NCS000562_Email Attachment 1904V15 SAMPLING REPORT_20190505

ANALYTICAL ENVIRONMENTAL SERVICES, INC.
AES
May 02, 2019
Jessica Vickers
Tetra Tech EM Inc.
1955 Evergreen Blvd.
Duluth GA 30096
RE: AZP Fire
Dear Jessica Vickers: Order No: 1904V 15
Analytical Environmental Services, Inc. received 5 samples on 4/30/2019 6:44:00 PM
for the analyses presented in following report.
No problems were encountered during the analyses. Additionally, all results for the associated
Quality Control samples were within EPA and/or AES established limits. Any discrepancies associated with the
analyses contained herein will be noted and submitted in the form of a project Case Narrative. AES'
certifications are as follows:
-NELAP/Florida State Laboratory ID E87582 for analysis of Non -Potable Water, Solid & Chemical Materials,
Air & Emissions for Organics, and Drinking Water Microbiology & Metals, effective 07/01/18-06/30/19.
-North Carolina Certification number 562 for analysis of Surface Water, Groundwater, Effluent, effective until
12/31/19.
-South Carolina Environmental Laboratory Certification number 98016003 effective until 6/30/19.
These results relate only to the items tested as received. This report may only be reproduced in full and with
written permission from the laboratory.
If you have any questions regarding these test results, please feel free to call.
Sincerely,
Paris Masoudi
Project Manager
3080 Presi4ential Drive • Atlanta, Georgia 30340 -Tel: 770.457,8177 • Fax: [phone] • Toll P.,e:800.972.4889
www.aesatlanta.com
Page 1 of 16

ANALYTICAL ENVIRONMENTAL SERVICES, INC
3785 Presidential Parkway, Atlanta GA 30340-3704
AE S TFL.: [phone] / TOLL -FREE [phone] / FAX: [phone]
CHAIN OF CUSTODY
Work Order: lq V q Yi 5-
Date: 4/30/2019 Page I of I
COMPANY: Tetra Tech EM, Inc.
ADDRESS:
1955 Evergreen Blvd, Bldg 200,
Suite 300, Duluth, GA 30096
ANALYSIS REQUESTED
Visit our website
www.aesattanta.com
¢
w
a
E¢
a
o
V
o
x
0
to check on the status of
your results, place bottle
orders, etc.
HONE: 404-849-7136
FAX: [phone]
SAMPLED BY: Paul Prys
SIG
#
SAMPLE ID
SAMPLED
c7
y
E
u
x
! v
DATE
TIME
PRESERVATION (See codes)
REMARKS
17
1
1
AZP-SR'-01-042919
4/29/2019
16:00
X
SW
X
X
MS/MSD
6
2
AZP-SW-02-042919
4/29/2019
16:07
X
SW
X
X
2
3
AZP-SW-03-042919
4/29/2019
16:23
X
SW
X
X
2
4
AZP-SOV-03-042919-DUP
4/29/2019
16:23
X
SW
X
X
2
S
AZP-SNV-04-042919
4/29/2019
16:30
X
SW
X
X
2
6
7
8
9
10
11
12
13
14
RELINQUISHED BY DATE/TIME
RECEIVED BY DATE/TIME
PROJECT INFORMATION
RECEIPT _T
1:
ry� r �
1:
A
PROJECT NAME:
AZP Fire
Total # of Containers
14
2: . �( n ��EH'ky
`1
PROJECT #:
Turnaround Time Request
O Standard 5 Business Days
O 2 Business Day Rush
• Next Business Day Rush
0 Same Day Rush (auth req.)
O Other
SITE ADDRESS: 484 Hicks Grove Road
Mooresboro, North Carolina
3:
SEND REPORT TO: Jessica.VICkerS(cNetratech.com
SPECIAL INSTRUCTIONS/COMMENTS:
Also email results to [e-mail] tetratech.com
SHIPMENT METHOD
OUT / 3 V / l VIA:
IN / / VIA:
T FedEx UPS MAIL COURIER
GREYHOUND OTHER
INVOICE TO:
(IF DIFFERENT FROM ABOVE)
STATE PROGRAM(irany):
E-mail' Y N; Fax? Y kND
DATA PACKAGE: I II III IV
QUOTE #: PO#:
AMPLES RECEIVED AFTER 3PM OR SATURDAY ARE CONSIDERED AS RECEIVED ON THE NEXT BUSINESS DAY; IF NO TAT IS MARKED ON COC AES WILL PROCEED AS STANDARD TAT.
AMPLES ARE DISPOSED OF 30 DAYS AFTER COMPLETION OF REPORT UNLESS OTHER ARRANGEMENTS ARE MADE.
MATRIX CODES: A = Air GW = Groundwater SE = Sediment SO = Soil SW = Surface Water W = Water (Blanks) O = Other (specify)
PRESERVATIVE CODES: H+I = Hydrochloric acid + ice I = Ice out), N = Nitric acid S+I = Sulfuric acid + ice S/M+I = Sodium Bisulfate/Methanol + ice O = Other (specify) NA = None
White Copy - Original; Yellow Copy - Client
Page 2 of 16

Analytical Environmental Services, Inc
Date: 2-May-19
Client: Tetra Tech EM Inc.
Project: AZP Fire Case Narrative
Lab ID: 1904V15
pH Analysis by Method E 150. 1 /SM4500 H+ B:
Samples for pH analysis by Method E150.1/SM4500 H+ B were received and analyzed outside holding time requirement of
"immediate or 15 minutes."
Page 3 of 16

