ v-X. ~ "' ~ ~, -~ SEP 17 .i93( ~, Hii@ROhPHC CttE!,HSTRY Extractables Parameter __ Barium l=Cadmium Chromium __ Lead --~~;~~;_:_ __ --Silver _ Results mg/1 I= __ _ Parameter __ Arsenic __ Barium __ Cadmium __ Chloride __ Chromium __ Copper __ Fluoride __Jron __ Lead __ Manganese __ Mercury __ Nitrate. __ Selenium Results mg/ 1 Total Parameter __ Silver __ Sulfates __ Zinc _Ph __ Conductivity _ms _TOC Results mg/1 ORGANIC CHEMISTRY ~Parameter Results mg/1 Parameter P&T:GC/MS _EDB eB/NExt. __ PCB's __ Petroleum __ Endrin --__ Lindane l,HE;RSBl91:801i Parameter I= (MF) Coliform Colonies/l00mls (MPN) Coliform Colonies/lO0mls -- I;.; Date cceivcd 'i? -.ii-':i 7 r-r3 ile Extracted----------------'---- lortecl Ily 3191 {Revised 7/85) SD 1d ::inrl H:i~P.~d0u~ W11sre (Revi<""w 7/R7l . Results mg/ 1 Parameter Results mg/ 1 __ Methoxychlor __ -Toxaphene _2,4-D __ 2,4,5-TP (silvex) -- :ft::tQ :i;ngc;wi.1 US~Y Parameter Results PCi/ 1 __ Gross Alpha __ Gross Beta ... -- -- Date Reported Date Analr.ed __________________ _ Lab Number ____ ,,..,c../_c_,,,__,_c_,_3_? _________ _ SE/NEUTRAL AND ACID EXTRACTABLES I COIIPOUND N-nitrosodimethvlamine is (2 ch loroethvllether chlor~henol nhenol I _3-dichlorobenzene 4-<lichlorobenzene .2-<lichlorobenzene bis(2 chlorois=r=ullether exach 1 oroethane nitroso-di -n-nrt'Vl.vlamine nitrobenzene 1 ·s~horone -nitr-henol .. 4-<limethvl ohenol I is(2-chloroethoxv)methane 4-<lichloroohenol 2 4-trichlorobenzene n•nhthalene lexachlorobutadiene -chloro-m-cresol lhlorocvcl~ntadiene -trichlo-henol oronaohthalene cen,nhthvlene dimethvl nhthalate .. 6-<linitrotoluene cenanhthene 2.4-<linitr~henol . 4--<linitrotoluene -nitroohenol fluorene i-chlo-henvlohenvlether iethvl nhthalate 6--<linitro-o-cresol diohenvlamine zobenzene -bramohenvlohenvlether hexachlorobenzene ntachlor~henol henanthrene anthracene dibutvl nhthalate 1 uoranthene -Estimated value. STATE LABORATORY OF PUBLIC HEALTH DIVISION OF HEALTH SERVICES, N.C. DEPARTMENT OF HUMAN RESOURCES P.O. BOX 28047 -306 N. WILHINGTON, ST., RALEIGH, N.C. 27611 ORGANIC CHEHICAL ANALYSIS LAB NO '.J0.:7,1,Y FIELD# 3,1.hJ TYPE L il ( ) ( ) ( l UNITS 1/ .. n/l h,n/ka ,on/1 ua/kq ua/ 1 .. n/ka .. n/ l .. n/ka I ti I'-. -:--/ A ! ! I I ! ! I ' I ' I I I I I I i I I I ! I I ' I I : I ,v L,o lo ',rJ / cJ / ti lu I ,,;o i so i ,.,-, ' ~· /(J ' ' /0 ' !:>"7 IJ i /!, /0 It! \:/ ii.1 OL_ /'tf/.t' ( l .. n/1 .. n/ka Actual value 1s known to be less than value given. Actual value is known to be greater than value given. Material was analyzed for but not detected. The numer is the Hinin>.111 Detection Limit. ::-1'7PL M -Not analyzed. I/ -Tentative identification. I -On NRDC List of Priority Pollutants. N. C. V.i.v.u.i.on 06 He.a.U.:h SVtv.i.cu .HS 3068-0 (4/86 Labo~a.to~y) ( l .. n/ l .. n/ka .. -IE/NEUTRAL ANO ACID _ EXTRACTABLES <XlMPOUNO ~e dine XJlvl benzvl ohthalate ,e alanthracene :h ·ene I 3-dichlorobenzidine ~thvlhexvllohthalate tvl ohthalate ,l fluoranthene >enzo(kl fluoranthene ,e (alnvrene ,n (1 2.3-cd)nvrene 1ibenzo(a h)anthracene ,e (a. h i l=rvlene lne ic acid 1 alcohol khl ni 1 ine Ii ran ' hvJn,nhthalene -'-<rethvl oheno 1 flhvlohenol roani line roani 1 ine Hlitroaniline ' trichloroohenol =t =I I IEstima.ted value. ( STATE LA80AATORY Of PUBLIC HEALIH DIVISION Of HEALTH SERVICES, N.C. DEPARTMENT Of HUMAN RESOURCES P.O. BOX 28047 -306 N. IIILMINGTON, ST., RALEIGH, N.C. 27611 ORGANIC CHEMICAL ANALYSIS LAB NO 7,;::, c. 3v FIELD# J'!YC TYPE ( ,' l ( ) ( ) ( ) UNITS A:,o/ I ". .. n/ko 00n/ I uo/kq uo/ I uo/kq oon/1 ,on/kq /0 \....:="'" l1 !,7' : /0 i JO /u i sV ' I,; It) C,[• ' ' I \ ,I ' 0 l1 0' ! I l.,,; ! I i I ' I I ' ' \;I : S,o I ; ' ' \!I \/ n;DL ur,i I I ( ) un/ I uo/kq .