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HomeMy WebLinkAboutNCG100091_MONITORING INFO_20160108STORMWATER DIVISION CODING SHEET NCG PERMITS PERMIT N0. IV �, • � 00 6 DOC TYPE ❑HISTORICAL FILE MONITORING REPORTS DOC DATE ❑ YYYYMMDD Mill Atlantic Engineering & Environmental Solutions December 28�-201-5-::' REECOVED JAN 0 8.2016 Central Files Division of Water Resources CENTRAL FILE S DWR SECTION 1617 Mail Service Center Raleigh, North Carolina 27699-1617 Subject: STORMWATER NON -DISCHARGE NOTIFICATION MCLAMB'S AUTO SALVAGE, INC. 315 PELT DRIVE FAYETTEVILLE, CUMBERLAND COUNTY, NORTH CAROLINA PERMIT NCGl00091 MID -ATLANTIC JOB NO. OOOR2165.00 To Whom It May Concern: 409 Rogers View Court Raleigh, NC 27610 office 919.250.9918 facsimile 919.250.9950 MAAONLINE.COM Attached please find the Stormwater Discharge Monitoring Report (DMR) and analytical report for the sampling conducted at the above -referenced site. Stormwater samples were collected from Outfall 001 on November 18, 2015 and analyzed for total suspended solids (TSS), total recoverable lead, oil and grease and ethylene glycol. As indicated on the attached DMR, all parameters were reported below or within their respective benchmark range. If you have any questions or need additional information, please contact me at 919-250-9918. Sincerely, MID -ATLANTIC ASSOCIATES, INC. Ron Davis Stormwater Services Manager Attachment: Stormwater Discharge Outfall Monitoring Report Laboratory Analytical Report EXPERIENCED CUSTOMER FOCUSED INNOVATIVE /f��r;ii r • r r I!� December 02, 2015 Chuck Hoffman Mid -Atlantic Associates, Inc 409 Rogers View Court Raleigh, NC 27610 RE: Project: MCLAMB'S AUTO SALVAGE Pace Project No.: 92277108 Dear Chuck Hoffman: Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (7N)B75.9092 Enclosed are the analytical results for sample(s) received by the laboratory on November 20, 2015. The results relate only to the samples included in this report. Results reported herein conform to the most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. If you have any questions concerning this report, please feel free to contact me. Nicole Gasiorowski nicole.gasiorowski@pacelabs.com Project Manager Enclosures cc: Ron Davis, Mid Atlantic Associatees, Inc. REPORT -OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 1 of 12 Pace Analytical Services, Inc. ' f•�}.�j M 9800 KinceyAve. Sulte loll 5 Huntersville, NC 28078 (704)875-9092 CERTIFICATIONS Project: MCLAMB'SAUTO SALVAGE Pace Project No.: 92277108 Indiana Certification IDS 7726 Moller Road, Indianapolis, IN 46268 Ohio VAP Certification #: CL-0065 Illinois Certification M 200074 Oklahoma Certification #: 2014-148 Indiana Certification #: C-49-06 Texas Certification #: T104704355-15-9 Kansas Certification #:E-10177 West Virginia Certification #: 330 Kentucky UST Certification #: 0042 Wisconsin Certification #: 999788130 Kentucky WW Certification #:98019 USDA Soil Permit #: P330-10-00128 Louisiana Certification #: 04076 Charlotte Certification IDS 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 Florida/NELAP Certification #: E87627 North Carolina Drinking Water Certification #: 37706 Kentucky UST Certification #: 84 North Carolina Field Services Certification #: 5342 West Virginia Certification #: 357 North Carolina Wastewater Certification #: 12 VirginiaNELAP Certification #: 460221 South Carolina Certification #: 99006001 Asheville Certification IDS 2225 Riverside Drive, Asheville, NC 28804 North Carolina Wastewater Certification #: 40 Florida/NELAP Certification #: E87648 South Carolina Certification #: 99030001 Massachusetts Certification #: M-NC030 West Virginia Certification #: 356 North Carolina Drinking Water Certification #: 37712 VirginiaNELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc- Page 2 of 12 Pace Analytical Services, Inc. ,- . •� 9800 KinceyAve. Suite 100 {; Huntersville, NC 28078 (704)875-9092 SAMPLE ANALYTE COUNT Project: MCLAMB'S AUTO SALVAGE Pace Project No.: 92277108 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92277108001 OUTFALL NO.1 EPA 1664B JMS 1 PASI-C EPA 8015 Alcohol -Glycol BJW 1 PASI-i EPA 6010 CDF 1 PASI-A SM 2540D SAM 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 3 of 12 ANALYTICAL RESULTS Project: MCLAMB'S AUTO SALVAGE Pace Project No.: 92277108 Pace Analytical Services, Inc. 9800 Kircey Ave. Suite 100, Huntersville, NC 28078 (704)875-9092 Sample: OUTFALL NO. 1 Parameters Lab ID: 92277108001 Collected: 11/19/15 00:00 Received: 11/20/15 11:00 Matrix: Water Results Units Report Limit OF Prepared Analyzed CAS No. Quaff 1664 SGT-HEM, TPH Analytical Method: EPA 1664B Total Petroleum Hydrocarbons ND mg1L 5.0 1 11/30/15 05:31 8015M Glycols In water Analytical Method: EPA 8015 Alcohol -Glycol Ethylene glycol NO mg/L 5.0 1 11/25/15 11:04 107-21.1 6010 MET ICP Analytical Method: EPA6010 Preparation Method: EPA 3010 Lead ND ug/L 5.0 1 11/25/15 22:00 12/02/15 05:23 7439-92-1 26400 Total Suspended Solids Analytical Method: SM 25400 Total Suspended Solids 59.7 mg/L 6.7 1 11/22/15 16:06 D6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/02/2015 05:13 PM without the written consent of Pace Analytical Services, Inc.. Page 4 of 12 yy �w''-stI �► s Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: MCLAMB'SAUTO SALVAGE Pace Project No.: 92277108 QC Batch: GCSV/23357 QC Batch Method: EPA 1664E Associated Lab Samples: 92277108001 METHOD BLANK: 1616056 Associated Lab Samples: 92277108001 Parameter Units Total Petroleum Hydrocarbons mg/L QUALITY CONTROL DATA Analysis Method: Analysis Description: Matrix: Water EPA 1664E 1664 SGT-HEM, TPH Blank Reporting Result Limit Analyzed Qualifiers ND 5.0 11/30/15 05:16 LABORATORY CONTROL SAMPLE: 1616057 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Petroleum Hydrocarbons mg/L 20 14.9 74 64-132 MATRIX SPIKE SAMPLE: 1616058 92276465001 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Total Petroleum Hydrocarbons mg/L ND 20 13.7 68 64-132 Results presented on this page are In the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. Date: 12/02/2015 05:13 PM without the written consent of Pace Analytical Services, Inc.. Page 5 of 12 �r JI v,;f 3• a Y� rat Pace Analytical Services, Inc. 9800 Kincey Ave, Suite 100 Huntersville, NC 28078 (704)875.9092 QUALITY CONTROL DATA Project: MCLAMB'S AUTO SALVAGE Pace Project No.: 92277108 QC Batch: GCSV/17645 Analysis Method: EPA 8015 Alcohol -Glycol QC Batch Method: EPA 8015 Alcohol -Glycol Analysis Description: EPA 8015 Modified Associated Lab Samples: 92277108001 METHOD BLANK: 1432937 Matrix: Water Associated Lab Samples: Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Ethylene glycol mg/L ND 5.0 111251115 10:39 LABORATORY CONTROL SAMPLE: 1432938 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Ethylene glycol mg/L 25 21.7 87 79-129 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1433087 1433088 MS MSD 92277108001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qua[ Ethylene glycol mg/L ND 25 25 20.4 23.6 82 94 67-133 14 Results presented on this page are In the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/02/2015 05:13 PM without the written consent of Pace Analytical Services, Inc.. Page 6of12 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: MCLAMB'S AUTO SALVAGE Pace Project No.: 92277108 QC Batch: MPRP/20124 Analysis Method: EPA 6010 QC Batch Method: EPA 3010 Analysis Description: 6010 MET Associated Lab Samples: 92277108001 METHOD BLANK: 1615899 Matrix: Water Associated Lab Samples: 92277108001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Lead ug/L NO 5.0 12/02/15 04:47 LABORATORY CONTROL SAMPLE: 1615900 Spike LCS LCS % Rec Parameter units Cone, Result % Rec Limits Qualifiers Lead ug/L 500 466 93 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1615901 1615902 MS MSD 92277042001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cone. Cone, Result Result % Rec % Rec Limits RPD Qual Lead ug/L 6.0 500 500 502 470 99 93 75-125 7 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 1210212015 05:13 PM without the written consent of Pace Analytical Services, Inc.. Page 7 of 12 Pace Analytical Services, Inc. 9800 KinceyAve. Suite 1o0 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: MCLAMB'S AUTO SALVAGE Pace Project No.: 92277108 QC Batch: WET141555 Analysis Method: SM 2540D QC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids Associated Lab Samples: 92277108001 METHOD BLANK: 1612801 Matrix: Water Associated Lab Samples: 92277108001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mg1L ND 2.5 11/22/15 16:01 LABORATORY CONTROL SAMPLE: 1612802 Spike LCS LCS % Roe Parameter Units Cone. Result % Rae Limits Qualifiers Total Suspended Solids .� mg/L 250 248 99 90-110 SAMPLE DUPLICATE: 1612803 92277065001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mglL 8.8 T6 15 D6 SAMPLE DUPLICATE: 1612804 92277108001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mglL 59.7 68,3 13 D6 Results presented on this page are In the units indicated by the "Units" column except where an alternate unit Is presented to the right of the resull. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. Dale: 1210212015 05:13 PM without the written Consent of Pace Analytical Services, Inc.. Page 8 of 12 Pace Analytical Servlcee, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)675-9092 QUALIFIERS Project: MCLAMB'S AUTO SALVAGE Pace Project No.: 92277108 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270, The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI -The NELAC Institute, LABORATORIES PAST -A Pace Analytical Services -Asheville PASI-C Pace Analytical Services - Charlotte PASI-I Pace Analytical Services - Indianapolis ANALYTE QUALIFIERS D6 The relative percent difference (RPD) between the sample and sample duplicate exceeded laboratory control limits. