NCS000235_COMPLIANCE_20170629

_- STORMWATER-DIVISION-CODI NG-SHEET
PERMIT NO.
N LS 000a S
DOC TYPE
❑ FINAL PERMIT
❑ MONITORING INFO
❑ APPLICATION
�? COMPLIANCE
❑ OTHER
DOC DATE
❑ 2 Ul 6 2
YYYYM M DD

:1
Energy, Mineral &
Land Resources
ENVIRONMENTAL QUALITY
John Myers, QC Manager
Southern Resins, Inc.
3440 Denton Road
Thomasville, NC 27360
June 29, 2017
Subject: Compliance Inspection I Spill Response
Permit No. NCS 000235
Southern Resins, Inc.
Davidson County
Dear Mr. Myers:
ROY COOPER
Governor
MICHAEL S. REGAN
Secretary
TRACY DAVIS
Director
On June 28, 2017 Glen White of the North Carolina Department of Environmental Quality;
Department of Energy, Minerals, and Land Resources met with you (Quality Control Manager)
and Bryce Young (Site Operations Manager) at the facility located at 3440 Denton Road,
Thomasville, to conduct an inspection as part of the response procedures following a spill of
sufficient volume to require reporting. This inspection consists of review of the Stormwater
Pollution Prevention Plan, training, monitoring and spills records, emergency response and
responsible party review as well as observation of the condition of the site with emphasis on
areas of the May 26, 2017 spill. Your assistance with the inspection was greatly appreciated.
Spill & Response:
On May 26, 2017, Southern Resin, Inc. reported a spill of approximately 2500 gallons of
formaldehyde and acetone based resin. On the day of the spill Shamrock Environmental had just
arrived onsite for a scheduled clean -out of another reactor/tank and had all of their equipment
onsite.
At approximately 6:30 am an employee noticed that one of the reactors was leaking product from
the hatch at the op of the ractor. Response was immediate. Shamrock Environmental, already
on site to conduct other scheduled work, began work to control and clean-up. Major clean-up
began at the reactor containment area and adjacent grassed area. One, Grate inlet was affected in
the grassed area. That inlet drains directly to one of the detention ponds. The pond inlet was
diked to prevent drainage from entering the pond and Shamrock began pumping out and flushing
the inlet pipe. NCDEQ was immediately notified. Bonnie Ware, P.G., Hydrogeologist with
NCDEQ took soil samples at the spill site and water samples from the ponds and downstream
locations. At the time of this visit, results were not back but Mr. Myers said he would forward a
copy as soon as available.
This facility is fortunate that it has the detention pond system and that it does not drain directly
into any waters of the state. Exceedance of formaldehyde and nitrogen continue and site is
State ofKortrtCaroUna t FnviranmenralOuality I Energy. Mineral and Land Resources
Winston-Salem Region a[ Of#ice t 450 Hanes ,1Ai1 Road, Suite 300 i Winston-Salem. NC 27103
33b 776 9800

currently operating in Tier II/Tier III response. Effluent flows into an unnamed tributary that
drains to Hamby Creek. Hamby Creek is encumbered by fecal coliform contamination,
unrelated to any activity conducted at this facility.
Soils were removed from the grassy area of the spill. All soil removed remains in Shamrock
waste containers with cover until test results are back on the soils.
John Myers (Quality Control Manager) and Bryce Young (Site Operating Manager) have
purchased specialty gate valves to be installed in the storm drain lines near pond inlets so they
can be shut off quickly in the event of another spill.
Operator error was found to be the cause of failure/spill. The operator forgot to tighten down the
hatch bolts and once reaction began, the product began to spill out. Mr. Myers has documented
the spill and response and is implementing new procedures and preventative measures to reduce
the chance of a similar incident in the future.
Permit:
This facility holds Individual Stormwater Permit NCS 000235 to discharge stormwater from
industrial activity associated with industrial processes under the National Pollutant Discharge
Elimination System (NPDES). The permit became effective November 1, 2010 and expired on
October 31, 2015. The facility remains covered under the expired permit until a new permit is
issued. A copy of the current permit is required to be maintained with the Stormwater Pollution
Prevention Plan (SPPP) documents. The permit was available for review at the time of
inspection.
Records/Reports:
This facility was required to develop and maintain a (Stormwater Pollution Prevention Plan)
SPPP in accordance with Part H, Section A of the permit. The facility has developed a SPPP.
Training and spills records are current and maintained. Monitoring has been performed as per
the permit. Rainfall records are recorded daily at Pond 3 Outfall. Weekly inspections are
conducted at each of the containment areas and samples are taken before any contained area can
be discharged. No deficiencies found.
Facility Site Review:
This facility manufactures the main ingredient for making Elmer's School Glue and makes the
resin used to make the fiberglass fiber used in air filters. The facility has several containment
areas that contain tanks and vats used in production processes. Many of the facilities are new
and added within the past year. The plant has three (3) stormwater ponds. They are designed to
function in series. Stormwater drains to Pond 1, then into Pond 2, then Pond 3 before it
discharges through two (2) pipes that outlet to Hamby Creek.
Effluent Receiving Waters:
Effluent from this facility drains to Hamby Creek, class "C" waters of the Yadkin Pee Dee River
Basin.
State of North Carolina I Environmental Qual ty I Energy. Minerat and Land Resources
Winston-Salem Regionai Office 1 450 Hanes Mill Road, 5uitc 300 1 'Winston-Salem. NC 27103
33b Th 9800