- -· . w;al value is known to be less than value given. -1 value is known to be greater than value given. I -erial was analyzed for but not detected. The nuTt>er 1s the Minim..rn Detection ..!:_imit. -=--1'1?{)L- IA .Not analyzed. I/ Tent.alive identification. ~/ On NRDC List of Priority Pollutants . . ,D.i.v-w.i.on o 6 H. 068-0 (4/86 /lealt/i Svi.v.zc.~-l Labo1ta.to1ty I ( ) ,on/] uo/kq • I· PWGcABLE CXJIIP(UIOS CXll!P(J(JND _; C orcme thane b ron::rrethane h lorodi fluorarethane T chloride ch I oroethane i hvlene chloride chlorofluorarethane ""ne. l 1-dichloro ethane 1, 1-dichloro- l -trans-dichloroethene C orofon:a ethane, 1 2-dichloro- ~ 1 1 1-trichloro- tetrachloride brorodi ch loranethane Doane 1,2-dichloro- -trat!S-<lichl ch loroe•~l ene chl ibroromethane -e .-t; 1,2-trichloro- 1 3-ds-<llchl ~<>roetr>vl vinyl ether ona 1 ·1 2,2-tetrachloro-E tetrachloro- robenzene ethvlbenzene ~ 2-ootanone -isulfide 2-xanone thvl-2..,,,.,,tanone ~,rene !..! 111 acetate _ lllenes f-lx+-al_} Est11nated value. I STATE LAIJOlATOOY Of f'\J1lLIC HEALTH DIVISION Of HEALTH SERVICES, N.C. OEPAATMENT Of lfJIIAH RESOORCES P.O. BOX 28041 .. 306 N. WILMINGTON, ST., RALEIGH, N.C. 21611 OOGANIC Qjl:M!CAL ANALYSIS I.AB HO 70 lt1-:>,y' FIELD I :ji/J1/;c1f' · TYi'£ c I l ( ) ( ) ( ) UNITS ,.. UQ/_. "" /kq uo/ l uo/k_g uo/ l ,on/ko uo/1 µg/ko /0 r' . Ji --,,I /D JO ) ;2u t, ' ' I ' I I I I i ' I ~I /0 0 I I I I \V !/ /O I' /ti ' ') /D ltJ ~ /o '-i .I/ /7J/lL._ u::./Y ,. " K ual value is krlOw'n to be 1 ess than ( ) uo/1 uo/kq value give~. l -..iii_~l value· is known to be greater thdn value 91ven. U -E1a1 was analyzed for but not detected. The nUlber is the Mininun Oete<:tiooJimit. :-1}?,VL... Not analyzed. Tentative identificatiOl'I ?I On NROC List of Priority Pollutants. N ■· Division of D11 3068-0 (4/86 Heal th Services Labnralory} ( ) uo/1 un/ko (-1. Department of Human Resources ( Sute Laboratory of Public Health Di,-ision of Hcolth Services SAMPLE ANALYSES REQUEST P. o. Box 28047 5 & 306 N. Wilmington Street e_,dcJ1 e Raleigh, 27611 s, umber 23 DO O 3 4 LJ t, 1 2. I -Field Sample Number .=o_0.....;~~'-0_-_9-'--------- +e of Sit•~ A f K A:!£ \4 -~I--.) 2 °) Site Location C, I e V!1. \ a.,.,.__J (o L1/r,, ~ c!fiected By Babb f i\ \ ½?(I ID# / '?-Date Collected 7-d 2-'8 I Ti~e O,vi; t1,r,J~ 5/.lrlr-/JJ~ ,:c'.•J~/.,,.Jt!_,l_ ;:..•e Ct?/1:!:J, J~,,..j/~ fe /JC.I✓, o/. r•1z,e,; fo ,,,.,.Nrl-/ysrJ, //c)S- '""" Comments l ofSample: nvironmental _x_ Groundwater (1) L__ Surface Water (2) Concentrate __ Solid (5) __ Liquid (6) __ Sludge (7) __ Other (8) '.]) s::""\,,'~ ~\v we,\\ ---~~\~ __ Soil (3) 1--Other (4) INORGANIC CHEMISTRY Extractables Parameter Arsenic __ Barium __ Cadmium Lchromium .LLcad I= ercury ~l~~iu~ __ '. lvcr Results mg/ 1 Parameter LArscnic LBarium LCadmium LChloride LChromium ....L.._eopper L Fluoride Iron Lead Manganese Mercury Nitrate _ Selenium Results mg/ 1 <o, I -<o,oo.S <o. os""" Total Silver Sulfates Zinc .-Ltit G Results mg/1 L3 <o,o.5- z(Za:111 ,,.,, C. ;'@ t 0ROA?UG GllRHSTR?.{ . -a= Parameter Results mg/ 1 Parameter Results mg/1 Parameter Results mg/1 P&T:GC/MS _EDB __ Methoxychlor __ Acid:B/N Ext. __ PCB's _· _ Toxaphene FTOX __ Petroleum _· 2,4-D __ Endrin --2,4,5-TP (silvex) __ Lindane -- I tlH6R8Bl9b88Y MCIOCUMI HS'Plt l" .. Parameter Parameter Results PC(/1 I= (MF) Coliform Colonics/lOOmls __ Gross Alpha (MPN) Coliform Colonies/lOOmls __ Gross Beta ---- ---- Da.eceived ' ----------------Date Reported ---~-l-/-'-!