NCS000255_MONITORING INFO_20180706

--STORIVIUVATER"DI VISfON-CODING-SHEET--
PERMIT NO.
ooD 25S
DOC TYPE
❑FINAL PERMIT
'MONITORING INFO
❑ APPLICATION
❑ COMPLIANCE
❑ OTHER
DOC DATE
❑ ZOl C6 a Dfo
YYYYMMDD

STORMWATER DISCHARGE OUTFALL (SDO)
MONITORING REPORT
Permit Number NCS 000255 SAMPLES COLLECTED DURING CALENDAR YEAR: 2018
(This monitoring report shall be received by the Division no later than 30 days from
the date the facility receives the sampling results from the laboratory.)
6 1 V U 0
FACILITY NAME Grede II-Biscoe LLC COUNTY Montgomery
PERSON COLLECTING SAMPLES) Lorenzo Jackson 2018 PHONE NO. 9f 10 ) 428-2111 (ext. 3268)
CERTIFIED LABORATORY(S) Pace Analytical Services Lab # 9151
Lal.CAN flRT`11__ FILES
D► IR SECTION SIGNATURE OF PERMITTEE OR DESIGNEE
' REQUIRED ON PAGE 2.
Part A: Specific Monitoring Requirements
Outfall
No.
Date
Sample
Collected
5009
Total
Flow if a
Total
'Rainfall
COD
Phenols
Total Cd
Total Cu
Total Pb
Total Ni
moldd/vr
MG
inches
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
001
05/18/18
0.058
0.44
116
0.021
ND
0.0413
0.0115
0.0126
002
05/18/18
0.002
0.44
ND
0.016
ND
ND
ND
ND
003
05/18/18
0.004
0.44
25.0
0.016
ND
0.0272
0.0061
0.0059
ND = Non Detect
Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? ©yes @no
(if yes, complete Part B)
Part B: Vehicle Maintenance Activity Monitorint: Requirements
Outfall
No.
Date
Sample
Collected
50050
1
00556
00530
00400
Total Flow
(if applicable)
Total
'R_ainfall
Oil & Grease "
(ifappl:)
Non -polar
O&G/TPH
(Method 1664
SGT-HEM); if
a 1.
Total
Suspended
Solids
pH
New,Motor
Oil Usage -
moldd/ -r
MG
inches
M10
m
unit
allm6
Not Apelleable
Form SWU-247, last revised 611212015
Page 1 of 2

STORMWATER DISCHARGE OUTFALL (SDO)
MONITORING REPORT
Permit Number NCS 000255
FACILITY NAME Grede 11-Biscoe, LLC
PERSON COLLECTING SAMPLE(S) Lorenzo Jackson
CERTIFIED LABORATORY(S) Pace Anatybeal Services Lab # 9151
Lab #
Part A: Specific Monitoring Requirements
SAMPLES COLLECTED DURING CALENDAR YEAR: 2018
(This monitoring report shall be received by the Division no later than 30 days from
the date the facility receives the sampling results from the laboratory.)
COUNTY Montgomery
PHONE NO. 9( 10 ) 428-2111 (ext._3268)
SIGNATURE OF PERKITTEE OR DESIGNEE
REQUIRED ON PAGE 2.
Outfall
No.
Date
Sample
Collected
50050
Total
Flow if a
Total
Rainfall
TSS
Oil & Grease
pH
mo/dd/ r
MG
inches
m L
mg/L
Standard
001
05/18/18
0.058
0.44
267
ND
002
05/18/18
0.002
0.44
153
ND
003
05/18/18
0.004
0.44
461
ND
001
06/27/18
0.060
0.46
6.93
002
06/27/18
0.002
0.46
7.02
003
06/27/18
0.004
0.46
7.37
ND = Non Detect
Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? oyes Ono
(if yes, complete Part B)
Part B: Vehicle Maintenance Activity Monitorina Requirements
Outfall
No.
Date
Sample
Collected
50050
00556
00530
00400
Total Flow
(if applicable)
Total'
Rainfall
Oil & Grease
(if appl.)
Non -polar
O&G1TPH
(Method 1664
SGT-HEM), if
apol.
Total
Suspended
Solids
pH
New Motor
Oil -Usage
mo/d Or
MG
inches
m
m
unit
gallmo
Not Applicable
Form SWU-247, last revised 611212015
Page 1 of 2

.;
STORM EVENT CHARACTERISTICS:
Date 5118I18
Total Event Precipitation (inches): 0.44
Event Duration (hours): 4.3 (only if applicable - see permit.)
(if more than one storm event was sampled)
Date 6I27118
Total Event Precipitation (inches): 0.46
Event Duration (hours): 0.3 (only if applicable - see permit.)
Mail Original and one copy to:
Division of Energy Mineral and Land Resources
Attu Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-16I7
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a
system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person
or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the
best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations."
(Signature of Permittee)
C,-?-5- I
(Date)
Form SWU-247, last revised 611212015
Page 2 of 2

JYN-29-2018 09:15A F'ROM:WAI 345349837 T0:19198076494 P.2
WILLOUG11BY &
ASSOCIATES, INC.
Envirunmsnta4 Health and Srfely 1M21 POORo4d,Sart FOWVA24551
June 29, 2018
North Carolina Department of Environmental Quality
Division of Energy Mineral and Land Resources
ATTENTION: Central Files
1617 Mail Service Center
Raleigh, NC 27699-1617
Re: Industrial Storm Water Discharge Monitoring Report
Grede TI, LLC
NPDES Permit NCS000255
Sir/Madam:
In accordance with NPDES Stormwater Permit NCS000255, Part TTT.E.1 and Part 111.E.2, Willoughby &
Associates, Inc., (WAT) is submitting to your office a Discharge Monitoring Report (DMR) for industrial stone
water monitoring conducted at Grade Tl, LLC during the monitoring period of October 1, 2017 -- June 30,
2018.
If any additional information is required, or should questions arise upon review, please contact me at
434.851.0293 or Mr. Lorenzo Jackson at 910.428.2111 (0268).
Sincerely,
W ,
e illoughby, CILMM,
President
Enclosure— Grade II —Biscoe, LLC Industrial Storm Water Discharge Monitoring Report
cc. Pile
Phone: [phone] www.waeb s.COM Fax: [phone]

9
S' R14WATER DISCHARGE OUTFAL L(SDO)
MONITORNG REPORT
Permit Number NCS 000255
FAMI7Y NAME Grede 11ascoe, LLC
PM SON COLLECt'�G SAMIFAS) Lamnzo Jackson
CF.RTHrMV I.ABORATORY(5) Pace Anahrllc:al Set foes Lab f 9151
Lab #
Part A: SpedBC Merftririg Regoiraments
SAMPLES COLLECTED DURING CALENDAR YEAEL- 2D18
(714is monitoring report shall he reeved by the i)iv wn no later than 30 days from
the date the fauTdy receives the sampling results from the laboratory.)
COUNTY Manta nmy
PHONE NO. (910 ) 428-2111 M 32E1S)
SIGNATURE OF PMMl ZE OR DFMGNEE
Rl•X)UIRED ON PAGE 2.
®
'� .+: :'+r'
� 5" • ' '.;�.1a "
n i f i
� i
®
� r. �
®
r r. ' r
r r_
Does this facility pmform Vehicle Maim nmce Activities using more than 35 gallons of new motor oil per month? Dyes .Ono
Cif yes, 0mviete Pats B)
Fart R- Vehiefe Maintmaaee Are;wity Monitarine Rw mfr&.r wnta
Outfall
No.
Dais
Sampbe
Collected
SDQSD
005%
09M
011M
Total Flory
(if applicable)
Total
R-hd6R
Oil do Creme
(if &ML)
Noa paw
O&GnM
(Method I664
SGT--BMUft if
TOW
Spipeaded
SoFds
PH
Neiv Motor
Oil uww
1waffliMir ING
iaiche4
malt
mo
Mat table
Farm 5WU-247, last mvised 6/12/26I3
Page L of 2
W
W
lD
m
W
-J
0
N
lA
N
W
m
m
JS
�n
v
W

STORMWATER DLSCl3ARGE OU'IVALL (SDO)
MONITORING REPORT
Pcrmit Number NCS 0002M
FAC JTY NAME Gmde 11-$%2m LLC
PERSON COLLECTING SAMPLEM Loamw ,ladman
CERTMM LABORATORY(S) Face AgLd cal Servkes Lab # 9151
Lib 0
Put A: Specific Monitoring Rcgnbvnw b
I
SAMPLES COLUKCT@D DURE4G CALENDAR YEAR: 2018
('Phis Monitoring report droll be recdved by the Division so bdw than 30 days from
the daft the Witty receives the slupling resort; from the lahoratury.)
COUNTY MorttQotjU
PHONE NO. 9(_ 1 428-211 ijeNL�3M
SIGNATURE OF PntMr TEE OR DESIGNEE
FAD ON PAGE 2.
Does this facility perform Vebele Maintcmnae Activities nsing more thm, 55 gallons of new motor all per month? Oyes Ow
(if yes, complete Part B)
Pert B: Veilde Maiowm=m Activity ?AmAr inv RAIaniremcutr
01130211
No.
Date
Sample
Colleetad
SM50
01556
00530
00400
TabI Pi lose
Qf gxplirabie)
'Total
Rohdall
OD & Grease
(if sppl )
Non-p
O&Grr H
(Method 1664
SGT-ice, if
TOM
Suspa dod
Solids
pH
New Motor
Oil Ussge
nWddhT
MG
i
unit
Not &pykabla
Fwm SWU-247, last reviwd W212015
Page l of 2

.C-4
STORM EVENT CHARACTERISTICS:
Daft 5118118
Total Event Pre oa (iaCheS): 0.44
$veal Du sdon (hours): 4"3 (only if applicable — see pen niL)
(If more term one Storm event was sampled)
Daft 6117118
Total Event Preciphzilm (mches)r 0.46
Evcat Duration (hours): 0.3 (only if applicable — see permit.)
Ma OrWad and use copy to
Dims m of EncW Mrmd and laud Rffmmw
Attu_ Caul Files
1617 Manz Savix Carter
Raleigh, Nor1b Cuolim 27699-1617
" I eeritfy, —d pcoafty of law, that this dome at and all *MWhments were prepared under my direction or mperviden In accordance with a
*,sh= designed to assure that gaaliiled persomnd Properly gatbeir aad eve hate the hdbrmabon snbmhtz& Based an my inquiry of the person
or persons who mom the system, or those persons directly responsible for gothrrine the imUrmnCk n, the informtion submb ed is, to the
best of M—kW 1edgt.reatLbeH4 true, ate -and comple4:.1-am aware that there are senif1cmi peaaElias 6f r Shut@ tmg false i$formatia
indading the pnssihflity of fines and imprizottmwt for knawiag viabdi nL"
(Si�nre oiPerwiYtrc) (Date)
Fotm 5WU-747, hmrcArad 611212015
Page 2 of 2
ro
T
Rl
m
co
m
lD
N
D
0
3
D
H
w
W
CD
W

JUN-29-2018 09:15A FROM:WAi 345349837 TO:19198076494 P.1
15421 Forest Road, Sulte A
Forest, VA 24551
PH: 434.534.9834
FX; 434.534.9837
Tas Energy Mineral and Land Resources Central Files From: J.E. Willoughby
Fax: [phone] Peeew 5 (Including cover)
Phone: Dates 06/29/18
Re: Grede Ii, LLC Storm Water DMR CCa
❑ Urgent X For Review ❑ Ploase Comment ❑ Please Reply ❑ Please Recycle
In accordance with NPDES Stormwater Permit NCS000255, Part III.E.1 and Part III.E.2, Willoughby &
Associates, Inc., (WAI) Is submitting to your office a Discharge Monitoring Report (DMR) for industrial
storm water monitoring conducted at Grede II, LLC during the monitoring period of October 1, 2017 --
June 30, 2018.
The DMR odginal'will be forwarded to your attention this date via standard mall.
Jeffrey E. Willoughby
President
WAI
434-851-0293

;f.
3ffi1WILLOU IiRy tic
ASSOC:IATIwS.INC_
Fnvirvnvw.n1a4 HraN and Safety 15421 Ft1lestRtmd, %tcA, FbmtVA24551
July 26, 2017
North Carolina Department of Environmental Quality
Division of Water Quality
Surface Water Protection Section
ATTENTION: Central files
1617 Mail Service Center
Raleigh, NC 27699-1617
Re: Industrial Storm Water Discharge Monitoring Report
Grede 11, LLC
NPDES Permit NCS000255
SirNadam:
RECEIVED
JUL 3 1 2011
CENTRAL EKES
DWR SECTION
In accordance with NPDES Stornnwater Permit NCS000255, Part III.E.I and Part III.E.2, Willoughby &
Associates, Inc., (WAI) is submitting to your office a Discharge Monitoring Report (DMR) for industrial storm
water monitoring conducted at Grede 11, LLC during the monitoring period of April 1, 2017 -- June 30, 2017,
If any additional information is required, or should questions arise upon review, please contact me at
434.851.0293 or Mr. Lorenzo Jackson at 910.428.2111 (0268),
Sincere]yoe
W'
Jel y E. illoughby, CHMM, REM
President
Enclosure — Grcdc 11— Biscoc, LLC Industrial Storm Water Discharge Monitoring Report
cc: File
Phone: [phone] www.wachaxom Fax: [phone]

STORMWATER DISCHARGE OUTFALL (SDO)
MONITORING REPORT
Permit Number NCS 000255 SAMPLES COLLECTED DURING CALENDAR YEAR: 2017
(This monitoring report shall be received by the Division no later than 30 days from
the date the facility receives the sampling results from the laboratory.)
FACILITY NAME Grede II, LLC (Formerly Citation Castings, LLC)
PERSON COLLECTING SAMPLE(S) Lorenzo Jackson
CERTIFIED LABORATORY(S) Pace Analytical Services, Inc. Lab #9151
Lab #
Part A: Specific Monitoring Requirements
COUNTY Montgomery
PHONE NO. 9( 10_) 428-2111(ext. 3268)
MREO
ATURE OF PERMITTEE OR DESIGNEE
UIRED ON PAGE 2.
Outfall
No.
Date
Sample
Collected
50050
Total
Flow if a
Total
Rainfall
COD
Phenols
Total Cd
Total Cu
TKN
Total Pb
mo/dd/ r
MG
inches
mill
m /L
m L
m L
m L
m L
001
06 22 17
0.00131
0.01
NS
NS
NS
NS
NS
NS
003
06 22 17
0.00009
0.01
NS
NS
NS
NS
NS
NS
S = Not Sam
led
Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? _yes X no
(if yes, complete Part B)
Part B: Vehicle Maintenance Activity Monitoring Requirements
Outfall
No.
Date
Sample
Collected
50050
00556
00530
00400
Total Flow
(if applicable)
Total
Rainfall
Oil & Grease
(if appl.)
Non -polar
O&GCfPH
(Method 1664
SGT-HEM), if
appl.
Total
Suspended
Solids
pH
New Motor
Oil Usage
mo/dd/ r
MG
inches
m
m
unit
al/mo
Not Applicable
Form SWU-247, Iasi revised 21212012
Page I of 2

STORM EVENT CHARACTERISTICS:
Date 06/22/17
Total Event Precipitation (inches): 0.01
Event Duration (hours): 11 min. (only if applicable— see permit.)
(if more than one storm event was sampled)
Date Not Applicable
Total Event Precipitation (inches):
Event Duration (hours): (only if applicable — see permit.)
Mail Original and one copy to:
Division of Water Quality
Ann: Central Files
1617 Mail Service Center
Raleigh, Forth Carolina 27699-1617
"1 certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a
system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person
or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the
best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations."
of
7 Z& /I z
(D te)
Form SW U-247, lust revised 212,12012
Page 2 of 2

06/08/2017 19:56 4345251446 WILLOUGHBY
PAGE 02/05
VVILLOUGHBY &
ASSOCIA'IT-S, INC.
,Eririro mMa4Hadrth=d.9&jiiy 1& ygkaa Sdic ForestVA14551
June 8, 2017
North Carolina Department of F-nvi)ronmental Quality
Division of Water Quality
Surface Water Protection Section
ATTENTION: Central Files
1617 Mail Service Center
Raleigh, NC 27699-1617
Re; Industrial Storm 'Water Discharge Monitoring Report
Grade 1I, LLC
NPDES Permit NCS000255
Sir/Madam:
RECEIVED
JUN 12 2017'
CENTRAL PILES
DIA/R SECTION
In accordance with NPDES Stormwater Permit NCS000255, Part 11I.E.1 and Part EZ.E.2, Willoughby &
Associates, Inc., (WAI) is submitting to your office a Discharge Monitoring Report (DMR) for industrial storm
water monitoring conducted at Grede Il, LLC during the monitoring period of April 1, 2017 — June 30, 2017.
If any additional information is required, or should questions arise upon review, please contact me at
434.851.0293 or Mr. Lorenzo Jackson at 910.428.2111 (x3268).
Sinc
4iekilloughby, CHMM, RE
President
Enclosure— Grede 1I -- Eiscoe, LLC industrial Storm Water Discharge Monitoring Report
cc: File
Phafte: 434.534,9834 — www.waehs.wra ---
Fax: [phone]