y 'Self -Monitoring Program:
The permit requires qualitative and analytical monitoring be conducted twice annually unless a
Tiered response is triggered. The facility is currently operating in Tier IUTier III response due to
consecutive parameter exceedance for Formaldehyde and Nitrogen.
This facility was very well maintained and stormwater records were well documented and
current. The facility followed proper reporting, response and documenting procedures during
and after the reported spill. Soouthern Resins was found to be compliant with requirements of its
industrial stormwater permit. If you have questions or need additional information, please
contact Glen White at [phone].
Sincerely,
Matthew E. Gantt, P.E.
Regional Engineer
Land Quality Section
Winston-Salem Regional Office
Enclosures: Inspection Report
cc: File Copy Division of Energy, Mineral and Land Resources (WSRO)
State cat tiorth Carolina Enviroornental Qualtty 1 Energy, A4incral and Land Rescxarcc:s
Winston-Sa!ern Regionai Office 1450 Hares A4i11 Read. S€rite 300 [ Winston-Salem NC 27103
336,176 9800

i'
Permit: NCS000235
SOC:
County: Davidson
Region: Winston-Salem
Contact Person: Allen Grubb
Directions to Facility:
System Classifications:
Primary ORC:
Secondary ORC(s):
On -Site Representative(s):
Related Permits:
Compliance Inspection Report
Effective: 11/01/10 Expiration: 10/31/15 Owner: Southern Resin Inc
Effective: Expiration: Facility: Southern Resin Incorporated
3440 Denton Rd
Title. Operations Mgr.
Inspection Date: 06/28/2017 Entry Time: 10:OOAM
Primary Inspector: Glen White
Secondary tnspector(s):
Reason for Inspection: Routine
Permit Inspection Type: Stormwater Discharge, Individual
Facility Status: Compliant ❑ Not Compfiant
Question Areas:
0 Storm Water
(See attachment summary)
Certification:
Thomasville NC 27360
Phone: [phone]
Phone:
Exit Time: 11:30AM
Phone: [phone]
Inspection Type: Spill/Emergency Response
Page: 1