-'-O'-t/'--Y_7 _________ _ lte Extr~cted --------------~--- Rc;mrred By IS 3i9I (Rc-vi~d i/85) ,,{ :.rid Ha:,rJou.s \'(/.a~rc (Re-view i/87) Date Analyzed D. Lab Number J __ ._d3tJ F,le Ge-.._. l . ,.;/t";,';;; f:t,;[:/';"'/ -r.t., I ry_zs-. ~-Department of Human Resources State l...aboratoTy of Public Health Division of Health Services SAMPLE ANALYSES REQUEST · P. o. Box 28047 306 N. Wilmington Stt~t . ~ Raleigh, 2761 I Jte Number 2..3 D o a 3 4 4 '2 '7-2. I Field Sample Number @~_;;;g;; 6 a 5 'l , 1 ll<ame of Site -~~,0~A'--'l2..--'-"'(l~O-Lf2"-(:J'--_:::.-:E=0"-'.l-J_1_r-::,_'\_'· -----Site Location C,\ e.0 e.~~1 c,,0\,,/Jf',-h '!:ollected By ~B=c,_~\:,~b"-'f~A'--'/-=~=2-.,__V\,..__ __ ID# ~\_2. ___ Date Collected q -;)f! -(il 7 Tim~ / / GS-f/A lype of Sample: Environmental 1---2(__ Groundwater ( 1) . ___ Surface Water (2) --Soil (3) 1--Other (4) Concentrate __ Solid (5) __ Liquid (6) __ Sludge (7) __ Other (8) Comments J),~n\s,"';S ~a.k W-f,\\ 60..m~\e /_$ :·: ·~ Ul@il!OA-?H:C Cll£liflSTRY (; SE? 2 193"7 il j Extractables Parameter Arsenic Chromium Lead Mercury ..,~Sd~Diurn~- . ·Silver Parameter ~P&T:GC/MS 2 Acid:B/N Ext. E'f0* Results mg/ 1 Results mg/1 1'wflGROUIOL001f Parameter __ Arsenic __ Barium __ Cadmium __ Chloride __ Chromium __ Copper __ Fluoride __ Iron __ Lead __ Manganese __ Mercury __ Nitrate _ __ Selenium Results mg/1 ORGANIC CHEMISTRY Parameter Results mg/ 1 _EDB __ PCB's __ Petroleum __ Endrin __ Lindane Total __ Silver __ Sulfates __ Zinc _Ph __ Conductivity _ms _TOC Parameter __ Methoxychlor __ . Toxaphene _2,4-D __ 2,4,5-TP (silvex) -- JV.oioCHE} (JS'vRY Results mg/1 Parameter Parameter Results PCi°/1 (MF) Coliform Colonies/!OOrnls (MPN) Coliform Colonies/lOOrnls __ Gross Alpha __ Gross Beta __ ~.,(~: ~'.:l~l.,.., -~£~+---~_r:_t_, ________ Date Reported -,--r~Y:_-_2-_._sc_-_,,r..,.7~---------c::/ · · /~y /'/•fl c'-,,, n,-i7-~'7 lte Extracted < l(/S ~w Date Analyzed v -11. -, / n/>· Reported By/~ ·. -Lab Number ----,°",=,"..;!11/"l.l 1 I S 3191 (Rcvi~d 7185) If iJ and Ha:nrdou.s \X/asce (Revie,...• i 187) ,. C. Department of Human Resources Division of Health Services SAMPLE ANALYSES REQUEST State Laborato'ry of Public Health P. 0. Box 28047 306 N. Wilmington Street -. Site Number . :/._ 1j Raleigh, 2761 I ~Z..:"?-3L.,D""""'-'o~o~3.,_4...L-.C4'-l..""'-''7-'--'2~1--Field Sample Number C1() 3 { 7 f~ ( L~ Jc~ Site Location C,\e0e.\Q.Md C,ol~ .me of Site Collected By Ba_\:,lgJ#\\eJo ID#~\_:2-__ DateCollecred 7-Jff-8 7 Tim~ f/(;S-/f-(11 tpe of Sample: Environmental 1_2(_ Groundwater (!) ---Surface Water (2) ■-Soil (3) Concentrate __ Solid (5) __ Liquid (6) __ Sludge (7) __ Other (8) Comments '1)\'"~Y1\_;l':_) l.Na.~ v-.,~\\ 6CL'.ffi¢f ~ Other (4) Extractables Parameter Results mg/ I Mercury ---._Se_l~r)iU~~--- . -Silver I= -------------- 1 Parameter Results mg/I ~P&T:GC/MS ~Acid:B/N Ext. TOX -- I J,UGROiHOLOOY Parameter I= (MF) Coliform Colonies/lOOmls (MPN) Coliform Colonies/ IOOmls -- £ Hi@RO .. \?HC CIIE1,HSTRY Parameter __ Arsenic __ Barium __ Cadmium __ Chloride __ Chromium __ Copper __ Fluoride __ Iron __ Lead __ Manganese __ Mercury __ Nitrate. __ Selenium Results mg/ I ORGANIC CHEMISTRY Parameter Results mg/I _EDB __ PCB's __ Petroleum __ Endrin __ Lindane Parameter __ Gross Alpha __ Gross Beta -- -- Total P~rameter __ silver __ Sulfates __ Zinc _Ph __ Conductivity _ms _TOC Parameter __ Methoxychlor __ . T oxaphene _Z,4-D __ 2,4,5-TP (silvex) -- RADIOCHF> USTRY Results mg/I Results PCi/I . Dat.ceived ___________________ Date Reported--~-----------------te Extracted ___________________ Date Analyzed ------:----::::--=--a---------- Reported !ly Lab Number 10 I 'I 9, ,. 