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/02/2015 05:13 PM without the written consent of Pace Analytical Services, Inc.. Page 9 of 12 x ��Jf rCil� �i �i QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: MCLAMB'SAUTO SALVAGE Pace Project No.: 92277108 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 10d Huntersville, NC 28078 (704)875.9092 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92277108001 OUTFALL NO. 1 EPA 1664E GCSV123357 92277108001 OUTFALL NO. 1 EPA 8015 Alcohol -Glycol GCSVI17645 92277108001 OUTFALL NO. 1 EPA 3010 MPRP120124 EPA 6010 ICP/18153 92277108001 OUTFALL NO. 1 SM 2540D WETl41555 Date, 12/02/2015 05:13 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 10 of 12 not ,O-Ae AM" ~Wlz- = = E"1 NN®� I � mowaw _1momm®i MWEN WO Mid Atlantic Engineering & Environmental Solutions December 21, 102 5) ElV D NCDEQIDWR DEC $ 0 2015 Attention: Central Files CENTRAL. Pike, 1617 Mail Service Center DWR SECTIoM Raleigh, North Carolina 27699-1617 Subject: BOB'S AUTO SALVAGE 2780 RICHLANDS HIGHWAY JACKSONVILLE, ONSLOW COUNTY, NORTH CAROLINA PERMIT NCGl00091 MID -ATLANTIC JOB NO. 00OR2436.00 To Whom It May Concern: 409 Rogers View Court Raleigh. NC 27610 office 919.250.9918 facsimile 919.250.9950 MAAONLIN E.COM Attached please find the Stormwater Discharge Monitoring Report (DMR) and analytical report for the sampling conducted at the above -referenced site. Stormwater samples were collected from Outfall 001 on October 28, 2015 and analyzed for total suspended solids (TSS), total recoverable lead, oil and grease and ethylene glycol. As indicated on the attached DMR, all parameters were reported below their respective benchmark values. If you have any questions or need additional information, please contact me at 919-250-9918. Sincerely, MID -ATLANTIC ASSOCIATES, INC. r Ron Davis Stormwater Services Manager Attachment: Stormwater Discharge Monitoring Report Laboratory Analytical Report EXPERIENCED CUSTOMER FOCUSED INNOVATIVE areAnal rcal* L www.pawlab&=n November 10, 2015 Chuck Hoffman Mid -Atlantic Associates, Inc 409 Rogers View Court Raleigh, NC 27610 RE: Project: BOB'S AUTO SALVAGE Pace Project No.: 92273900 Dear Chuck Hoffman: Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875.9092 Enclosed are the analytical results for sample(s) received by the laboratory on October 29, 2015. The results relate only to the samples included in this report. Results reported herein conform to the most current TN standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. If you have any questions concerning this report, please feel free to contact me. Sincerely, Nicole Gasiorowski nicole.gasiorowski@pacelabs.com Project Manager Enclosures cc: Ron Davis, Mid Atlantic Associatees, Inc. REPORT OF LABORATORY ANALYSIS This report shall not he reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 1 of 12 Pace Analytical Services, Inc. �aqeAnalyficale 9800 Kincey Ave. Suite 100 ' Huntersville, NC 28078 www.pewsbs.w n (704)875-9092 CERTIFICATIONS Project: BOB'S AUTO SALVAGE Pace Project No.: 92273900 Indiana Certification IDs 7726 Moller Road, Indianapolis, IN 46268 Ohio VAP Certification M CL-0065 Illinois Certification #: 200074 Oklahoma Certification M 2014-148 Indiana Certification #: C-49-06 Texas Certification M T104704355-15-9 Kansas Certification ME-10177 West Virginia Certification M 330 Kentucky UST Certification M 0042 Wisconsin Certification M 999788130 Kentucky WW Certification #:98019 USDA Soil Permit #: P330-10-00128 Louisiana Certification #: 04076 Charlotte Certification IDs 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 Florida/NELAP Certification #: E87627 North Carolina Drinking Water Certification M 37706 Kentucky UST Certification M 64 North Carolina Field Services Certification #: 5342 West Virginia Certification M 357 North Carolina Wastewater Certification #: 12 VirginiafVELAP Certification #: 460221 South Carolina Certification M 99006001 Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 North Carolina Wastewater Certification M 40 Florida/NELAP Certification M E87648 South Carolina Certification M 99030001 Massachusetts Certification #: M-NC030 West Virginia Certification #: 356 North Carolina Drinking Water Certification #: 37712 Virginia/VELAP Certification M 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Anatytical Services, Inc.. Page 2 of 12 ,avnalytkale www.paCOWS aom SAMPLE ANALYTE COUNT Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: BOB'S AUTO SALVAGE Pace Project No.: 92273900 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92273900001 OUTFALL NO. 1 EPA 1664E JMS 1 PASI-C EPA 8015 Alcohol -Glycol BJW 1 PASI-I EPA 6010 CDF 1 PASI-A , SM 2540D SAM 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of PaceAnalytical Services, Inc.. Page 3 of 12 aceAnalytical www.pacdm.com ANALYTICAL RESULTS Project: BOB'S AUTO SALVAGE Pace Project No.: 92273900 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: OUTFALL NO. 1 Parameters Lab ID: 92273900001 Collected: 10/28/15 16:30 Received: 10/29/15 11:15 Matrix: Water Results Units Report Limit DF Prepared Analyzed CAS No. Qua] 1664 SGT-HEM, TPH Analytical Method: EPA 1664B Total Petroleum Hydrocarbons ND mg1L 5.0 1 11/05/15 08:04 8015M Glycols in water Analytical Method: EPA 8015Alcohol-Glycol Ethylene glycol ND mg1L 5.0 1 111D4115 12:49 107-21-1 6010 MET ICP Analytical Method: EPA6010 Preparation Method: EPA 3010 Lead ND ug1L 5.0 1 11/07/15 20:00 11/09/15 14:16 7439-92-1 2640D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids 3.8 mg/L 2.5 1 11/01/15 15:09 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11 /10/2015 04:17 PM without the written consent of Pace Analytical Services, Inc.. Page 4 of 12 aceAnalytical • t www.pecehiftcom Project: BOB'S AUTO SALVAGE Pace Project No.: 92273900 QC Balch: GCSV123115 QC Batch Method: EPA 1664B Associated Lab Samples: 92273900001 METHOD BLANK: 1599310 Associated Lab Samples: 92273900001 Parameter Units Total Petroleum Hydrocarbons mglL QUALITY CONTROL DATA Analysis Method: EPA 1664B Analysis Description: 1664 SGT HEM, TPH Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 5.0 11/05/15 07:44 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 1599311 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Petroleum Hydrocarbons mglL 20 14.3 72 64-132 MATRIX SPIKE SAMPLE: 1599312 92273900001 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Total Petroleum Hydrocarbons mglL ND 20 14.3 72 64-132 Results presented on this page era in the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11 /10/2015 04:17 PM without the written consent of Pace Analytical Services, Inc.. Page 5 of 12 acgeAnalytical. www.psceilam.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28076 (704)875-9092 QUALITY CONTROL DATA Project: BOB'S AUTO SALVAGE Pace Project No.: 92273900 QC Batch: GCSV117351 Analysis Method: EPA 8015 Alcohol -Glycol QC Batch Method: EPA 8015 Alcohol -Glycol Analysis Description: EPA 8015 Modified Associated Lab Samples: 92273900001 METHOD BLANK: 1415880 Associated Lab Samples: Parameter Units Ethylene glycol mg/L LABORATORY CONTROL SAMPLE: 1415881 Parameter Units Ethylene glycol mg/L Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 5.0 11104/1512:30 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 25 23A 93 79-129 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1415992 1415993 MS MSD 92273900001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Ethylene glycol mgtL ND 25 25 29.7 30.9 119 123 67-133 4 Results presented on this page are In the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11/10/2015 04:17 PM without the written consent of Pace Analytical Services, Inc.. Page 6 of 12 areAnalyfical" r sww.pttoefa6a.Com QUALITY CONTROL DATA Project: BOB'S AUTO SALVAGE Pace Project No.: 92273900 Pace Analytical Services, Inc. 9800 Kinsey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QC Batch: MPRP/19985 Analysis Method: EPA 6010 QC Batch Method: EPA 3010 Analysis Description: 6010 MET Associated Lab Samples: 92273900001 METHOD BLANK: 1601584 Matrix: Water Associated Lab Samples: 92273900001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Lead uglL ND 5.0 11/09/1513:52 LABORATORY CONTROL SAMPLE: 1601585 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Lead uglL 500 471 94 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1601586 1601587 MS MSD 92273821001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Lead uglL 8.2 500 500 466 470 92 92 75-125 1 Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11 /1012015 04:17 PM without the written consent of Pace Analytical Services, Inc.. Page 7 of 12 acLeAnalytical� -: www.pacelahs oom QUALITY CONTROL DATA Project: BOB'S AUTO SALVAGE Pace Project No.: 92273900 Pace Analytical Services, Inc. 9800 KlnceyAve. Sulte lo0 Hurltersville, NC 28078 (704)875-9092 QC Batch: WET/41157 Analysis Method: SM 2540D QC Batch Method: SM 2540D Analysis Description: 25400 Total Suspended Solids Associated Lab Samples: 92273900001 METHOD BLANK: 1596407 Matrix: Water Associated Lab Samples: 92273900001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mg/L ND 2.5 11/01/15 15:06 LABORATORY CONTROL SAMPLE: 1596408 Spike LCS LCS % Rec Parameter Units Cone. Result % Rec Limits Qualifiers Total Suspended Solids mg/L 250 240 96 90-110 SAMPLE DUPLICATE: 1596409 92274207001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 173 179 3 SAMPLE DUPLICATE: 1596410 92273916001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mglL ND NO Results presented on this page are in the units Indicated by the "Units" calumn except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Dale: 11/10/2015 04:17 PM without the written consent of Pace Analytical Services, Inc.. Page 8 of 12 aCeAnalytrcals www.pacelabs.com QUALIFIERS Project: BOB'S AUTO SALVAGE Pace Project No.: 92273900 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. POL - Practical Ouantitation Limit. RL - Reporting Limit. Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. i Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis ofAcrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI -The NELAC Institute. LABORATORIES PASI-A Pace Analytical Services -Asheville PASI-C Pace Analytical Services - Charlotte PASI-I Pace Analytical Services - Indianapolis This report shall not be reproduced, except in full, Date: 11/10/2016 04:17 PM without the written consent of Pace Analytical Services, Inc.. Page 9 of 12 y , ar<,Analytical' wm pacsfabs.com QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: BOB'S AUTO SALVAGE Pace Project No.: 92273900 Lab ID Sample ID QC Batch Method 92273900001 OUTFALL NO. 1 EPA 1664E 92273900001 OUTFALL NO.1 EPA 8016 Alcohol -Glycol 92273900001 OUTFALL NO.1 EPA 3010 92273900001 OUTFALL NO. 1 SM 2540D Date: 11/10/2015 04:17 PM Pace Analytical Services, Inc. 9801) Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Analytical QC Batch Analytical Method Batch GCSV123115 GCSV117361 MPRP119985 EPA 6010 WETl41157 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. ICP118020 Page 10 of 12 4Paceftilytical' Condition Upon Recei Document Number: F-CHR-CS-003-rev.16 1 Issuing Auth Pace Huntersville Q Client Name. ,' y r " - A 4 `f n ' Page 2 of 2 is for Internal Use Only Courier: ❑ Fed E)❑ UP USP❑ Clier❑ CommerclQ Pace Other Custody Seal on Cooler/Box Present: ❑ yes Q o Seats Intact: y ❑ no ea t ❑ es ProJ,tiName: Packing Material: ❑Bubble Wrap ❑ Bubble Bags ❑ None ❑ Other Thermometer Used: IR Gunr402 Type of Ice: j0�! v Blue None amples on ice, cooling process has begun Temo Correction Factor To Correction Corrected Cooler Temp.:�. 