Permit: NCS000235 owner - Facility: Southern Resin Inc
inspection Date: 06/28/2017 Inspection Type: Spill/Emergency Response Reason for Visit: Routine
Inspection Summary:
This inspection was conducted as part of NCDEQ's response following a spill of an estimated 2500 gallons of formaldehyde
and acetone based resin. On the date of the spill, Shamrock had just arrived on site to clean out one of the tanks as
scheduled and had all of their equipment ready for use.
At approximately 6.30am on 5/26/17 an employee noticed that one of the reactors was leaking product from the hatch at the
top of reactor. Response was immediate. Shamrock Environmental, already on site to conduct other scheduled work,
began work to control and dean -up. Major clean-up began at on the reactors containment area and adjacent grassed area.
one grate inlet was affected in the grassed area. That inlet drains directly to one of the detention ponds. That ponds inlet
was diked to prevent drainage from entering the pond and Shamrock began pumping out and flushing the inlet pipe. NCDEQ
was notified. Bonnie Ware, P.G. , Hydrogeologist with NCDEQ took soil samples at the spill site and water samples from
the ponds and downstream. At the time of this visit, results were not back but Mr. Myers said he would forward a copy as
soon as available.
This facility is fortunate that it has the detention ponds and that it does not drain directly into an waters of the state.
Exceedance of formaldehyde'and nitrite continue and site is currently operating in Tier llfrierlll response. Effluent flows into
an unnamed tributary that drains to Hamby Creek. Hamby Creek is encumbered by fecal coliform contamination, unrelated
to any activity conducted at this site.
Soils were removed from the grassy area of the spill. All soil removed remains in Shamrock waste containers with cover
until test results are back on soils.
John Myers (Quality Control Manager) and Bryce Young (Site Operations Manager) have purchased specialty gate valves to
be installed in the storm drain lines near pond inlets so they can be shut off quickly in the event of another spill.
Operator Error was found to be the cause of the failure/spill. The operator forgot to tighten down the bolts on the hatch and
once reaction began, the product began to spill out. Mr, Myers has documented the spill and response and is implementing
new procedures and preventative measures to reduce the likelihood of a similar incident in the future.
Page: 2

�T permit NCS000235 Owner - Facility: Southem Resin Inc
Inspection Data: 06128/2017 Inspection Type: SpilVEmergency Response Reason for Visit: Routine
Stormwater Pollution Prevention Plan
Does the site have a Stormwater Pollution Prevention Plan?
# Does the Plan include a General Location (USGS) map?
# Does the Plan include a "Narrative Description of Practices"?
# Does the Plan include a detailed site map including outfall locations and drainage areas?
# Does the Plan include a list of significant spills occurring during the past 3 years?
# Has the facility evaluated feasible alternatives to current practices?
# Does the facility provide all necessary secondary containment?
# Does the Plan include a BMP summary?
# Does the Plan include a Spill Prevention and Response Plan (SPRP)?
# Does the Plan include a Preventative Maintenance and Good Housekeeping Plan?
# Does the facility provide and document Employee Training?
# Does the Plan include a list of Responsible Party(s)?
# Is the Plan reviewed and updated annually?
# Does the Plan include a Stormwater Facility Inspection Program?
Has the Stormwater Pollution Prevention Plan been implemented?
Yes No NA NE
■❑❑❑
❑ ❑ ❑
❑ ❑ ❑
❑ ❑ Cl
❑ ❑ ❑
❑ ❑ ❑
M ❑ ❑ ❑
❑ ❑ ❑
M ❑ ❑ ❑
M ❑ ❑ ❑
❑ ❑ ❑
M ❑ ❑ ❑
❑ ❑ ❑
❑ ❑ ❑
❑ ❑ ❑ ❑
Comment: Mr. Myers has done a good bb of maintaining the SPPP and keeping an updated record of spills,
spills response, employee training, facility inspections and maintenance Iotas_
Qualitative Monitorin
Yes No NA NE
Has the facility conducted its Qualitative Monitoring semi-annually? 0 ❑ ❑ ❑
Comment:
Monitoring conducted as permit requires.
Analytical Monitoring
Has the facility conducted its Analytical monitoring?
# Has the facility conducted its Analytical monitoring from Vehicle Maintenance areas?
Yes No NA NE
■❑❑❑
❑ ❑ N ❑
Comment: Monitoring conducted monthly under Tier IIITierill response for exceedance of formaldehvde and
nitrogen. This is an old superfund site and contamination likely remains.
Permit and OUtfails
Yes No NA NE
# Is a copy of the Permit and the Certificate of Coverage available at the site? E ❑ ❑ ❑
# Were all outfalls observed during the inspection? E ❑ ❑ ❑
# If the facility has representative outfall status, is it properly documented by the Division? ❑ ❑ E ❑
# Has the facility evaluated all illicit (non Stormwater) discharges? 0 ❑ ❑ ❑
Comment: Spill response prompted inspection.
Facility has one outfall, through two 15" HDPE_storm pipes outfalling from one of the ponds.
Page: 3