STORMWATER DISCHARGE OUTFALL (SDb)
P,lf)NrrORING WORT
Permit NumberNl'—S 000255
FACILMINAME Grede_l1,LLC(F-ormerJyCftat1 on Castings, UQ
PERSON CGLLECTINQ$AMFLJE(§) Lorenzo -Jac "son
CERTIFIED LAiB4jiZATORY($):Pace Ahalllfci&15,eNic:e ;-Inc- LA6#22,40-&633
—Lab A.
PFkrtA,Spe�ciTicMbuitejip Requirements
. .9 .
-SAMPLES COLLECTED DURING CAI;EKDARVEAR.. 2017
(This monitoring z.vp6.rt'sh9lJlie i4Ne ived byt#V!?fv.Wqp no later than-30 days from
the date the racility reettm the sam,ptkg results frem. the labomtoiyj
-U,ouNTy., -Mgt erne omery.
PHONE NO. (91D 5428-2111 (e)d. 32,6,87
SIG NATURE OF-PFRMITFEF, OR DESrGk&-
MYM ON.PAGE2., . I
Iff"d I - wo I Z mi-
III'
som-Am
MMKM�mmcu
Bell
DBEs this Facilityerfvrm Vehicle Muteoanae:Aetivities using mare laR55efl€rii4 of�tev�r mot4ril peij�lont}t? yes. X no
yes. M-pline p1q.rt B)
Part B. Vehicto Maintenance Attivity maaitovinmRequirtwebts
Outfol
Doti
Sample
Collected
.5005.0
005%
"Dwo
00460
Total Ft.%"
(Irslkpmv&14
TOW'
Rainfall
Od * Gviisi
(juippi)
14oz,,7pdkr
O&G/TPH
aDDL
Total
Sopended
Of
New motor
Oil uiss.ge
mwddlyi 1-mr,
I 1whes
I Wei[
unit
iVatA !cable
Fomn SWU-247, 1611 OwLsed-2,12012
Page [-of 2
r. CD
CD
CD
m

STORM EVENT CHARACTE1ZiS'i'LCS:
Date £14f /17 - 04/2-5/17
Totai Event Precipitation (inehcs)r 2.53
Event Duration (hours): 69.43_ (atilt' if"appticable- see permit:)
(if iuore than one siorm event was sampled).
Bate Not Applicable
Tahl.Event Pretloitstion (inches):
Event Duration (hours). (only. ifappliaable-Seepzrmit:}
SUB Original and we copy to:
b) vision of Water Quality
Atilt: Central riles
1617 Mail Service Crater
'Raleigh,. North CarolFisa.276994617-
"i certify, ieii.der penpity of law, that this document and oil aitsehments were prepared under my 4irecdoo or supervisign In eccorda.ace with a
sotein de4gsaed to ass.um that qualified personnel properly gather and evaluate the information submitted. Based on my inqudiy ofthe -person
or persons who manage ttie.syaterti; or these persons -directly responsible lergathering file inlatmation; lhe,lnt'oranatian submitted .is, to the
best afmy knorvlcdgt and Mief, true, aerurate, aad contple#e. [.aid awarethat.tbeMare slgufiesnt pc;ttties far submitting 6bc information,
includiag the passibility of fines and imprisoAmeat for knowing viotations."
(Signature of Permittee) (Date)
D
M
m
Foust-Sti U-247,iarrrevlsedl2�21011 CD
cn
se 2 of-2
- m
to

06/08/2017 19:56 4345251446
15421 Forest Road, Sulte A
Forest, VA 24551
PH; 434.534.9834
FX; 434,534.9837
LM
WILLOUGHBY
To: Surface Water Protection Central Files From: J.E. Willought
Face 919-807-6498 Wages: 5 (including cover)
Date: 06/08/17
Re: Grede 11, LLC Storm Water fOMR CC:
❑ Urgent X For Review ❑ Please Comment ❑ Please Reply ❑ Please ROLyde
PAGE 01/05
In accordance with NPDES Stormwater Permit NC8000255, Part III.E.1 and Part 11I.E.2, Willoughby &
Associates, Inc., (WAI) is submitting to your office a Discharge Monitoring Report (DMR) for industrial
storm water monitoring conducted at Grede 11, LLC during the monitoring period of April 1, 2017 — June
30, 2017.
The DMR original will be forwarded to your attention this date via standard mail,
Jeffrey E. Willoughby
President
WAI
434-851-0293

08/10/2016 17:14 4345251446 WILLOUGHBY PAGE 01/05
IN,14,
15421 Forest Road, Suite
Forest, VA 24551
PH: 434.534.9834
FX: 434.634.9537
RECEIVED
ftx AUG I 1 Z016
TRAL FILES
DWR SECTION
7b: Surface Water Protection Central Files From. J. E. Willcughb
Fax: 91M07.6498 Pageso 5 (including cover) (Submitted twice)
Phone.
Date. 08/10/16
Re. Grade II, LLC Storm Water DMR CC:
0 Urgent X For Review © Please Comment ❑ Please Reply O Please Recycle
In accordance with NPl7ES Stormwater Permit NCS000255, Part III.E.1 and Part IILE.2, Willoughby &
Associates, Ina, (WAI) is SUbmitting to your office a discharge Monitoring Report (DMR) for industrial
storm water monitoring conducted at Grade II, LLC during the monitoring period of April 1, 2016 — June
30, 2016,
The DMR original will be forwarded to your attention this date via standard mail.
Jeffrey E. Willoughby
President
WAI
434-851-0293

STORMWATER DISCHARGE OUTFALL (SDO)
MONITORING REPORT
Permit Number NCS 000255 SAMPLES COLLECTED DURING CALENDAR YEAR: 2016
(This monitoring report shall be received by the Division no later than 30 days from
the date the facility receives the sampling results from the laboratory) ,
FACILITY NAME Grede li, LLC (Formerly Citation Castings, LLC
PERSON COLLECTING SAMPLES) Lorenzo Jackson
CERTIFIED LABORATORY(S) Pace Analytical Services, Inc. _i ah # 12, 40 & 633
Lab #
Part A; Specific Monitoring Requirements
COUNTY MontRonlery _
PHONE NO. 4( 10 } 428-2111 (ext. 3268)
SIGNATURE OF PERMT]rrEg OR DESIGNEE
REQUIRED ON PAGE 2.
Ouffatb
No.
Date : r :rx::
::SitiJ$Ie _
Collected
-.50050
Totil
:'Flow fif-a .
Toth - �
:Rainfall
COD.,
P�ienols . _
. _Total Cd
Tatal Cu,
= TKN
Total Pb..
mold
MG.
tncbes
m L
m L ,::
mg L
mg L
_rug Lg
� L -
001
05 28 16
0.1011
0.77
45.0
0.077
<0.001
0.0787
2.6
0.0234
003
06 28 16
0.0072
0.77
212
0.030
<0.001
0.0315
1.2
0,0063
r— I V
C
t-
Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month?
(if yes, complete Part B)
Part B: Vehicle Maintenance Activity Monitoring Requirements
uvwm or_u 11UN
yes X no
Outfail .- =-
}Date x
5Q050
D1iS5b
00538 - =
00400
'No.
Sainple
Total Flow
_Total' F_
Oil & Grease'-
Non -polar!'
Total
gA
View i4lotar
Collectgil. =. "
(if applicable)
Balrifall -
(If apply:
O&C#PH.
Suspended .. _
Oct] Usage
{Meihod;1664 '
Solids
5GT=HF�MJ 5f
mold . _
MO
fach
m
ma
unit
javrno z
Not Applicable
Form SWU 247, last revised 21212012
Page 1 of 2
m
N
m
rQ
m
N
07
H
r
r
0
C
G)
31
ad
G)
m

STORM C, VMT CHARACTERISTICS:
Dn1e €16/28/16
"Total Event Precipitation (iarhes): 0.77
Event Du r :shots (lours): 6.62 jonly if applicable —see permit.)
(ir more than one storm event seas sampled)
Date Not Applicable
Total Event Precipitation (inches):
Event Duration (hours): ______(only if applicable --see permit)
Mail Original and one copy to:
Division of Water Qnality
Attu: Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
"I certify, nudcr penalty of law, that this document and all attaelzments were prepared under my Wrection or supervision its accordance With a
system designed to assure that qualified personnel properly gather and evaluate the informatiou submitted. Based on my inquiry of the peisan
or persons Wire 4nanage the system, or those persons directly responsible for gathering the Information, the information submitted is, to the
best of my knowledge and belief, true, ncctarate, and complete 1. am aware that there are significantpennities for submitting false information,
including the possibility of fines and imprisonment for knowing v lolntioos."
AV 116
(Signature of Permittee) (slate)
Form SWO-217, last revised 2Y2':'3012
.Page 2 of 2
La
A
Ln
N
UI
Z'
a
m
n
G)
m
La
Ln
La
cn

11�
STORMWATER DISCHARGE OUTFALL (SDO)
MONITORING REPORT
Permit Number NCS 000255
FACILITY NAME Grede 11, LLC (Formerly Citation Castings, LLC)
PERSON COLLECTING SAMPLE(S) Lorenzo Jackson
CERTIFIED LABORATORY(S) Pace Analytical Services, Inc. Lab # 1_ 2 40 & 633
Lab #
Part A: Specific Monitoring Requirements
SAMPLES COLLECTED DURING CALENDAR YEAR: 2016
(This monitoring report shall be received by the Division no later than 30 days from
the date the facility receives the sampling results from the laboratory.)
COUNTY Montgomery
PHONE NO. 9( 10 ) 428-2111(ext. 3268)
SIGNATURE OF PERMITTEE OR DESIGNEE
REQUIRED ON PAGE 2.
IL"I
{iLEI
r
_i
r y
If
Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? _yes X no
(if yes, complete Part B)
Part B: Vehicle Maintenance Activity Monitorine Requirements
'Outfall
Date
50,050
_ _
©0556 ._�
�.
KAZW
{00530'0040©:,
No.,
'
Sample,
;Total Flow
�To 1 : `
Oil &Grease
INon p lar
-.
i ial
pH ' '
New 119ofor
Collecte d
(dapphcable}:=
Rainfall
(if apply
OPN
,Suspended .
Oil Usage
�'
F
(Method 1664
°Solids
..
SGT-H .1Vj[R-1if
Q
Y
=a 1.
;t:
,OIL
lmol'd'dl ,:.
MCA"
inehes _.
:<
�m:.;
unit
llrno
Not Applicable
Form SWU-247, last revised 21212012
Page I of 2

STORM EVENT CHARACTERISTICS:
Date 06/28/16
Total Event Precipitation (inches): 0.77
Event Duration (hours): 6.62 (only if applicable —see permit.)
Oftnore than one storm event was sampled)
Date Not Applicable
Total Event Precipitation (inches):
Event Duration (hours): _ (only if applicable — see permit.)
Mail Original and one copy to:
Division of Water Quality
Ann. Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
"I certify, tinder penalty of law, that this document and all attachments ►were prepared under my direction or supervision in accordance with a
system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person
or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the
best of my knowledge and belief, true, accurate, and complete. 1 am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations."
(Signature of Permittee) (Date)
Form SWU-247, last
Page 2 of 2

VVILLOUGHBY &
ASSOCIATES, INC.
F,,,,' menlad Heallh and Safely 15421 FotwLto StritCA)+omIVA24551
August 10, 2016
North Carolina Department of Environmental Quality
Division of Water Quality
Surface Water Protection Section
ATTENTION: Central Files
1617 Mail Service Center
Raleigh, NC 27699-1617
Re: Industrial Storm Water Discharge Monitoring Report
Grede II, LLC
NPDES Permit NCS000255
Sir/Madam:
In accordance with NPDES Stormwater Permit NCS000255, Part I1I.E.1 and Part III..E.2, Willoughby &
Associates, Inc,, (WAI) is submitting to your office a Discharge Monitoring Report (DMR) for industrial storm
water monitoring conducted at Grede I1, LLC during the monitoring period of April 1, 2016 — June 30, 2016.
If any additional information is required, 'or should questions arise upon review, please contact me at
434.851.0293 or Mr. Lorenzo Jackson at 910,428.2111 (x3268).
Sincer
L1C��
Jeffrey E. Willoughby, CHMM, REM
President
Enclosure — Grede II — Biscoe, LLC Industrial Storm Water Discharge Monitoring Report
cc: File
Phone: `434.534.9834 www.waehs.com Fax: [phone]

Permit Number NCS, •i
STORMWATER DISCHARGE OUTFALL (SDO) prz
MONITORING REPORT
SAMPLES COLLECTED DURING CALE A Y 0
(This monitoring report shall be received by the Division no later than 30 days from
the date the facility receives the sampling results from the laboratory.)
FACILITY NAME GREDE II COUNTY MONTGOMERY
PERSON COLLECTING SAMPLE(S) TIM MCCASKILL PHONE NO. [phone]
CERTIFIED LABORATORY(S) PACE Lab #�633
Lab #
SIGNATURE OF PERMITTEE OR DESIGNEE
REQUIRED ON PAGE 2.
Part A: Specific Monitoring Requirements
Outfall
No.001
DateII
SampleTotal
Collected
I
Flow (if :,,
':
IIIOZ.
I I
I
Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month?_ yes X_no
(if yes, complete Part B)
C�
Part B: Vehicle Maintenance Activity Monitoring Requirements
Outfall
No.
Date
Sample
Collected
50050
00556
00530
00400
Total Flow
(if applicable)
Total
Rainfall
Oil & Grease
(if appl.)
Non -polar
O&G/TPH
(Method 1664
SGT-HEM), if
appl.
Total
Suspended
Solids
pH
New Motor
Oil Usage
molddl r
MG
inches
m VA
m
unit
allmo
NA
NA
NA
NA
NA
NA
NA
NA
NA
Form SWU-247, last revised 21212012
Pagel of 2

STORM EVENT CHARACTERISTICS: Mail Original and one copy to:
Division of Water Quality
Date _10110115 Attn: Central Files
Total Event Precipitation (inches): _0.4 in 1617 Mail Service Center
Event Duration (hours): _1.0_(only if applicable - see permit.) Raleigh, North Carolina 27699-1617
(if more than one storm event was sampled)
Date NA
Total_Event Precipitation (inches):
Event Duration (hours): (only if applicable - see permit.)
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a
system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person
or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the
best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations."
i Jr-� �� lx,� /06 Zd/sue
(Si nature of Permittee) (Dat
Richard Cabadas
Form SWU-247, last revised 21212012
Page 2 of 2

WII,LOUGHBY &
ASSOCIATES. INC.
E:uaironmenr4 Ninth and SgfeV
October 26, 2015
Grede 11- Biscoe, LLC
Mr. Chuck Wolffls
530 East Main Street
Biscoe NC 27209
rcy000a5F-
Final Report
WAI EHS
15421 Forest Road Order No: 92271485
Suite A
Forest, VA 24551 Client: Grede II - Biscoe LLC
Ph: 434-45"919
Fax: [phone] Project: October 2015 Storm Water Sampling
Event
RE: Project: October 2015 Storm Water Sampling Event
WAI Order: 92271485
Dear Mr. Wolffis:
Enclosed are the analytical results for samples received on October 13, 2015.
These results conform to the most current NELAC standards unless otherwise indicated.
Results are only reflective of the conditions during the sample(s) collection date(s) and
time(s).
If you have any questions concerning this report, please feet free to contact me.
office tupemlior Analytical Report:19 Pages
tiffany.lambert9waehs.com Chain of Custody: i Page
,w waea NCDENR Form: 2 Pages
ba• �f SCU Receipt:1 Page
Total: 22 Pages
REPORT OF LABORATORY ANALYSIS
This report sets forth the results of outsourced laboratory analysis of samples delivered to WAI EHS and shall not be construed as a
representation by WAI EHS as to the source or method of procuring such samples. Ail reports are submitted as confidential property of
the then and authorization for publication of any statements contained In our reports Is reserved pending WAt EHS Issued written consent.