3 •C Temp should be above freezing to 64C Biological Tissue is Frozen: Yes No Nl Comments: Date and Initials of person examining J-, , contents:! (? �; ,2 l _..S Chain of Custody Present: 13 es EjNo ❑NIA 1. Chain of Custody Filled Out: es ❑No PNIA 2. Chain of Custody Relin uished: ❑Yea o ❑NIA 3. Sampler Name & Signature on COC: E 6' No ❑N!A 4• Samples Arrived within Hold Time: Glre'90Na 2141A 5. Short Hold Time Analysis L<72hr : ❑Yes 1211o"EINIA B. Rush Turn Around Time Requested: ❑Yes o ❑NIA 7, Sufficient volume: 2 Yes o ❑N!A a. Correct Containers Used: -Pace Containers Used: Yes ❑No ©e�❑No ❑NIA ❑N!A 9. Containers Intact: s ❑No ❑NIA 10. Filtered volume received for Dissolved tests ❑Yes ❑No Da 11, Sample Labels match COC: -Includes dateltime/ID/Anal sis Matrix: Ofes ❑No W A11 ❑NIA 12. All containers needing preservation have been checked. All containers needing preservation are found to be In compliance with EPA recommendation. exceptions; VOA, ooliform, TOC, 0&G, WURO (wateO es ❑N e❑4 s ©No :a's 0 4IYes ONo ❑N!A ❑N!A 13. Samples checked for dechlorination: Dyes ❑No ❑N A 14, Heads ace In VOA Vials >Bmm : Dyes ON* (2IA 10, Trip Blank Present: Trip Blank Custody Seals Present Pace Trip Blank Lot # If purchased): ❑Yea ❑No Dyes ONO ❑N!A NIA Client Notification/ Resolution: Field Data Required? Y 1 N Person Contacted: Date/Time: Comments/ Resolution: SCURF Review: UW Date: I 14-Zq-IS SRF Review: t:� Date: Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office ( Le out of hold, incorrect preservative, out of temp, Incorrect containers) WOp:92273900 I I Ial173 I Page 11 of 12 — aceAnalytical J w,.w Wcruos mrtr f Section A RequbW CbeN Wforrymj=L CHAIN -OF -CUSTODY 1 Analytical Request Document The Ct airsol-Custody is a LEGAL DOCUMENT. An ►eievant fields must be tamptetea acaaat*. Section B Section C RzoL*ed Proiea 1rAwrobarr I- O N pa: of m pa m m C-Para Mid-AtiantiC ASSOCeales. inc. Report To: Chuck Hoffman (choffman@maaonline.com) Chuck Hoffman 409 Rogers View Court Covr To- Joanna Crow (icro maaonhnexorn) Canary Name: hOd tic A soctabe5, inc. REGULATORY AGENCY Raleigh, NC 27610 - 409 Rogers View Court. Raleigh, NC r NPDES r- GROUNDWATER r• DRINKING WATER r UST f RCRA r' OTHER Errol To: choyfman@nUIa0nfine.00M Pmdvm Order No.: R2436.00 -- Phone. 919-250-9918 F— 919-250-9950 Prole+ N—! BOWS Aldo Salvage F. Nicole Gasiorowski Sup Locatioln STATE: NC Recpi nee DaWTAT: sword Project Numb--R2436.00 P7ame a: Requested Analysis Filtered (YIN) SeWen D VaN Ma&b Codes 8 z RoWdand Cberd hdaeMMM mix e 2 COLLECTED Preservatives s N Y N Y dRWrKMWATER OW u z m WATER WVi WASTE WATER w u V CASE Cerp'own L] v Z_ PRODUCT p fiDefSGJD SL ' i m tg START m SAMPLE ID WP `��' W (A-Z, 0A t,-) AR Sample IDS MUST 9E UNIQUE Ta U CL W Z m m m o x J J ka m h o �. A 2 m Im 1(51 (a _ lix DATE TIME DATE TIME aa) a � rn � � = z z 2 O y to of � m Pace Project NoJ Lab LD. 1 Outfall No. 1 WT 7 4 1 2 1 1 x x x x Rainfall (inches): 2 F pH: 3 - .'a /0 4 S 6 7 e 9 10 11 12 ADVIInor AL COMMENT" mmmOtl7^. w BY r Affn ATION MATE TIME ACCEPTrm eY r AFFILIATION DATE TM SANFU C01rDMN4 • SAMPLER NAME AND Sr -,NATURE U o 1 Y PRINT None of SAMPLER: + Cot u t) E y SIGNATURE of SAMPLER: DATE signed - + MblldtNYYI, O -Irnpeetap Now: RY sigrng ads Tara you we acceFaar9 Pace's NET 30 der payewrs mmo are apee'a n to Tam amen of 1.5% per more for dry imoi= rat paid wilk 30 days. + F-ALL-"20rev.08. 12-Oct-2007 STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT CERTIFICATE OF COVERAGE NO. NCG100091 SAMPLES COLLECTED DURING CALENDAR YEAR: 2015 (This monitoring report shall be received by the Division no later than 30 days from the date the facility receives the sampling results from the laboratory.) FACILITY NAME McLamb's Auto Salvage, Inc., Fayetteville. NC _ _ COUNTY Cumberland PERSON COLLECTING SAMPLE(S) W.D. McLamb PHONE NO. 919 8-5255 CERTIFIED LABORATORY(S) PaceAnalytical „ Lab #12 Lab # PLEASE REMEMBER TO SIGN ON THE REVERSE Part A: Stormwater Benchmarks and Monitoring Results For sampling periods with no discharge, you must submit this discharge monitoring form noting "No Flow" or "No Discharge" within 30 days of the end of that period to comply with permit reporting requirements. Outfall No. Date Sample Collected, 'mo/dd/year -Total Rainfall, inches 00400 - : - - 00530 ; ... .: _ :. - - - = `.'.77023 .: v • 01051- ,78141 pH, Standard Units Total Suspended , Solids (TSS), mg/L Non -polar O&G/TPH (Method 1664 SGT-HEM), mg/L Ethylene Glycol; mg/L .. Lead, Total Recoverable_ , mg/L Total Toxic Organics3, mg/L Benchmark - - 5.0 - 9.01 100/502 i5 8,000 (Tiers 2 and 3) 0.03 1.0 Outfall 001 11/19/2015 1.2 7.5 59.7 <5.0 <5.0 < 0.0050 NA Note: if you report a sampled value in excess of the benchmark value, or outside the benchmark range for pH, you must implement Tier 1 or Tier 2 responses in the General Permit. 1See If pH values outside this range are recorded in sampled stormwater discharges, but ambient precipitation pH levels are lower, then the lower threshold of this benchmark range is the pH of the precipitation (within instrument accuracy)instead of 6 S.U. Readings from an on -site or local rain gauge (or local precipitation data) must be documented to demonstrate background concentrations were below the benchmark pH range of 6-9. 2See General Permit text to identify whether the more protective benchmark applies for especially sensitive receiving waters. 3For purposes of this permit the definition of Total Toxic Organics is that list as stated in Appendix D, Table II of Chapter 40 Code of Federal Regulations (CFR) Part 122. Form SW U-251, last revised October 25, 2012 Page 1 of 2 STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may request that DWQ waive monitoring of total toxic organics. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities allowed such a waiver, the discharger shall sign the following certification statement: Solvent Management Plan Certification Statement "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics MO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing all the provisions of the solvent management plan included in the stormwater Pollution Prevention Plan." ti) o" (I e- V%__ Name (Print name) Title (Print title) 4 �')b wt _) T_ Signature Date Mail Original and one copy to: Division of Water Quality Attn: Central Files 1617 MailServiceCenter Raleigh, North Carolina27699-1617 "1 certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. am aware that there are significant p nalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Permittee or Designee) (Date) Form SW U-251, last revised October 25, 2012 Page 2 of 2 STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT CERTIFICAT-2 OF COVERAGE NO. NCG100091 SAMPLES COLLECTED DURING CALENDAR YEAR: 2015 (This monitoring report shall be received by the Division no later than 30 days from the date the facility receives the sampling results from the laboratory.) FACILITY NAME Bob's Auto Salvaee, Jacksonville, NC COUNTY Onslow PERSON COLLECTING SAMPLE(S) RobbieYopp _ PHONE NO. (910) 346-3220 CERTIFIED LABORATORY(S) PaceAnalytical Lab #12 Lab # PLEASE REMEMBER TO SIGN ON THE REVERSE Part A: Stormwater Benchmarks and Monitoring Results For sompling periods with no discharge, you must submit this discharge monitoring form noting "No Flow" or "No Discharge" within 30 days of the end of that period to comply with permit reporting requirements. Outfall' No. Uafe:: Sample Collected, mo/dd/year Total Rainfall, inches 004b0 00530 - = - :.. ::;; 77623`"' ., 01051 . .:.., 78141 pH, Standard Units Total Suspended Solids (TSS), mg/L Non -polar O&G/TPH (Method 1664 SGT-HEM), mg/L Ethylene Glycol, mg/L Lead, Total Recoverable, mg/L Total Toxic Organics3, mg/L Benchmark - - 6.0 — 9.01 100/502 is SA00 (Trers 2 and 3) 0.03 1.0 Outfall001 10/28/15 0.5 3.8 <5.0 <5.0 <0.005 NA Note: If you report a sampled value in excess of the benchmark value, or outside the benchmark range for pH, you must implement Tier 1 or Tier 2 responses in the General Permit. 1See If pH values outside this range are recorded in sampled stormwater discharges, but ambient precipitation pH levels are lower, then the lower threshold of this benchmark range is the pH of the precipitation (within instrument accuracy)instead of 6 S.U. Readings from an on -site or local rain gauge (or local precipitation data) must be documented to demonstrate background concentrations were below the benchmark pH range of 6-9. 2See General Permit text to identify whether the more protective benchmark applies for especially sensitive receiving waters. 3For purposes of this permit the definition of Total Toxic Organics is that list as stated in Appendix D, Table II of Chapter 40 Code of Federal Regulations (CFR) Part 122. Form SWU-251, last revised October 25, 2012 Page 1 of 2 STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may request that DWQ waive monitoring of total toxic organics. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities allowed such a waiver, the discharger shall sign the following certification statement: Solvent Management Plan Certification Statement "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." (19j) �ta_L)ua Name (Print name) Title (Print title) S ature Date Mail Original and one copy to: Division of Water Quality Attn: Central Files 1617 MailServiceCenter Raleigh, North Carolina27699-1617 "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel property gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Date) Form SW U-251, lost revised October 25, 2012 Page 2of2 qicc'-/000 d Atlantic Engineering & Environmental Solutions May 22, 2015 NCDENR/DWQ Attention: Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 Subject: BOB'S AUTO SALVAGE 2780 RICHLANDS HIGHWAY JACKSONVILLE, ONSLOW COUNTY, NORTH CAROLINA PERMIT NCG100091 MID -ATLANTIC JOB NO.000R2436.00 To Whom It May Concern: •349 V10", ; rE t NKI I (r hrsirzn1r 9l`1.7.f�[;i, Attached please find the Stormwater Discharge Monitoring Report (DMR)1 and analytical report for the sampling conducted at the above -referenced site. Stormwater samples were collected from Outfali 001 on April 15, 2015 and analyzed for total suspended solids (TSS), total recoverable lead, oil and grease and ethylene glycol. As indicated on the attached DMR, all parameters were reported below their respective benchmark value. Please note that pH measurements will be collected in the field during the next semi- annual monitoring event (July -December 2015). If you have any questions or need additional information, please contact me at 919-250-9918. Sincerely, MID -ATLANTIC ASSOCIATES, INC. RECEIVED MAY 27 2015 DENR-tea Nb QUALlTI' Charles B. Hoffman, PG STPRIOWATER Project Geologist Attachment: Stormwater Discharge Monitoring Report Laboratory Analytical Report aceAnalytical' wwwpaceMbs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 April 22, 2015 Darin McClure Mid Atlantic Associates, Inc. RE: Project: BOBS AUTO SALVAGE R2436.00 Pace Project No.: 92245732 Dear Darin McClure: Enclosed are the analytical results for sample(s) received by the laboratory on April 16, 2015. The results relate only to the samples included in this report. Results reported herein conform to the most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. If you have any questions concerning this report, please feel free to contact me. Sincerely, Nicole Gasiorowski nicole.gasiorowski@pacelabs.com Project Manager Enclosures cc: Joanna Crow, Mid Atlantic Associates, Inc. Chuck Hoffman, Mid Atlantic Associates Beverly Oglesby, Mid Atlantic Associates, Inc. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 1 of 12 aceMalxical www.paceraba.cam Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersvilte, NC 28078 (704)875.9092 Project: BOBS AUTO SALVAGE R2436.00 Pace Project No.: 92245732 Indiana Certification IDs 7726 Moller Road, Indianapolis, IN 46268 Illinois Certification M 200074 Indiana Certification #: C-49-06 Kansas Certification ME-101771 E-10247 Kentucky UST Certification #: 0042 Kentucky WW Certification #:98019 Louisiana/NELAP Certification #: 04076 CERTIFICATIONS Ohio VAP Certification M CL-0065 Oklahoma Certification #: 2014-148 Pennsylvania Certification #: 68-05340 Texas Certification #: T104704355-15-8 West Virginia Certification #: 330 Wisconsin Certification #: 999788130 USDA Soil Permit #: P330-10-00128 Charlotte Certification IDs 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 FloridalNELAP Certification #: E87627 North Carolina Drinking Water Certification M 37706 Kentucky UST Certification M 84 North Carolina Field Services Certification #: 5342 West Virginia Certification M 357 North Carolina Wastewater Certification #: 12 VirginiaNELAP Certification M 460221 South Carolina Certification M 99006001 Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 North Carolina Wastewater Certification M 40 Florida/NELAP Certification M E87648 South Carolina Certification #: 99030001 Massachusetts Certification M M-NCO30 West Virginia Certification #: 356 ' North Carolina Drinking Water Certification #: 37712 VirginialVELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 2 of 12 ' aceAmlytrcals x+Ywpacatoftcom Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)975.9092 SAMPLE ANALYTE COUNT Project: BOBS AUTO SALVAGE R2436.00 Pace Project No.: 92245732 Lab ID Sample ID Method Analysts Analytes Reported Laboratory 92246732001 OUTFALL NOA EPA 16644B CLW 1 PASI-C EPA 8015 Alcohol -Glycol RID 1 PASI-I EPA6010 JMW 1 PASI-A SM 2540D JTJ 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 3 of 12 aceAnalytical wwwpeca186sc= Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: BOBS AUTO SALVAGE R2436.00 Pace Project No.: 92245732 Sample: OUTFALL NOA Lab ID: 92245732001 Collected: 04/15/15 16:00 Received: 04/16/15 10:45 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 1664 SGT-HEM, TPH Analytical Method: EPA 1664B Total Petroleum Hydrocarbons ND mg/L 5.0 1 04/22/15 15:51 8015M Glycols in water Analytical Method: EPA 8015 Alcohol -Glycol Ethylene glycol ND mg/L 5.0 1 04/20/15 14:48 107-21-1 6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010 Lead ND ug/L 5.0 1 04/17/1516A0 04120/1516:05 7439-92-1 2640D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids 8.0 mg/L 4.2 1 04/21/15 10:52 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. Date: 04/22/2015 05:27 PM without the written consent of Pace Analytical Services, Inc.. Page 4 of 12 ,aceAnalytrcal www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: BOBS AUTO SALVAGE R2436.00 Pace Project No.: 92245732 QC Batch: GCSV/21045 Analysis Method: EPA 1664B QC Batch Method: EPA 1664B Analysis Description: 1664 SGT-HEM, TPH Associated Lab Samples: 92245732001 METHOD BLANK: 1440883 Associated Lab Samples: 92245732001 Matrix: Water Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Petroleum Hydrocarbons mg1L ND 5.0 04/22/15 15:48 LABORATORY CONTROL SAMPLE & LCSD: 1440884 1440885 Spike LCS LCSD LCS LCSD % Rec Max Parameter Units Conc. Result Result % Rec % Rec Limits RPD RPD Qualifiers Total Petroleum Hydrocarbons mg1L 20 17.3 15.5 87 78 64-132 11 30 Results presented on this page are In the units Indicated by the "units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in lull. Date: 04/22/2015 05:27 PM without the written consent of Pace Analytical Services, Inc.. Page 5 of 12 .aceAnalyicals www.pacews.twm Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Hunlersville, NC 28078 (704)875.9092 QUALITY CONTROL DATA Project: BOBS AUTO SALVAGE R2436.00 Pace Project No.: 92245732 QC Batch: GCSV115059 Analysis Method: EPA 8015 Alcohol -Glycol QC Batch Method: EPA 8015 Alcohol -Glycol Analysis Description: EPA 8015 Modified Associated Lab Samples: 92245732001 METHOD BLANK: 1278841 Matrix: Water Associated Lab Samples: Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Ethylene glycol mg/L ND 5.0 04/2011611:58 LABORATORY CONTROL SAMPLE: 1278842 Spike LCS LCS % Rec Parameter Units Cone. Result % Rec Limits Qualifiers Ethylene glycol mg1L 25 20.1 80 79-129 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1279111 1279112 MS MSD 92245732001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual Ethylene glycol mg/L ND 25 25 21.8 24.4 87 98 67-133 11 Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/22/2015 05:27 PM without the written consent of Pace Analytical Services, Inc.. Page 6 of 12 aceApalytical. www.pacelabaCom Pace Analytical Services, Inc. 9800 Kinsey Ave. Suite 100 Huntersville, NC 28078 (704)875.9092 Project: BOBS AUTO SALVAGE R2436.00 Pace Project No.: 92245732 QC Batch, MPRP118302 QC Batch Method: EPA 3010 Associated Lab Samples: 92245732001 METHOD BLANK: 1437425 Associated Lab Samples: 92245732001 Parameter Units Lead ug1L LABORATORY CONTROL SAMPLE: 1437426 Parameter Units Lead ug1L QUALITY CONTROL DATA Analysis Method: EPA 6010 Analysis Description: 6010 MET Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 5.0 04/2011514:57 Spike LCS LCS % Rec Cone. Result % Rec Limits Qualifiers 500 488 98 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1437427 1437428 MS MSD 92245380001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Lead ug/L ND 500 500 482 482 96 96 75-125 0 Results presented on this papa are In the units Indicated by the "Units" column except where an Alternate unit Is presented to the right of the result REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/22/2015 05:27 PM without the written consent of Pace Analytical Services, Inc - Page 7 of 12 aceAnalytical wwwpaeelaba.com Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: BOBS AUTO SALVAGE R2436.00 Pace Project No.: 92245732 QC Batch: WET/36971 Analysis Method: SM 2540D QC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids Associated Lab Samples: 92245732001 METHOD BLANK: 1439485 Matrix: Water Associated Lab Samples: 92245732001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mglL ND 2.5 04/21/15 10:50 LABORATORY CONTROL SAMPLE: 1439486 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Suspended Solids mg/L 250 248 99 90-110 SAMPLE DUPLICATE: 1439487 92246217001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L ND ND SAMPLE DUPLICATE: 1439488 92245814001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg1L 88.0 92.0 4 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result, REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/22/2015 05:27 PM without the written consent of Pace Analytical Services, Inc.. Page 8 of 12 aceAnalytical" wwwpacalafra.00m Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALIFIERS Project: BOBS AUTO SALVAGE R2436.00 Pace Project No.: 92245732 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. NO - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenyla mine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI -The NELAC Institute. LABORATORIES PASI-A Paoe Analytical Services -Asheville PASI-C Pace Analytical Services - Charlotte PASI-I Pace Analytical Services - Indianapolis REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/22/2015 05:27 PM without the written consent of Pace Analytical Services, Inc.. Page 9 of 12 .aceAnalytrcal wwwpacelaha.c= Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Hunteraville, NC 28078 (704)875-9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: BOBS AUTO SALVAGE R2436.00 Pace Project No.: 92245732 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92245732001 OUTFALL NO.1 EPA 1664B GCSV121045 92245732001 OUTFALLNO.1 EPA 80 15 Alcohol -Glycol GCSV115059 92245732001 OUTFALL NO.1 EPA 3010 MPRP118302 EPA 6010 ICP116436 92246732001 OUTFALL NO.1 SM 2540D WET136971 Date: 04/22/2015 05:27 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 10 of 12 ceAW1yticAl • Document Name: Condition Upon Raced Document Number: F-CHR-CS-003-rev.15 Client Name:M t`d- Uci nM A.-6oc,'C44 5 Document Revised: September 22. 2014 Page 1 of 2 Issuing Authority: Pace Huntersville Quality Office Courier: ❑ Fed Ex ❑ UPSZUSPS❑ Client❑ ,rlConlmercial❑ Pace Other Custody Seal on CoolerlBox Present: ,- yea no Seals intact: ❑ yes ❑ no Packing Material: ❑ Bubble VDp ._(Bubble Bags ❑ None ❑ Other Thermometer Used: IR Gun T1401 Type of Ice: We7 Blue None 8 Samples on ice, cooling process has begun Temq Correction Factor T1401 No Correction Corrected Cooler Temp.: •C P•: Temp should be above freezing to 8•C Biological Tissue Is Frozen: Yea N,,/N) L' Comments: Date and Initials of person exam, l Ind contants:d) Chain of Custody Present: QYes ONO ❑NIA 1. Chain of Custodx Filled Out: L7Yes ONO ❑NIA 2. Chain of Custody Relinquished: ej Yes 0o ❑NIA 3. Sampler Name 6 Signature on COC: .17& ONO ❑NIA 4. Samples Arrived within Hold Time: Oyes No ❑NIA 5. Short Hold Time Anal eie 021hr : ❑Yea ,ONo ❑NIA G. Rush Turn Around Time Requested: ❑Yes -O o ❑NIA 7. Sufficient Volume: .0tres ONO ❑NIA 8. Correct Containers Used: -Pace Containers Used: ,ZYes ONO Yes No ❑NIA ❑NIA g. Containers Intact: Yes ❑No ❑NI 10. Filtered volume received for Dissolved tests ❑Yes ❑No NIA 11. Sample Labels match COC: -Includes date/time/ID/Analysis Matrix: ❑Yes o W ❑NIA 12. O of kwq 0V,1'� All containers needing preservation have been checked. All containers needing preservation are found to be in compliance with EPA recommendation. exceptions: VOA, oaliform, TOC, O&G, WI-DRO water) a ❑No ❑NIA ❑Yea ONO ❑NIA M' Zes,No �I l 13. Samples checked for dechlorination: ❑Yes ❑No 06A 14. Heads ace In VOA Vials >6mm : C' es 9do ❑NIA 15. Trip Blank Present: Trip Blank Custody Seals Present Pace Trip.Blank Lot # if purchased): ❑Yas ONO ❑Yea ONO dWA &A 16. Client Notification/ Resolution: Field Data Required? Y 1 N Person Contacted: Date/Time: Comments/ Resolution: SCURF Reviewl IV rr L0 Date: Y IV �) SRF Review: " l Date: Note: Whenever there Is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office ( Le out of hold, Incorrect preservative, out of temp, Incorrect containers) Is _,_ •_ T.