iF a
Energy, Mineral &
Land Resources
ENVIRONMENIAL QUALITY
John Myers, QC Manager
Southern Resins, Inc.
3440 Denton Road
Thomasville, NC 27360
Z"o oo
PAT McCRORY
C,nvermu
DONALD R. VAN DER VAART
Secrvary
October 17, 2016 TRACY DAVIS
Dim -for
Subject- Compliance Evaluation Inspection
Permit No. NCS 000235
Southern Resins — Thomasville
Davidson County
Dear Mr. Myers:
On October 12, 2016 Glen White of the North Carolina Department of Environmental Quality;
Department of Energy, Minerals, and Land Resources met with you at the facility located at
3440 Denton Road, Thomasville, to conduct a compliance inspection per the Industrial
Stormwater Permit requirements. Inspection consists of review of the Stormwater Pollution
Prevention Plan, training, monitoring and spills records as well as observation of the general
condition of the site, the outfalls and any possible exposures to downstream stormwater. Your
assistance with the inspection was greatly appreciated.
Permit:
This facility holds Individual Stormwater Permit NCS 000235 to discharge stormwater from
industrial activity associated with industrial processes under the National Pollutant Discharge
Elimination System (NPDES). The permit became effective November 1, 2010 and expires on
October 31, 2015. The facility remains covered under the expired permit until a new permit is
issued. A copy of the current permit is required to be maintained with the Stormwater Pollution
Prevention Plan (SPPP) documents. The permit was available for review at the time of
inspection.
Records/Reports:
This facility was required to develop and maintain a (Stormwater Pollution Prevention Plan)
SPPP in accordance with Part II, Section A of the permit. The facility has developed a SPPP.
Training and spills records are current and maintained. Monitoring has been performed as per
the permit. Rainfall records are recorded daily at Pond 3 Outfall. Weekly inspections are
conducted at each of the containment areas and samples are taken before any contained area can
be discharged. No deficiencies found.
si'euR t�€ the r tPf L rrJlina I Elrvironmcntal Quality I Energy, Mineral and Lar?rl Resources
tNinston Salem kegianal €�f{ice 1450 Hanes Mill Road, Suite 300 [ Winsion-Salem, NC 27103
3750 i IG <?800

Facility Site Review:
This facility manufactures the main ingredient for making Elmer's School Glue and makes the
resin used to make the fiberglass fiber used in air filters. The facility has several containment
areas that contain tanks and vats used in production processes. Many of the facilities are new
and added within the past year. The plant has three (3) stormwater ponds. They are designed to
function in series. Stormwater drains to Pond 1, then into Pond 2, then Pond 3 before it
discharges through two (2) pipes that outlet to Hamby Creek.
Effluent Receiving Waters:
Effluent from this facility drains to Hamby Creek, class "C" waters of the Yadkin Pee Dee River
Basin.
Self -Monitoring Program:
The permit requires qualitative and analytical monitoring be conducted twice annually unless a
Tiered Response is triggered. The facility is currently operating in Tier II Response due to
consecutive parameter exceedance for Formaldehyde and Nitrogen.
This facility was very well maintained and stormwater records were well documented and
current. The facility was found to be compliant with requirements of its industrial stormwater
permit. If you have questions or need additional information, please contact Glen White at (336)
776-9660.
Sincerely,
Matthew E. Gantt, P.E.
Regional Engineer
Land Quality Section
Winston-Salem Regional Office
Enclosures: Inspection Report
cc: File Copy Division of Energy, Mineral and Land Resources (WSRO)
Stab of North Carolina 1 Environmental Quality I Energy, Mineral and Land Resources
Winston-Salem Regional Qffice 1450 (lanes Mil( Road Suite 300 I Winston-Salem NC 27103
336 776 9800

ill
Permit: NCS000235
SOC:
County: Davidson
Region: Winston-Salem
Contact Person: Allen Grubb
Directions to Facility:
System Classifications:
Primary ORC:
Secondary ORC(s):
On -Site Representative($):
Related Permits:
Compliance _Inspection Report
Effective: 11/01/10 Expiration: 10/31/15 owner-: Southern Resin Inc
Effective: Expiration: Facility: Southern Resin Incorporated
3440 Denton Rd
Title: Operations Mgr.
Inspection Date: 1011212016 Entry Time: 1 t:30AM
Primary Inspector: Glen White
Secondary Inspector(s):
Reason for Inspection: Routine
Permit Inspection Type: Stormwater Discharge, Individual
Facility Status: Compliant Not Compliant
Question Areas:
Storm Water
(See attachment summary) -
Certification:
Thomasville NC 27360
Phone: [phone]
Phone:
Exit Time: 12:30PM
Phone: [phone]
Inspection Type: Compliance Evaluation
Page: 1