Analytical Environmental Services, Inc
Date: 2-May-19
Client:
Tetra Tech EM Inc.
Client Sample ID:
AZP-SW-01-042919
Project Name:
AZP Fire
Collection Date:
4/29/2019 4:00:00 PM
Lab ID:
1904V15-001
Matrix:
Surface Water
Analyses
Result
Qual MDL
ReportingUnits
Limit
BatchID
DF
Date Analyzed Analyst
METALS, TOTAL SW6010D
(SW3010A)
Aluminum
0.439
0.0211
0.200
mg/L
278431
1
05/01/201916:48
DG
Antimony
BRL
0.0072
0.0200
mg/L
278431
1
05/01/201916:48
DG
Arsenic
BRL
0.0072
0.0500
mg/L
278431
1
05/01/201916:48
DG
Barium
0.0164
J 0.0027
0.0200
mg/L
278431
1
05/01/201916:48
DG
Beryllium
BRL
0.0015
0.0100
mg/L
278431
1
05/01/201916:48
DG
Cadmium
BRL
0.0019
0.0050
mg/L
278431
1
05/01/201916:48
DG
Calcium
2.62
0.0356
0.100
mg/L
278431
1
05/01/201916:48
DG
Chromium
BRL
0.0032
0.0100
mg/L
278431
1
05/01/201916:48
DG
Cobalt
BRL
0.0029
0.0200
mg/L
278431
1
05/01/201916:48
DG
Copper
BRL
0.0015
0.0100
mg/L
278431
1
05/01/201916:48
DG
Iron
0.467
0.0442
0.100
mg/L
278431
1
05/01/201916:48
DG
Lead
BRL
0.0038
0.0100
mg/L
278431
1
05/01/201916:48
DG
Magnesium
1.11
0.0088
0.100
mg/L
278431
1
05/01/201916:48
DG
Manganese
0.0226
0.0009
0.0150
mg/L
278431
1
05/01/201916:48
DG
Nickel
BRL
0.0036
0.0200
mg/L
278431
1
05/01/201916:48
DG
Potassium
0.959
0.115
0.500
mg/L
278431
1
05/01/201916:48
DG
Selenium
BRL
0.0074
0.0200
mg/L
278431
1
05/01/201916:48
DG
Silver
BRL
0.0026
0.0100
mg/L
278431
1
05/01/201916:48
DG
Sodium
2.05
0.109
1.00
mg/L
278431
1
05/01/201916:48
DG
Thallium
BRL
0.0088
0.0200
mg/L
278431
1
05/01/201916:48
DG
Vanadium
BRL
0.0012
0.0100
mg/L
278431
1
05/01/201916:48
DG
Zinc
BRL
0.0073
0.0200
mg/L
278431
1
05/01/201916:48
DG
Mercury, Total SW7470A
(SW7470A)
Mercury
BRL
0.00006
0.00020
mg/L
278500
1
05/02/201916:56
CD
Hydrogen Ion (pH) by SM4500 H+ B
PH
7.35
H 0.0100
0.0100
pH Units
R397084
1
05/01/2019 08:25
BK
Qualifiers: •
Value exceeds maximum contaminant level
BRL
Not detected at MDL
H
Holding times for preparation or analysis exceeded
N
Analyte not NELAC certified
B
Analyte detected in the associated method blank
NC
Not confirmed
E Estimated value above quantitation range
S Spike Recovery outside limits due to matrix
J Estimated value detected below Reporting Limit
> Greater than Result value
< Less than Result value
Narr See case narrative
Page 4 of 16

Analytical Environmental Services, Inc
Date: 2-May-19
Client:
Tetra Tech EM Inc.
Client Sample ID:
AZP-SW-02-042919
Project Name:
AZP Fire
Collection Date:
4/29/2019 4:07:00 PM
Lab ID:
1904V 15-002
Matrix:
Surface Water
Analyses Result Qual MDL ReportingUnits BatchID DF Date Analyzed Analyst
Limit
METALS, TOTAL SW6010D
Aluminum
Antimony
Arsenic
Barium
Beryllium
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Nickel
Potassium
Selenium
Silver
Sodium
Thallium
Vanadium
Zinc
Mercury, Total SW7470A
Mercury
Hydrogen Ion (pH) by SM4500 H+ B
pH
Qualifiers: •
Value exceeds maximum contaminant level
BRL
Not detected at MDL
H
Holding times for preparation or analysis exceeded
N
Analyte not NELAC certified
B
Analyte detected in the associated method blank
NC
Not confirmed
(SW3010A)
0.597
0.0211
0.200
mg/L
278431
1
05/01/201917:04
DG
BRL
0.0072
0.0200
mg/L
278431
1
05/01/201917:04
DG
BRL
0.0072
0.0500
mg/L
278431
1
05/01/201917:04
DG
0.0175
J 0.0027
0.0200
mg/L
278431
1
05/01/201917:04
DG
BRL
0.0015
0.0100
mg/L
278431
1
05/01/201917:04
DG
BRL
0.0019
0.0050
mg/L
278431
1
05/01/201917:04
DG
2.71
0.0356
0.100
mg/L
278431
1
05/01/201917:04
DG
BRL
0.0032
0.0100
mg/L
278431
1
05/01/201917:04
DG
BRL
0.0029
0.0200
mg/L
278431
1
05/01/201917:04
DG
BRL
0.0015
0.0100
mg/L
278431
1
05/01/201917:04
DG
0.612
0.0442
0.100
mg/L
278431
1
05/01/201917:04
DG
BRL
0.0038
0.0100
mg/L
278431
1
05/01/201917:04
DG
1.16
0.0088
0.100
mg/L
278431
1
05/01/201917:04
DG
0.0270
0.0009
0.0150
mg/L
278431
1
05/01/201917:04
DG
BRL
0.0036
0.0200
mg/L
278431
1
05/01/201917:04
DG
1.00
0.115
0.500
mg/L
278431
1
05/01/201917:04
DG
BRL
0.0074
0.0200
mg/L
278431
1
05/01/201917:04
DG
BRL
0.0026
0.0100
mg/L
278431
1
05/01/201917:04
DG
2.11
0.109
1.00
mg/L
278431
1
05/01/201917:04
DG
BRL
0.0088
0.0200
mg/L
278431
1
05/01/201917:04
DG
BRL
0.0012
0.0100
mg/L
278431
1
05/01/201917:04
DG
BRL
0.0073
0.0200
mg/L
278431
1
05/01/201917:04
DG
(SW7470A)
BRL 0.00006 0.00020 mg/L 278500 1 05/02/201917:08 CD
7.41 H 0.0100 0.0100 pH Units R397084 1 05/01/2019 08:25 BK
E Estimated value above quantitation range
S Spike Recovery outside limits due to matrix
J Estimated value detected below Reporting Limit
> Greater than Result value
< Less than Result value
Narr See case narrative
Page 5 of 16