� ;�� Page`11-of12 aceAnalyiical " Section A Regidred Chant Wft ma =: CHAIN -OF -CUSTODY 1 Analytical Request Document The Chain -of -Custody Is a LEGAL DOCUMENT. AN relevant fdds must be Caanpteted accwatey. Section B Section C Reeudrad PMRKI ITdo m on: x.. L— lrlfro o !V - Co Page: of fO O fir- Mid -Atlantic Associates, htc- Repon TO: Chuck Hoffman (doffman@maaontme.cDm) Anardwc Chuck Hoffman Address: 409 Rogers View Court Copy To; Joanna Crow (ou.v@maaontine.com) Caaqmv N— Mod -Atlantic Associates. inc. REGULATORY AGENCY Raleigh, NC 27610 Adore= 409 Rogers view Court, Raleigh, NC i— NPDES r GROUNDWATER r DRWKING WATER I— UST f RCRA r OTHER Sao Location Emaa To: choffman@mkiamline.com Pur h— Ordw NO-- R2436.00 Name: Sob's Auto Salvage Pxa OU&M — Rarxence: s p Nicole Gaskwowski PhD-: 919-250-9918 Faw 919-250-9950 Pry t� NC STATE Ragp,estee Due DaterTAT: st:naare Pro-rt rurtroer R2436.00 axe Ptdas r, _ Z = Requested I Analysis Filtered (YIN) Secdov D Vaad Matrix Codas e E. l 'g g COLLECTED A2servafives P N Y N Y DRaa@q WATER Dw e U Zp WATER WT WASTE WATER Ww s V COrs+434T£ COMIPONM U PRODUCTP `w mm START ENDIGRA9 0 SOaXOCD SL Dr SAMPLED W � R' P [�P U �' CIO a m C rA (A-Z,"r.-) oTw < to Z m H a. m c Sample IDs MUST BE UNIQUE TS Q p.CS m U X o C IL m aC _� 0, t�tl 4 M p a Z U sonm m t CO = t td m ~ a DATE TIME _ DATE TIME Goat 2 2 x z z 2 .� N D' tu JI I I I I I4' Pace PfiDject NoJ Lab LO. 1 Oulfall No. 1 Ilvr G -DO 0 8 7 4 1 21 1 x x x x Rainfall es): 2 H: 3 4 5 C 6 { 7 8 9 10 11 12 ADDITIONAL COM11IOM REiMOUMED BY r AIRMIATM OAT$ TOLE ACCEPTED DY r AFM IATION DATE TM SAMPLE C.DHOrIMAIS vv SAMPLER NAME AND SIGNATURE PRINT Nave Of SAMPLOt _ E SIGNATURE or SAMPLER: % - DATE Slgnod — fh ,.,n D (�D+m: F m 3 U 'Impanam Note: ey slpNn9 dda fMm you are acagilq Pa='a MET 30 day payetaed temp arc agl m*q to LVA dk%,w of 1.5% Pat M Mh Tor dry kMMM not pals j 0 dap. l ,A11-0 DZOrev.138, 1 z-O<:-zo07 STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT CERTIFICATE OF COVERAGE NO. NCG100091 SAMPLES COLLECTED DURING CALENDAR YEAR: 2015 (This monitoring report shall be received by the Division no later than 30 days from the date the facility receives the sampling results from the laboratory.) FACILITY NAME McLamb's Auto Salvage, Inc. Fayetteville, NC COUNTY Cumberland PERSON COLLECTING SAMPLE(S) W.D. McLamb PHONE NO. 919 488-5255 CERTIFIED LABORATORY(S) Pace Analytical Lab # 12 Lab # PLEASE REMEMBER TO SIGN ON THE REVERSE 4 r Part A: Stormwater Benchmarks and Monitoring Results "No For sampling periods with no discharge, you must submit this discharge monitoring form noting "No Flow" or Discharge" within C* 30 days of the end of that period to comply with permit reporting requirements. 80110 Outfall Date 00400 00530 ---- 7707-3 01051 78141. No. Sample Collected, Total pH, Total Suspended Non -polar Ethylene Glycol, Lead, Total Total Toxic rno/dd/year Rainfall, Standard Solids (TSS), O&G/TPH mg/L Recoverable, 3 c s Organimg/c inches Units mg/L (Method 1664 mg/L , SGT HEM), mg/L Benchmark - - 6.0 — 9.01 100/502 15 8,000 (Tiers 2 and 3) 0.03 1.0 Outfall001 05/21/2015 1.2 6.1 67.3 <5.0 <5.0 0.0074 NA Note: If you report a sampled value in excess of the benchmark value, or outside the benchmark range for pH, you must implement Tier 1 or Tier 2 responses in the General Permit. ISee If pH values outside this range are recorded in sampled stormwater discharges, but ambient precipitation pH levels are lower, then the lower threshold of this benchmark range is the pH of the precipitation (within instrument accuracy) instead of 6 S.U. Readings from an on -site or local rain gauge (or local precipitation data) must be documented to demonstrate background concentrations were below the benchmark pH range of 6-9. 2See General Permit text to identify whether the more protective benchmark applies for especially sensitive receiving waters. 3For purposes of this permit the definition of Total Toxic Organics is that list as stated in Appendix D, Table II of Chapter 40 Code of Federal Regulations (CFR) Part 122. Form SWU-251, last revised October25, 2012 Page 1 of 2 STORMWATER DISCHARGE OLITFALL (SDO) MONITORING REPORT Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may request that DWQ waive monitoring of total toxic organics. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities allowed such a waiver, the discharger shall sign the following. certification statement: Solvent Management Plan Certification Statement "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the Stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." .h LV u,�J Name (Print name) Title (Print title) \0 � M—) Signature Date Mail Original and one copy to: Division of Water Quality Attn: Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Permittee or Designee) (Date) Form SWU-251, last revised October 25, 2012 Page 2 of 2 aceAnalytical. ` w ..pacalaba.c= Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 25078 (704)875.9092 May 29, 2015 Darin McClure Mid Atlantic Associates, Inc. RE: Project: McLamb's Auto Salvage Pace Project No.: 92251164 Dear Darin McClure: Enclosed are the analytical results for sample(s) received by the laboratory on May 22, 2015. The results relate only to the samples included in this report. Results reported herein conform to the most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. If you have any questions concerning this report, please feel free to contact me. Sincerely, Nicole Gasiorowski nicole.gasiorowski@pacelabs.com Project Manager Enclosures cc: Joanna Crow, Mid Atlantic Associates, Inc. Chuck Hoffman, Mid Atlantic Associates Beverly Oglesby, Mid Atlantic Associates, Inc. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 1 of 12 Pace Analytical Services, Inc. • 9800 Kincey Ave. Suite 100 aceAnalytical Huntersville, NC 28078 ww*pwelabs.com (704)875-9092 CERTIFICATIONS Project: McLamb'sAuto Salvage Pace Project No.: 92251164 Indiana Certification IDs 7726 Moller Road, Indianapolis, IN 46268 Ohio VAP Certification #: CL-0065 Illinois Certification #: 200074 Oklahoma Certification #: 2014-148 Indiana Certification #: C-49-06 Pennsylvania Certification #: 68-05340 Kansas Certification #:E-101771 E-10247 Texas Certification #: T104704355-15-8 Kentucky UST Certification #: 0042 West Virginia Certification M 330 Kentucky WW Certification #:98019 Wisconsin Certification #: 999788130 LouisianalNELAP Certification #: 04076 USDA Soil Permit #: P330-10-00128 Charlotte Certification IDs 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 FloridalNELAP Certification #: E87627 North Carolina Drinking Water Certification #: 37706 Kentucky UST Certification #: 84 North Carolina Field Services Certification #: 5342 West Virginia Certification #: 357 North Carolina Wastewater Certification #: 12 Virginia/VELAP Certification #: 460221 South Carolina Certification #: 99006001 Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 North Carolina Wastewater Certification #: 40 Florida/NELAP Certification #: E87648 South Carolina Certification #: 99030001 Massachusetts Certification #: M-NC030 West Virginia Certification M 356 North Carolina Drinking Water Certification #: 37712 VirginiafVELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 2 of 12 aceAnalytical" *"pace►aba.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 SAMPLE ANALYTE COUNT Project: McLamb's Auto Salvage Pace Project No.: 92251164 Lab ID Sample ID Method Analysts Analytes Reported Laboratory 92251164001 Outfall No. 1 EPA 1664E CLW 1 PASI-C EPA 8015AIcohol-Glycol I3JW 1 PASI-I EPA 6010 JMW 1 PASI-A SM 2540D WRC 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except In full, without the written consent of Pace Analytical Services, Inc.. Page 3 of 12 aceAnalytical • ' wwwcpaceleW.own Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: McLamb's Auto Salvage Pace Project No.: 92261164 Sample: Outfall No. 1 Lab ID: 92251164001 Collected: 05/21/15 00:00 Received: 05/22/15 09:30 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 1664 SGT-HEM, TPH Analytical Method: EPA 1664B Total Petroleum Hydrocarbons ND mg/L 5.0 1 05/29/15 09:25 8016M Glycols In water Analytical Method: EPA 8015 Alcohol -Glycol Ethylene glycol ND mg1L 5.0 1 05/27/15 12:44 107-21-1 6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010 Lead 7A ug/L 5.0 1 05/27/15 19:00 05/29/15 03:40 7439-92-1 2640D Total Suspended Solids Analytical Method: SM 25400 Total Suspended Solids 67.3 mg1L 8.3 1 05/28/15 15:15 Date: 05/29/2015 05:36 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 4 of 12 ace Analytitcal. ` www.peceiabs.crom Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: McLamb's Auto Salvage Pace Project No.: 92251164 QC Batch: GCSV/21473 QC Balch Method: EPA 1664B Associated Lab Samples: 92251164001 METHOD BLANK: 1470249 Associated Lab Samples: 92251164001 Parameter Units Total Petroleum Hydrocarbons mg/L QUALITY CONTROL DATA Analysis Method: EPA 1664B Analysis Description: 1664 SGT-HEM, TPH Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 5.0 05/29/15 09:07 LABORATORY CONTROL SAMPLE: 1470250 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Petroleum Hydrocarbons mg/L 20 19.2 96 64-132 MATRIX SPIKE SAMPLE: 1470251 92251664001 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Total Petroleum Hydrocarbons mg1L ND 20 19.7 97 64-132 Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the tight of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/29/2015 05:36 PM without the written consent of Pace Analytical Services, Inc.. Page 5 of 12 aceAnalytical e www.pwWabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: McLamb's Auto Salvage Pace Project No.: 92251164 QC Batch: GCSV/15468 QC Batch Method: EPA 8015 Alcohol -Glycol Associated Lab Samples: 92251164001 METHOD BLANK: 1304139 Associated Lab Samples: Parameter Units Ethylene