Project: OREDE 11-BISCOE, LLC
Pace Project No.: 92271485
Charlotte Certification IDS
9800 Kincey Ave. Ste 100, Huntersviile, NC 25078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #; 99000001
Asheville Certification IDS
2225 Riverside Drive, Asheville, NC 28804
FioridalNELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #; 37712
Eden Certification IDs
205 East Meadow Road Suite A, Eden, NC 27288
North Carolina Drinking Water Certification #: 37738
CERTIFICATIONS
FloridalNEIAP Certification #: E87627
Kentucky UST Certification #: 84
West Virginia Certification #: 357
VirginiaNELAP Cer6Bcation #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification M 99030001
West Virginia Certification #: 356
MrginiaNELAP Certification #: 480222
North Carolina Wastewater Certification #: 633
VirginiaNELAP Certification #: 460025
REPORT OF LABORATORY ANALYSIS
Willoughby & Associates, Inc.
16421 Forest Road, Suite A
Forest, VA 24551
Phone:[phone] Fax:[phone]
Page 2 of 22

SAMPLE SUMMARY
Project: GREDE II-BISCOE. LLC
Pace Project No.: 92271485
Lab ID
Sample ID
Matrix
Data Collected
Date Received
92271485001
570062 OUTFALL 001
Water
10/10115 08:15
10/13/15 10:00
92271485002
474458 OUTFALL 001
Water
10/10/15 08:32
10/13115 10:00
92271485003
951299 OUTFALL 001
Water
10/10/15 08:25
10/13/15 10:00
92271485004
570012 OUTFALL 001
Water
10/10/15 08:20
10113/15 10:00
92271485005
973005 OUTFALL 001
Water
10/10/15 0810
10/13/15 10:00
92271485006
643122 OUTFALL 001
Water
1011CV15 08:37
10/13/15 10:00
REPORT OF LABORATORY ANALYSIS
Willoughby & Associates, Inc.
15421 Forest Road, Suite A Page 3 of 22
Forest, VA 24551
Phone:[phone] Fax:[phone]

SAMPLE ANALYTE COUNT
Project: GREDE II.8ISCOE, LLC
Pace Project No.: 92271485
Lab ID
Sample ID
Method
Analysts
Analytes
Reported
Laboratory
92211485001
510062 OUTFALL 001
SM 5220D
WRC
1
PASI-A
92211485002
474456 OUTFALL 001
EPA420.4
DMN
1
PASI-A
92271485003
951299 OUTFALL 001
EPA 2001
COF
5
PASI-A
92271485004
570012 OUTFALL 001
EPA 351.2
SER
1
PASI-A
92271485005
973005 OUTFALL 001
SM 25400
KCE
1
PASI-E
92271495006
643122 OUTFALL 001
EPA 16648
JMS
1
PASI-C
REPORT OF LABORATORY ANALYSIS
Willoughby & Associates, Inc,
15421 Forest Road, Suite A Page 4 of 22
Forest, VA 24551
Phone:[phone] Fax:[phone]
hL

ANALYTICAL RESULTS
project: GREDE II-BISCOE, LLC
Pace Project No.: 92271485
Sample: 570062 OUTFALL 001 Lab ID: 92271485001 Collected: 10110I15 08:15 Received: 101i 3fi510:00 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
5220D COD Analytical Method: SM 5220D
Chemical Oxygen Demand ND mg/L 25.0 12.5 1. 10/20/1510:00
REPORT OF LABORATORY ANALYSIS
Willoughby & Associates, Inc.
15421 Forest Road, Suite A Page 5 of 22
Forest, VA 24551
Phone:[phone] Fax:[phone]

ANALYTICAL RESULTS
Project: GREDE II-BISCOE, LLC
Pace Project No.: 92271485
Sample: 474456 OUTFALL 001 Lab ID: 92271485002 Collected: 10/10115 08:32 Received: 10/13/1510:00 Matrix: Water
Report
Parameters Results Units Limit MDL OF Prepared Analyzed CAS No. Qual
420.4 Phenolics, Total Analytical Method: EPA 420.4
Phenol 0.073 mg/L 0.010 0,0050 1
REPORT OF LABORATORY ANALYSIS
Willoughby & Associales. Inc.
15421 Forest Road, Suite A
Forest, VA 24551
Phone:[phone] Fax:[phone]
I M1115 10:58 108-95-2
Page B at 22

ANALYTICAL RESULTS
Project: GREDE il•BISCOE, LLC
Paco Project No.: 92271485
Sample: 951299 OUTFALL 001
Lab ID: 92271485003
Coilected:
10/10/15 08:25
Received: 10/1311610:00 Matrix: Water
Report
Parameters
Results
Units
Limit
MOIL
OF
Prepared
Analyzed CAS No, Qual
200.7 MET 1CP
Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
Cadmium
NO
ug/L
1.0
0.50
1
10/16/15 19:00
10/19/15 23:15 7440.43-9
Copper
35A
ug/L
5.0
2.5
1
10/16/15 19:00
10/19115 23:15 7440-50-8
Lead
7.2
ug/L
5.0
2.5
1
10/16/15 19:00
10/19/15 23:15 7439-92-1
Nickel
13.1
ug/L
5.0
2.5
1
10/16115 19:00
10119/15 2115 7440-02-0
Zinc
294
ug/L
10.0
2.5
1
10/16/15 19:00
10/19/15 23:15 7440-66-6
REPORT OF LABORATORY ANALYSIS
Willoughby & Associates, Inc.
15421 Forest Road. Suite A Page 7 of 22
Forest, VA 24551
Phone:[phone] Fax:[phone]

ANALYTICAL RESULTS
Project: GREDE II-BISCOE, LLC
Pace Project No.: 92271485
Sample: 570012 OUTFALL 001 Lab ID: 92271485004 Collected: 10/10115 08:20 Received: 10113/15 10:00 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Ouai
351.2 Total Kjeldahl Nitrogen Analytical Method: EPA351.2
Nitrogen, Kjeldahl, Total 3.2 mg1L 0.50 0.25 1 10/22/15 06:42 7727-37-9
REPORT OF LABORATORY ANALYSIS
Willoughby 6 Associates, Inc.
15421 Forest Road. Suite A
Forest, VA 24551
Phone:[phone] Fax:[phone]
Page 8 of 22

ANALYTICAL RESULTS
Project: GREDE 11-81SCOE, LLC
Pace Project No.: 92271485
Sample: 973005 OUTFALL 001 Lab ID: 92271485005 Collected: 10/10/15 08:10 Received: 10/13/1510:00 Matrix: Water
Report
Parameters Results Units Limit MDL OF Prepared Analyzed CAS No. Qual
2540D TSS, Low -Level, Eden Analytical Method: SM 2540D
Total Suspended Solids 501 mg1L 11.1 11.1 1 10/13115 11:41
REPORT OF LABORATORY ANALYSIS
Willoughby & Associates, Inc.
15421 Forest Road, Suite A Page 9 of 22
Forest, VA 24551
Phone:[phone] Fax:[phone]

ANALYTICAL RESULTS
Project: GREDE II•BISCOE, LLC
Pace Project No.: 92271485
Sample: 643122 OUTFALL 001 Lab ID: 92271485006 Collected: 10/10/15 08:37 Received: 1 D11311510:D0 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Quaff
HEM, Oil and Grease Analytical Method: EPA 1664B
Oil and Grease ND mg1L 5.0 1.1 1 10/22/15 08:32
REPORT OF LABORATORY ANALYSIS
Willoughby & Associates, Inc.
15421 Forest Road, Suite A Page 10 of 22
Forest, VA 24551
Phone:[phone] Fax:[phone]

QUALITY CONTROL DATA
Project: GREDE II-BISCOE, LLC
Pace Project No.: 92271485
QC Batch: EDEN/20323 Analysis Method: SM 2540D
QC Batch Method: SM 2540D Analysis Description: 2540D TSS, Low Level, Eden
Associated Lab Samples: 92271495005
METHOD BLANK: 1581173 Matrix: Water
Associated Lab Samples: 92-271485005
Blank Reporting
Parameter Units Result Limit MDL Analyzed Qualifiers
Total Suspended Solids mg1L ND 1.0 1.0 10IM1511:34
LABORATORY CONTROL SAMPLE: 1581174
Spike LCS LCS % Rec
Parameter Units Cane. Result % Rec Limits Qualifiers
Total Suspended Solids mglL 250 230 92 90-110
SAMPLE DUPLICATE; 1581175
92271288005 Dup Max
Parameter Units Result Result RPD RPD Qualifiers
Total Suspended Solids mglL 2970 3180 7 5 D6
SAMPLE DUPLICATE: 1581176
92271279008 Dup Max
Parameter Units Result Result RPD RPD Qualifiers
Total Suspended Solids mg1L 3070 3250 8 5 D6
Results presented on this paps are In the units indlotod by Me" Unne' eetumn except where an alternate unit In presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
Willoughby & Associates, Inc.
15421 Forest Road. Suite A Page 11 of 22
Forest, VA 24551
Phone:[phone] Fax:[phone]

QUALITY CONTROL DATA
Project: GREDE II-BISCOE, LLC
Pace Project No.: 92271485
QC Batch: GCSV122974 Analysis Method: EPA 1664E
QC Batch Method; EPA 1664B Analysis Description: 1664 HEM, Oil and Grease
Associated Lab Samples: 92271485006
METHOD BLANK: 1588629 Matrix; Water
Associated Lab Samples: 92271485006
Blank Reporting
Parameter Units Result Limit MDL Analyzed Qualifiers
Oil and Grease mg/L ND 5.0 1.1 10=15 08:24
LABORATORY CONTROL SAMPLE: 1588630
Spike LCS LCS % Rae
Parameter Units Cone. Result % Rec Limits Qualifiers
Oil and Grease mg1L 40 35.9 90 78-114
MATRIX SPIKE SAMPLE: 1588631
92271022001 Spike MS MS % Rec.
Parameter Units Result Cone. Result % Rae Limits Qualifiers
Oil and Grease mg1L NO 40 34.3 86 78-114
Results presented on this page are In the units Indicated by the -units" column except when an alternate unit to presented to the right a( the result.
REPORT OF LABORATORY ANALYSIS
Willoughby 8 Associates, Inc.
15421 Forest Road, Suite A Page 12 of 22
Forest, VA 24551
Phone:[phone] Fax:[phone]

QUALITY CONTROL DATA
Project: GREDE II-BISCOE, LLC
Pace Project No.: 92271485
OC Batch: MPRP119825
Analysis Method:
EPA 200.7
QC Batch Method: EPA200.7
Analysis Description:
200.7 MET
Associated Lab Samples: 92271485003
METHOD BLANK: 1584611
Matrix: Water
Associated Lab Samples: 92271485003
Blank Reporting
Parameter
Units
Result Limit
MDL
Analyzed Qualifiers
Cadmium
ug/L
ND
1.0
0.50
10/19115 22:32
Copper
ug/L
ND
5.0
2.5
10/19/15 22:32
Lead
uglL
ND
5.0
2.5
1011911522:32
Nickel
ug/L
ND
5.0
2.5
10/1911522:32
Zinc
ug/L
ND
10.0
2.5
10/1911522:32
LABORATORY CONTROL SAMPLE:
1584612
Spike
LCS
LCS
% Rec
Parameter
Units
Canc.
Result
% Rec
Limits QuafiFlers
Cadmium
ug1L
56D
477
95
85-115
Copper
ug/L
500
477
95
85-115
Lead
ug/L
500
476
95
85-115
Nickel
ug/L
500
477
95
85-115
Zinc
ug1L
500
473
95
85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 15$4613
1584614
MS
MSD
92271625002
Spike
Spike
MS
MSD
MS
MSD
% Rec
Max
Parameter
Units
Result
Canc.
Canc.
Result
Result
% Rec
% Rec
Limits
RPD
RPD Qua$
Cadmium
ug1L
ND
500
500
472
537
94
107
70.130
13
20
Copper
ug/L
30.1
500
500
503
579
94
110
70-130
14
20
Lead
uglL
ND
500
500
464
526
92
104
70.130
12
20
Nickel
ug/L
ND
500
500
467
- 529
93
105
7DA30
13
20
Zinc
ug/L
46.3
500
500
510
573
93
105
70-130
12
20
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1584815
1584616
MS
MSD
92271789001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Max
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
RPD Qual
Cadmium
ug/L
2.2
500
500
465
466
93
93
70-130
0
20
Copper
ug1L
763
500
600
1210
1190
91
87
70-130
2
20
Lead
ug/L
35.6
500
500
467
467
86
86
70-130
0
20
Nickel
ug/L
46.1
500
500
489
488
89
88
70-130
0
20
Zinc
ug/L
1450
500
500
1880
1880
85
81
70-130
1
20
Results presented an this page are in the units Indicated by the 'Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
Willoughby & Associates, Inc.
15421 Forest Read, Suite A Page 13 of 22
Forest, VA 24551
Phone:[phone] Fax:[phone]

QUALITY CONTROL DATA
Project: GREDE II-BISCOE, LLC
Pace Project No.: 92271485
QC Balch: WETA125052 Analysis Method: EPA 351.2
OC Batch Method: EPA 351.2 Analysis Description: 351.2 TKN
Associated Lab Samples: 92271485004
METHOD BLANK: 1687321 Matrix: Water
Associated Lab Samples: 92271485004
Blank Reporting
Parameter Units Result Limit
Nitrogen, Kjeldahl, Total mg/L ND 0.50
LABORATORY CONTROL SAMPLE: 1587322
Spike LCS
Parameter Units Conc, Result
Nitrogen, Kjeldahl, Total mglL 10 9,2
MDL Analyzed Qualifiers
0.25 10/22l15 06:35
LCS % Rec
% Rec Limits Qualifiers
92 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1587323 1587324
MS MSD
92271317005 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Cons. Result Result % Rec % Roc Limits RPD RPD Qual
Nitrogen, Kjeldahl, Total mg/L ND 10 10 10 10.7 96 104 90-110 7 10
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1687325 1587326
MS MSD
92272182003 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc, Conc. Result Result % Rec % Rec Limits RPD RPD Qual
Nitrogen, Kjeldahl, Total mg1L 212 200 200 415 411 101 99 90-110 1 10
Results presented an this page pre In the whits Indicated by the "UrIlks" column except where an altsmis unit is presented to the right of the must.
REPORT OF LABORATORY ANALYSIS
Willoughby & Associates, Inc.
15421 Forest Road, Suite A Page 14 of 22
Forest, VA 24551
Phone:[phone] Fax:[phone]

QUALITY CONTROL DATA
Project: GREDE II-BISCOE, LLC
Pace Project No.: 92271485
QC Batch: WETAl25006 Analysis Method: EPA 420.4
OC Batch Method: EPA 420.4 Analysis Description: 420A Phenolics
Associated Lab Samples: 92271485002
METHOD BLANK: 1585283 Matrix: Water
Associated Lab Samples: 92271485002
Blank Reporting
Parameter Units Result Limit MDL Analyzed Qualifiers
Phenol mglL ND 0.010 0.0050 10/21/15 %50
LABORATORY CONTROL SAMPLE: 1585284
Spike LCS LCS % Rea
Parameter Units Cone. Result % Rea Limits Qualifiers
Phenol mglL .05 0.050 99 90-110
MATRIX SPIKE 8r MATRIX SPIKE DUPLICATE: i585285 1585286
MS MSD
92272068011 Spike Spike MS MSD MS MSD % Roe Max
Parameter Units Result Cone. Cone. Result Result % Rec % Rea Limits RPD RPD Qual
Phenol mg/L NO .05 .05 0.051 0.054 Be 91 90-110 5 10 Mi
Results presented on this page ore in the units Indicated by the "Units" column except where an etiernote unit la presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
Willoughby & Associates, Inc.
15421 Forest Road, Suite A
Forest, VA 24551 Page 15 of 22
Phone:[phone] Fax:[phone]

QUALITY CONTROL DATA
Project: GREDE II-BISCOE, LLC
Pace Project No.: 92271485
OC Batch: WETAI25030 Analysis Method: SM 5220D
OC Batch Method: SM 5220D Analysis Description: 5220D COD
Associated Lab Samples: 92271485001
METHOD BLANK: 1586259 Matrix: Water
Associated Lab Samples: 92271485001
Blank Reporting
Parameter Units Result Limit MDL Analyzed Qualifiers
Chemical Oxygen Demand mg/L ND 25.0 12.5 10/2011510:00
LABORATORY CONTROL SAMPLE: 1586260
Spike
LCS
LCS
% Rec
Parameter Units
Cone.
Result
% Rec
Limits Qualifiers
Chemical Oxygen Demand mg&
750
739
99
90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1586261
1588262
MS
MSD
92272048003
Spike
Spike MS
MSD
MS MSD % Rec Max
Parameter Units Result
Cone.
Cone. Result
Result
% Rec % Rec Limits RPD RPD Qua$
Chemical Oxygen Demand mg/L 160
750
750 792
792
84 84 90-110 0 3 M1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1686263 1686264
MS MSD
92271627001 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD RPD Oual
Chemical Oxygen Demand mg/L 904 1500 1500 1480 1480 39 39 90.110 0 3 M1
Asulb presented on this Pape are In the units Indicated by the "Units" column except when an alternate unit Is presented to the fight or the result.
REPORT OF LABORATORY ANALYSIS
Willoughby & Associates, Inc.
15421 Forest Road, Suite A Page 16 of 22
Forest. VA 24551
Phone:[phone] Fax:[phone]

QUALIFIERS
Project: GREDE II-BISCOE, LLC
Pace Project No.: 92271485
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL-Adjusted Method Detection LImiL
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2•Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chlomethylvinyl ether. Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrofein and Acryfonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI arxredtted. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC institute.
LABORATORIES
PAST -A Pace Analytical Services - Asheville
PASI-C Pace Analytical Services - Charlotte
PASI-E Pace Analytical Services - Eden
ANALYTE QUALIFIERS
D6 The relative percent difference (RPD) between the sample and sample duplicate exceeded laboratory control limits.
M1 Matra spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
REPORT OF LABORATORY ANALYSIS
Willoughby & Associates, Inc.
15421 Forest Road, Suite A Page 17 of 22
Forest, VA 24551
Phone:[phone] Fax:[phone]

QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: GREDE [I-BISCOE, LLC
Pace Project No.: 92271485
Analytical
Lab In Sample ID QC Batch Method QC Batch Analytical Method Batch
92271485005
973005
OUTFALL 001
SM 2540D
EDEWI20323
92271485006
643122
OUTFALL OD
EPA 1604B
GCSV/22974
92271485003
951299
OUTFALL 001
EPA200,7
MPRP/19825 EPA 200.7 ICP117879
92271485004
570012
OUTFALL 001
EPA361.2
WETA125052
92271485002
4T4456
OUTFALL 001
EPA 420.4
WETA1250D6
92271485001
570062
OUTFALL 001
SM 5220D
WETA(25030
REPORT OF LABORATORY ANALYSIS
Willoughby & Associates. Inc.
15421 Forest Road. Suite A Page 18 of 22
Forest. VA 24551
Phone:[phone] Fax:[phone]

UGHBY
oAMr &
AM
Analytical Request and Chain of Custody Form
gas y
WAICkdwfse.:
15421 RMW Road, Subs A
Paas 1 or 1
Forest, VA 24551
Order Compkts7lCbde) Ter No
latortnatiDri: PM
lttrorrttatloet
C o�ract NI
TSrm Arrxaed Tbae Ragaest
Sepndand a Day as Days}
7-9 asgNr,a:, Day Rosh (_Days)
46 am*" a Day Rosh L—Da")
t3 ausbass Day RMA C—DaTsl
Ow. ^IP.A d-wnwnrmmawireaamwran
OM
CAmpany: Grade IN - a Ur
C=P w.
WMO & Associates Inc.
ntion: Many larnbed
Attention:
MuWtambert
Address: 15421 Forest Road Suite A
mn:
LWI Forest Road Suite A
SUM Zip: VA 24551
G% Sute, ZIP
VA 24551
eliphone: 434 4SS0919
etePhO—
434 4SS-0929
Fax: [phone]a37
Fax:
434 534 9837
Enlaik tHtamr.lambertA4waehLM
Env&
tft Mtlam
Prood Ramp
Sample Type
CoOefon Qatar / Tbaes
Grade tl - ftwoe "
ID15b+dSmai•Amtual
'�
s>.oree+w
�
g
�
�
-b
mMo,>aa�
� �
� �
�
�
Sample
Ltxatton m pD
3 t3
e3
S
S
A
!3
Outran 001
X
i,P e
w
ST
P
i
H2SO4
COD
Outtallool
X
g•3 it Q
ST
G
1
H1SOi
Phenol
rI -to -
Outrailo0l
X
6-0-
1
ST
P
L
HNO3
Total Cadmium, Copper, lead, Nickel &Zinc
4 AP
Outran 002
X
is 0
ST
P
1'
H2SO4
TKN
{ C
Outrall001
X
� ( t45T011001
P
1
N/A
TSS
-{
Outr
X
j7
G
1
HO
Oil&Grease
OMR (UhualRy), duo by ;date}
) (Name & sFycatarer a Time)
QA/QC Padngp Request (please *de ons1: I a
In IV Clrstom
/� ���%
am 11i `GK % A c"w-- / �a ' / � D
m Supply ddotiewtad7 Yes No
I tww bll (�0. DOta aVOW)
v7_, l�I ✓ter"/[•f' 0
RLS CL PPM
Rece wd (Slaeatruw, Data &Taf)
,? ra f
by . Date & Ttma}
Rewired (S�WMV, Date a Thee)
famyfaeeva m a dbpoead d w Dare aRa time of trcetpt, uNan shy an for BAor a 6a+,dltfF, er uNm euwnaba ;;Noel.
aample mspos-4. O Phan dwA ham d cUm wild aka to mW n=n* 6o Oaye aleet tab's cmipt. (I►box is net chwJw , fab w61 dFspnae of um* 60 dop aPoar tab eaaiPL)
Q Pben check hm of caeca would 0h lab to mbkt w mple beer then 60 D"-L (Phan h*" thh appeowtd wNh ttw bb, ar bm Is rot dweked tab anti dnrpeo of amph 60l4s dtu lab n Ipt)
AddRional Notn/Cw m Wz
-
.

�#V
WCDF R
Stormwater Discharge Outfall (SOO)
Qualitative Monitoring Report
Forguidance on filling out this form, please visit:
Permit No.: RX/s./.QI-0I_/0tI010 or Certificate of Coverage No.:
Facility Name: Grede LLC
County. MontgomeryPhone No. 910-428-2111
inspector: Tim McCaskill
Date of Inspection: 10-10-15
Time of inspection: 8,35 AM
Total Event Precipitation (inches): .4
Was this a'Representative Storm Event'" or'Measureable Storm Event" as defined by the permit?
(See information below.)
xER Yes ❑ No
Please verify whether Qualitative Monitoring must be performed during a "representative storm
event" or "measureable storm event' (requirements vary, depending an the permit).
Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be
performed during a "representative storm event" or during a "measureable storm event" However,
some permits do not have this requirement. Please refer to these definitions, if applicable.
A "representative storm event" is a storm event that measures greater than 0.1 Inches of rainfall
and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than
0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no
precipitation.
A "measurable storm event' is a storm event that results in an actual discharge from the
permitted site outfall. The previous measurable storm event must have been at least 72 hours
prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter
interval is representative for local storm events during the sampling period, and the permittee
obtains approval from the local DWQ Regional Office.
By this signature, I certify that this report is accurate and complete to the best of my knowledge:
--r, 7� . 4VOW—
(Signature of Permittee or Designee)
Page 1 of 2
Page 20 of 22

1. Outfall Description:
Outfall No. 01 Structure (pipe, ditch etc) Ditch
Receiving Stream: V N A/g_ f e./ rCr b � �n�r .s
Describe the industrial activities that. occur within the outfall drainage area:
2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint
(light, medium, dark) as descriptors: Grev lei c of Iy /t
3. Odor. Describe any distinct odors that the discharge may have (i.e., smells strongly of oil,
weak chlorine odor, etc): gone
4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is
clear and 5 is very doudy:
1 2 4 5
S. Floating Solids: Choose the number which best describes the amount of floating solids in
the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids:
1 2 ti.J 4
6. Suspended Solids; Choose the number which best describes the amount of suspended
solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy-
1 2 3) 4 5
7. Is there any foam in the stormwater discharge? Yes
8. Is there an oil sheen in the stormwater discharge? Yes
9. Is there evidence of erosion or deposition at the outfall? Yes nNo
10. Other Obvious Indicators of Stormwater Pollution:
list and describe
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition
may be Indicative of pollutant exposure. These conditions warrant further investigation.
Page 2 of 2
Page 21 of 22

i
DocLrmo It N"k. $AifiPIo v 0d oti M- -
po—=14 Re►A d: May 16, 2016
`
ReFei $
FIMS 1 ofr.'
'
gocxurr$iit Nt�:.� ._` �
Isaitdtg`Ai�t�ea:':
P-EDNrCS-003-rev.1 i
Pa Aden OAMY OfflCe
R2 of 2.ia ter inter w Use aw
Clienttx
Couder [dmlo]: UPS USPS coent lin Co"Mw Pace Other
Cub" Seal on Pressnt: ' Uyes no Seals b6or ❑ Yea [] no
PacMdo iatei lal: [WIsWrap 2 j60* Bags ❑ None: pother
Tharftromoter sscl: [R t3ui1 lrDD07 TI+ idled: • wet. BW - N&W . n amoli,s en iroe. mom d . rm h.
Temp Cofrectfon F d6r.' Add!$at>xract
Pof psr�h aao e.
Canea6ad Cooler7einp. Cbloglcal'Fisstre
to Frei Yei"ko N►n,
al�eiac = i
Tanip'aho:lld be OWieftaft to rO
Cor prKertta:
,
Chain of Fll69d Qut
a '-Q* -, AW
2.
Chain of u[stred:,6yo
. aw..i3WA
Sampler Name S S affae on.000: '
moo.. ONtA.
4:.,
SBim iBsArtive�.flrtffrirt Hoiri Tfine: .. ..
a:.t:7No..J7hVA
b:..: ..
� .
00 14M Time is +e7sh :.
oyii-V4. t]*A
Rush T'tirir 'rntd Thee esied�.]rei±
G' I l
7.
-
t:lotrt'Yolrurier • -
es; •Ct!!4 ,.p�l1
�.
� . ' .
t�omeot{�br�hrers Used:
V: lam. - A
8:=
,Pans Contalnerg Used: '
l:1Nd.:: p _ -
Conxalnere Inlaid
r»vGNc is
. 0..
>=gtered volume received for 014soh►ed leers
l rai:-dW
Sample labels match COC:.
ros 6w ©WA
12.
_
T
-Indudes d*,tlmefiDIAn Ira
oontslners r preservstloEr have been diedfed.
e� C1Mo • . ,WA
19.
- •
Am ocn0ainero asedta9 pmmvaft amfclmdto.toin
�ea 13W --13WA
-
conpAsnce wM EPA reaor=w*%n.
YHj�Rfj
Ores t7No
_
Samples di for deahlortnaff h: t
Oyes ow
14..
Heads ce In YQ
th'es DO'
rlpBlankPresent .
Ora QNo,
Blank Cpstody Seals Present • -
r
4]ree:. Oft,t A
e'I Sle& Lot S urCi►aBed
ODOM NOtdleattonl Resoludon: Pleld Dais.Requfrod7 Y 1 N.
Person Contacted: l�atolYtmo;
Commentel Resolution:
SCURFISRF VD :., rail 115'
Review:.
Note: Whstrer there Fa a North Cam
samples, sow otfhls form wMte serdto the NoO Carolina DEHNR
Cert ft*n Office (La e wR of hold, moor fact pme rvallvs, out of temp;' ' •
loon
' Ineameat oontahrsrs} '
Page 22 of 22

�o
MC®ENR
Stormwater Discharge Outfall (SDO)
Qualitative Monitoring Report
Forguidance on filling out thfsjor n, please vWt r o jweb jlrjnydes- rmwaterj
Permit No.: BVIC15-f0Q/.91—AloL-0, or Certificate of Coverage No.: NIC/fi/_/JJ...1JJ
Facility Name: Grede lal,
County: MontgomeryPhone No. 910-428-2111
Inspector: Tim McCaskill
Date of Inspection: 10-10-15
Time of Inspection: 8:35
Total Event Precipitation (inches): f'' 1 0, f T e ✓,4 t
Was this a "Representative Storm Event" or "Measureable Storm Event" as defined by the permit?
(See information below) 6) l v .L� �� i y
x(R Yes ❑ No /—,, � T
Please verify whether Qualitativd Monitoring must be performed during a 'representative storm
event" or "measureable storm event" {requirements vary, depending on the permit).
Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be
performed during a "representative storm event" or daring a "measureable storm event" However,
some permits do not have this requirement. Please refer to these definitions, If applicable.
A "representative storm event" is a storm event that measures greater than 0.1 Inches of rainfall
and that is preceded by at.least 72 hours (3 days) in which no storm event measuring greater than
0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no
precipitation. ■
A "measurable storm event" is a storm event that results in an actual discharge from the
permitted site outfall. The previous measurable storm event must have been at least 72 hours
p rior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter
interval is representative for local storm events during the sampling period, and the permittee
obtains approval from the Loral DWQ Regional Office.
By this signature, I certify that this report is accurate and complete to the best of my knowledge.
(Signature of Permittee or Designee)
Page 1 of 2

1. Outfall Description:
Outfall No. 01 Structure (pipe, ditch] etc) Ditch
Receiving stream: ll H lV4 K t� Trr6 r,7Y _ 6r�Gt�------y-
Describe the industrial activities that occur within the outfall drainage area:
2. Color. Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint
(light, medium, dark) as descriptors: _-Grey ---M e OF fy h -I-,-4 -
3. Odor. Describe any distinct odors that the discharge may have (i.e., smells strongly of oil,
weak chlorine odor, etc): �^]`Lone
4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is
clear and 5 Is very cloudy:
1 2 4 5
S. Floating Solids: Choose the number which best describes the amount of floating solids in
the stormwater discbarge, where 1 is no solids and 5 is the surface covered with floating solids:
1 2 V
4 5
G. Suspended Solids: 'Choose the number which best describes the amount of suspended
solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy:
1 2 3) 4 5
7. Is there any foam In the stormwater discharge? Yes Info
B. Is there an oil sheen in the stormwater discharge? Yes
9. Is there evidence of erosion or deposition at the outfa117 Yes DNID
10. Other Obvious Indicators of Stormwater Pollution:
List and describe
eh
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition
may be indicative of pollutant exposure. These conditions warrant further investigation.
Page 2 of 2

WILLA3 IGI-HY &
ASSOCIATES. INC
Forst R04 Suits A
VA 24SSI
lnforrnado":Mr. lande I]
�.
Ana"cal Request and Chain of Custody form
rxr& etA
IISuapuare to be d+paerdof 60 OmItty tlme d nee[pr, Unit"thw we for EPAer a Uad1311, a wdm aliwrww rdrd.
�PIO DWOM l% 0 Plana d" hm If cb§d wadd Am to ra ltsumple 60 flays of r tab's r+vlYL la box dmt dodwd. lsbwf4 d�tpoa of =j%Om ' days afpr by ►eA*Q
C] Piew dtedc fr.ra a rAmt wouFd Gb tab m retdn tams.!.laver ttnn 6C DaYf IPleste Es>w the eppraeed wsd the btb if box b nwdwdrad4 brbwilldtwose of farsoie Go don alter w rarioil
NAi Otdw Nat
f p1of]
DrderComptate?Cards) Yes No
Turn Around Thm Request
_ StmAwd D"Im st Day (10 Days)
_ 74 9udmra Day Rush L—jh")
_ "Budruw Day RasAI____Dayf)
_ �i BudnaaDayRusA [ - -Days)
tee. /rerrwranrwal.auppwe wWefOWW
0MR

Weather History for Albemarle, NC I Weather Underground
Page 3 of 3
Dally Weather History & Observations
2015 Temp.
('F3
Dew Point (•F)
Hurrldlty 1%)
Sea Level Press.
(in)
Visibility (ml)
VAnd (mph)
Predp. tin)
Events
Oct hloh
avg
law
high
avp
low
high
avg
low
high
avg
low
high
avg
low
high
avg
high
sum
66
62
S7
66
62
57
100
96
88
29,96
2992
2928
10
10
5
21
12
29
0.49
Rain ,
Thunderstorm
59
55
51
59
56
52
100
99
94
29.9S
29.68
2934
10
9
4
Z5
17
36
1.10
Rain
62
56
50
63
56
50
100
100
100
29.90
29.86
29.84
10
9
2
23
18
36
tAO
Rein,
Thunderstorm
68
64
59
63
61
57
100
95
83
29.99
29.92
29AG
10
10
7
24
18
34
0.04
Rain,
Thunderstorm
62
SS
55
61
56
54
100
91
77
30.D9
30.D4
29.98
10
10
7
22
16
34
0.01
Rain
73
62
51
S7
53
50
100
79
44
3032
30.Oa
30.03
10
10
10
16
7
22
0.00
80
453
46
61
55
46
too
80
44
30.15
30m
30.07
10
10
10
5
0
0.00
80
66
53
64
59
54
100
83
51
3021
30.16
30.13
10
10
3
9
1
-
0100
80
66
53
58
63
54
100
87
58
30.18
30.11
30.01
10
10
5
14
3
22
0.00
69
62
55
68
61
55
100
99
as
30.10
30-OS
30.02
10
9
3
18
6
24
0.80
Rein,
Thunderstorm
73
63
53
61
55
52
100
84
53
30.08
30.02
2994
10
10
10
12
5
-
0.00
Rain
75
62
50
63
S7
50
100
87
61
29.97
29.91
29AZ
10
10
10
9
1
-
0.00
78
66
55
63
59
85
100
85
5D
29.67
29.79
2914
10
10
10
13
5
21
D.00
75
60
46
55
51
46
100
77
38
30.04
2994
Z9.87
10
10
7
10
1
0.00
73
58
42
52
47
41
100
79
31
3D.20
50.13
30.04
10
10
10
9
1
16
0.00
71
5a
44
55
49
37
100
79
43
3021
30.15
30.10
10
10
7
12
1
-
0.00
66
50
35
46
38
32
100
64
30
3D.35
30.25
3020
10
10
10
12
3
16
0.00
59
46
32
37
32
25
100
66
27
30.49
30AZ
3035
10
10
10
15
4
21
0.00
60
45
30
39
32
28
100
69
29
30S8
3041
30AS
10
10
10
8
2
-
CLOD
69
50
30
45
37
30
100
74
27
3OA9
3OA2
3D35
10
10
10
7
1
-
0.00
73
53
33
48
42
34
l O
77
27
3OA4
3038
3033
10
10
0
7
1
0.00
Fog
78
68
39
54
47
39
100
78
30
3038
3032
3025
10
10
1
8
1
-
0.00
80
62
44
61
53
45
100
al
42
30.26
30.22
30,16
10
10
TO
9
1
D.00
71
62
53
59
56
54
700
84
56
30.33
30.27
3023
10
9
3
8
3
-
moo
75
65
55
66
60
55
100
87
64
30.2S
30M
30.15
10
10
10
a
1
-
OAD
64
5a
51
61
46
43
88
70
59
30.43
30.35
30.25
1D
10
10
18
10
28
0.00
Rain
60
54
48
61
53
46
100
98
82
30AZ
30.29
3032
10
10
3
la
10
26
0."
Rain
75
68
60
72
67
61
100
99
83
30.10
29.119
29.77
10
9
2
TS
6
20
0.72
Rain
69
62
59
64
63
59
100
97
78
29.92
29.83
29.78
10
9
5
7
5
-
0.00
report this
ad
http://www.wunderground.com/history/airport/KVUJ/2015/1 0/1 O/Month]yHistory.btml?r... 10/29/201 S