Analytical Environmental Services, Inc
Date: 2-May-19
Client:
Tetra Tech EM Inc.
Client Sample ID:
AZP-SW-03-042919
Project Name:
AZP Fire
Collection Date:
4/29/2019 4:23:00 PM
Lab ID:
1904V 15-003
Matrix:
Surface Water
Analyses Result Qual MDL ReportingUnits BatchID DF Date Analyzed Analyst
Limit
METALS, TOTAL SW6010D
Aluminum
Antimony
Arsenic
Barium
Beryllium
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Nickel
Potassium
Selenium
Silver
Sodium
Thallium
Vanadium
Zinc
Mercury, Total SW7470A
Mercury
Hydrogen Ion (pH) by SM4500 H+ B
pH
Qualifiers: •
Value exceeds maximum contaminant level
BRL
Not detected at MDL
H
Holding times for preparation or analysis exceeded
N
Analyte not NELAC certified
B
Analyte detected in the associated method blank
NC
Not confirmed
(SW3010A)
0.482
0.0211
0.200
mg/L
278431
1
05/01/201917:06
DG
BRL
0.0072
0.0200
mg/L
278431
1
05/01/201917:06
DG
BRL
0.0072
0.0500
mg/L
278431
1
05/01/201917:06
DG
0.0168
J 0.0027
0.0200
mg/L
278431
1
05/01/201917:06
DG
BRL
0.0015
0.0100
mg/L
278431
1
05/01/201917:06
DG
BRL
0.0019
0.0050
mg/L
278431
1
05/01/201917:06
DG
2.72
0.0356
0.100
mg/L
278431
1
05/01/201917:06
DG
BRL
0.0032
0.0100
mg/L
278431
1
05/01/201917:06
DG
BRL
0.0029
0.0200
mg/L
278431
1
05/01/201917:06
DG
BRL
0.0015
0.0100
mg/L
278431
1
05/01/201917:06
DG
0.495
0.0442
0.100
mg/L
278431
1
05/01/201917:06
DG
BRL
0.0038
0.0100
mg/L
278431
1
05/01/201917:06
DG
1.15
0.0088
0.100
mg/L
278431
1
05/01/201917:06
DG
0.0230
0.0009
0.0150
mg/L
278431
1
05/01/201917:06
DG
0.0062
J 0.0036
0.0200
mg/L
278431
1
05/01/201917:06
DG
0.984
0.115
0.500
mg/L
278431
1
05/01/201917:06
DG
BRL
0.0074
0.0200
mg/L
278431
1
05/01/201917:06
DG
BRL
0.0026
0.0100
mg/L
278431
1
05/01/201917:06
DG
2.11
0.109
1.00
mg/L
278431
1
05/01/201917:06
DG
BRL
0.0088
0.0200
mg/L
278431
1
05/01/201917:06
DG
BRL
0.0012
0.0100
mg/L
278431
1
05/01/201917:06
DG
BRL
0.0073
0.0200
mg/L
278431
1
05/01/201917:06
DG
(SW7470A)
BRL 0.00006 0.00020 mg/L 278500 1 05/02/201917:16 CD
7.42 H 0.0100 0.0100 pH Units R397084 1 05/01/2019 08:25 BK
E Estimated value above quantitation range
S Spike Recovery outside limits due to matrix
J Estimated value detected below Reporting Limit
> Greater than Result value
< Less than Result value
Narr See case narrative
Page 6 of 16