Permit NCS000235 Owner - Facility: Southern Resin Inc
Inspection Date: 10112t2016 Inspection Type : Compliance Evaluation Reason for Visit: Routine
Inspection Summary:
(See Compliance Letter)
Page: 2

r
• ' Permit: NCS000235 Owner - Facility: Southem Resin Inc
Inspection Data: 1011212016 Inspection Type: Compliance Evaluation Reason for Visit: Routine
Analytical Monitoring Yes No NA NE
Has the facility conducted its Analytical monitoring? E ❑ ❑ ❑
# Has the facility conducted its Analytical monitoring from Vehicle Maintenance areas? ❑ 110 ❑
Comment: Analyticai monitoring being conducted monithly in Tier II Response due to consecutive
exceedance of Formaldehyde and Nitrogen. Continue to monitor monthly until three consecutive
sambles result within threshold.
Permit and Outfalls Yes No NA NE
# Is a copy of the Permit and the Certificate of Coverage available at the site? M ❑ ❑ ❑
# Were all outfalls observed during the inspection? E ❑ ❑ ❑
# If the facility has representative outfall status, is it property documented by the Division? ❑ ❑ ® ❑
# Has the facility evaluated all illicit (non stormwater) discharges? N ❑ ❑ ❑
Comment: No deficiencies.
Qualitative Monitoring Yes No NA NE
Has the facility conducted its Qualitative Monitoring semi-annually? i ❑ ❑ ❑
Comment: Conduct Monitorinq per permit.
Stormwater Pollution Prevention Plan
Yes No NA_bIrz
Does the site have a Stormwater Pollution Prevention Plan?
E ❑ ❑ ❑
# Does the Plan include a General Location (USGS) map?
0 ❑ ❑ ❑
# Does the Plan include a "Narrative Description of Practices"?
® ❑ ❑ ❑
# Does the Plan include a detailed site map including outfall locations and drainage areas?
E ❑ ❑ ❑
# Does the Plan include a list of significant spills occurring during the past 3 years?
E ❑ ❑ ❑
# Has the facility evaluated feasible alternatives to current practices?
0 ❑ ❑ ❑
# Does the facility provide all necessary secondary containment?
E ❑ ❑ ❑
# Does the Plan include a BMP summary?
0 ❑ ❑ ❑
# Does the Plan include a Spill Prevention and Response Plan (SPRP)?
0 ❑ ❑ ❑
# Does the Plan include a Preventative Maintenance and Good Housekeeping Plan?
E ❑ ❑ ❑
# Does the facility provide and document Employee Training?
0 ❑ ❑ ❑
# Does the Plan include a list of Responsible Party(s)?
E ❑ ❑ ❑
# Is the Plan reviewed and updated annually?
E ❑ ❑ ❑
# Does the Plan include a Stormwater Facility Inspection Program?
E ❑ ❑ ❑
Has the Stormwater Pollution Prevention Plan been implemented?
0 ❑ ❑ ❑
Page: 3

Permit NCS000235 Owner - Facility: Southern Resin Inc
Inspectlon Date: 10112/2015 Inspection Type : Compliance Evaluation Reason for Via It: Routine
Stormwater Pollution Prevention Plan
Yes No NA NE
Comment: All records complete. Training conducted annually. Currently in Tier 11 for consecutive
exceedance of Formaldehyde and Nitrogen. Monitoring as required. Weekly site inspections
conducted throughout the facility. Well documented. No deficiencies.
Page: 4