3191 (Rcv;,,d 7185) sai 3nrl H3:;irdous WRstc (Review 7187) l. C. Department of Human Resources Division of Health Services SAMPLE ANALYSES REQUEST State LaboraroTy of Public Health P. 0. Box 28047 ·306 N. Wilmington Street It, N~rnber ~ame of Site ~ollecred By ' ype of Sample: Erivironrnental I _L Groundwater (I) ___ Surface Water (2) __ Soil (3) 1--Other (4) Concentrate __ Solid (5) __ Liquid (6) __ Sludge (7) __ Other (8) Ui~a8MU8 ettEt,HS~Y I I Extractable& Parameter Results mg/ 1 I L--Arsenic_ , __ Barium 1 __ Cadmium 1---Chromium ,__Lead MercurY :--S~J~Di~!Il_:. ._ ~·Silvei -- E== -- I Parameter Results mg/ 1 ~P&T:GC/MS /Acid:B/N Ext. TOX I= MIGR0!310L00'l Parameter --(MF) Coliform Co!onies/lOOrnls (MPN) Coliform Colonies/lO0mls Parameter Results mg/1 __ Arsenic __ Barium . __ Cadmium __ chloride __ Chromium __ Copper __ fluoride __ Iron __ Lead __ Manganese __ Mercury __ Nitrate __ Selenium ORGANIC CHEMISTRY ·. Parameter _EDB __ PCB's __ Petroleum __ Endrin __ Lindane Results mg/1 Parameter __ Gross Alpha __ Gross Beta Raleigh, 276 I I Total· Parameter Results mg/1 __ Silver __ Sulfates __ Zinc _·Ph __ Conductivity _TDS _Toe ---- -- -- -- -- Parameter Results mg/1 __ Mechoxychlor __ . Toxaphene _2,4-D __ 2,4,5-TP (silvex) -- ·Rt\DIOCHi! USTRY Results PCi/ 1 ~ceived __________________ _ Date Reported--~----------------- .te Extracted Date Analyzed !ported By·------------Lab Number ---~'~/)'-'-/~2._...,'/7 1,,..,._ ___ _ 11S 3191 (Rcv;,cd 7185) iJ and Ha:mfous \Y/11src (Review 7187) I It I PURGEAB LE COl1POUNDS COl1POUND I ch lorarethane brorarethane dichlorodifluororethane lvinvl chloride ch loroethane methvlene chloride ltrichlorofluoromethane ethene 1-1--dichloro ethane 1. 1--<lichloro- 1 2-trans--<lichToroethene I chloroform · ethane. 1.2--dichloro- ethane. 1.1. 1-trichloro-I carbontetrach 1 or i de brarodichlororethane oronane 1 2--<lichloro- 11 3-trans--<lichlo, ne trichloroethvlene· chlorodibrorarethane ~ene ne 1 1 2-trichloro- --cis--dichlo. ne 2--chloroethvl vinvl ether broroform ethane. 1.1 2.2-tetrachloro- ethene. tetrachloro- toluene ch l orobenzene ethvlbenzene acetone -butanone carbondi sulfide ~xanone thvl-2~ntanone stvrene vinvl acetate xvlenes l+d-ai> J -Esturu.ted value. ( STATE LABORATORY OF PUBLIC HEALTH DIVISION OF HEALTH SERVICES, N.C. DEPAATMENT OF HUIIAN RESOURCES P.O. BOX 28047 -306 N. WILMINGTON, ST., RALEIGH, N.C. 27611 ORGANIC 01EMICAL ANALYSIS LAB NO 70tCf9(, FIELD I :Jt.cJJ TYPE I I l ( l ( l ( ) UNITS 1/ua/t/ua/ka un/ l --0 /ka --0 11 ••0 /ka .. nfl .. n/ka /,l'l " /'D ,o /l) Jv 1- 'JO !, , /6 S' ' •/ /() I ' N t," Mo '" ,; Jo s-' I/ IJtbL ,,LIP ' .. ( ) un/1 un/ka I -Actual value is known to be less than value given . • -Actua! value· is known to be greater than value given. Material was analyzed for but not detected. The nuroer NJ Not analyzed. is the Mini"'-'" Detection Limit. cc: /J1i>L- i/ -Tentative identification. I -On NROC List of Priority Pollutants. N.C. Division of Health Services rHS 3068--0 (4/86 Laboratory) ( l un/] ••n/kn • I BASE/NEUTRAL ANO ACID EXTRACT ABLES COMPOUND N nitrosodimethvlamine bis(2-chloroethvl)ether ch l orrv"\heno l henol l -3--d i ch 1 orobenzene 1 4-dichlorobenzene l-2--dichlorobenzene bis(2-chlorois ,,))ether exach l oroethane nitroso--di-n--nr""'"lamine nitrobenzene is~horone nitr,.,,....henol .4-dimethvlohenol bis(2-chloroethoxv)methane 4-dichloroohenol 1 2 4-trichlorobenzene n•nhthalene 1 'exachlorobutadiene '-chloro--m-cresol hexachlorocvcl~ntadiene ~6-trichlo-henol 1loron•nhthalene nanhthvlene dimethvl nhthalate --6-dinitrotoluene cenanhthene .. 4-di ni tr~heno 1 2 4-dinitrotoluene -nit-henol luorene 4-chlo-henvlohenvlether iethvl ohthalate .. 