Analytical Environmental Services, Inc
Date: 2-May-19
Client:
Tetra Tech EM Inc.
Client Sample ID:
AZP-SW-03-042919-DUP
Project Name:
AZP Fire
Collection Date:
4/29/2019 4:23:00 PM
Lab ID:
1904V 15-004
Matrix:
Surface Water
Analyses Result Qual MDL ReportingUnits BatchID DF Date Analyzed Analyst
Limit
METALS, TOTAL SW6010D
Aluminum
Antimony
Arsenic
Barium
Beryllium
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Nickel
Potassium
Selenium
Silver
Sodium
Thallium
Vanadium
Zinc
Mercury, Total SW7470A
Mercury
Hydrogen Ion (pH) by SM4500 H+ B
pH
Qualifiers: •
Value exceeds maximum contaminant level
BRL
Not detected at MDL
H
Holding times for preparation or analysis exceeded
N
Analyte not NELAC certified
B
Analyte detected in the associated method blank
NC
Not confirmed
(SW3010A)
0.528
0.0211
0.200
mg/L
278431
1
05/01/201917:08
DG
BRL
0.0072
0.0200
mg/L
278431
1
05/01/201917:08
DG
BRL
0.0072
0.0500
mg/L
278431
1
05/01/201917:08
DG
0.0167
J 0.0027
0.0200
mg/L
278431
1
05/01/201917:08
DG
BRL
0.0015
0.0100
mg/L
278431
1
05/01/201917:08
DG
BRL
0.0019
0.0050
mg/L
278431
1
05/01/201917:08
DG
2.60
0.0356
0.100
mg/L
278431
1
05/01/201917:08
DG
BRL
0.0032
0.0100
mg/L
278431
1
05/01/201917:08
DG
BRL
0.0029
0.0200
mg/L
278431
1
05/01/201917:08
DG
BRL
0.0015
0.0100
mg/L
278431
1
05/01/201917:08
DG
0.553
0.0442
0.100
mg/L
278431
1
05/01/201917:08
DG
BRL
0.0038
0.0100
mg/L
278431
1
05/01/201917:08
DG
1.12
0.0088
0.100
mg/L
278431
1
05/01/201917:08
DG
0.0232
0.0009
0.0150
mg/L
278431
1
05/01/201917:08
DG
BRL
0.0036
0.0200
mg/L
278431
1
05/01/201917:08
DG
0.938
0.115
0.500
mg/L
278431
1
05/01/201917:08
DG
BRL
0.0074
0.0200
mg/L
278431
1
05/01/201917:08
DG
BRL
0.0026
0.0100
mg/L
278431
1
05/01/201917:08
DG
2.00
0.109
1.00
mg/L
278431
1
05/01/201917:08
DG
BRL
0.0088
0.0200
mg/L
278431
1
05/01/201917:08
DG
BRL
0.0012
0.0100
mg/L
278431
1
05/01/201917:08
DG
BRL
0.0073
0.0200
mg/L
278431
1
05/01/201917:08
DG
(SW7470A)
BRL 0.00006 0.00020 mg/L 278500 1 05/02/201917:20 CD
7.44 H 0.0100 0.0100 pH Units R397084 1 05/01/2019 08:25 BK
E Estimated value above quantitation range
S Spike Recovery outside limits due to matrix
J Estimated value detected below Reporting Limit
> Greater than Result value
< Less than Result value
Narr See case narrative
Page 7 of 16

Analytical Environmental Services, Inc
Date: 2-May-19
Client:
Tetra Tech EM Inc.
Client Sample ID:
AZP-SW-04-042919
Project Name:
AZP Fire
Collection Date:
4/29/2019 4:30:00 PM
Lab ID:
1904V 15-005
Matrix:
Surface Water
Analyses Result Qual MDL ReportingUnits BatchID DF Date Analyzed Analyst
Limit
METALS, TOTAL SW6010D
Aluminum
Antimony
Arsenic
Barium
Beryllium
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Nickel
Potassium
Selenium
Silver
Sodium
Thallium
Vanadium
Zinc
Mercury, Total SW7470A
Mercury
Hydrogen Ion (pH) by SM4500 H+ B
pH
Qualifiers: •
Value exceeds maximum contaminant level
BRL
Not detected at MDL
H
Holding times for preparation or analysis exceeded
N
Analyte not NELAC certified
B
Analyte detected in the associated method blank
NC
Not confirmed
(SW3010A)
1.24
0.0211
0.200
mg/L
278431
1
05/02/201912:44
DG
0.111
0.0072
0.0200
mg/L
278431
1
05/02/201912:44
DG
BRL
0.0072
0.0500
mg/L
278431
1
05/02/201912:44
DG
0.0060
J
0.0027
0.0200
mg/L
278431
1
05/02/201912:44
DG
BRL
0.0015
0.0100
mg/L
278431
1
05/02/201912:44
DG
0.0808
0.0019
0.0050
mg/L
278431
1
05/02/201912:44
DG
84.5
0.0356
0.100
mg/L
278431
1
05/02/201912:44
DG
0.0104
0.0032
0.0100
mg/L
278431
1
05/02/201912:44
DG
0.0301
0.0029
0.0200
mg/L
278431
1
05/02/201912:44
DG
0.417
0.0015
0.0100
mg/L
278431
1
05/02/201912:44
DG
1.31
0.0442
0.100
mg/L
278431
1
05/02/201912:44
DG
0.0246
0.0038
0.0100
mg/L
278431
1
05/02/201912:44
DG
6.87
0.0088
0.100
mg/L
278431
1
05/02/201912:44
DG
105
0.0891
1.50
mg/L
278431
100
05/02/201913:02
DG
0.138
0.0036
0.0200
mg/L
278431
1
05/02/201912:44
DG
23.4
0.115
0.500
mg/L
278431
1
05/02/201912:44
DG
0.0186
J
0.0074
0.0200
mg/L
278431
1
05/02/201912:44
DG
0.0085
J
0.0026
0.0100
mg/L
278431
1
05/02/201912:44
DG
6500
10.9
100
mg/L
278431
100
05/02/201913:02
DG
0.0104
J
0.0088
0.0200
mg/L
278431
1
05/02/201912:44
DG
0.0275
0.0012
0.0100
mg/L
278431
1
05/02/201912:44
DG
247
0.728
2.00
mg/L
278431
100
05/02/201913:02
DG
(SW7470A)
BRL 0.00006 0.00020 mg/L 278500 1 05/02/201917:24 CD
7.09 H 0.0100 0.0100 pH Units R397084 1 05/01/2019 08:25 BK
E Estimated value above quantitation range
S Spike Recovery outside limits due to matrix
J Estimated value detected below Reporting Limit
> Greater than Result value
< Less than Result value
Narr See case narrative
Page 8 of 16