Weather History for Albemarle, NC I Weather Underground
Page 1 of 3
Weather History for KVLIJ - October. 2015
October
10
2015
View
Month of October. 2015
Daily Weekly Monthly Custom
Temperature
Max Temperature
Mean Temperature
Min Temperature
Degree Days
Heating Degree Days lbase 651
Cooling Degree Days lbase 651
Growing Degree Days (base 50)
Davy Point
Dew Point
Precipitation
Predpiration
Snowdepth
Wind
Wind
Gust Wind
Sao Level Pressure
Sea Level Pressure
Monthly Weather History Graph
report this ad
Max
80 `F
68"F
50 IF
20
2
16
Avg
70 IF
59 IF
48 IF
6
0
9
Min
59 IF
45°F
30 IF
0
0
0
25°F
0.00 in
25 mph
6 mph
0 mph
36 mph
21 mph
10 mph
30.58 in
30.12In
29.74 in
sum
http://www.wunderground.comAhistory/airport/KVU]/2015/10/10/MonthlyHistory.htm1?r... 10/29/2015

Weather History for Albemarle, NC I Weather Underground
Page 2 of 3
IF faMsue Dew Pail c
46 r
r
y
15
0
1 r 3 4 5 6 7 1 1 10111213141S 1617 u11202t 22232425A 2rA 21M >4
76
in Ho BXCIIitNews
hft
S6's
i i- j , s j
to"
303
r
ion
-
n�
t ! i
1013
� 71
Lila
2 3 4 S 6 7 6 1 10 11 12 13 14 16 1S 11 11 11 20 21 22 23 24 25 26 21 26 26 10 21
t'ilrld Swild lem rilsl h
1 2 1 4 S 6•T 1 0`10it 121314IS.1617 u192021 2223242526213213031
Yilnd Ot
SiOD
161D
'
s �• ir• a1 ii jl
!0D
E± i
66
1 2 3 4 s 6 7 1 110111211141Eu171e112021222324252627212130;„,o
repaiI this ad I why ads?
Search for Another Location
i KVUJ
Submit
Trip Planner
search our weather history database for the weather conditions in past years. The results will help you decide how W. cold, wet, or windy it might bel
Date:
October
10
Submit
Astronomy
Oct. 10, 2015
Actual Time
Civll TwillBht
Nau[Ical 7wdirPub
Astronomical Twllil,M
Moon
Length o! Visible L�ht
ty�m.o� nay
Waning Crescent. 5% of the Moon is llluminaled
Oct 10 Oct 12
Waning Crescent New
report this ad I why ads?
Rise
set
7:22 AM EDT
6:52 PM EDT
6:56 AM E7r
7A7 PM EDT
6.27 AM EDT
7u47 PM EDT
5:57 AM EDT
8:16 PM EDT
5:12 AM EDT 110tIOJ
SA7 PM EDT 110/101
T2h 20m
11h 29m
at 20
Oct 27 Nov 3
First Quartar
Full Last Quarter
http://www.wunderground.com/history/airport/KVUJ/2015/1 0/10/MonthlyHistory.htnOr... 10/29/2015

.y
STORMWATER DISCHARGE OUTFALL (SDO)
MONITORING REPORT
Permit Number NCS 000255 SAMPLES COLLECTED DURING CALENDAR YEAR: 2015
(This monitoring report shall be received by the Division no later than 30 days from
the date the facility receives the samplin'Rr�s MA"ratory.)
FACILITY NAME GREDE II COUNTY MONTGOMERY I'C CC
PERSON COLLECTING SAMPLE(S) TIM MCCASKILL PHONE NO. (910_)975-2 H O 4 2015
CERTIFIED LABORATORY(S) PACE Lab # 633i
Lab # ~ma
SIGNATURE OF PER1&tfttM8$IGNEE '~
Ell EDED ON PAGE 2.
Part A: Specific Monitoring Requirements
No:�1 '�
-'... :. ' .::.�` _t',
Sample �+f�
.:Collected .+'.�..t'�
Total �`� �-
- Flout: if a • } ..RaipfS!!
Total � ; �
.i
PH � ~� �
;y F ri
qk,_ � ��
,
��f `� •�
� `:i lam
�}
4x vry +
3 4 k�r�-
L,..-
'�
�� f , Z::,
001
06/27/15
0.5 in.
&47
Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? _yes X_no
(if yes, complete Part B)
Part B: Vehicle Maintenance Ae Ity Monitoring Requirements
outfa!!
Date
soas©:�
i - � it
It- }a'.�x, - d�
:VUa7.7V_.{:�'}I : �:
+'JY�
:Ooaott
`'S..7r� !1�
No'
, s
Sample f
Tnta! F1o� �F
Totalr r
`OW&`Grease r
tNon paler
Tatsl <
pH x
Ne�vMotbr
a,
Collected}
(if applfcable}r
Rai�%1!�
(ifppl }F,' tf
°O&G/TPHrSnspended
- R r {
Dil Usage A
;E
NA
NA
NA
NA
NA
NA
NA
INA
NA
Form SWU-247, last revised 21212012
Page 1 of 2

STORM EVENT CHARACTERISTICS: Mail Original and one copy to:
Division of Water Quality
Bate _6t27/15 Attn: Central Files
Total Event Precipitation (inches): _0.5 in I617 Mail Service Center
Event Duration (hours): 0.75 (only if applicable — see permit.) Raleigh, North Carolina 27699-1617
(if more than one storm event was sampled)
Date _NA
Total Event Precipitation (inches):
Event Duration (hours): (only if applicable — see permit.)
"I certify, under penalty of law, that this document and all attachments were prepared under ray direction or supervision in accordance with a
system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person
or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted I% to the
best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations."
- %126/ ZoI,�
(Signature of Permittee) (Date)
Richard Cabadas
Form SWU-247, fast revised 21212012
Page 2 of 2

Aal 3A i.
DEER
Stormwater Discharge Outfall (SDO)
Qualitative Monitoring Report
Forguidance on filling out this form, please visit: httn /// ppi•tal.ncdgar,p[gl Deb/lrinl2dC5_,gW[inwater/
Permit No,: J/�//_Q/�/_Q/�/�/�/ or Certificate of Coverage No.:
Facility Name: GREDE II
County: MONTGOMERY Phone No. 910-428-2111
Inspector: TIM MCCASKILL
Date of Inspection: 06/27/15
Time of Inspection: 1820
Total Event Precipitation (inches): _.5
Was this a "Representative Storm Event" or "Measureable Storm Event" as defined by the permit?
(See information below.)
® Yes ❑ No
Please verify whether Qualitative Monitoring must be performed during a "representative storm
event" or "measureable storm event" (requirements vary, depending on the permit).
Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be
performed during a "representative storm event" or during a "measureable storm event." However,
some permits do not have this requirement. Please refer to these definitions, ifapplicable.
A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall
and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than
0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no
precipitation.
A "measurable storm event" is a storm event that results in an actual discharge from the
permitted site outfall. The previous measurable storm event must have been at least 72 hours
prior. The 72-hourstorm interval does not apply if the permittee is able to document that a shorter
interval is representative for local storm events during the sampling period, and the perm' ittee
obtains approval from the local DWQ Regional Office.
By this signature, I certify that this report is accurate and complete to the best of my knowledge:
(Signature of Permittee or Designee)
Page 1 of 2
SWU•242, Last modified 7/31/2013

1. Outfall Description:
Outfall No. 01 Structure (pipe, ditch, etc.) pipe
Receiving Stream:
Describe the industrial activities that occur within the outfall drainage area:
2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint
(light, medium, dark) as descriptors: grcy Medium tint
3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil,
weak chlorine odor, etc.): No distinCt order
4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 Is
clear and 5 is very cloudy:
1 2 3 4 5
S. Floating Solids: Choose the number which best describes the amount of floating solids in
the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids:
1 3 4 5
6. Suspended Solids: Choose the number which best describes the amount of suspended
solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy:
1 2 0 4 5
7. Is there any foam in the stormwater discharge? Yes 0cN
8. Is there an oil sheen in the stormwater discharge? Yes No
9. Is there evidence of erosion or deposition at the outfall? Yes No
10. Other Obvious Indicators of Stormwater Pollution:
List and describe
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition
may be Indicative of pollutant exposure. These conditions warrant further investigation.
Page 2 of 2
SWU-242, last modified 7/31/2013

STORMWATER DISCHARGE OUTi1 ALL (SDO)
MONITORING REPORT
Permit Number NCS 000255 SAMPLES COLLECTED DURING CALENDAR YEAR: 2015
(This monitoring report shall be received by the Division no later than 30 days from
the date the facility receives the sampling results from the laboratory.)
FACILITY NAME GREDE 11 COUNTY MONTGOMERY
PERSON COLLECTING SAMPLE(S) TIM MCCASKILL PHONE NO. (910__)975-2727
CERTIFIED LABORATORY(S) PACE Lab #_633
Lab #
SIGNATURE OF PERMITTEE OR DESIGNEE
REQUIRED ON PAGE 2.
Part A: Specific Monitoring Requirements
Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? _yes X_no
(if yes, complete Part B)
Part B: Vehicle Maintenance Ac ivity Monitoring Requirements
Na 5am} le, Total IMw Total s Oil & Greaser Nan'palar _ Total R NeK+ M©tor
Collected , pftappltcable) Ramfal! (dappL} . O&G1TP13 Suspended ` oil..Usage
�. � (Me#hod 1664 � Sci}ids -
N
mold l/ r... MG- inciie§ :m I . `. :: in .unit,` all[no'..
Form SWU-247, last revised 21212012
' . Page 1 of 2

STORM EVENT CHARACTERISTICS: Mail Original and one copy to:
Division of Water Quality
Date 6/27/15 Attn: Central Files
Total_Event Precipitation (inches): —0.5 1617 Mail Service Center
Event Duration (hours): 30 minutes (only if applicable — see permit.) Raleigh, North Carolina 27699-1617
(if more than one storm event was sampled)
Date
Total Event Precipitation (incites):
Event Duration (hours): (only if applicable — see permit.)
"1 certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a
system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person
or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the
best of my knowledge and belief, true, accurate, and complete. 1 am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations."
C. ?
-7�� 6�1(,, C��a C- �- r - /-(�
(Signature of Permittee) (Date)
Form S W U-247, fast revised 21212012
Page 2 of 2

d i t
WILLOUGHBY &
ASSOCIATES, INC.
Enoim unrura; Htalrh and Sa,41y
July 13, 2015
Grade it r Biscoe, LLC
Mr. Chuck Wolffis
530 East Main Street
Biscoe NC 27209
Final Report
WAI EHS
15421 Forest Road Order No: 92256598
Suite A
Forest, VA 24551 Client: Grede II - Biscoe LLC'
Ph: 434-455-0919
Fax: [phone] Project: June 2015 Storm Water Sampling
Event
RE; Project: June 2015 Storm Water Sampling Event
WAI Order: 92256598
Dear Mr. Wolffis:
Enclosed are the analytical results for samples received on June 30, 2015.
These results conform to the most current NELAC standards unless otherwise Indicated.
Results are only reflective of the conditions during the sample(s) collection dates) and
time(s).
If you have any questions concerning this report, please feel free to contact me.
[e-mail]
Analytical Report:13 Pages
Chain of Custody: 2 Pages
SCU Receipt: Ji Page
Total:16 Pages
REPORT OF LABORATORY ANALYSIS
This report sets forth the results of outsourced laboratory analysis of samples delivered to WAI EHS and shall not be construed as a
representatlon by WAI EHS as to the source or method of procuring such samples. All reports are submitted as confidential property of
the client and authorization for publication of any statements contained in our reports Is reserved pending WAI EHS issued.written consent.

CERTIFICATIONS
Project GREBE II- SISCOE, LLC.
Pace Project No.: 022SB598
Charlotte Certification IDs
9800 Kin* Ave. Ste 100, Huntersvllle, NC 28078
FioridAELAP Certification C E87627
North Carolina Drinking Water Certification M 37700
Kentucky UST Certification #: 84
North Carolina Field Services C&Ukatlon N: 5342
West Virginia Certification M 357
North Carolina Wastewater Certification #: 12•
VirglnIWELAP Certification #: 480221
South Carolina Certification #: 99DO6001
Asheville Certification be
2225 Riverside Drive, Asheville, NC .28804
North Carolina Wastewater Certification #: 40
Flodda/NEIAP Certification #: E87648
South Carolina Certification #: 99030001
Massachusetts Certification #: M-NC030
West Virginia Certification #: 35e
North Carolina Drinking Water Certification #: 37712
VirginialVELAP Certification #: 460222
Eden Certification IDs
205 East Meadow Road Suits A, Eden, NC 27288 North Carolina Wastewater Certification #: 633
North Carolina Drinking Water Certification #: 37738 VirginialVELAP Certification #: 460025
REPORT OF LABORATORY ANALYSIS
Willoughby & Associates, Inc.
15421 Forest Road, Suite A
Forest, VA 24551
Phone:[phone] Fax:[phone]
Page 2 of 16

SAMPLE SUMMARY
Project: GREDE 11- BISCOE, LLC,
Pace Project No.: 92256596
Lab ID Sample ID Matrix Date Collectod Date Received
92256598001 OUTFALL 001 Water. 06/27/15 18:20 OW30115 11:20
REPORT OF LABORATORY ANALYSIS
Willoughby & Assooiales, Inc,
15421 Forest Road, Stills A
Forest, VA 24551
Phane:434-455.0918 Fax:[phone]
Page 3 of 16

SAMPLE ANALYTE COUNT
Project• GREDE il• BISCOE, LLC
Pace Project No.: 922565N
Anslytes
Lab IA Sample In Method
Analysts
Reported
Laboratory
92256598001 OUTFALL 001 SM 2540D
CHM
1
PASI•E'
EPA 1064E
JMS.
1
PASI•C`
EPA 200.7
JMW
5
PASI•A
EPA 351.2
JDA
1
PASI•A
EPA420.4
DMN
1
PASI•A
SM 5220D
EWS
1
PASI•A
REPORT OF LABORATORY ANALYSIS
Willoughby r} Associates. Inc.
15421 Forest Road, Suite A Page 4 of 1$
Forest, VA 24551
Phone:[phone] Fax:[phone]

ANALYTICAL RESULTS
Project:- GREDE Ih SISCOE, LLC.
Pace Project No.: 92256598
Sample: OUTFALL 001
Lab ID:92258598001 Collected:'
08127/1518:20
Received: 06/30/151110 Matrix: Wales
Report
Parameters'
Results Units Limit,
MDL
DF
Piepared
Analyzed CAS No. Oual
2540D TSS, Low -Level, Eden
Analytical Method: SM 2540D.
Total Suspended Solids
66.4 mg1L .2.8
2.8
1
07/01/15 15:12
HEM, Oil and Grease
Analytical Method:. EPA 16648
Oil and Grease
ND mg/L 5.0
1.1
1
07102M5 14:39
200.7 MET tCP
Analytical Method: EPA200.7 Preparation Method:.EPA200.7
Cadmium
ND ug1L 1.0
0.50
1
07/02/15 17:30
07/06/15 W27 7440-43-9
Copper
20.6 ug/L 5.0
2:5
t
0710211517:30
07/0611516*27 7440-50-8
Lead
ND ug1L 5,0
2.5
t
07/02l1517:30
07/06/151627 7439-92-1
Nickel
ND ug1L 5.0
2.5
1
07/02/1517:30
0710811516:27 7440-02-0
Zinc
1.99 ug1L 10.0
2.5
1
07102/1517:30
07106/1516:27 7440-66-6
351.2 Total Kjeldahl Nitrogen
Analytical Method: EPA 351.2
Nitrogen, Neldahl, Total
1.0 mg1L 0.50
0.25
1
07/D4/15 12:11 7727-37.9
420.4 Phenolics, Total
Analytical Method: EPA420.4
Phenol
0.022 mg/L 0.010
0.0050
1
07l0811514:43 108.95-2 M1
5220D COD
Analytical Method: SM 5220D
Chemical Oxygen Demand
43.0 mg1L 25.0
12.6
1
07106115 16:00
REPORT OF LABORATORY ANALYSIS
Wllloughby'& Associates. Inc.
16421 Forest Road, Suite A Page 5 of 16
Forest, VA 24551
Phona; 434-455.0919 Fax: [phone]