6--dinitro-o-cresol dinhenvlamine I :1zobenzene -b-henvlohenvlether hDxachlorobenzene =ntach lor~heno 1 I henanthrene nthracene dibutvl ohthalate 11 uoranthene ,TATE LABORATORY Of PUBLIC HEALTH DIVISION OF HEALTH SERVICES, N.C. DEPARTMENT Of HUMAN RESOURCES P.O. BOX 28047 -306 N. WILMINGTON, ST., RALEIGH, N.C. 27611 ORGANIC CHEMICAL ANALYSIS LAB NO "JOl'i</1- FIELD# 3 LJ. 77 TYPE ( /) ( ) ( ) ( ) UNITS /4n/)'\ua/ko .. n/) .. n/ka "n/ 1 un/kq uo/ 1 un/kq 10 -.:-IA , -·-1 0 ,,,_ 1/1 , ,, "'0 /o ,; 0 /o //) /t> 5o S?) 5'V /U /0 ,f 6 /;-, JI) /i) Ii> ' I fr) L l) J -Estimated value. ;-t,W~ . ( } un/) .. n/ka Actual value 1s known to be less than value given. Actual value is kOOW'n to be greater than value given. Material was analyzed for but not detected. The nurber Not analyzed. is the Mininun Detection Limit. =/>J l,?L.. lt -Tentative identification. ,I_ -On NROC list of Priority Pollutants. N.C. V~v.w~on 06 Hea.Uh SVI.v~cv., jHS 3068-0 (4/86 Labo~a,to~y) ( ) "SI 1 ~9/k9 I It • __[E/NEUTRAL NIO ACID EXTRACT ABLES <XlMPOONO j ne idine ,ut I benzvl ohtha late j :(a)anthracene sene I 3--dichlorobenzidine ) 2--ethvlhexvl )ohtha late I --octvl ohthalate ,en,o (bl fl uoranthene lo(k)fluoranthene o(a)nvrene no ( 1 , 2. 3--<:d) nvrene :libenzo(a. h)anthracene o(o h, iloervlene line oic aCld ,vl alcohol ."Oaniline furan · lnaohthalene ... 1--m,thvl oheno 1 ._ thvlohenol I troaniline 3-'n 1 troani 1 i ne '-'litroani line fs-trichloroohenol j - STATE LABORAIOHY OF PUBLIC HEAL!H DIVISION OF HEALTH SERVICES, N.C. OEPAR111EN1 OF HUMAN RESOURCES P.O. BOX 28047 -306 N. lo/lLIIINGTON, 51., RALEIGH, N.C. 27611 OOGNHC OJEIIICAL ANALYSIS LAB 00 7o l't'li FIELD# 31/-77 TYPE ( I ) ( ) ( ) ( ) UNITS /4;] "\.,n/ka un/ 1 ua/ka ua/1 ua/ko un/ I un/kq /0 ,.,_.IA So. /I) ID VJ ,;;, /[} //) S-0 . , Yi> L1 .<o /() fo /R n ,, h ,t;7 , ,; ' MDL u,~/17 , . K ual value is known to be less than value glven. l -u.a.l value is known to be greater than value given. ( ) ~Q/1 uo/kq J ~stimated value. U -terial was analyzed for but not detected. The nurber 1s the ~nirrun~tection _himit.~/'nl)L-Not analyzed. Tentative identific,Hion. _ On NROC List of Priority Pollutants. ~-, 0.i.v.U-t0t1 Oo 91 3068-0 (4/86 11wttli SVtv-tc.<'.-!o LaboJJ.ai:oJJ.y) ( ) Hn/) un/ka I I I I I I I I I I I I I I I I I I I LutheranChildren's Home I I I ••• I Slf'\TE L/\BORATORY OF PUBLIC HEALTH DIVISJ □N OF HEALTH SERVICES N .C. DEF'f':F:1MHH OF HUMM-! F:ESDURCES P .. 0 ~ [-:1t1Y: 280/47 ... 306 N. l·.IIL.M I~iGTON ST. ,. nr,LE n::H 27 6 J ). I INORGANIC CHEMlC~l-~NAi_YSIS SlTE: D(:TE: 1.2/18/86 Field Sample Nu~bEr: 002151 I N0r.:~ cf Si"i..r-: Fiber Industries-Inc I I I Collected on: P!,R!tM • JD I ~-,oosr i010T i.0JST _ J~f:ME. !,RSENIC \j(,RIUM CllDMli.JM I I I i0i7 CHLORIDE 10'.!0T CHROMIUM l 022 COF'PEF-: i02S FLUORIDE 1028 JF:ON 1030T LE/:D 1032 Mr.NG/,NE:SE 1035T r\EF:CURY i01:1J NlT~:fiTE: i◊ilST SELENIUM 12/03/86 Tims-: 01':SPM Colleckd 8v~ 8/\88//:LLEN- MG/L .. MEJHDD_ .. RESULTS '')C 1.:. ., 101 101 101 i () :i 107 101 101. iOi 103 163 12S < 0 -<HOO 0 _ J 000 0.00!:,0 i.0000 0.0i00 o _.0500 0.1000 O.ObOO 0.0300 0. o:,oo 0.0002 1. 0000 0.0050 Pf':Rf':M .... _ .. .IP. . NAMF. 1050T SILVER 1055 SULH:TE 1095 ZINC 1925 F'H .. _ t:lEJHOP . 101 137 101 135 1926 CONDUCTIVITY 000 1930 TDS 139 lOiO TDC 000 MG/I. .. ~:!';SUI-TS . 0.0500 1':-.0000 0.0600 6.8000 151:. 0000 120.0000 7.0000 I D.::;°i.C' ~:ece-i',Td~ }2/0b/86 Dzd.e Rer-ortc-d:· 12/18/86 Dc:te Ati~lvzed~ 12/18/86 I I •• I I Lcbor·atorv Nur,bcr: 62':767 Rc·rortcd Bv: Com,:cnls: DRf'..lJAT.lJEU_ NEf'\F: CEI ... FI\3.PLT. Mi.1.dr~d ~-L KcrbiiUQh Dl rt·ctor ~/V" {Yu.ld~AJ /f.o~ o:J F /JcuJ C!tJ.';d~ -z-;7 -;;,p I/ I i le I I I I I I I STATE LABORATORY OF PUBLIC HEALTH DlVlS!ON OF HE/1LTH SERVICES N.C. DEPARTMENT OF HUMAN RESOURCES r P.O. BUX 280~7 -306 N. ~ILMINGTON ST., RALEIGH 276Ji HEP0R1: E70RSl_:C,() INORG/\NlC CHEMJC!11_ i1,'1\USIS SITE DhTE: 12/29/86 23D003~~6721 Field Sam~le NuEber: 002j_52 N.:!nr-of Sil£•: Fib~r Industries lnc Tvrc of Samrle: ENVIRONMENTAL GROUND (oll.ected on: Dc:tc: 12/03/86 Time: 01':SF'M Collected 8v: /1LLEN/ 13/1138 MC/L P?1R?1M MG/L • iD _ .. Nl'ME. I iO0S T /1RSEN IC _ MEIHOP .... BESULTS .. l2S 0.0100 ID .. NAt1f:. _ . _____ METHOD __ F:ESUL TS iOSOT SILVER 101 0.0500 I I 1010T 8!1F:lUM 101ST CADMIUM 10 i7 CHLORIDE iO::COT CHFWMlUM j on COF'PEF: 1025 ).028 :i030T 1032 FLUOHlDE lRON LE40 H/\NGhNESE i035T MERCURY iOl:,j NITRATE 101:sT SELENIUM 101 0. i 000 101 0.0050 2.00()0 101 0.0100 101 0.0500 107 0.1000 101 0.0500 101 0 .. 