ANA1.mcAi, Clear Save as
jENviRoNmF-NTAi.
AES SERvicFS, rNc. SAMPLE/COOLER RECEIPT CHECKLIST
1. Client Name: Tetra Tech EM Inc. AES Work Order Number: 1904V15
2. Carrier: FedEx ❑ UPS ❑ USPS❑ Client[m] Courier❑ Othei
Yes No N/A Details Comments
3.
4.
5.
6.
7.
8.
9.
10.
11.
12.
Shipping container/cooler received in good condition?
•
I
damaged ❑ leaking ❑ other[_]
Custody seals present on shipping container?
•
Custody seals intact on shipping container?
•
Temperature blanks present?
•
Cooler temperature(s) within limits of 0-6°C? [See item 13 and 14 for
temperature recordings.]
O
O
O
Cooling initiated for recently collected samples / ice
present ❑
Chain of Custody (COC) present?
•
Chain of Custody signed, dated, and timed when relinquished and received?
•
Sampler name and/or signature on COC?
•
Were all samples received within holding time?
•
ilf
TAT marked on the COC?
•
no TAT indicated, proceeded with standard TAT per Terms &Conditions. ❑
13. Cooler 1 Temperature 3•9
14. Cooler 5 Temperature
15. Comments:
16.
17.
18.
19.
20.
21.
22.
23.
24.
25.
26.
°C Cooler 2 Temperature °C Cooler 3 Temperature °C Cooler 4 Temperature °C
°C Cooler 6 Temperature °C Cooler 7 Temperature °C Cooler 8 Temperature °C
I certify that I have completed sections 1-15 (dated initials).
Yes No N/A Details Comments
VIJ4/30/19
Were sample containers intact upon receipt?
•
Custody seals present on sample containers?
•
Custody seals intact on sample containers?
o•
Do sample container labels match the COC?
O
O
O
incomplete info ❑ illegible ❑
no label ❑ other ❑
Are analyses requested indicated on the COC?
•
Were all of the samples listed on the COC received?
O
O
O
samples received but not listed on COC ❑
samples listed on COC not received ❑
Was the sample collection date/time noted?
•
Did we receive sufficient sample volume for indicated analyses?
•
0-8-
Were samples received in appropriate containers?
Were VOA samples received without headspace (< 1/4" bubble)?
k
it
•
Were trip blanks submitted?
•
listed on COC Elnot listed on COC ❑
27. Comments:
This section only applies to samples where pH can be
I certify that I have completed sections 16-27 (dated initials). BC 5/1/19
checked at Sample Receipt. Yes No N/A Details Comments
28.
29.
30.
Have containers needing chemical preservation been checked? * •
Containers meet preservation guidelines?
•
Was pH adjusted at Sample Receipt? 0
010
Note: Certain analyses require chemical preservation but must be checked in the laboratory and not upon Sample Receipt such as Coliforms, VOCs and Oil & Grease/TPH.
certify that I have completed sections 28-30 (dated initials). BC 5/1/19
Checklist 6.9.17 Rev 2 Locked
Page 9 of 16

Analytical Environmental Services, Inc Date: 2-May-19
Client: Tetra Tech EM Inc.
Project Name: AZP Fire Dates Report
Lab Order: 1904V15
Lab Sample ID
Client Sample ID
Collection Date
Matrix Test Name
TCLP Date Prep Date
Analysis Date
1904V15-001A
AZP-SW-01-042919
4/29/2019
4:00:OOPM
Surface Water TOTAL METALS BY ICP
5/1/2019 11:02:00 AM
05/01/2019
1904V15-001A
AZP-SW-01-042919
4/29/2019
4:00:OOPM
Surface Water TOTAL MERCURY
5/2/2019 1:00:00 PM
05/02/2019
1904V15-001 B
AZP-SW-01-042919
4/29/2019
4:00:OOPM
Surface Water Hydrogen Ion (pH) by SM4500 H+ B
05/01/2019
1904V15-002A
AZP-SW-02-042919
4/29/2019
4:07:OOPM
Surface Water TOTAL METALS BY ICP
5/1/2019 11:02:00 AM
05/01/2019
1904V15-002A
AZP-SW-02-042919
4/29/2019
4:07:OOPM
Surface Water TOTAL MERCURY
5/2/2019 1:00:00 PM
05/02/2019
1904V15-002B
AZP-SW-02-042919
4/29/2019
4:07:OOPM
Surface Water Hydrogen Ion (pH) by SM4500 H+ B
05/01/2019
1904V15-003A
AZP-SW-03-042919
4/29/2019
4:23:OOPM
Surface Water TOTAL METALS BY ICP
5/1/2019 11:02:00 AM
05/01/2019
1904V15-003A
AZP-SW-03-042919
4/29/2019
4:23:OOPM
Surface Water TOTAL MERCURY
5/2/2019 1:00:00 PM
05/02/2019
1904V15-003B
AZP-SW-03-042919
4/29/2019
4:23:OOPM
Surface Water Hydrogen Ion (pH) by SM4500 H+ B
05/01/2019
1904V15-004A
AZP-SW-03-042919-DUP
4/29/2019
4:23:OOPM
Surface Water TOTAL METALS BY ICP
5/1/2019 11:02:00 AM
05/01/2019
1904V15-004A
AZP-SW-03-042919-DUP
4/29/2019
4:23:OOPM
Surface Water TOTAL MERCURY
5/2/2019 1:00:00 PM
05/02/2019
1904V15-004B
AZP-SW-03-042919-DUP
4/29/2019
4:23:OOPM
Surface Water Hydrogen Ion (pH) by SM4500 H+ B
05/01/2019
1904V15-005A
AZP-SW-04-042919
4/29/2019
4:30:OOPM
Surface Water TOTAL METALS BY ICP
5/1/2019 11:02:00 AM
05/02/2019
1904V15-005A
AZP-SW-04-042919
4/29/2019
4:30:OOPM
Surface Water TOTAL MERCURY
5/2/2019 1:00:00 PM
05/02/2019
1904V15-005B
AZP-SW-04-042919
4/29/2019
4:30:OOPM
Surface Water Hydrogen Ion (pH) by SM4500 H+ B
05/01/2019
Page 10 of 16