glycol mg1L QUALITY CONTROL DATA Analysis Method: EPA 8015 Alcohol -Glycol Analysis Description: EPA 8016 Modified Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 5.0 0512711511:54 LABORATORY CONTROL SAMPLE: 1304140 Spike LCS LCS % Rec Parameter Units Cone. Result % Rec Limits Qualifiers Ethylene glycol mg1L 25 22.5 90 79-129 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1304376 1304377 MS MSD 92251164001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cone. Conc, Result Result % Rec % Rec Limits RPD Qual Ethylene glycol mg1L ND 25 25 19.4 19.2 78 77 67-133 1 Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Dale: 05/29/2015 05:36 PM without the written consent of Pace Analytical Services, Inc.. Page 6 of 12 aceAnalytrcal " wwwpacelbbi.com Pace Analytical services, Inc. 9800 Kincey Ave. Suite 100 Huntersviile, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: McLamb's Auto Salvage Pace Project No.: 92251164 QC Batch: MPRP/18553 Analysis Method: EPA 6010 QC Batch Method: EPA 3010 Analysis Description: 6010 MET Associated Lab Samples: 92251164001 METHOD BLANK: 1468581 Matrix: Water Associated Lab Samples: 92251164001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Lead ug1L ND 5.0 05/29/15 02:35 LABORATORY CONTROL SAMPLE: 1468582 Spike LCS LCS % Rec Parameter Units Cone. Result % Rec Limits Qualifiers Lead ug/L 500 477 95 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1468583 1468584 MS MSD 92251166006 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual Lead ug/L 32A 500 500 448 420 83 78 75-125 6 Results presented on this page are In the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/29/2015 05:36 PM without the written consent of Pace Analytical Services, Inc.. Page 7 of 12 aceAnalyiical® www.pecelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)B75-9092 Project: McLamb'sAuto Salvage Pace Project No.: 92251164 QC Batch: WET137738 QC Batch Method: SM 2540D Associated Lab Samples: 92251164001 METHOD BLANK: 1469739 Associated Lab Samples: 92251164001 Parameter Units Total Suspended Solids mglL LABORATORY CONTROL SAMPLE: 1469740 Parameter Units Total Suspended Solids mglL QUALITY CONTROL DATA Analysis Method: SM 2540D Analysis Description: 2540D Total Suspended Solids Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 2.5 05128/1515:10 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 250 262 105 90-110 SAMPLE DUPLICATE: 1469741 92251021001 Dup. Parameter Units Result Result RPD Qualifiers Total Suspended Solids mglL ND ND SAMPLE DUPLICATE: 1469742 92251044001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mglL ND ND Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/29/2015 05:36 PM without the written consent of Pace Analytical Services, Inc.. Page 8 of 12 aceAnalytical & WW..pacalbbst= Pace Analytical Services, Inc. 9800 Kinsey Ave. Suite 100 Huntersville, NC 28078 (704)875.9092 QUALIFIERS Project: McLamb's Auto Salvage Pace Project No.: 92251 t64 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL-Adjusted Method Detection Limit. PQL- Practical Quantitation Limit. RL - Reporting Limit. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 C h loroethylvi nyl ether, Styrene, and Vinyl chloride. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-N itrosodiphenyla mine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI -The NELAC Institute. LABORATORIES PASI-A Pace Analytical Services -Asheville PASI-C Pace Analytical Services - Charlotte PASI-t Pace Analytical Services - Indianapolis WORKORDER QUALIFIERS WO: 92251164 Ill The sample was received outside of the required temperature range for Ethylene glycol analysis at Pace Indianapolis on 5/26/15. Analysis was completed upon client approval. 5126/15 RRB REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/29/2015 05:36 PM without the written consent of Pace Analytical Services, Inc.. Page 9 of 12 aceAnalytical www.pacelaba.c= Pace Analytical Services, Inc. 980O KinceyAve. Suite 100 Huntersvilte, NC 28078 (704)875.9092 E QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: McLamb's Auto Salvage Pace Project No.: 92251164 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92251164001 Outfall No. 1 EPA 1664E GCSV/21473 92251164001 Outfall No. 1 EPA 8015AIcohol-Glycol GCSV/15458 92251164001 Outfall No. 1 EPA3010 MPRP/18553 EPA6010 ICP/16647 92251164001 Outfall No. 1 SM 25400 WET/37738 Date: 05/29/2015 05:36 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 10 of 12 �r-swurukuysr�sr� Document Number: F-CHR-CS-003-rev.16 Issuing Authority: Huntersville Qualitl Client Name: M%A -A Ila - Page 2 of 2 is for Internal Use Only Courier. ❑ Fed Ex ❑ UI"Y LISPS❑ Client❑ Commercial❑ Pace Other X;"1 Custody Seal on Cooler/Sox Prese:;�Z ❑ no Seals intact: �] yes ❑ nol �Qi —50Packing Material: ❑ Bubble 11Dp Bags ❑ No�Q Other Thermometer Used: IR Gun T1401 Type of Ice; Ve*t Blue None ❑ Samples on ice, cooling process has begun Temo Correction Factor T1401 No Correction ' •C Biological Tissue is Frozen: Yes. Nor IA Date and Initi I of person examining Corrected Cooler Temp.: contents Temp should be above freezing to 6*C Comments: Chain of Custody Present: ©r�es ❑No ❑NIA 1. Chain of Custody Filled Out: Yes ❑No ❑NIA 2, Chain of Custody Relinquished: "©r❑No 11 WA 3, Sampler Name & Signature on COC: as ❑No ❑NIA 4. Samples Arrived within Hold Time: Yes '❑No ❑NIA 5. Short Hold Time Anal sls c72hr ; ❑Yes ff ❑N1A B. Rush Turn Around Time Reguested: ❑Yes -GWo ❑NIA 7• Sufficient Volume: Yos ❑No ❑NIA 8. Correct Containers Used: Jd as ❑No ❑NIA 9. -Pace Containers Used: Yes ❑No ❑NIA Containers Intact: A'as ONO ❑NIA 10, Filtered volume received for Dissolved tests Yes ONO ❑NIA 11, Sample Labels match COC: Riles ❑No ❑NIA 12, 11 -includes dateltime/ID/Anal sis Matrix: 47 All containers needing preservation have been checked. JWes ❑No 11 NIA 13, All containers needing preservation are found to be In Al es ❑No ❑N1A compliance with EPA recommendation. exceptions: VOA, coliform, TOC, 090, Wi-DRO (watel Yes ❑No Samples checked for dechlorfnation: es ❑No ❑NIA 14, Heads ace In VOA Vials >6mm ; PYes ❑No ❑NIA 15. Trip Blank Present: ❑Yes ONO ;2 1A 16. Trip Blank Custody Seals Present ❑Yes ❑No )2Q Pace-Tri Blank hot# if purchased): ------- -- ---- -_ ..-.._. - _ - - . _ _ _ .._ .. _....- _ . _ .. - .._. _ - - _. _..--.----.—..._ ._ Client Notification/ Resolution: Field Data Required? Y 1 N Person Contacted: Date/Time: Comments/ Resolution: SCURF Reviewl Ild L Data, 1,Z� SRF Review: Date: 5 Z5%15 Note: Whenever there Is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office ( i.e out of hold, incorrect preservative, out of temp, Incorrect containers) Place label here W®#:92251164 111111 IN 111111111111 02261164 Page 11 of 12 -2CEAI72loC2f � wwr OaGOl+OSY_. CHAIN -OF -CUSTODY I Analytical Request Document _ a The Chan- -Custody r3 a LEGAL DOCUMENT. Ag refev rrt fidds awst be completed 3ecurat*. kV m 01 KWn A Section B Section C rgrilred Clem Irdomration: Required project bVemwtion: Inreke Irdemurrian: = of ter. Mid-Adantio Associates. ine, Report Tv. Chuck Hoffman (Choffmdn@maarfine-tam) Afteraorc Chuck Hoffman Iuress: 409 Rogers View Court Cagy Tgr .Joanna Crow (Icrow(a@maaonbm corn) C-k-v N—: Mid -Atlantic Associate, it= REGULATORY AGENCY Raleigh, NC 27610 - 409 Rogers View Court. Raleigh. NC NPDES J` i UST i^ GROUND i RCRA WATER r- a DRMNG OTHER WATER Tml To: choffi an@maaor4ne-Caul Purchase Order No.: Pace Cuaa _ • ane: 919-25G-9918 F= 919-250-9950 Propct N—: MdZMVs Auto Salvage a Piojv° Niue Gasiwowsid site quested OwDateffAT_ Standard project Ntrrnber. Pam An �. it _ ZZ I —, 3 • sraM- NC Requested Analysis Filtered (YIN), Section D valid Matrix Codes a z I i0iqLdmd cae,a kdarmstion GM e M COLLECTED Preservatives >: N Y N Y Grmear.WATSR OW WATER Wr n q m WASTE WATER Mw PROD= P V U m START COMM W emnRm r J M cCx Z Idr.rSOtlO 3L SAMPLE ID W s = aAR m _ to to p ? (MZa-4fr1 CT d — of o. Z M ~ O ?—�°' t serve IDs ARUST eE UNIQUE ra O a = C9 E U ULLI LU " o z m= 32 'Ay a c k3 m a vNi a w `� DATE TIME DATE TIME se Z r z x O r` w Q Pace Project Nod Lab LD. Outfali No. 1 t+trr 7 4 1 2 x x x X1 I 2 3 n ,t 4 5 i I i' 1 0' Z'. - ADEWWNAL COYiitMM _ - - BY r AFFILIATION -• - - - -- DATE TAKE Ar�CC�FPiED BY! AFFIl.IiAT70NI ' • T11tE SAMPLE CONErF10!!5 LDATE (� 7� SAMPLER NAME AND SIGNATURE v o w q PFMff Name of SAMPLER: Q $ SIGNATURE of SAMPLER. E 'kr*Onwd Now BY siury t = Iorm • v - you era +caPW+p Paw's NEEr 30 pay paymca temp and agrpeYrg m fats ranges d S.5% per mane mr any inroloes no said w0er 30 days. �• � 1 - 1, F-ALL-0-020rCv.08. 12-0et-2007 Mid Atlantic Engineering & Environmental Solutions June 15, 2015 RrEFCe1vEE) JUN 19 2015 Central Files CENTRAL. FILES Division of Water Resources DWR SECTION 1617 Mail Service Center Raleigh, North Carolina 27699-1617 Subject: STORMWATER NON -DISCHARGE NOTIFICATION MCLAMB'S AUTO SALVAGE, INC. 316 PELT DRIVE FAYETTEVILLE, CUMBERLAND COUNTY, NORTH CAROLINA PERMIT NCG100091 MID -ATLANTIC JOB NO. 000112165.00 To Whom It May Concern: 409 Rogers View Court Raleigh. NC 27610 office 919.250.9916 facsimile 919.250.9950 MAAONLINE.COM Attached please find the Stormwater Discharge Monitoring Report (DMR) and analytical report for the sampling conducted at the above -referenced site. Stormwater samples were collected from Outfall 001 on May 21, 2015 and analyzed for total suspended solids (TSS), total recoverable lead, oil and grease and ethylene glycol. As indicated on the attached DMR, all parameters were reported below or within their respective benchmark range. If you have any questions or need additional information, please contact me at 919-250-9918. Sincerely, MID -ATLANTIC ASSOCIATES, INC. Charles B. Hoffman, P.G. Project Geologist Attachment: Stormwater Discharge Outfall Monitoring Report EXPERIENCED CUSTOMER FOCUSED INNOVATIVE STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT CERTIFICATE OF COVERAGE NO. NCG100091 SAMPLES COLLECTED DURING CALENDAR YEAR: 2015 (This monitoring report shall be received by the Division no later than 30 days from the date the facility receives the sampling results from the laboratory.) FACILITY NAME Bob's Auto Salvage, Jacksonville, NC COUNTY Onslow PERSON COLLECTING SAMPLE(S) Robbie Yopp PHONE NO. (910) 346-3220 ..,� CERTIFIED LABORATORY(S) Pace Analytical Lab # 12 Lab # PLEASE REMEMBER TO SIGN ON THE REVERSE r� r*7 Part A: Stormwater Benchmarks and Monitoring Results For sampling periods with no discharge, you must submit this discharge monitoring form noting "No Flow" or "No Discharge" within 30 days of the end of that period to comply with permit reporting requirements. �01 mwao Outfall No. Date Sample Collected, mo/dd/year Total Rainfall, inches 00400 00530 ---- 77023 01051 78141 pH, Standard Units Total Suspended Solids (TSS), mg/L Non -polar O&G/TPH (Method 1664 SGT HEM), mg/L Ethylene Glycol, mg/L Lead, Total Recoverable, mg/L Total Toxic Organics3, mg/L Benchmark - - 6.0 — 9.01 100/502 15 8,000 (Tiers 2 and 3) 0.03 1.0 Outfall 001 04/15/15 1.0 8.0 <5.0 <5.0 <0.005 NA Note: If you report a sampled value in excess of the benchmark value, or outside the benchmark range for pH, you must implement Tier 1 or Tier 2 responses in the General Permit. 