Appendix F
Southern Resin, Inc.
Thomasville, North Carolina
PREVENTIVE MAINTENANCE INSPECTION FORM
Associated with sampling on 9/27/2016
Date/Time
of
Shift
Team Member
Area Inspected &
Corrective -
Problem Observed
Action
Inspection
9/29/2016
1st
John Myers
1170 Dyke area -
Is clean and free of trash
'
and buckets
t
9/29/2016
1st
John Myers
500 Dyke area -
Is being cleaned. Old
dried material being
chiseled out
9/29/2016
1st
John Myers
Coron Dyke area -
No issues
9/29/2016
1st
John Myers
Product pump
No issues
9/29/2016
1st
John Myers
Truck lot
No issues
9/29/2016
1st
John Myers
Truck Scale
a
No issues
9/29/2016
1st
John Myers
Tote Storage
No issues
9/29/2016
1st
John Myers
Shop Area and ditch to
Ponds
Ditch clear
9/29/2016
1st
John Myers
Wastewater handling
area- No spills
9/29/2016
1st
John Myers
ketone loading area -
Clean. Buckets closed
9/29/2016
1st
John Myers
Urea blowing area
No spilled matieral

AmrKWA
NCDENR
North Carolina Department of Environment and Natural Resources
Division of Water Quality
Beverly Eaves Perdue Coleen H. Sullins Dee Freeman
Governor Director Secretary
August 18, 2010
Mr. Alien Grubb, Operations Manager
Southern Resin, Inc.
3440 Denton Drive
Thomasville, NC 27360
Subject: Compliance Evaluation Inspection
Certificate of Coverage #NCS000235
Southern Resin, Inc.
Davidson County
Dear Mr. Grubb:
A Compliance Evaluation Inspection was performed at Southern Resin in Thomasville, North Carolina on
July 22, 2010 by Jenifer Carter of the Winston-Salem Regional Office. You were present for the inspection. The
purpose of the inspections was to review compliance with the National Pollutant Discharge Elimination System
(1VPDES) Individual Stormwater Permit. The following are the findings from the subject inspection:
• A Stormwater Pollution Prevention Plan (SPPP) has been developed and properly implemented.
• Qualitative monitoring has been conducted as required and recorded in accordance with permit requirements at
one (1) stormwater outfall.
Analytical monitoring has been conducted as required and recorded in accordance with permit requirements at
one (1) stormwater outfall. Exceedences of benchmark values for formaldehyde and nitrate f nitrite nitrogen as
well as corrective actions taken were well -documented. Exceedences continue to be a problem and
investigations and further corrective actions are ongoing. When your permit is renewed, please note new
required procedures for dealing with benchmark exceedences.
It was noted that pH samples were most likely measured outside the required 15-minuted holding time, though
the contract lab never notified the facility of that fact, and the permit does not mention the requirement.
Clarification will be provided when the permit is renewed. One option is to use on -site pH monitoring
equipment, though the industry would need to obtain field parameter certification. prior to doing so. Visit
http://PortaLiiedestr.org/weblwgllableertlfield for more information on obtaining field parameter certification. �©
• Manifests for removal of strip water, process water and process sludge wer�vailabl for review. -�0 &_�?
• There were no residuals from spills or leaks obsered on the ground, nor in or near surface waters. ("Loalo��tl'
+ Evidence of rodent damage to the dam of the pond near the outfall was observed. Woody vegetation should be
removed and controlled for, and significant damage should be repaired in order to prevent the dam from being
breached, releasing pond water directly to the stream below the outfall.
• A second undocumented outfall was observed during the inspection that only receives stormwater from some of
the roof drains. It was agreed that the pipe directing the stormwater to this outfall would be capped and the
flow redirected in order to drain the roofs to other documented outfall.
continued on reverse...
North Carolina Division of water Quality, Winston-Salem Regional Office
Location: 585 Waughtown St Winston-Salem, North Carolina 27107 One
Phone: [phone] l FAX: [phone] Customer Service: 1-877.623-6748 North C aro tin a
Internet: www.ncwaterquaiity.org ;Vaturally
An Equal Opportunity 1 Affirmative Action Employer `

The Division greatly appreciates your efforts to maintain compliance. You should be receiving a draft version of
your permit soon, as part of the renewal process. Please take the time to read it carefully as there will be changes.
Should you have any questions, please contact Jenifer Carter at [phone].
Sincerely,
Steve W. Tedder
Surface Water Regional Supervisor
Winston-Salem Regional Office
Division of Water Quality
cc: SRO=Files
SWP — Central Files
NPS ACO Unit
Mr. Mike Waddey, P.E. (Engineering Solutions, Inc; 131 Lonetree Cir; Advance, NC 27006)