Analytical Environmental Services, Inc Date: 2-May-19
Client: Tetra Tech EM Inc. ANALYTICAL QC SUMMARY REPORT
Project Name: AZP Fire
Workorder: 1904V15 BatchID• 278431
Sample ID: MB-278431
Client ID:
Units: mg/L
Prep Date: 05/01/2019
Run No: 397204
SampleType: MBLK
TestCode: METALS, TOTAL SW6010D
BatchID: 278431
Analysis Date: 05/01/2019
Seq No: 8896686
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
Aluminum
BRL
0.200
Antimony
BRL
0.0200
Arsenic
BRL
0.0500
Barium
BRL
0.0200
Beryllium
BRL
0.0100
Cadmium
BRL
0.0050
Calcium
BRL
0.100
Chromium
BRL
0.0100
Cobalt
BRL
0.0200
Copper
BRL
0.0100
Iron
BRL
0.100
Lead
BRL
0.0100
Magnesium
0.009450
0.100 J
Manganese
BRL
0.0150
Nickel
BRL
0.0200
Potassium
BRL
0.500
Selenium
BRL
0.0200
Silver
BRL
0.0100
Sodium
0.1207
1.00 J
Thallium
BRL
0.0200
Vanadium
BRL
0.0100
Zinc
BRL
0.0200
Sample ID: LCS-278431
Client ID:
Units: mg/L
Prep Date: 05/01/2019
Run No: 397204
SampleType: LCS
TestCode: METALS, TOTAL Sw6010D
BatchID: 278431
Analysis Date: 05/01/2019
Seq No: 8896687
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
Qualifiers: > Greater than Result value < Less than Result value B Analyte detected in the associated method blank
BRL Below reporting limit E Estimated (value above quantitation range) H Holding times for preparation or analysis exceeded
J Estimated value detected below Reporting Limit N Analyte not NELAC certified R RPD outside limits due to matrix
Rpt Lim Reporting Limit S Spike Recovery outside limits due to matrix
Page 11 of 16

Analytical Environmental Services, Inc Date: 2-May-19
Client: Tetra Tech EM Inc. ANALYTICAL QC SUMMARY REPORT
Project Name: AZP Fire
Workorder: 1904V15 BatchID• 278431
Sample ID: LCS-278431
Client ID:
Units: mg/L
Prep Date: 05/01/2019
Run No: 397204
SampleType: LCS
TestCode: METALS, TOTAL SW6010D
BatchID: 278431
Analysis Date: 05/01/2019
Seq No: 8896687
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
Aluminum
9.738
0.200
10.00
97.4
80
120
Antimony
1.007
0.0200
1.000
101
80
120
Arsenic
1.008
0.0500
1.000
101
80
120
Barium
1.014
0.0200
1.000
101
80
120
Beryllium
0.9781
0.0100
1.000
97.8
80
120
Cadmium
0.9556
0.0050
1.000
95.6
80
120
Calcium
10.11
0.100
10.00
101
80
120
Chromium
0.9773
0.0100
1.000
97.7
80
120
Cobalt
0.9961
0.0200
1.000
99.6
80
120
Copper
0.9466
0.0100
1.000
94.7
80
120
Iron
9.720
0.100
10.00
97.2
80
120
Lead
0.9733
0.0100
1.000
97.3
80
120
Magnesium
9.815
0.100
10.00 0.009450
98.1
80
120
Manganese
0.9950
0.0150
1.000
99.5
80
120
Nickel
0.9956
0.0200
1.000
99.6
80
120
Potassium
9.571
0.500
10.00
95.7
80
120
Selenium
0.9591
0.0200
1.000
95.9
80
120
Silver
0.09591
0.0100
0.1000
95.9
80
120
Sodium
10.25
1.00
10.00 0.1207
101
80
120
Thallium
0.9808
0.0200
1.000
98.1
80
120
Vanadium
1.002
0.0100
1.000
100
80
120
Zinc
0.9888
0.0200
1.000
98.9
80
120
Sample ID: 1904V15-001AMS
Client ID:
AZP-SW-01-042919
Units: mg/L
Prep Date: 05/01/2019
Run No: 397204
SampleType: MS
TestCode:
METALS, TOTAL SW6010D
BatchID: 278431
Analysis Date: 05/01/2019
Seq No: 8896690
Analyte
Result
RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
Aluminum 10.39 0.200 10.00 0.4393 99.5 75 125
Qualifiers: > Greater than Result value < Less than Result value B Analyte detected in the associated method blank
BRL Below reporting limit E Estimated (value above quantitation range) H Holding times for preparation or analysis exceeded
J Estimated value detected below Reporting Limit N Analyte not NELAC certified R RPD outside limits due to matrix
Rpt Lim Reporting Limit S Spike Recovery outside limits due to matrix
Page 12 of 16