QUALITY CONTROL DATA
Project: GREDE II- BISCOE, LLC.
Pace Project No,: 92266598
QC Hatch: EDEN/19102 Analysis Method: SM 2540D
QC Batch Method: SM 2540D Analysis Description:' 2540D TSS, Low Level, Eden
Associated Lab Samples: 92256598001
METHOD BLANK: 1499639 Matrix: Water
Associated Lab Samples: 92256598001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Total Suspended Solids. mglL ND 1.0 07/01/15 15:09
LABORATORY CONTROL SAMPLE: 1499640
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Total Suspended Solids mg1L 250 250 100 90-110
SAMPLE DUPLICATE: 1499641
92256348001 Dup Max
Parameter Units Result Result RPD RPD Qualifiers
Total Suspended Solids mg1L 345 302 13 5 D6
SAMPLE DUPLICATE: 1499642
92256444003 Dup Max
Parameter Units Result Result RPD RPD Qualifiers
Total Suspended Solids mglL 439 $03 14 5 DO
Results presented on this page ore In the units Indicated by Ow -Jnas' column except when on atternole unit Is presented to the right of the reauh.
REPORT OF LABORATORY ANALYSIS
Willoughby & Assocleles, Inc.
15421 Forest Road, Suite A Page 6 of 16
Forest, VA 24551
Phone:[phone] Fex:434-534-9837

QUALITY CONTROL DATA
Project GREDE il• BISCOE. LLC.
Pace Project No.: 92256698
OC Balch: GCSV121839 Analysis Method: EPA 1664E
QC Balch Method: EPA 1864B Analysis Dascdption: 1664 HEM, Oil and Grease
Associated Lab Samples: 92256598001
METHOD BLANK: 1501113 Matrix: Water
Assot:tated Lab Samples: 02256598001
Stank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Oil and ©cease MOIL NO 5.0 07/02/15 14:20
LABORATORY CONTROL SAMPLE & LCSD: 1501114 1501115
Spike LCS LCSD LCS LCSD % Rae Max
Parameter Units Conc. Result Result % Rec % Rae Limits RPD RPD OuallBers
Oil and Grease mglL 40 35.4 34.4 88 86 78-114 3 30
Results presented on this pope are In the unlb Indicated try the'UnftV column except where an sltemste unit in presented to the rlphi of the result.
REPORT OF LABORATORY ANALYSIS
Willoughby & Associates, Inc.
15421 Forest Road, Suite A Page 7 of 18
Forest, VA 24551
Phone:[phone] Fax:[phone]

DUALITY CONTROL DATA
Project: GREDE II- BISCOE, LLC
Pace Project No.: 92256598
QC Balch,. MPRP118902 Analysis Method: EPA 200.7
QC Balch Method: - EPA 200.7 Analysis Description: 200.7 MET
Associated Lab Samples: 92256598001•
METHOD BLANK: 1600971 Matrix: Water
Assocated Lab Samples: 02256598001
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Cadmium
ug1L
ND
1.0
07/06/1514:02
Copper
ug1L
NO.
5.0
0710611514:02
Lead
ug1L
ND
5,0
07/0811514:02
Nickel
ug1L
ND
6.0
07/0611514:02
Zinc
ug1L
NO
10,0
0710811514:02
LABORATORY CONTROL SAMPLE:
1500972
Spike
LCS
LCS
% Rec
Parameter
Units
Cone,
Result
% Rec
Limits Qualifiers
Cadmium
uglL
500
450
90
85-115
Copper
ug1L
500
465
93
85-116
Lead
uglL
Soo
451
90
85.115
Nickel
uglL
Soo
447
89
85-115
Zinc
ug1L
500
445
89
85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1500073
1600974
MS
MSD
92256348001
Spike
Spike
MS
MSD
MS
MSD
% Rae
Max
Parameter
Units
Result
Cone,
Cone,
Result
Result
% Rec
% Rec
Limits
RPD
RPD Qual
Cadmium
ug1L
ND
500
500
381
409
72
82
70.130
13
20
Copper
uglL
27.0
500
Soo
422
468
79
88
70.130
10
20
Lead
ug1L
ND
500
Soo
359
403
70
79
70-130
12
20
Nickel
uglL
192
500
500
510
546
64
71
70-130
7
20 M7
Zinc
ug1L
326
Soo
500
880
88e
167
M
70-130
3
20
MATRIX SPIKE B MATRIX'SPIKE DUPLICATE: 1500975
1500976
MS
MSD
92266683004
Spike
Spike
MS
MSD
MS
MSD
% Rec
Max
Parameter
Units
Result
Cone.
Cane.
Result
Result
% Rae
% Rec
Limits
RPD
RPD oval
Cadmium
ug1L
ND
Soo
Soo
462
468
92
94
70.130
1
20
Copper
uglL
0.15 mg1L
500
Soo
637
642
97
96
70-130
1
20,
Lead
ug1L
0.074
500
500
484
490
82
83
70-130
1
20
mgtl.
Nickel
uglL
2.6 mg1L
Soo
500
3040
3110
85
1D0
70-130
2
20
Zinc
ug1L
ND
500
500
428
433
84
85
76-130
1
20
Results presented on this papa are in the units Indicated by the "ifnlw column except where an MEMO unit Is presenled to the right of the result.
REPORT OF LABORATORY ANALYSIS
Willoughby & Associates, Inc.
15421 Forest Road, Suite A Page 6 of 16
Forest, VA 24561
Phone:[phone] Fax:[phone]

QUALITY CONTROL DATA
Project GREDE 11- BISCOE, LLC.
Pace Project No.: 92256598
QC Balch: WETA/23584 Analysis Method:, ' EPA 351.2
OC Batch Method; EPA 351.2 Analysis Description: 3512 TKN
Associated Lab Samples: 02256598001
METHOD BLANK: 1501653 Matrix: Water
Associated Lab Samples: 92256598001
Stank. Reporting
Parameter Units Result Limit Analyzed Qualifiers
Nitrogen, Kjeldahl, Tote1 mg1L ND 0.50 0710411512:05
LABORATORY CONTROL SAMPLE: 1501654
Spike LCS LCS %Rec
Parameter Units Uric. Result % Rae Limits QuafiBers
Nitrogen, Kjeldahl, Total mg1L 10 10.2 102 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1501655 1601056
MS MSO
92256512004 Splke Spike MS MSD "MS MSD % Rae Max
Parameter Units Result Conc. Conc. Result Result % Rae % Rae Limits RPD RPO Qual
Nitrogen, Kjoldahl, Total mg1L 31.0 50 50 75.2 83.4 87 104 90-110 10 10 M1
Results prnented on this pe0e ate In the units indicated by the "linos" column except when an alternate unit Is presented to the rtyht of the result.
REPORT OF LABORATORY ANALYSIS
Willoughby & Associates, Inc.
15421 Forest Road. Suite A Page 9 of 16
Forest, VA 24551
Phone:[phone] Fax:[phone]

QUALITY CONTROL DATA
Project; GREDE It- BISCOE, LLC.
Pace Project No.: 92256598
QC Batch: WETAf23620 Analysis Method: EPA 420A
QC Batch Method; EPA420.4 Analysis Description: 420.4 Phenolics
Associated Lab Samples: 92256598001
METHOD BLANK: 1603353 Matrix: Water
Associated Lab Samples: 92256598D01
Blank Reporting
Parameter Units Result Limit Analyzed Qualmers
Phenol mgfL ND 0,010 0710811514:42
LABORATORY CONTROL SAMPLE: 1503354
Spike
LCS
LCS
% Rae
Parameter Units
Cone.
Result
% Rec
Limits Qualifiers
Phenol mg1L
.05
0.051
101
90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1503355
1503356
MS
MSD
92.256588001
Spike
Spike MS
MSD
MS. MSD % Rec Max
Parameter Units Result
Cone.
Cone. Result
Result
e% Rec % Rec Limits RPD RPD Qua1
Phenol mg1L 0.022
.05
.05 01079
0.080
113 114 90-110 1 10 M1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1503367 1503358
MS MSD
92255927002 Spike Spike MS MSD MS MSD % Roc Max
Parameter Units Result Cone, Cone. Result Result e% Rec e% Rec Limits RPD RPD Qual
Phenol mg1L 0,011 A5 .05 0,049 0,046 76 69 90.110 7 10 M1
Results presented on this page ere In the unite Indicated by tha'UnW cctumn except where on stternate unit Is presented Who right of the result.
REPORT OF LABORATORY ANALYSIS
Willoughby & Associates, Inc.
15421 Forest Road, Suite A Page 10 of 16
Forest, VA 24551
Phone:[phone] Fax:[phone]

QUALITY CONTROL DATA
ProjecL GREDE II- BISCOE, I.I.C.
Pace Project No.: 92256598
QC Batch: WETA123803 Analysis Method: SM 5220D
QC Batch Method:: SM 52200' Analysis Description: 52201) COD
Associated Lab Samples: 92256598001
METHOD BLANK:. 1502072 Matrix: Water
Associated Lab Samples: 92256598001
Blank
Parameter Units Result
Chemical Oxygen Demand mg1L
LABORATORY CONTROL SAMPLE: 1502073
Spike
Parameter Units Cone.
Chemical Oxygen Demand mg1L 750
Reporting
Limit Analyzed Qualifiers
ND 26.0 0710611516:00
LCS LCS % Rec
Result % Rec Limits Qualifiers
776 103 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE; .1502074 1502076
MS MSD
92256348001 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Cone. Cone. Result Result % Roe % Rec Limits RPD RPD Qual
Chemical Oxygen Demand mglL 14500 30000 30000 30600 30600 54 54 W110 0 3 MO
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1502076 1502077
MS MSD
92256976001 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD RPD Quat
Chemical Oxygen Demand mg1L 687 750 750 1440 1440 101 101 00-110 0 3.
'Results presented on this page are in the units Indicated by the •Units" column exeaptwhery an ellemate unit Is presented to the right or the resuh.
REPORT OF LABORATORY ANALYSIS
Willoughby & Associates, Inc.
15421 Forest Road, Suite A Page 11 of 16
Forest, VA 24551
Phone:[phone] Fax:[phone]

QUALIFIERS
Project GREDE II- BISCOE. LLC.
Pace Project No.: 92266698
DEFINITIONS
OF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilullon of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MOL-Adjusted Method Detection Limit
PCIL - Practical Cluantilation Limit.
RL- Reporting Limit.
S Surrogate
1,2-131pheny1hydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each anslyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethyivinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrotein and Acrylonitrile by EPA
Method 8260.
N-Nltrosodiphenylamina decomposes and cannot be separated from Diphenylemine using Method 6270. The result reported for
each anatyte is a combined concentration.
Pace Analytical Is TNl accredited. Contact your Pace PM for the current list of accredited anatytes.
TNI -The NELAC Institute.
IASORATORIES
PASI-A Pace Analytical Services - Asheville
PAS1-C Pace Analytical Services - Charlotte
PASI-E Pace Analytical Services - Eden
ANALYCE QUALIFIERS
D6 The relative percent difference (RPD) between the sample and sample duplicate exceeded laboratory control limits,
M.I. Matrix spike recovery exceeded QC limits. Batch accepted'based on laboratory control sample (LGS) recovery.
Me Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution.
REPORT OF LABORATORY ANALYSIS
Willoughby & Associates, Inc.
15421 Forest Road, Suite A Page 12 of 16
Forest, VA 24551
Phone:434-455-t1919 Fax:[phone]

QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: GREDE II- BISCOE, LLC.
Pace Project No.: 92266698
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch Analytical Method Batch
92256598001
OUTFALL 001
5M 2540D
EDEN119102
92256598001
OUTFALL 001
EPA 16648
GCSV121839
92256595001
OUTFALL 001
EPA 200.7
MPRP118902 EPA 200.7 ICP116971
92266598001
OUTFALL 001
EPA 3512
WETA123584
92256596001
OUTFALL 001
EPA 420.4
WETA123820
92256598001
OUTFALL 001
SM 5220D
WETA123803
REPORT OF LABORATORY ANALYSIS
Willoughby & Associates, lnc:
15421 Forest Road, Suite A Page 13 of 16
Forest, VA 24551
Phone:[phone] Fax:[phone]

CHAIN43F-CUSTODY 1 Anatytical Request Document
m.CRNOOC "lNELEG&O00UMCWAF"kft.WAm b..ert.irM.eeurN/.
e�e�e��ie7�eee
MOM
WMATA
MMM2M■■M■■■■
■■■M15M■■■■■■■
rre�rra�r�a�rra�r�■ri■■■■■■
■■M■■■■■■■■■■
■■■■■■■R■■■■■
■■■■■■■■■■■■■
° ■■■■■■■■■■■■■
■■■■■■■■■■■■■
■■■■■■■■■■■a■
wlFm rmwimwr?�—
NW-WWnrr""
i■r■■■r■■M■
■�ri■■�■�■■■■■■■■■■
■■■��ri■■■�■■■■■■mom
®
■■�■■■���■■�■■■■■■■■
_
r
II77�T��
r_y
WAVE
�
w'Amr
..
Ilion,
�..,
wwswrwy.nxarPrrr�.r�.r�rrrw.rin....t r..�r..,.�.w riw F4 LQ4Lt..D1, ISYq.2p01

1!2
A
-.-I
.
CKAIN-OF-CUSTQDY I -Ana"cal Request Document
NUMB
ll-rl
IMPFAMMEN
ARNMEMOMMEMEN
NNOMMEMEMENNE
am
nM,
0
"IM,
MP" f
M TIM
W3,
M,
IM
InVA
IW�■

a
Ir
a
WWII
P
P
N
P.
A
m
r
vpe'
w . c

Michael F. Easley, Governor
William G. Ross Jr., Secretary
North Carolina Department of Environment and Natural Resources
Coleen H. Sullins, Director
Division of Water Quality
December 19, 2008
Ron Welker, Maintenance Manager
Citation Corporation
PO Box 748
Biscoe, NC 27209
Subject: Analytical Monitoring Results
Citation Corp -Foundry Service '
Montgomery County
Dear Mr. Welker:
On December 15, 2008, our office received your letter concerning the results of analytical
monitoring from a sampling event that occurred on November 14, 2008 at stormwater outfalls SDO-001
and SDO-002 Alley. In reviewing those results and comparing them to the Benchmark Values contained
within the permit, it is noted that exceedances are present for COD, Copper, Lead, TSS and Zinc for
SDO-001 and Copper and Zinc for SDO-002 Alley. Also, the reporting limit of <0.005 mg/L for
Cadmium is above the Benchmark Value in the permit of 0.001 mg/L. If the laboratory you are using
cannot report down to that level, you will need to find one that can. As stated in the permit, the
Benchmark Values are not limits, but are to be used as a guide to help identify and ultimately eliminate
possible sources of pollution.
According to your letter, you have contacted Myrick Construction to construct multiple silt
barrier/traps ahead of the settling basin as well as installing some additional measures in the drainage
ditch between Citation and K & M Machine. You are asked to please provide a reasonable time frame
that you expect these and any other measures to be completed.
If our office can provide any assistance, please contact me at [phone].
Sincer ly,
Michael Lawyer
Environmental Specialist
cc: FRO -Surface Water Protection
01,C
NophCaroiina
Aakrrally
North Carolina Division of Water Quality 225 Green Street -suite 714 Fayetteville, NC 28301 Phone [phone] Customer Service
Inlcrnet: www.newaler unlit mrg Fax [phone]
An Equal apportunitylAfSrmative Action Employer-50% Recycled110% Post Consumer Paper

t •
QlkTION
Innovative Metal Components
Citation Niscoe a Division of Citation Corporation
December 11; 2008 .
RECEI ED
mr. 1520
OE1+1R-FAYEiTEVILLEREG4(]NA1
Mr. Mike'Lawyer
N.C. Dept of Environment and Natural Resources
225 Green Street — Suite 714
Fayetteville, North Carolina 28301-5043
Dear Mike:
Citation Corporation
530 East Main Street
P.O. Box 748
Biscoe, NC 27209
Tel: 910,428.2111
Fax: [phone]
Enclosed are test results from samples taken at the Citation Biscoc location. The
rain event was light, then very heavy for approximately 35 minutes, and then went to a
sprinkle for the next 4-5 hours. I was able to collect good samples from SD001 and the
catch basin in the alleyway during the first thirty minutes of the discharge but was unable
to collect a quantitative sample for SDO02 parking lot drain as this was more sheet flow
than a discharge stream. Also, Tri-test shorted the kit by one test sample container for oil
and grease. I choose to use the sample for SDO02 alleyway to pull an oil and grease test
instead of phenol as this also has run off from the parking area and street. I felt that
phenols would be more important on the SD001 sample. I have notified Tri-Test as to
the mistake and was assured the kits would be complete next shipment.
That being said you will notice on the SD001 results that we were high on a
number of areas: - COD, copper, zinc and slightly high in lead. 1 attribute these levels
to the extremely high solids in the sample. I know that I saw very high flow at the
discharge due to the storm's intensity at sample taking time, approximately 20 minutes
into the main rainfall event.
These results are not consistent with what we have seen in the past. I feel we
must make some improvements to the system to cover when there is extremely heavy
flow.
I have contacted Myrick Construction and have set up for their company to
construct multiple silt barrier /traps ahead of the settling pit. We will also install some
measures in the drainage ditch between K & M Machine and Citation Corporation to
reduce solids going to SD001. There are other measures I am investigating at this time
and we will also be taking another sample prior to spring to see if our efforts are working
in controlling releases with benchmark values.
If you need any further assistance please call me at [phone], extension
3234, and we can discuss.
/ _ c. `el, y� al,
Ron Welker
Maintenance Mgr.