1See If pH values outside this range are recorded in sampled stormwater discharges, but ambient precipitation pH levels are lower, then the lower threshold of this benchmark range is the pH of the precipitation (within instrument accuracy) instead of 6 S.U. Readings from an on -site or local rain gauge (or local precipitation data) must be documented to demonstrate background concentrations were below the benchmark pH range of 6-9. 2See General Permit text to identify whether the more protective benchmark applies for especially sensitive receiving waters. 3For purposes of this permit the definition of Total Toxic Organics is that list as stated in Appendix D, Table II of Chapter 40 Code of Federal Regulations (CFR) Part 122. Form SWU-251, lost revised October 25, 2012 Page 1 of 2 STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may request that DWQ waive monitoring of total toxic organics. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities allowed such a waiver, the discharger shall sign the following certification statement: Solvent Management Plan Certification Statement "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." Name (Print name) T-Cps f j ?n t Title (Print title) 5 Si nature Date Mail Original and one copy to: Division of Water Quality Attn: Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." r li 5- (Date) Form SW U-251, last revised October 25, 2012 Page 2 of 2 R t 0 mod Atlantic Engineering & Environmental Solutlons May 22, 2015 NCDENR/DWQ Attention: Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 Subject: BOB'S AUTO SALVAGE 2780 RICHLANDS HIGHWAY JACKSONVILLE, ONSLOW COUNTY, NORTH CAROLINA PERMIT NCG100091 MID -ATLANTIC JOB NO.000R2436.00 To Whom It May Concern: 409 Rogers View Court Raicigh, NC 27610 office 919.250.99Ia facsimile 919.250,9950 MAAON UNE.COM Attached please find the Stormwater Discharge Monitoring Report (DMR)1 and analytical report for the sampling conducted at the above -referenced site. Stormwater samples were collected from Outfall 001 on April 15, 2015 and analyzed for total suspended solids (TSS), total recoverable lead, oil and grease and ethylene glycol. As indicated on the attached DMR, all parameters were reported below their respective benchmark value. Please note that pH measurements will be collected in the field during the next semi- annual monitoring event (July -December 2015). If you have any questions or need additional information, please contact me at 919-250-9918. Sincerely, MID -ATLANTIC ASSOCIATES, INC. RECEIVED MAY 2 7 2015 Charles B. Hoffman, PG DE WLANO QOALlrT Project Geologist Q NOT€Rl rT11qG Attachment: Stormwater Discharge Monitoring Report Laboratory Analytical Report EXPERIENCED CUSTOMER FOCUSED INNOVATIVE aceAnalytical. www.pscwlabamm Pace Analytical Services, Inc. 9800 Kincey Ave, Suite 100 Huntersvilie, NC 20078 (704)875-9092 April 22, 2015 Darin McClure Mid Atlantic Associates, Inc. RE: Project: BOBS AUTO SALVAGE R2436.00 Pace Project No.: 92245732 Dear Darin McClure: Enclosed are the analytical results for sample(s) received by the laboratory on April 16, 2015. The results relate only to the samples included in this report. Results reported herein conform to the most current TN standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. If you have any questions concerning this report, please feel free to contact me. Sincerely, ,,� Nicole Gasiorowski nicole.gasiorowski@pacelabs.com Project Manager Enclosures cc: .Joanna Crow, Mid Atlantic Associates, Inc. Chuck Hoffman, Mid Atlantic Associates Beverly Oglesby, Mid Atlantic Associates, Inc. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 1 of 12 Pace Analytical Services, Inc. aceAnalytrcal 9eoo Kincey Ave. Suite 100 Huntersville, NC 28078 www.pacelabs.com (704)875-9092 CERTIFICATIONS Project: BOBS AUTO SALVAGE R2436.00 Pace Project No.: 92245732 Indiana Certification IDs 7726 Moller Road, Indianapolis, IN 46268 Ohio VAP Certification M CL-0065 Illinois Certification #: 200074 Oklahoma Certification #: 2014-148 Indiana Certification M C-49-06 Pennsylvania Certification #: 68-05340 Kansas Certification #:E-10177/ E-10247 Texas Certification #: T104704355-15-8 Kentucky UST Certification #: 0042 West Virginia Certification M 330 Kentucky WW Certification #:98019 Wisconsin Certification M 999788130 Louisiana/NELAP Certification #: 04076 USDA Soil Permit #: P330-10-00128 Charlotte Certification IDs 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 Florida/NELAP Certification #: E87627 North Carolina Drinking Water Certification M 37706 Kentucky UST Certification M 84 North Carolina Field.Services Certification M 5342 West Virginia Certification #: 357 North Carolina Wastewater Certification M 12 VirginiaNELAP Certification #: 460221 South Carolina Certification M 99006001 Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87648 Massachusetts Certification #: M-NC030 North Carolina Drinking Water Certification M 37712 North Carolina Wastewater Certification #: 4D South Carolina Certification #: 99030001 West Virginia Certification #: 356 VirginiaNELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 2 of 12 aceAnalytical. www.pecefabs.eom Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Hunteravilie, NC 28078 (704)875-9092 SAMPLE ANALYTE COUNT Project: BOBS AUTO SALVAGE R2436.00 Pace Project No.: 92245732 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92246732001 OUTFALL NO.1 EPA 1664B CLW 1 PASI-C EPA 8015 Alcohoi-Glycol RID 1 PASI-I EPA 6010 JMW 1 PASI-A SM 2540D JTJ 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 3 of 12 ace Analytical' *".paC&W3.0= Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: BOBS AUTO SALVAGE R2436.00 Pace Project No.: 92245732 Sample: OUTFALL NOA Parameters Lab ID: 92246732001 Collected: 04/15/15 16:00 Received: 04M6115 10:45 Matrix: Water Results Units Report Limit DF Prepared Analyzed CAS No. Quaff 1664 SGT-HEM, TPH Analytical Method: EPA 1664E Total Petroleum Hydrocarbons ND mg/L 5.0 1 04/22/15 15:51 8015M Glycols in water Analytical Method: EPA 8015 Alcohol -Glycol Ethylene glycol ND mg1L 5.0 1 04/20/15 14:48 107-21-1 6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010 Lead ND ug/L 5.0 1 04/17/1516:40 0412011516:05 7439-92-1 2640D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids 8.0 mg1L 4.2 1 G4121115 10:52 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except In full, Date: 04/22/2015 05:27 PM without the written consent of Pace Analytical Services, Inc.. Page 4 of 12 aceAnalytical" www.pacelabs.com Pace Analytical services, Inc. 9800.KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: BOBS AUTO SALVAGE R2436.00 Pace Project No.: 92245732 QC Batch: GCSV121045 Analysis Method: EPA 1664B QC Batch Method: EPA 1664B Analysis Description: 1664 SGT-HEM, TPH Associated Lab Samples:. 92245732001 METHOD BLANK: 1440B83 Associated Lab Samples: 92245732001 Parameter Units Total Petroleum Hydrocarbons mg1L Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 5.0 0412211515:48 LABORATORY CONTROL SAMPLE & LCSD: 1440884 1440885 Spike LCS LCSD LCS LCSD % Rec Max Parameter Units Conc. Result Result % Rec % Rec Limits RPD RPD Qualifiers Total Petroleum Hydrocarbons mg/L 20 17.3 15.5 87 78 64-132 11 30 Results presented on this papa are in the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/22/2015 05:27 PM without the written consent of Pace Analytical Services, Inc.. Page 5 of 12 aceAnalytical www.pacelabs.mm Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntefsville, NC 28078 (704)875-9092 Project: BOBS AUTO SALVAGE R2436.00 Pace Project No.: 92245732 OC Batch: GCSV/15059 QC Batch Method: EPA 8015 Alcohol -Glycol Associated Lab Samples: 92245732001 METHOD BLANK: 1278841 Associated Lab Samples: Parameter Units Ethylene glycol mg/L QUALITY CONTROL DATA Analysis Method:, EPA 8015 Alcohol -Glycol Analysis Description: EPA 8015 Modified Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 5.0 0412011511:58 LABORATORY CONTROL SAMPLE: 1278842 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Ethylene glycol mg/L 25 20.1 80 79-129 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1279111 1279112 MS MSD 92245732001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Ethylene glycol mg/L ND 25 25 21A 24A 87 98 67-133 11 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in Full, Date: 04/22/2015 05:27 PM without the written consent of Pace Analytical Services, Inc.. Page 6 of 12 aceAnalyrlcal www.paMabo.com Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)B75-9092 QUALITY CONTROL DATA Project: BOBS AUTO SALVAGE R2436.00 Pace Project No.: 92245732 QC Batch: MPRP118302 Analysis Method: EPA 6010 OC Batch Method: EPA 3010 Analysis Description: 6010 MET Associated Lab Samples: 92245732001 METHOD BLANK: 1437425 Matrix: Water Associated Lab Samples: 92245732001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Lead ug1L ND 5.0 04120/1514:57 LABORATORY CONTROL SAMPLE: 1437426 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Lead ug/L 500 488 98 80-120 MATRIX SPIKE 8 MATRIX SPIKE DUPLICATE: 1437427 1437428 MS MSD 92245380001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Lead uglL ND 500 500 482 482 96 96 75-125 0 Results presented on this page are In the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. Date: 04/22/2015 05:27 PM without the written consent of Pace Analytical Services, Inc.. Page 7 of 12 aceAnalytrcaI s www.pacelaftcom Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: BOBS AUTO SALVAGE R2436.00 Pace Project No.: 92245732 QC Batch: WET136971 Analysis Method: SM 2540D QC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids Associated Lab Samples: 92245732001 METHOD BLANK: 1439486 Associated Lab Samples: 92245732001 Parameter Units Total Suspended Solids mglL LABORATORY CONTROL SAMPLE: 1439486 Parameter Units Total Suspended Solids mgA_ SAMPLE DUPLICATE: 1439487 Parameter Units Total Suspended Solids mglL Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 2.5 0412111510:50 Spike LCS LCS % Rec Cone. Result % Rec Limits Qualifiers 250 248 99 90-110 92246217001 Dup Result Result RPD Qualifiers ND ND SAMPLE DUPLICATE: 1439488 92245814001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mglL 88.0 92.0 4 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/22/2015 05:27 PM without the written consent of Pace Analytical Services, Inc.. Page 8 of 12 �CeAnalytical' W" PacelabsC= Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALIFIERS Project: BOBS AUTO SALVAGE R2436.00 Pace Project No.: 92245732 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. POL - Practical Quantitation Limit. RL - Reporting Limit. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited, Contact your Pace PM for the current list of accredited analytes. TNI -The NELAC Institute. LABORATORIES PASI-A Pace Analytical Services - Asheville PASI-C Pace Analytical Services - Charlotte PASI-I Pace Analytical Services - Indianapolis f V 4001:111912Ws1:191:7_ri•]X013 2 I13WI &f This report shall not be reproduced, except in full, Date: 04/22/2015 05:27 PM without the written consent of Pace Analytical Services, Inc.. Page 9 of 12 aceAnalytical e www.pacerabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28076 (704)875-9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: BOBS AUTO SALVAGE R2436.00 Pace Project No.: 92245732 Lab ID 92245732001 92246732001 92245732001 92245732001 Sample ID QC Batch Method OUTFALL NO.1 EPA 1664B OUTFALL NO.1 EPA 8015 Alcohol -Glycol OUTFALL NOA EPA 3010 OUTFALL NO.1 SM 2540D Date: 04/22/2015 05:27 PM Analyticat OC Batch Analytical Method Batch GCSV/21045 GCSV115059 MPRP118302 EPA 6010 ICP116436 WET136971 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 10 of 12 Document Name: Document Revised: September 22. ZU14 eeAnalytical' Sample Condition Upon Recei t (SCUR) Page I of 2 Document Number: Issuing Authority: ' F-CHR-CS-003-rev.15 Pace Huntersville Quality Office Client Name:M A jlci of r A*roc,,'eA5 Courier: ❑ Fed Ex ❑ UPS[3"USPS0 Cllent❑A,,`rtConamercial❑ Pace Other Custody Seal on Cooler/Box Present: ,yes °1')I�1" no�Ybb Seals intact: ❑ yes ❑ no Packing Material: ❑ Bubble VE)p Qr6ubble Bags ❑ None ❑ Other Thermometer Used: IR Gun T1401 Type of Ice: Cw3e Blue None 0 Samples on ice, cooling process has begun Temo Correction Factor T1401 No Correction Corrected Cooler Temp.:•C Temp should be above freezing to 8'C Biological Tissue Is Frozen: Yea Ngj_Q L Comments: Date and Initials of person exam[ In contents:x M. G[ Chain of Custody Present: QYee ❑No ❑NIA 1. Chain of Custody Filled Out: Mae ❑No ❑NIA 2. Chain of Custody Relinquished: q Yea C94o ❑NIA 3. Sampler Name & Signature on COC: loYes ❑No DIVA 4. Samples Arrived within Hold Time: ' Dyes PNo ❑NIA 5, Short Hold Time Analysis <72hr : ❑Yea RINo ❑NIA 8. Rush Turn Around Time Requested: Dyes _Elko ❑NIA 7. Sufficient Volume: ZWes ❑No ❑NIA 8. Correct Containers Used: -Pace Containers Used: ,0Yas ❑No j3Yas No ❑NIA ❑NIA 9. Containers Intact: Yea ❑No ❑NI 10. Filtered volume received for Dissolved tests ❑Yes ❑No EfNIA 11, Sample Labels match COC: -Includes date/time/lD1Ane1 sls Matrix: ❑Ye 8<0 W ❑NIA 12. No of -10V) l3 j M. All containers needing preservation have been checked. All containers needing preservation are found to be In compliance with EPA recommendation. axoapl(one: VOA, oollfonn, TOC, Od,o, VN-QRO water) 0.41 ❑No ❑NIA ❑No❑NIA ' Yeas No 13. Samples checked for dechlodnation: Dyes ❑No /A 14. Heads ace in VOA Vials >Bmm : lea Gdo ❑NIA 15. Trip Blank Present: Trip Blank Custody Seals Present Pace Trip Blank Lot # if purchased): ❑Yea ❑No ❑Yes ❑No ZN1A 1�141A 1f3. Client Notification/ Resolution: Field Data Required? Person Contacted: Date/Time: Comments/ Resolution: SCURF Review: rrtt.� I Date; I T VI I SRF Review: Date: Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office (Le out of hold, Incorrect preservative, out of temp, Incorrect containers) Y 1 N b 1 i 192245132 _'. ' Y� {�f +. 1'F fir i�,+��F. { ,•• •A Is CHAIN -OF -CUSTODY I Analytical Request Document aceArnalytical " The Chain-O-Cuandy Is a LEGAL °OCU • An remmard rows must be cI'ple1ed el. o n Section A Rcquimd Client b tanaatjcn: Section B Section C Reoulred P mact trdQmatim: i.,...r. Ir.frv.nnf:rvr Page: of W a company: Mid -Atlantic Associates, Inc. Report TV: Chuck Holtman (choffman@maaonline.com) AHerdwo Chuck Hoffman Addr—: 409 Rogers VieW Court Cwy TO: Joanna Crow (jc o maaonline.com) No— Mid- Atlantic Associates, Inc. Address: 409 Rogers View Court, Raleigh, NC REGULATORY AGENCY F NPDES r GROUND WATER r DRINKING WATER UST [- RtrRA r OTHER Raleigh, NC 27610 Email To: chofiman@maaordine.com Pwrhaae off' No.: R2436.00 Dan Q1 " - I : PMna 919-250-9918 F919-250-9950 Pict Nw: Bob's Auto Salvage Paw Praiva Nicole GasionN ski c Lotatloft 1Mar-w- ST/1T1= NC Requested Due DaferrAT: sa aoard PV*a Nw ter: R2436.00 paa p r" a- — Z ( Requested Analysis Fiftered (YfN) Section D Valid Mabt: Codes Z z I Req"diQ COW kdan +ten o COLLECTED Preservatives > N Y N Y ORaAUNQw Ivi ew WATER WT $ • O Q1 WAWATER ww STE PROOUCT P v U of E STAM CGIIPOWE A: EM0RA6 U 3 03 OL ^T 0. = [J J O Crj m Q } SAMPLE ID � �? 0 ca � o m (A-7-0-9 r ..) ARcrr w c z m u }, EL' `o Sampre IDS MUST BE UNIQUE TS p f !A t U` ca U U (L z U m .. $ A m - m p l— m a j W LC Ja 4 i E _ W cc in m L � 111 1 11 f �r r ~ Q C = z U {ii m L a , a' m DATE TIME DATE TIME aL S x z z o ♦ u1 3 1 Pace Project NoJ Lab LD. 1 I Outfall No. 1 Wr G -so O ti 7 4 1 1 2 x X. x x Rainfall (inches): 2 3 ! I 4 5 1 6 � 7 8 9 1a 71 12 ADDITIONAL COMMENTS REi-MQUWED W 1AFM lATI0N DATE TIME ACCEPTED BY r AFFMIATIQN DATE TIRE SAMPLE CONDITIONS - i LdC?rVVr:l< SAMPLER NAME AND SIGNATURE La C '9 E si= .S o "� PWNT Name of SAMPLER: s E a SIGNATURE of SAiMPLEFC DATE Slgned �` d 'bepta0 Kota: eIri y rigm s roanou ywe accap" Pace's NET Sv day paymew Imes aid agisaing m tba dssages at t.5% par mmuM1 tar+nv tnaices not void M em. F,ALL-0-DZQrev.l>8. i 2-Oct-2U67 o Mid Atlantic Engineering & Environmental Solutions February 8, 2019 Central Files RECEIVE!-'! Division of Water Quality FEB 21 2019 1617 Mail Service Center �;ENTRAL FILES Raleigh, North Carolina 27699-1617 DWR SECTION Subject: STORMWATER NON -DISCHARGE NOTIFICATION MCLAMB'S AUTO SALVAGE, INC. 315 PELT DRIVE FAYETTEVILLE, CUMBERLAND COUNTY, NORTH CAROLINA PERMIT NCGIO0091 MID -ATLANTIC JOB NO.000R2165.00 To Whom It May Concern: 409 Rogers View Court Raleigh, NC 27610 office 919.250.9918 [acsimllc 919.250.9950 MAAONLINE.COM On behalf of McLamb's Auto Salvage, Inc., this letter and the attached Stormwater Discharge Outfall Monitoring Report serve as notification that stormwater samples were unable to be collected from the facility outfall during the previous semi-annual sampling period (July -December 2018). During this timeframe, a measurable storm event did not occur at the facility at a time when a stormwater sample could be safely collected (Le. during daylight when the facility was occupied). Therefore, this submittal is intended to serve as notification of "No Discharge" and to satisfy the requirements outlined in Part Il, Section B of General Permit NCG100000 and NCAC T15A 0213.0506. If weather conditions permit, McLamb's Auto Salvage personnel will endeavor to collect representative stormwater samples during the current sampling period (January -June 2019). If you have any questions or need additional information, please contact me at 919-250-9918. Sincerely, MID -ATLANTIC ASSOCIATES, INC. ?'�Q4S7e_� Ron Davis Stormwater Services Manager Attachment: Discharge Outfall Monitoring Reports EXPERIENCED CUSTOMER FOCUSED INNOVATIVE STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT CERTIFICATE OF COVERAGE NO. NCGiomi SAMPLES COLLECTED DURING CALENDAR YEAR: 2018 FACILITY NAME McLamb's Auto Salvage, Inc., Fayetteville, NC COUNTY Cumberland PERSON COLLECTING SAMPLE(S) W.D. McLamb PHONE NO. 919 48&52SS CERTIFIED LABORATORY(S) Pace Analytical Lab # 12 Lab # PLEASE REMEMBER TO SIGN ON THE REVERSE Part A: Stormwater Benchmarks and Monitoring Results For sampling periods with no discharge, you must submit this discharge monitoring form noting "No Flow" or "No Discharge" within 30 days of the end of that period to comply with permit reporting requirements. x,0utfali �No: {Date `Sample Collected, mo/dd/year. Natal -:Rainfall, laclees 00400 „� a 00530 t - �, { L77d23,� 01051 ,z8142 pH, Standard Llnns £Total Suspended'°Non*polar s5o[ids (T55); " mg/L< N, ` ,O&GjTPH ;" (Method 1664" .Y�71.�f74�*,))irng/L ,7 "'Etiijrfene�Glycol, , iireg/L _ . _ ! _, Leah; Total' ;:7Recoverable,a:Orga3 ig%L: : 'Total Tonic nics,:.; mg]L - Benchmark. - 6Q:-9:0 tl 10Q/50 ' 15.. (Tiers2'and>3) 0.03 1.0 Outfall 002 No Discharge No Discharge No Discharge No Discharge No Discharge No Discharge No Discharge No Discharge Note: If you report a samDled value in excess of the benchmark value. or outside the benchmark ranee for oH. you must imoleme nt Tier 1 or Tier 2 resoonses in the General Permit. 'See If pH values outside this range are recorded in sampled stormwater discharges, but ambient precipitation pH levels are lower, then the lower threshold of this benchmark range is the pH of the precipitation (within instrument accuracy) instead of 6 S.U. Readings from an on -site or local rain gauge (or local precipitation data) must be documented to demonstrate background concentrations were below the benchmark pH range of 6-9. 2See General Permit text to identify whether the more protective benchmark applies for especially sensitive receiving waters. 3For purposes of this permit the definition of Total Toxic Organics is that list as stated in Appendix D, Table II of Chapter 40 Code of Federal Regulations (CFR) Part 122. Form SWU-251, last revised October 25, 2012 Page 1 of 2 STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may request that DWQ waive monitoring of total toxic organics. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities allowed such a waiver, the discharger shall sign the following certification statement: Solvent Management Plan Certification Statement "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since fling the last discharge monitoring report. I further certify that this facility is implementing all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." Name (Print name) Title (Print title) Signature Mail Original and one copy to: Division of Water Quality Attn: Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 Date "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penaltie for submitting false information, including the possibility of fines and imprisonment for knowing violations." �1! L (Signature of Permittee or Designee) (Date) Form SW U-251, lost revised October 25, 2012 Page 2 of 2