Analytical Environmental Services, Inc Date: 2-May-19
Client: Tetra Tech EM Inc. ANALYTICAL QC SUMMARY REPORT
Project Name: AZP Fire
Workorder: 1904V15 BatchID• 278431
Sample ID: 1904V15-001AMS
Client ID:
AZP-SW-01-042919
Units: mg/L
Prep Date: 05/01/2019
Run No: 397204
SampleType: MS
TestCode:
METALS, TOTAL SW6010D
BatchID: 278431
Analysis Date: 05/01/2019
Seq No: 8896690
Analyte
Result
RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
Antimony
1.009
0.0200
1.000
101
75
125
Arsenic
1.010
0.0500
1.000
101
75
125
Barium
1.033
0.0200
1.000
0.01635
102
75
125
Beryllium
0.9856
0.0100
1.000
98.6
75
125
Cadmium
0.9558
0.0050
1.000
95.6
75
125
Calcium
12.69
0.100
10.00
2.615
101
75
125
Chromium
0.9826
0.0100
1.000
98.3
75
125
Cobalt
0.9983
0.0200
1.000
99.8
75
125
Copper
0.9543
0.0100
1.000
95.4
75
125
Iron
10.22
0.100
10.00
0.4670
97.6
75
125
Lead
0.9707
0.0100
1.000
97.1
75
125
Magnesium
10.95
0.100
10.00
1.111
98.4
75
125
Manganese
1.020
0.0150
1.000
0.02259
99.8
75
125
Nickel
0.9817
0.0200
1.000
98.2
75
125
Potassium
10.62
0.500
10.00
0.9586
96.6
75
125
Selenium
0.9632
0.0200
1.000
96.3
75
125
Silver
0.09617
0.0100
0.1000
96.2
75
125
Sodium
12.36
1.00
10.00
2.048
103
75
125
Thallium
0.9812
0.0200
1.000
98.1
75
125
Vanadium
1.008
0.0100
1.000
101
75
125
Zinc
0.9855
0.0200
1.000
98.6
75
125
Sample ID: 1904V15-001AMSD
Client ID:
AZP-SW-01-042919
Units: mg/L
Prep Date: 05/01/2019
Run No: 397204
SampleType: MSD
TestCode:
METALS, TOTAL SW6010D
BatchID: 278431
Analysis Date: 05/01/2019
Seq No: 8896693
Analyte
Result
RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
Aluminum
10.25 0.200
10.00 0.4393 98.1 75
125 10.39 1.35 20
Antimony
0.9976 0.0200
1.000 99.8 75
125 1.009 1.09 20
Qualifiers:
> Greater than Result value
< Less than Result value
B Analyte detected in the associated method blank
BRL Below reporting limit
E Estimated (value above quantitation range)
H Holding times for preparation or analysis exceeded
J Estimated value detected below Reporting Limit
N Analyte not NELAC certified
R RPD outside limits due to matrix
Rpt Lim Reporting Limit
S Spike Recovery outside limits due to matrix
Page 13 of 16

Analytical Environmental Services, Inc Date: 2-May-19
Client: Tetra Tech EM Inc. ANALYTICAL QC SUMMARY REPORT
Project Name: AZP Fire
Workorder: 1904V15 BatchID• 278431
Sample ID: 1904V15-001AMSD
Client ID:
AZP-SW-01-042919
Units: mg/L
Prep Date: 05/01/2019
Run No: 397204
SampleType: MSD
TestCode:
METALS, TOTAL SW6010D
BatchID: 278431
Analysis Date: 05/01/2019
Seq No: 8896693
Analyte
Result
RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
Arsenic
1.003
0.0500
1.000
100
75
125
1.010
0.676
20
Barium
1.020
0.0200
1.000
0.01635
100
75
125
1.033
1.26
20
Beryllium
0.9740
0.0100
1.000
97.4
75
125
0.9856
1.18
20
Cadmium
0.9460
0.0050
1.000
94.6
75
125
0.9558
1.04
20
Calcium
12.46
0.100
10.00
2.615
98.5
75
125
12.69
1.81
20
Chromium
0.9722
0.0100
1.000
97.2
75
125
0.9826
1.06
20
Cobalt
0.9870
0.0200
1.000
98.7
75
125
0.9983
1.14
20
Copper
0.9427
0.0100
1.000
94.3
75
125
0.9543
1.22
20
Iron
10.09
0.100
10.00
0.4670
96.2
75
125
10.22
1.29
20
Lead
0.9578
0.0100
1.000
95.8
75
125
0.9707
1.34
20
Magnesium
10.80
0.100
10.00
1.111
96.9
75
125
10.95
1.41
20
Manganese
1.008
0.0150
1.000
0.02259
98.6
75
125
1.020
1.18
20
Nickel
0.9690
0.0200
1.000
96.9
75
125
0.9817
1.31
20
Potassium
10.40
0.500
10.00
0.9586
94.4
75
125
10.62
2.08
20
Selenium
0.9530
0.0200
1.000
95.3
75
125
0.9632
1.07
20
Silver
0.09494
0.0100
0.1000
94.9
75
125
0.09617
1.29
20
Sodium
12.06
1.00
10.00
2.048
100
75
125
12.36
2.44
20
Thallium
0.9736
0.0200
1.000
97.4
75
125
0.9812
0.780
20
Vanadium
0.9946
0.0100
1.000
99.5
75
125
1.008
1.39
20
Zinc
0.9788
0.0200
1.000
97.9
75
125
0.9855
0.688
20
Qualifiers: > Greater than Result value
BRL Below reporting limit
J Estimated value detected below Reporting Limit
Rpt Lim Reporting Limit
< Less than Result value
E Estimated (value above quantitation range)
N Analyte not NELAC certified
S Spike Recovery outside limits due to matrix
B Analyte detected in the associated method blank
H Holding times for preparation or analysis exceeded
R RPD outside limits due to matrix
Page 14 of 16