05/10/2810 10:07 336-99E0526 P & ^ L-ABOR-ATORIES P'GE 02/03
RESEARCh & ANA[YACAL
LAbORAM ES, INC.
Analytical/Process Consultations
Southern Resin
Date Sample Collected
= OS/19/3.0
3440 Denton
Road
Date Sample Received
05/19/10
Thomasville,
NC 27360
Date Sample Analyzed
05/19/10
-----A
P.nal-yses Performed by
DW -AR -KL -TP
Lab sample Number
--------------------
674176
Parameter
Storet 4
Results
Formaldehyde
(71880) •�-
3 _ 19 mg/_
Ua�
fA�I/}1 6y f �
COD -HIGH
(00340) ---
so mg/1
,
/�Ic:A
t 9a7
mG%�
NH-3-N
(00610).
0.92-7 mgfl
/QC,)),
TKN
(00625)
7.40 mg/1
0,o2
NO2+NO3
(00630)
0.540 mg/l
PH
(00400) To Li>s
5-93 std. Units
--------------------
Clients Sarnple Sazzrce OUTFAU.
Numae;'
Time Collected (,Hzs) 1230

I
RESEARCh & ANA1yTICA1
LAbORATORIES, INC.
Analytical/Process Consultations
Soutbern_Resin
Dat..e.Sample Collected
11/13/09
3440 Denton
Road
Date Sample Received
11/13/09
Thomasville,
NC 27360
Date Sample Analyzed
11/13/09
Attn: BOBBY
HILL
Date of Report
11/23/09
---Analyses Performed by
AR -KL
Lab Sample Number
---------------------
660844
Parameter
Storet #
Results
Formaldehyde
(71880)
COD -HIGH
(00340)
88 mg/1
NH-3-N
(00610)
0.295 mg/1
TKN
(00625)
6.51 mg/1
NO2+NO3
(00630)
1.29 mg/1
pH
{00400)
'6.49 std. Units
Clients Sample Source
Number
Time Collected (Firs)
k
--------------------
DISCHARGE PIPE
1300
P 0. Box 473 • 105 Short Street • Kernersville, North Carolina 27284 • 336-996-2841 • Fax [phone]
www..-andaisbs,com

RESEARCh & ANA[yTICAI
LAbORATORIES, INC.
Analytical/Process Consultations
Southern Resin Date Sample Collected 06/16/09
1510 Denton Road Date Sample Received 06/16/09
Thomasville, NC 27360 Date Sample Analyzed 06/16/09
Attn: Ray Simmons Date of Report 07/13/09
Analyses Performed by AR -KL -DD -DW
LabL Sample' 13umber
-----------------
648453
-------------------------------------------------------
Parameter Storet # Results
TKN (00625) 3.74 mg/1
BOD-5 (00310) 4.11 mg/1
COD -HIGH (00340) 18 mg/l
Formaldehyde (71880) �2mg
NH-3-N (00610) 0.464 mg/l
NO-2-N (00615) 0.326 mg/1
a�
NO-3-N (00620) 0.445 mg/1
-- --­ --------------
Clients Sample Source #2 SMALL LAKE
•Nurtrber
Time Collected (Hrs) 1120
P.O. Box 473 • 106 Short Street • Kernersville, North Carolina 27284 • 336-996-2841 • Fax [phone]
www.randalabs.com

06/13/2008 12:57 33G--9960326 R & A LABORATORIES PAGE 02/03
RESEARCH & ANAlyTICAI
LABORATORIES,, INC.
Analytical/Process ConsuttationS
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Southern Resin
Date Sample collected
05/29/08
1510 Denton
Road
Date Sample Received
05/29/08
Thomasville,
NC 27360
Date Sample Analyzed
_ 05/29/08
Attn: Alan
Grubb
Date of Report
06/13/08
Analyses Performed by
DW -KP -KL -TD
Lab Sample Number
--------------------
618220
Parameter
Storet
Results
Formaldehyde
(71880)
7.�m�/l
COD -HIGH
(00340)
71.0 mg/l
NH- 3-N (00610) 4.32 mg/l
TKN (006�5) 8.10 mg/l
NO2+NO3 (00630) �� ,0.516 mg/1 ✓J
PH (004001 7.01 Std. Units
vl
--------------------
Clients Sample Source LOWER POND
Number
Time ColJ,ected (Hrs) 1100
PC, , Box 473 • 108i Short Street . KCrnersville, North 09rn(ina 272S4 • 335-996-2049 - Fax [phone]
www.randalabs.com