0300 101 0.0300 103 < 0.0002 163 i.0000 i2S 0.0050 :i_O~S SULFATE 137 15.0000 1095 ZINC 101 0.0600 1.925 F'H 135 7.8000 1926 CONDUCTI'JITY 000 155.0000 1930 TOS 139 12(). 0000 1010 TDC 000 5.0000 I I I I Dale Received: 12/0&/86 D~1£ Rerorled: 12/22/86 D~le Analvzed: 12/08/86 •• I I Lc:bc,rc>i.orv Nur.,ber: b2~8'i9 RE'rorkd [w: E33 Comrr.:,nts: DRINf'.ING IU1FER/ NE~R CELENESE MildrPd A. J(erbau~h Di r'E:c·\.or _,,_ ..... "';'" .,/';-·.~--:~.:. __ .: • 1_ -: t . I •• I PURGEABLE COMPOONDS COMPOUND ch 1 oranethane brcrnanethane dichlorodifiuorarethane vinvl chloride chloroethane rrethvlene chloride trichlorofluorarethane ethene 1.1...<Jichloro ethane. 1.1-dlchloro- 1.2-trans-<lichloroethene ch lorofonn ethane. l.2-dichloro- ethane 1 1 1 trichloro- carbontetrachloride brorrodichloranethane I I I I I I nr ....... ane 1.2-<lichloro- 1.3-trans-<lichlo ne ltrichloroethvlene chlorodibroionethane ;~ 1. 1.2-trichloro-Ii -c1s-<lichlo ne 2-chloroethvl vinvl ether brorofonn STATE LABORATORY Of PUBUC HEAL TH DIVISION Of HEALTH SERVICES, N.C. DEPARTMENT Of HUMAN RESOURCES P.O. BOX 28047 -306 N. WILMINGTON, ST., RALElGY, N.C. 27611 ORGANIC CHEMICAL ANALYSIS LAB NO (,1:.·:,,·~,., / .. / . . FIELD# 3:rL.:i'.1-3._,-v 1 / . . TYPE (.J ) (/ ) .( ... ) .( ... ) UNITS / .. n/1 \,n/ka , •'"I 1 un/ka .;;n/ l un/ka ..,;Q/1 ua/kQ 0 ~---· I.A- /._! . tu {/.I ' le .) ') ,_; / !, I I I/ /.J! '>T .ethane. 1 1 2.2-tetrachloro-----~- ethene. tetrachloro-·1/ C, \:.I • CI. toluene .{ ... ch 1 orobenzene 'I[;} ethvlbenzene \/ ' i Q & .. ~ .. .. ~ acetone /) u....,... ' l'>-. , 2--butanone /:;> ' ~w;; carbondi SU I fide j 'i, .. 2-hexanone Iv ; ~thv1-2~ntanone /J ene \ vinvl acetate ;;;, . . xvlene"' /i...LJ) -• I s fl/ Jl. l.,l,;) /_/ J -Estimated value. ..~· (. . l /,,cit I "a/ka ""'-.-:-·1 '\. '"'.'··•, \ '(CJ -.~?.>\ -, ,., •·,-1~..;; .~-., :;,,,. Actual value is known to be less than value given. Actual value· is known to be greater than value given. llaterial was analyzed for but not detected. The nurrber Not analyzed. is the Mini111.111 Detection Limit. Tentative identification . • , -On NROC List of Priority Pollutants. ~.C. Division of Health Services 3068-0 (4/86 Laboratory) / (./) u6/1 .. n/ko I N. C. Department of Human Resources Division of Health Services SAMPLE ANALYSES REQUEST 0 ••• State Laborato'ry of Public Health P. 0. Box 28047 306 N. Wilmington Street Raleigh, 2761 I -2.31) 0 o 3 4 4 '2 7 2 i Field Sample Number ~D~C)"-"-3'-'~"-0~0---~-----Site Number II Name of Site [..,+\w,qoGbild r.'n:-, t-~, {)',g C,Qo,7lPD<I.Ai':&2, Site Location (1,\e0e\Q.,<,:)d C.-01v,\i::C,. Bo.\:,\a { ;.),A\ \en ID# I 2-Date Collected 1 'l -:, -Z<...Q Tim~ Collected By 1 · Type of Sample: R Envi_ronmental _ _x_ Groundwater (I) ___ Surface Water (2) Concentrate __ Solid (5) __ Liquid (6) __ Sludge (7) __ Other (8) Comments v,~"'"''":J ~o..~( v-.,~\\ 60-m ~f B H II I I D D I g __ Soil (3) __ Other (4) Extractable, Parameter __ Arsenic __ Barium __ Cadmium __ Chromium __ Lead _ Mercury _Selenium __ Silver Parameter 1 z& T:GC/MS °"2_ :tid:B/N-ht TOX -- -- Parameter Results mg/ I Results mg/I I~! A- '-H6R:8Bl01::88~"' __ (MF) Coliform Colonies/lO0mls __ (MPN) Coliform Colonies/l00mls -- -- UiOR01\:NIC €11Ef¥HSTRY Parameter __ Arsenic __ Barium __ Cadmium __ Chloride __ Chromium __ Copper __ Fluoride __ Iron __ Lead __ Manganese __ Mercury __ Nitrate. __ Selenium Results mg/I ORGANIC CHEMISTRY Parameter Results mg/ I _EDB __ PCB's __ Petroleum __ Endrin __ Lindane Parameter __ Gross Alpha __ Gross Beta -- -- Total Parameter __ Silver __ Sulfates __ Zinc _Ph Results mg/I _· _ Con .,-·.