Analytical Environmental Services, Inc Date: 2-May-19
Client: Tetra Tech EM Inc. ANALYTICAL QC SUMMARY REPORT
Project Name: AZP Fire
Workorder: 1904V15 BatchID• 278500
Sample ID: MB-278500
Client ID:
Units: mg/L
Prep Date: 05/02/2019
Run No: 397281
SampleType: MBLK
TestCode: Mercury, Total SW7470A
BatchID: 278500
Analysis Date: 05/02/2019
Seq No: 8898721
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
Mercury BRL 0.00020
Sample ID: LCS-278500
Client ID:
Units: mg/L
Prep Date: 05/02/2019
Run No: 397281
SampleType: LCS
TestCode: Mercury, Total SW7470A
BatchID: 278500
Analysis Date: 05/02/2019
Seq No: 8898722
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
Mercury 0.004004 0.00020 0.0040 100 80 120
Sample ID: 1904V15-001AMS
Client ID:
AZP-SW-01-042919
Units: mg/L
Prep Date: 05/02/2019
Run No: 397281
SampleType: MS
TestCode:
Mercury, Total SW7470A
BatchID: 278500
Analysis Date: 05/02/2019
Seq No: 8898724
Analyte
Result
RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
Mercury 0.004013 0.00020 0.0040 100 75 125
Sample ID: 1904V15-002AMS
Client ID:
AZP-SW-02-042919
Units: mg/L
Prep Date: 05/02/2019
Run No: 397281
SampleType: MS
TestCode:
Mercury, Total SW7470A
BatchID: 278500
Analysis Date: 05/02/2019
Seq No: 8898727
Analyte
Result
RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
Mercury 0.003972 0.00020 0.0040 99.3 75 125
Sample ID: 1904V15-001AMSD
Client ID:
AZP-SW-01-042919
Units: mg/L
Prep Date: 05/02/2019
Run No: 397281
SampleType: MSD
TestCode:
Mercury, Total SW7470A
BatchID: 278500
Analysis Date: 05/02/2019
Seq No: 8898725
Analyte
Result
RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
Mercury 0.003940 0.00020 0.0040 98.5 75 125 0.004013 1.84 20
Qualifiers: > Greater than Result value < Less than Result value B Analyte detected in the associated method blank
BRL Below reporting limit E Estimated (value above quantitation range) H Holding times for preparation or analysis exceeded
J Estimated value detected below Reporting Limit N Analyte not NELAC certified R RPD outside limits due to matrix
Rpt Lim Reporting Limit S Spike Recovery outside limits due to matrix
Page 15 of 16

Analytical Environmental Services, Inc Date: 2-May-19
Client: Tetra Tech EM Inc. ANALYTICAL QC SUMMARY REPORT
Project Name: AZP Fire
Workorder: 1904V15 BatchID• R397084
Sample ID: LCS-R397084
Client ID:
Units: pH Units Prep Date:
Run No: 397084
SampleType: LCS
TestCode: Hydrogen Ion (pH) by SM4500 H+ B
BatchID: R397084 Analysis Date: 05/O1/2019
Seq No: 8894259
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit High Limit RPD Ref Val %RPD
RPD Limit Qual
pH 7.000 0.0100 7.000
100 90 110
Sample ID: 1904U26-001ADUP
Client ID:
Units: pH Units Prep Date:
Run No: 397084
SampleType: DUP
TestCode: Hydrogen Ion (pH) by SM4500 H+ B
BatchID: R397084 Analysis Date: 05/O1/2019
Seq No: 8894269
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit High Limit RPD Ref Val %RPD
RPD Limit Qual
pH 7.370 0.0100 7.370
0 20 H
Sample ID: 1904V15-001BDUP
Client ID:
AZP-SW-01-042919
Units: pH Units Prep Date:
Run No: 397084
SampleType: DUP
TestCode:
Hydrogen Ion (pH) by SM4500 H+ B
BatchID: R397084 Analysis Date: 05/O1/2019
Seq No: 8894728
Analyte
Result
RPT Limit SPK value SPK Ref Val
%REC Low Limit High Limit RPD Ref Val %RPD
RPD Limit Qual
pH 7.370 0.0100
Qualifiers: > Greater than Result value
BRL Below reporting limit
J Estimated value detected below Reporting Limit
Rpt Lim Reporting Limit
< Less than Result value
E Estimated (value above quantitation range)
N Analyte not NELAC certified
S Spike Recovery outside limits due to matrix
7.350 0.272 20 H
B Analyte detected in the associated method blank
H Holding times for preparation or analysis exceeded
R RPD outside limits due to matrix
Page 16 of 16