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REsFARch & ANA[yTICA[ _ `• ' �`•
LAbORATORIE_$ INC •
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r NC #34, • ;
Anahjt si/Process Consultations '; ?
Southern Resin Date Sample Collected 11/16/06
3440 Denton Road Date Sample Received 11/16/06
Thomasville, NC 27360 Date Sample Analyzed : 11/16/06
Attn: Allen Grubb Date of Report 12/04/06
Analyses Performed by DW -JK -MC -DW -TD
Lab Sample Number
--------------------
576261
---.�-....�---------=•^-� �.. --�...-=====a==-�---'-----------a-'a----=====�x�=ate===
Pazameter Storet # Results
Formaldehyde (71880) 5.34 mg/1
COD -LOW (00340) 40.0 mg/l
NH- 3-N (00610) 6.19 mg/1
. TKN (0062S) 12.0 mg/l
NO2tNO3 (00630) E-5 mg/1'
PH (00400) 7.29 Std- Units
-
Clients Sample Source DISCHARGE PIPEAT
�,•� Number BACK OF POND
Time Collected (Hrs) 1240
RCL Box 473 - 106 Short Street • Kerneraville. North Carolina 27284 • 226-996-2841 • Fax [phone]
www.researchandanalydcal.com

RESEARCh & ANA1Y TICA1
LABORATORIES, INC.
Analytical/Process Consultations
Sr-nt er:. Resin -
"Date 'Sa-, le ,,lid—:
A
11/30i 05 _ -
3-40 Dei�ten
Road
Date Sample Received
11/30/05
Thomasville,
NC 27360
Date Sample Analyzed
11/30/05
Attn: Doug
Stewart
Date of Report
12/08/05
Analyses Performed by
DW -JK -IBC
Lab Sample Number
--------------------
5491558
Parameter
Storet #
Results
Formaldehyde
(71880)
7.45 mg/�
COD -HIGH
(00340)
38 mg/l
NH-3 V
(00610)
7.47 mg/1
TKN
(00625)
mg/1
--_-- _ - NO2+NO3_
— (00_630)
-144..9
\ l cJ3 ma/17�1
Clients Sample Source POND ON RIGHT AT
Number DISCHARGE PIPE
Time Collected (Frs) 1445
P.D. Box 473 • 106 Short Street • Kernersville. North Carolina 27284 • 336-996-2841 ,• Fax [phone]
www. resea rch a n da n e lyti c e!_c om

RESEARCH & ANA1YTiCA[
LABORATORIES, INC.
AnalyticaVProcess Consuftations
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NC#34 z� �= -
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Southern Resin
Date Samp.7_P Collected
: 06/04/04
1510 Denton
Road
Date Sample Received
: 06/04/04
Thomasville,
NC 27360
Date Sample Analyzed
06/04/04
Attn: Doug
Stewart
Date of Report
06/11/04
Analyses Performed by
SW -DW
Lab Sample Number
--------------------
506294
Parameter
Storet #
Results
COD -LOW
(00335)
73 mg/1
Formaldehyde
(71880)
7.54
I
Clients Sample Source
Number
Time Collected (Hrs)
--------------------
A
1145
P.Q. Box 473 - 106 Short Street - Kernersville, North Carolina 27284 - 336-996-2841 - Fax [phone]S

ti.
RESEARCh & ANAIyTICAI
LAbORATO&S, INC.
Analytical/Process Consultations
Southern Resin
1510 Denton Road
Thomasville, NC 27360
Attn: Kevin Conway
Date Sample Collected
Date Sample Received
Date Sample Analyzed
Date of Report
Analyses Performed by
04/11/03
04/11/03
04/11/03
04/24/03
SW
Lab Sample Number
--------------------
474310
--------------------------------------------------------------------------------
-------------------------------------------------------------------------------
Parameter Storet # ��Reesults
Formaldehyde (71880) �4.74 mg/l
COD -LOW (00335) 65 mg/l
Clients Sample Source
Number
Time Collected (Hrs)
PO, Box 473 • 106 Short Street • Kernersville. North Carolina 27284 • 336-996-2841 • Fax [phone]