O
�U' O TE ST
6701 Conference Drive Page 1 of 1
Raleigh, NC 27607-
Telephone: [phone] NC1WW Cert. #: 067
Fax: [phone] NCIDW Cert. #: 37731
Laboratory Report
--- Prepared for ---
RON WELKER
Report Date:
12/4/2008
CITATION CORPORATION
Date Received:
11/17/2008
530 EAST MAIN STREET
BISCOE, NC 27209
Work Order #:
0811-01023
Project No.:
Cust. Code:
Ci2111
Project ID: Semi -Annual Wastewater
Cust. P.O.#:
STORMWATER
Jo. Sample ID
Date Sampled Time Sampled Matrix
Sample Type Condition
001 SDO 001
11/14/2008 12:00
SW
Grab 4 +1- 2 deg C
Analyzed
Test Performed
Method
Results
Date Time Qualifier
Chemical Oxygen Demand
EPA 410.4
445 mglL
1111810E 9:17
Phenols wlchloroform extr.
EPA 420.1
14.9 ug1L=Q.o10""111 1111810E 14:00
Cadmium
EPA 200.8 �'
<0.005 mg/L
1112510E 17:44
Copper
EPA 200.8
0,113 mg/L*
1112510E 17:44
Total Kjeldahl Nitrogen
EPA 351.2
5.25 mg1L
1112510E 16:32
Lead
EPA 200.8
0.036 mg/L
1112510E 17:44
Nickel
EPA 200.8
0.018 mg/L
1112510E 17:44
Total Suspended Solids
SM 2540D
450 mg/L"l,
1112010E 11:17
Zinc
EPA 200.8
2.10 mg/L,.Y--
1211108 15:05
pH
EPA 150.1
7.15 S.U.
1112010E 13:31
pH disclaimer
Exceeds holding time.
1112010E 16:28
aeS
G
n eeo( 4Cd , cro l
r'b , o 3
75S /0
-
Reviewed by:
Ui✓
for Tritest, Inc.

1; o
0
TLfuTEST
6701 Conference Drive
Raleigh, NC 27607.
Telephone: [phone]
Fax: [phone]
Laboratory Report
--- Prepared for --
RON WELKER
CITATIO CORPORATION
530 EAST MAIN STREET
BISCOE, NC 27209
Project No.:
Project ID: Semi -Annual Wastewater
Page 1 of 1
NCIWW Cent. M 067
NCIDW Cert. M 37731
Report Date:
12/4/2008
Date Deceived:
11/1712008
Work Order#:
0811-01022
Cust. Code: C12111
Cust. P.O.#: STORMWATER
4o. Sample ID Date Sampled Time Sampled Matrix Sample Type Condition
001 SDO 002 ALLEY 11114/2008 12:20 Sw Grab
4 +1- 2 deg C
Analyzed
Test Performed Method Results Date Time Qualifier
Chemical Oxygen Demand
EPA 410.4
<10.0 mg1L
1111810E 9:17
Cadmium
EPA 200.8
<0.005 mg1L
1112510E 17:44
Copper
EPA 200.8
0.011 mglL�K
1112510E 17:44
Total Kjeldahl Nitrogen
EPA 351.2
1.15 mglL
1112510E 16:32
Lead
EPA 200.8
<0.005 mg1L
1112510E 17:44
Nickel
EPA 200.8
<0.020 mg1L
1112510E 17:44
Total Suspended Solids
SM 2540D
36.0 mg1L
1112010E 11:17
Zinc
EPA 200.8
0.472 mglLI;K
1112510E 17:44
pH
EPA 150.1
7A9 S.U.
1112010E 13:31
pH disclaimer
Exceeds holding time.
1112010E 16:28
Oil & Grease
EPA 1664A
7.4 mglL
1112410E 8:00
Reviewed by:
r
for Tritest, Inc

CTE-AXj,ON
innovative Metal Components
y
To:
Company:
Fax Number
Phone Number:
Re.
Citation Corporation
530 East Main
Post DIIicc Box 748
Biscoc, NC 27209
Tel: [phone]
Fax, 910.428-4986
FA-esimile
From: ! O..J
l�riF-�joy✓. ram- !S C o �
Date:
Total no. of pages including cover:
Sender's Reference Number:
Your, Reference Number:
E00l 100 'd VS :01 OnflE002-20-d3S

v
7RoTEST
6701 Conference drive
Raleigh, NC 27601
Telephone: [phone]
Feat: [phone]
Laboratory Report
-- Prepared for -�
RON WELKER
CITATION CORPORATION
530 EAST MAIN STREET
BISCOE, NC 27209
Pagel all
NCMU Cert. V. 067
NC1DW Celt. N: 37731
Report Date: B12612008
Date Received- 7=2008
Work Order #: 0807-01961
Project No.: Cost. Code: C12111
Project ID: STORMWATER MONITORING Cust. P.O.#: STORMWATER
No. Samplo ID Date Sampled Time Sampled Matrix Samplo Type Condition
00t 31)0.001 7/1912008 15:00 SW Grob 4 *1. 2 deg C
Anatyzed
Test Performed Method Results Date Tlme Quallfler
Total Suspended Solids
EPA 160.2
140 mg/L ;W-
7*9108
13:05
Chemical Oxygen Demand
EPA410.4
59.5 mg1L
7124108
9:33
Total Kjeldahl Nltrogpn
EPA 351.2
1.02 mg1L
elil08
15.58
Cadmium
EPA 20D,8
t0.005 mg1L
81110E
11:44
Coppor
EPA 200.E
0.026mg1L.-k
811108
11AA
Load
EPA 200.8
0.905 mg1L
811108
11:44
Nickel
EPA 200.8
0.013 mg/L
1111108
11:44
Zinc
EPA 200.8
0240 mglLls�
811108
11:44
Phenols wlchlorofarm extr.
EPA 420.1
20A u$1L
8115108
14:00
pH
EPA 150.1
8.0 S.U.
7125/08
10:16
p„ divelalmer
Exceeds holding time.
7125108
10:50
Reviewed by:
for Tritest, Inc,
E/Z 'd LM •oN
200'a lbv9+i?E9+fi l6
I'll 1111!1i NVE61H
ke:ui (3nim62-92-9nu
DS :OI
8001 '9Z 'Inv
aw;J/aapa xa
(3f11)9002-20-d35
EOOIEOO 'd

7ROOTEST
Telephone: [phone]
Fax: (919) 834`6497
6701 Conference Drive
Raleigh, NC 27607
Laboratory Report
-- Prepared for --
RON WELKF-R
CITATION CORPORATION
530 EAST MAIN STREET
BISCOR, NC 27209
Project No.:
Prolact ID: STORMWATER MONITORING
Page 1 of 1
NCNM Cort_ #: 067
NC10W Cert. #: 3T731
Roport Date: 9126/2008
Date Reeelved: '712312008
Work Order A OBOT-01960
Cust. Cade: CM111
Cuss. P.O.#: STORMWATER
No. Sample ID Date Sampled Time Sampled.. Matrix Sample Type Condltian
1101 500-002 ALLEY 7119/2008 14:40 SW Grab a +1- 2 deg C
Analyzed
Test Performed
Method
Re3ulta
pate Time Qualifier
Total Suspended Selkls
EPA 160.2
9.2 mg1L
7129108 13:05
Chemical Oxygen Demand
EPA 410.4
26.6 mg1L
7124/05 9:33
Total Kjaldahl Nitrogen
EPA 351.2
1.34 mull.
811108 15:56
Cadmium
EPA 200.8
c0.005 mg1L
8N109 11.44
Ceppor
EPA 2uu,6 •
t0,010 MOIL
811108 11:44
Wad
EPA 200.8
0.005 mg1L
811108 11:44
Nickel
EPA 200.8
e0.010 mg/L
8/1108 11:44
Zinc
EPA 200.8
1.16 mgll_
8/1108 11:44
Phenols w/chloroform extr.
EPA 420.1
58.0 uglL
U11510B 14:60
PH
EPA `160.1
7.55 S.U.
7125108 10:16
PH disclaimer
Muoods holding time.
7125f06 10:50
Reviewed by:
46
for Tritest, Inc.
CA 'd LD9 'ON
E00 'd l6179+DEB+fil6
x1f 1"P 11 w0l-1 l t 800i 9z •Rnv
lE:01 (B08002-92-enu amll/a:ipa xa
E001200 'd
VS :01 (3f11) 8002-20-d3S

CrMON
Innovative Metal Components
Citation Biscoc a Division of Citation Corporation
March 25, 2008
Ms. Belinda S. Henson, Regional Supervisor
NC Dept. of Environment and Natural Resources
225 Green Street — Suite 714
Fayetteville, NC 28301-5043
Dear Ms. Henson:
OFNR-FRO
MAR z 6 2008
DING
In response to your report we will be addressing the following:
1.As Mr. Welker expressed during your visit we will be cleaning out
and remediating the sediment pit for SDO-001. We have contracted
with Myrick Construction to perform this work, as they were also the
company to originally construct the pit. At this time we will be cleaning
out the ditch to SD070001 outfall, and also the area at the south end of the
property between K & M company and Citation. This will improve flow
characteristics from McCaskill Street access to Citation, as the upper end
of the ditch going to sediment pit, has built up with sediment.
2.Sand storage area behind plant; we shall reduce the amount of spent sand
kept in this area to approximately 200 tons. During your visit there was
approximately 2500 tons. We have been.hauling to the landfill weekly to
reduce the pile. Also we will grade and gravel the drive area to reduce
tracking of sand and mud during wet weather events. This should greatly
reduce the sand getting to the catch basin area and in turn to SDO-001. It
would be expected that this should greatly reduce carry out of sand from
this area to SDO-001 and in turn to Lick Creek tributary.
3.We will continue for the next two rain events to take a sample from catch
basin 41-42 are between the buildings to confirm results are acceptable
to meet state requirements. At this time we will also try to attain a sample
from SDO-002 if flows are available.
Citation Corporation
530 East Main Street
P.O. Box 748
Biscoe, NC 27209
Tel: [phone]
Fain: 910.428.4986
We would expect to have these items'completed by May 301h or before. Please
contact Ron. Welker or myself at 910/428-2111 if either you or Mr. Lawyer have,
questions, suggestions or rQmments on the above.
Sincerely,
Shaddix
i1 Manager
Cc: Ron Welker

County:
MONTGOMERY
River basin
Report To
FROSP
Collector.
D STRICKLAND
Region:
FRO
Sample Matrix:
Surfacewater
Loc. Type:
RIVER/STREAM
Emergency Yes/No YES
CCIC Yes/No
YES
XC r13_`WQ Laboratory Section Wesults
Sample ID: AB26500
DN_FRO �ak vIA)r PO Number# Bw0951
Date Received: 0210B12008
Lr5
FEB 11 2048 _ Time Received: 12:40
Labworks LoginlD MMATHIS
D, Y Y � Q Date Reported: 2121108
Report Generated: 02/21 /2008
VisitlD
Loc. Descr.: DISCHARGE PIPES CITATION
Location ID: FROSPNLC _ I Collect Dale: 02/08/2008 I Collect Time:: 10:46 I Sample Depth
Sample Qualifiers and Comments
Routine Qualifiers
For a more detailed description of these qualifier codes refer to www.dwglab.org under Staff Access
A -Value reported is the average of two or more determinations
N3-Estimated concentration is < PQL and >MDL
Bi-Countable membranes with <20 colonies; Estimated
NE -No established PQL
62- Counts from all filters were zero.
P-Elevated PQL due to matrix interference and/or sample dilution
83-Countable membranes with more than 60 or 80 colonies; Estimated
01-Holding time exceeded prior to receipt at lab.
134-i=filters have counts of bath >60 or 80 and < 20; Estimated
q2- Holding time exceeded following receipt by lab
85-Too many colonies were present; too numerous to count (TNTC)
PQL- Practical Quantitation Limit -subject to change due to instrument sensitivity
.I2- Reported value failed to meet IIC criteria for either precision or accuracy; Estimated
U- Samples analyzed for this compound but not detected
.13-The sample matrix interfered with the ability to make any accurate determination; Estimated
X 1- Sample not analyzed for this compound
.16-The lab analysis was from an unpreserved or improperly chemically preserved sample; Estimated
N1-The component has been tentatively identified based on mass spectral library search and has an estimated value
LAB
Laboratory Section» 1623 Mall Service Center, Raleigh, NC 27699-1623 [phone] Page 1 of 2

-' WC (DWQQ Laboratory Section ResultsSamplelO AB26500
Location ID- FROSPNLC Collect Date: 0210812008
Lac. Descr.: HA GE PIPE �ION Collect Time:: 10:45
Visit 0
I C:AS rF Analyte Name PQL Result Guatifier Units Analyst/Date Approved By /Date
Method Reference 218/08 218M
MIC
BOD, 5-Day In liquid 2.0 41 G5 mg/L ADEXTER MOVERMAN
Method Reference APHA5210B 21801 2/15108
Turbidity 1.0 8.9 NTU BSWANSON MOVERMAN
Method Reference APHA213013•20th
WET
Idue d Ir111 uld 6.2 216
ili:lX 7iIEc.
mg/L AWILLIAMS MOVERMAN
Method Reference APHA254013-20th 2111138 2114M
Grease and 00 In liquid 10 10 U mg/L MIBRAHIMI MOVERMAN
Method Reference EPA1664A 2112108 2114108
MET
7440-22-4 Ag by ICPMS
5.0 5.0 U ug1L
PGAUTHIER
ESTAFFORD
Method Reference EPA 200-8
2112M
2120roe
7429-90-5
50 ug1L _ pZj
DSTANLEY
ESTAFFORD
Method Reference EPA 200.7
1 C•
2112f08
2/20/08
7440-43-9 Cd by ICPMS -
1.0 1.0 U ug/L
PGAUTHIER
ESTAFFORD
Method Reference EPA 200.8 2/12108 2/20/08
7440-47-3 Cr by ICPMS 10 28 ug/L DSTANLEY ESTAFFORD
Method Reference
EPA 200.8
2/1201
2120=
7440-50-8
2.0
87
STANLEY
ug1L+0
ESTAFFORD
Method Reference
EPA200.8
fe?
!2112/08
2120108
7440-48-4
IC
THEM
50
rmowo I
ug1L
_�
DSTANLEY
ESTAFFORD
Method Reference
EPA 200.7
2/12108
220=
7439-96-5
Mn by ICPMS
10
490
ug/L
DSTANLEY
ESTAFFORD
Method Reference
EPA 200,8
2 I2108
220108
7440-02-0
Ni by ICPMS
10
24
ug/L
DSTANLEY
ESTAFFORD
Method Reference
EPA200,8
2112108
220/08
7439-92-1
Pb by ICPMS
10
14
ug1L
DSTANLEY
ESTAFFORD
Method Reference
EPA 200,8
2112108
220ro8
7440-66-6
by
10
ug1L _ L
0.
DSTANLEY
ESTAFFORD
Method Reference
EPA 200.8
2112/08
220108
Laboratory Section>> 1623 Malt Service Center, Raleigh, NC 27699-1623 [phone] Page 2 of 2

r1
DIVISION
OF WATER QUALIT
fl (/
I W _/��
Chemistry
Laboratory Report / Water Qua
'ty
�J
bNurnher ����
COUNTY L"(OATq�/
PRIORM
SAMPLE TYPE
Date Received :
Time Received :
RIVER BASIN: At` FQA�
EAMBIENT
� QA
� STREAM EFFLI3ENT
Received By
S
REPORT TO f �% Regional ORim
COMPLIANCE
CHAIN OF CUSTODY
LAKE INFLUENT
Other :
ga EMERGENCY
VTSITrD
ESTUARY
DataRclwwd
COLLECTOR(S) : ^Q r Sir j p»
Date Reported;
Estimated ROD Range:
Station Location:
11P� I ron
Seed: Chlorinated:
Remarks: .IJ\71%lrge-
Station #/Location Code Date Begin (yy/mmldd)
Date End (yylmmldd)
Time Begin
Time End
Depth - DM, DR, DBM
Value Type - A, H, L
Composite-T, S, B
Sample Type
0'S U
SOD 310 mg/L
COD High 340 M91L
COD Low 335 meL
Coliform: MY Fecal 31616 1100m!
Coliform: MF Total 31504 /100m!
Coliform: tube Fecal 31615 /100m1
Coliform: Fecal Strep 31673 /loom!
Residue: Total 500 mgfL
--
Volatile 505 meL
Fixed 514) n wL
Residue: Suspended 530 m91L
Volatile 535 mg/L
Fixed 540 mgfL
pH 403 units
Acidity to pH 4.5 436 mg(L
Acidity to pH 8.3 435 mg/L
Alkalinity to pH 8.1 415 mg/L
Alkalinity to pH 4.5 410 mg1L
TOC 680 mg/L
Turbidity 76 NTU
Coliform Total Tube I100 ml
Chloride 940 mgfL
Chlorophyll a EPA 445.0 modified option ugrL.
Color: Taste 80 Cu-.
Color: (pH) 83 pH- c.u.
Color: pH 7.6 V c.u.
Cyanide 720 mlrf L
Fluoride 951 mg/L
Formaldehyde 71880 nwL
Grease and Oils 556 meL
Hardness Total 900 m9rL
Specific Coud. 95 umhos/cm
M13AS 18260 MWL
Phenols 32730 ug/L.
Sulfate 945 mp/L
Sulfide 745 mg/L
Boron
Tannin & Lignin ug/L
Hexavalent Chromium ugfL
Bicarbonate m91L
Carbonate ngJL
Total Dissolved Solids m91L
N143 as N 610 mg/L
TKN an N 625 mg/L
NO2 plus NO3 as N 630 mcJi-
P: Total as P 665 mg/L
PO4 as P 70507 mg/L
P: Dissoved as P 666 mwL
K-Potassium mg/L
Cd- Cadmium 1027 ug(L
Cr1Thromium:Total 1034 ug/L
Cu- Copper 1042 up/L
Ni-Nickel 1067 ugfL
b- Lead 1051 ug/L
Tat- Zinc 1092 uglL
V-Vanadium ugfL
Ag- Silver 1077 uglL.
Al- Aluminum 1105 ug/L
Be -Beryllium 1012 ug/L
Ca- Calcium 916 mgfL
Co- Cobalt 1037 ugl1,
✓
Fe- bon 1041 ug/L
Mo-Malybdenum uglL
Sb-Antimony ug/L.
Sn-Tin ug/L
TI-Thallium ug/L
Ti-Titanium ug/L
Hg-I631 ng/L
Li -Lithium 1112 ug/L
Mg- Magnesium 927 mglL
jZ
Mn-Manganese 1055 uWL
Na- Sodium 929 mg/L
Amnic:Tatal 1002 ug/L
Se- Selenium 1147 ug/L
Hg- Mercury 71900 ug/L
Ba-Harium UWL
Organochlorine Pesticides
Organophosphorus Pesticides
0rganonitrogn Pesticides
Acid Herbicides
Rase/NeutraMAcid Extractable Organics
TPH Diesel Range
Purgeable Organics (VOA bottle req d)
TPH Gasoline Range
TPHBTEX Gasoline Range
Phytoplankton
Temperature on arrival (oq
I! r