··Vf::. · --~---,;,+.------ Parameter Results mg/ I __ Methoxychlor __ . T oxaphene _2,4-D __ 2,4,5-TP (silvex) -- R~.i:QIQCW•! HS;.R~ Results PCi°I I I Date Extracted _1...,,-,l_•~-f-_/:.,.• 1 · 1 ___ ,-c:-,::,~.,.., ,-/., __ -.-.. -.c-.-1::..-;",..._-_--__ -_-______ Date Analyzed Reported By· --i:,,.-!-=-'-'"'-"''---'-'-'--"-_;:__:c....... ________ Lab Number ___________________ _ ., I [)HS 3191 (Revised 7185) SoliJ and Harnrdous Waste (Review 7 /87) II._,. C. De~rtme~t of Human Resources ~ivision of Health Services SAMPLE ANALYSES REQUEST State Laboratol'y of Public Health P. 0. Box 28047 306 N. Wilmington Street [ me of Site llected By Raleigh, 2761 I IType of Sample: Environmental Concentrate _2(_ Groundwater (I) __ Solid (5) I --Surface Water (2) __ Liquid (6) Comments ::D\" ~ YI\,\~ V::.a. ¼ \,_,~ \\ Q °=® ~ f __ Soil (3) __ Sludge (7) u __ Other (4) __ Other (8) Iti@R0/r'.!ile SltEl,HSTRY I Extractables a•· Parameter I __ Arsenic __ Barium __ Cadmium I __ Chromium __ Lead Mercury I .Selenium __ Silver Results mg/ 1 Parameter __ Arsenic __ Barium __ Cadmium __ Chloride __ Chromium __ Copper __ Fluoride __ Iron _Lead Results mg/ 1 Total Parameter Results mg/ 1 __ Manganese __ Mercury __ Nitrate __ Selenium I ==--------1---------':-~~-------:-1 I Parameter I l_y'_,P&T:GC/MS I_ 7c:tl:-B/N-Extc TOX I= Parameter Results mg/1 l.HGROBIOLOOri.t __ (MF) Coliform Colonies/lOOmls (MPN) Coliform Colonies/l00mls ORGANIC CHEMISTRY Parameter _EDB __ PCB's __ Petroleum __ Endrin __ Lindane Results irig/1 Parameter __ Gross Alpha __ Gross Beta Parameter Results mg/ 1 __ Methoxychlor __ . Toxaphene _2,4-D __ 2,4,5-TP (silvex) R::\~JOCHFl US:FRY Results PCi/ 1 Received __________________ Date Reported __________________ _ ~are Extracted __________________ Date Analyzed "'•ported By Lab Number __ _,_.,.·-'-'-'~·-'5,""J.:..,_;'-f------------ l HS 3191 (R,vis,d 71B5) olid and Hazardous Wasre {Review 7187) IN. C. De~artment of Human Resources Di\'ision of Health Services SAMPLE ANALYSES REQUEST • Type of Sample: Environmental Concentrate ~ Groundwater (1) __ Solid (5) I --Surface Water (2) __ Liquid (6) Comments ::D, ~ Y\\ '':J v:oo.. ¼ \;._,~ \\ 6 Clrffi ~\ e __ Soil (3) __ Sludge (7) I --Other (4) __ Other (8) Ui~R8~ife @ttf!f,ffSTR:Y I Extracta bles Total I I I I I I I Parameter Results mg/ 1 __ Arsenic __ Barium __ Cadmium __ Chromium __ Lead -~~:~~;'. ... --. · Silver . -- Parameter Results mg/ 1 / '" -,. ·~ ~cid:B/N E;;;. ox ,,: I c'.': -- -- '.hHGROBIOLOO7t Parameter __ (MF) Coliform Colonies/lOOmls (MPN) Coliform Colonies/ IO0mls Parameter Results mg/1 __ Arsenic __ Barium __ Cadmium L<·r:::11:: ~·,. __ Chloride . C, •·' .•. :_; "· __ Chromium J,f \' /-·. fl~ •. __ Copper __ fluoride ,' t3 __ Iron '1--:.. ~~o __ Lead \~ __ Manganese '-"»/), __ Mercury ,._ X'-~~ t,v_.:. ~-\ 'i-. ·'> \ .. -__ Nitrate i ., __ Selenium ., .. .="'~-- ORGANIC CHEMISTRY Parameter _EDB __ PCB's __ Petroleum __ Endrin __ Lindane Results mg/1 Parameter __ Gross Alpha __ Gross Beta Parameter Results mg/1 __ Silver __ Sulfates __ Zinc _Ph __ Conductiviry . IDS ~. \ TOC -- -- -- -- -- -- Parameter Results mg/ 1 __ Methoxychlor __ . Toxaphene _2,4-D __ 2,4,5-TP (silvcx) -- RlaDlQCWFl CS'.R\ Y Results PCi/ I Received -------~----------Date Reported---~---------------VI,' lt"te Extracted 1-5/7k£r? ·6M Date Analyzed ------------------ 1\eported By _________________ Lab Number __ __,,/,"';.,_C::::c.\_,.1.,:J""( ... ,,../.Z'----------- .HS 3191 (Reviscd 7185) ll°liJ and Hazardous Waste {R~view 7187) I I I • BASE/NEUTRAL AND ACID EXTRACT ABLES COMPOONO N-ni trosodimethvlami ne lbi s (2-ch loroethvl )ether 2-ch l orooheno l oheno l .l.3-dichlorobenzene 1.4-dichlorobenzene 1.2-dichlorobenzene bis(2-chloroisnnrnnvllether hexachloroethane N-nitroso-di-n--nrnnvlamine nitrobenzene i<:IY"lhorone 2-nit~henol 2.4-dimethvloheno l lbis(2-chloroethoxvlmethane 2.4-dichloroohenol 1.2 4-trichlorobenzene hthalene STATE LABORATORY OF PUBLIC HEALTH DIVISION OF HEALTH SERVICES, N.C. DEPARTMENT OF HUMAN RESOURCES P.O. BOX 28047 -306 N: WILHINGTON, ST., RALEIGH, N.C. 27611 ORGANIC CHEMICAL ANALYSIS LAS NO (, • .--,}2/7 / / /' FIELD# } ) C·:l.., / / / / / TYPE ( i) (/ ) (/ ) /( ) UNITS ,,;'o/ l '.uo/kQ ,uo/1 uo/kq />;n/l un/kQ /.,n/ l uo/kQ ID ~,......-/.,., I ,, / / <✓/) _,,,-; l un/kQ hexachlorobutadiene ... -:-r:-1-\/r- 4-ch l oro.;n-creso l h h lo;-ocvc]nn,,ntadiene I ,,6-trichloroohenol .• I -chloronaohthalene acenaphthvlene ... imethvl ohthalate 6-di nitrotoluene acenanhthene ' 4-dinit=henol 'i V I .4-dinitrotoluene I,;) -n i t rooheno l -S l fluorene /d -ch lor,-,,henvl ohenvl ether /u iethyl phthalate /U 4.6-dinitro-o-cresol ½-Z' IJiphenvlamine ',[.' zobenzene Jo -brorophenvlohenvlether /o' hexachlorobenzene ;, fntachlo=henol .5?' enanthrene /u anthracene /,:J ,)' libutvl ohthalate /! /-! /c, L( I uoranthene /o //1 ., I '! -· · rn1JJ_ I /) ---F;.:vf~\t 1 ,.,1 L>.01·r (.::___ ( ,(,_'>/f \ Actual value is known to be less than value given. Actual value is known to be greater than value given. /</;--' P~c, ·~ :~ ' "' ,:!?., i '- "¼ x11a, . .. Estim.lted value. l~--· u -Material was analyzed for but not detected. The nuroer is the Minirrun Detection Limit. EA -Not analyzed. I -Tentative identification. _I -On NROC List of Priority Pollutants. Ill· C. V-tv,i,,,/,-ton 06 He.a.Uh Svw-tc.e.J.> 1f1S 3068-0 (4/86 LaboJta,toJty) -~ '""-.... ,(?_,;-, cc 4. ~ol ::. -;:;:; -s; ·, . __ t..-:, 'J .;_~--,,..~.,, hr1,)I\.. '. . ,/ ( /) ,.nf l un/ko lie BASE/NEUTRAL ANO ACID EXTRACTABLES COIIPOJNO rene nzidine butvl benzvl nhthalate 'nzfalanthracene rvsene . 3-dichlorobenzidine It!' 12--ethvl hexvl lnhtha late -n-octvl nhthalate nzolblfluoranthene benzo(k'fluoranthene ltnzo (a' nurene deno(l 2 3-cd---=rene dibenzola hlanthracene benzo,;:-h il00rvlene ani 11 ne benzoic acid benzvl alcohol ~loroaniline nzofuran thvlnanhthalene 2-rrethvlnhenol 4-rrethvlnhenol STATE LABORATORY Of PUBLIC HEALTH DIVISION OF HEALTH SERVICES, N.C. DEPARTMENT OF HUMAN RESOURCES P.O. BOX 28047 -306 N. WILMINGTON, ST., RALEIGH, N.C. 27611 ORGANIC CHEMICAL ANALYSIS LAB NO l;,t' _J_2[ .. -::' , . FIELD# -:; _)t.·2. ,. / / / / TYPE (_f) {/. l ,(/ ) (,,/) UNITS ./.n/] ,C,n/ka .""/1 ,on/kn ,A•0 / l ·•0 /ka uni l .. n/ka I 1-.., , ,, \..:-,~, (;; )) /) I., m; V /0 IJ /(,,>/,!._ ;.-' ' , su ,' 'fZ/ ,-z; I? l (' J ~I ' '>7 c,, ;,o S7 /) /, /1 /.• I ~,: , (/,) un'; l un/ka nitroani line 9 ---:-_-__ - nitroani line Y7} 4-nitroani 1 ine '77' 4 5-trichlo-henol ? .,1 \ (!7j}l, 111/'.I Actual value is known to be less than value given. Actual value is known to be greater than value given. , ,.&,C,"- If\,' ![g ,o , .. <".t'~ '\'-Z. ,.,_,,..,. I\_ -- ·::.\ ,--(';." ~J r,.; 1]1"-,1 le_ Estimated value. U -Material was analyzed for but not detected. The nunber is the Minil!Ull Detection Limit. INA -Not analyzed. 1/ -Tentative identification. £1 -On NROC List of Priority Pollutants. ~ ft~. C. V-i.v-u-i.on o 6 Hea.Uh SVI.v-<.c.e/2 r\"{HS 3068-0 14/86 LaboJta.to~y) ✓>, v,.~1.\ -'c<> \ h ~~,., z,' ~-"i ~i . ,'t-'rJ 11•,,J'_..;.>- / , ( /'> .. n/1 .. n/ka ' '