Report to: _FRO Sample Anomaly Report (SAR)
Lab Number: AB26500
Station Location: Discharge Pipe @
Citation
;ample "Type: Stream Effluent
Date collected: 2/8/08
Affected Parameter(s): BOD
Sample ID:
County: Montgomery Region: Fayetteville
Priority: Emergency Collector: D. Strickland
Date received: 2/8/08 Date analyzed: 2/8/08
Analytical Area (check one):
❑WCH ❑METALS
[--]NUT ®MICRO
The following anomalies occurred (check all that apply):
❑ Samples
❑Improper container used
❑VOA vials with headspace
❑Sulfide samples with headspace
❑Samples not received, but listed on fieldsheet
❑Samples received, but not listed on fieldsheet
❑Mislabeled as to tests, preservatives, etc.
❑Holding time expired
❑Prior to receipt in lab
❑After receipt in lab
❑Insufficient quantity for analysis
El Sample exhibits gross non -homogeneity
❑Sam le not chemically preserved properly
PH out of range (record pH):
❑Improper chemical
❑Residual chlorine present in sample
❑Color interference
[]Heavy emulsion formed during extraction
❑Sample bottle broken in lab - no reportable results
❑Other (specify):
❑VOA ❑SVGA
❑PEST
RQuality Control
❑Instrument failure — no reportable results
❑Analyst error — no reportable results
❑ Surrogates
❑None added
❑Recovery outside acceptance limits
[]Spike recovery
❑None added
❑Recovery outside acceptance limits
❑Failed to meet criteria for precision
❑internal standards
❑Blank contamination
®QC data reported outside of controls (e.g., QCS, L.CS)
El Incorrect procedure used
❑SOP intentionally modified with QA and Branch Head
a roval
Invalid instrument calibration
❑Elevated detection limits due to:
❑Insufficient sample volume
Comments: Both of the two glucose glutamic acid standards were below the acceptable range of 167.5 to 228.8 mg1L at 154.7mg/L
and 152.2mg/L. Sample was not seeded.
Corrective Action:Ongoing investigation to determine the cause of low GGA standard results.
❑Samples were rejected by DWQ Lab. Authorized by: Date:
❑Accepted and analyzed after notifying the collector or contact person and determining that another sample could not be secured.
❑Sample(s) on hold until:
®Sample reported with qualification. Data qualification code used:G5
❑Other (explain):
Notification Required? ❑ Yes ❑ No
Person Contacted: Date:
Form completed by: Krigela Dex Date: 2/15/2008
60­11ft 1 ' Dlkzt
Lead Chemist Review (initial):
LUBIOCHEM --t2:L
❑METALS
Branch Head Review (initia
QA/QC Review_ (inil,
0 PEST
❑VOA
OSVOA
Logged into database by (initial):
2A%FormsV.sbomtoryOAR 10/23/01 dbs

,I County: MONTGOMERY Sample ID: AB26498
River Basin RO O�O� wA tqQ (/ Time
Number # 8w0949
Report To FROSP ����! y V Date Received: 210812008
Collector: D STRICKLAND me Received: 12:46
+ •� •]' 4� G Y Labworks t-oginlD MMATHIS
Region: FRO iL L 6L U`
Sample Matrix: Surfacewater Date Reported: 2/21l06
Loc. Type: RIVERISTREAM DWQ U Report Generated: 02121l2D08
Emergency Yes/No YES
VisrtlD
COC Yes/No YES
Loc. Descr.: LICK CREEK @ POST OFFICE RD
Location ID: FROSPNLC Collect Date: 021OW2008 Collect Time:: 10:00 Sample Depth 0.1
Sample Qualifiers and Comments
Routine Qualifiers
For a more detailed description of these qualifier codes refer to www.dwgiab.org under Staff Access
A -Value reported is the average of two or more determinations
N3-Estimated concentration is < POL and >MDL
B1-Countable membranes with <20 colonies; Estimated
NE -No established POL
132- Counts from all filters were zero.
P-Elevated POL due to matrix interference and/or sample dilution
B3- Countable membranes with more than 60 or 80 colonies; Estimated
Oi-Holding time exceeded prior to receipt at lab.
B4-Filters have counts of both >60 or 80 and < 20; Estimated
02- Holding time exceeded follovuing receipt by lab
B5-Too many colonies were present; too numerous to count (TNTC)
PQL- Practical Quantitafion Limit -subject to change due to instrument sensitivity
J2- Reported value failed to meet OC criteria for either precision or accuracy; Estimated
ll- Samples analyzed for this compound but not detected
J3-The sample matrix interfered with the ability to make any accurate determination, Estimated
XI- Sample not analyzed for this compound
J6-The lab analysis was from an unpreserved or improperly chemically preserved sample; Estimated
Ni -The component has been tentatively identified based on mass spectral library search and has an estimated value
LAB
Laboratory Section» 1623 Mail Service Center, Raleigh, NC 27699.1623 [phone] Page 1 of 2

WC (DW.QQ Laboratory Section Results Sample ID AB26498
Location ID: , FROSPNLC Collect Date: 0210812008
Loc, Descr.: LICK CREEK @ POST OFFICE RD Collect Time:: 10:00
Visit ID
CAS # Analyte Name PQL Result Qualifier Units AnalystJDate Approved By !Date
Sample wmperature at receipt by lab
2.1
'C
DSAUNDERS
MMATHIS
Method Reference
218/08
2/8ro8
MIC
BOO, S-Day in liquid
2,0
2 U G5
mgfL
ADEXTER
MOVERMAN
Method Reference APHA52108
218108
2115198
Turbidity '
1.0
9.9
N[TU
BSWANSON
MOVERMAN
Method Reference APHA213013-20th
2/8=
2/11/08
WET
Resldue_Suspended In liquid
6-2
13
m91L
AWILLIAMS
MOVERMAN
Method Reference APHA2540D-20th
2111108
2114108
Grease and Oil InMuld
10
10 U
t11g1L
MIBRAHIMI
MOVERMAN
Method Reference EPA1664A
2112MB
2114108
MET
7440-22-4 Ag by ICPMS 5-0 5.0 U ugfL PGAUTHIER ESTAFFORD
Method Reference EPA 200.8 7J12108 22=8
7429-90-5
A1byICP
50
1200
1-1911-
/ Z�_ /G DSTANLEY
ESTAFFORD
Method Reference
EPA 200 7
�/ 2/i2/08
220168
7440-43-9
Cd by ICPMS
1.0
1.0
U
ug1L
PGAUTHIER
ESTAFFORD
Method Reference
EPA 200.8
2112108
2/20/00
7440.47-3
CrbyICPMS
10
10
U
u9fL
DSTANLEY
ESTAFFORD
Method Reference
EPA 2001
2112108
2J201W
7440-50-8
Cu by ICPMS
2.0
6.2
11911-
DSTANLEY
ESTAFFORD
Method Reference
EPA 200-8
2/12108
220/08
7440-48A
Fe by ICP
.. 50
920
L91L
4 DSTANLEY
O
ESTAFFORD
Method Reference
EPA 200.7
2112f08
2120M
7439-96-5
Mn by ICPMS
10
37
u91L
DSTANLEY
ESTAFFORD
Method Reference
EPA 200,9
2/12/08
2/20108
7440-02-0
M by ICPMS
10
10
U
u9fL
DSTANLEY
ESTAFFORD
Method Reference
EPA200.8
2J12108
22=8
7439-92-1
Pb by ICPMS
10
10
U
uglL
DSTANLEY
ESTAFFORD
Method Reference
EPA201H
2/12M
2120108
7440-66-6
ZnbyICPMS
10
40
ug(L
DSTANLEY
ESTAFFORD
Method Reference
EPA 200.8
2/12=
220f08
Laboratory Section» 1623 Mail Service Center, Raleigh, NC 27699.1623 [phone] Page 2 of 2

DIVISIOCOFA TY
WaterChemistry Report/
Quality ` x
PL TYPE
COUNTY /4 o#" r PR10Rf[Y
RIVER BASH: A ❑ AMBIENT QA © STREAM EFFLUENT
REPORTTO Regional Office COMPLIANCE CHAIN OF CUSTODY LAKE El INFLUENT -�
Other : J 0£MERGENCY VISIT
ESTUARY \ �'
COLLECTOR(S) : -_S IG an Q T. ❑ VVV}}
'Lab Number : r'
Date Received:
Time Received : t J v
Received By "I
Data Released :
Date Reported:
Estimated ROD Range: Station Location: % �/'
Seed: Chlorinated: Remarks: '-^! Meek ® PO-1 F71 i`/ re_ Ava
Station ##Location Code Date Begin (yylmm/dd) Date End (yy/mmldd) Time Begin Time End Depth - i� DR, DRM Value Type - A, H, L Composite-T, S, B Sample Type
0% 00
BOD 310 M91L
COD High 340 mg/L..
COD Low 335 MO.
Coliform: MF Fecal 31616 - 1100m1
Coliform: MF Total 31504 110ftl
Coliform: tube Fecal 31615 /106011
Coliform: FecA Strep 31673 1100ml
Residue: Total 100 mP/L
Volatile 505 m8/L
Fixed 510 m91L
Residue: Suspended 530 mg/L
Volatile 535 nwjL
Fixed 540 mg/L
pH 403 units
Acidity to pH 4-5 436 m91L
Acidity Is, pH 113 435 m9fL..
Alkalinity to pH 8.3 415 TnWL.
Alkalinity to pH 4.5 410 mefL
OC 680 mg/L
Turbidity 76 NT11
Coliform Total Tube 1100m]
Chloride 940 mgiL
Chlorophyll a EPA 445.0 modified option ug+L
Color. True 80 C.U.
Color. (pH) 83 pH- C.U.
Color: pH 7.6 82 C.U.
Cyanide 720 m91L
Fluoride 951 mg/L
Formaldehyde 71880 rwL
Grease and Oils 556 mg'L
Hardness Total900 m9rL
Specific Cond. 95 umhos/cm
MBAS 38260 mg(L
Phenols 32730 ugfL
Sulfite 945 _fvL
Sulfdc 745 _wL.
Boron
Tannin & Ligrin UWL
Hexavalenl Chromium ug(L
Bicarbonate m8/L
Carbonate MEX
Total Dissolved Solids mg/L
NH3 as N 610 m j#L.
TKN an N 625 mg/L
NO2 plus NO3 as N 630 mg/L
P: Total as P 665 mel,
PO4 as P 70507 tltp/L
P: Dissolved as P 666 mill
-Potassium mg/L
Cd- Cadmium 1027 ugfL
Cr-Chromium-Total 1034 ug/L
Cu. Copper 1042 ug/L,
Ni-Nickcl 1067 up/L.
Pb- Lead 1051 ugfL
7m- Zinc 1092 ugrL
V-Vanadium ug/L
Ag- Silver 1077 ugIL
Al- Aluminum 1105 ug(L.
Be- Beryllium 1012 ug/L
Ca- Calcium 916 mg/L
Co- Cobalt 1037 ugIL
Fe- iron 1045 up/L
Mo-Molybdenum uEVL
Sb-Antimony upL
Sn-Tin ug/L
TI-Thath m ug(L
Ti-Titanium ug1L
149-1631 nwL.
Li-Litbium 1132 ug/L
Mg -Magnesium 927 m91L
Mn-Manganese 1055 uWL
Na� Sodium 929 mwL
Amnic:Tatal 1002 u8tL
Se- Selenium 1147 u8/L.
Hg- Mercury 71900 ug/L
Ba-Barium ug1L,
Organochlovine Pesticides
Organophosphoms Pesticides
Organunitrogen Pesticides
Acid Herbicides
BawNeutral&Acid Extractable Organics
TPH Diesel Range
Purgeable Organics (VOA bottle mq'd)
TPH Gasoline Range
TPH/BTEX Gasoline Rang
Phytoplanktun
Temperature on arrival (°C)
1
141

Report to: _FRO
Sample Anomaly Report (SAR)
Lab Number:
Station Location
AB2b498
Sample ID:
Lick Creek @ Post County: Montgomery
Office Rd
Sample Type: Stream Priority: Emergency Collector:
Date collected: 2/8/08- Date received: 2/8/08 Date analyzed:
Affected Parameter(s): BOD
Analytical Area (check one):
❑ WCH []METALS
[]NUT ®MICRO
The following anomalies occurred (check aU that apply):
❑Samples
❑Improper container used
❑VOA vials with headspace
❑Sulfide samples with headspace
❑Samples not received, but listed on fieldsheet
❑Samples received, but not listed on fieldsheet
❑Mislabeled as to tests, preservatives, etc.
❑Hoiding time expired
❑Prior to receipt in lab
❑After receipt in lab
❑Insufficient quantity for analysis
❑Sample exhibits gross non -homogeneity
❑Sam ie not chemically preserved properly
�pH out of range (record pH):
El Improper chemical
❑Residual chlorine present in sample
❑Color interference
❑Heavy emulsion formed during extraction
❑Sample bottle broken in lab - no reportable results
❑Other (specify):
Region: Fayetteville
D. Strickland
2/8/08
❑VOA ❑SVOA
[]PEST
®Quality Control
❑Instrument failure — no reportable results
❑Analyst error — no reportable results
❑Surrogates
❑None added
❑Recovery outside acceptance limits
El Spike recovery
❑None added
❑Recovery outside acceptance limits
❑Failed to meet criteria for precision
❑Internal standards
❑Blank contamination
®QC data reported outside of controls (e.g., QCS, LCS)
[]Incorrect procedure used
❑SOP intentionally modified with QA and Branch Head
a proval
Invalid instrument calibration
❑Elevated detection limits due to:
❑Insufficient sample volume
Comments: Both of the two glucose glutamic acid standards were below the acceptable range of 167.5 to 228.8 mg/L at 159.7mg/L
and 152.2mg/L. Sample was not seeded.
Corrective Action:Ongoing investigation to determine the cause of low GGA standard results.
❑Samples were rejected by DWQ Lab. Authorized by: Date:
[]Accepted and analyzed after notifying the collector or contact person and determining that another sample could not be secured.
❑Sample(s) on hold until:
®Sample reported with qualification. Data qualification code used.G5
❑Other (explain):
Notification Required? ❑ Yes ❑ No
Person Contacted: Date:
Form completed by:[Angela Dext 01 Date: 2/15/2008
Lead Chemist Review (initial):
SBIOCHEM vO
[]METALS
Branch Head Review (initi �''1 S - G i
QAIQC Review (ini al): , a,
!AXFonnALabamtnryLSAR J , `
❑PEST
❑ VOA
❑SVGA
Logged into database by (initial):
10173101dbs

1. .
County:
MONTGOMERY
River Basin
Report To
FROSP
Collector. '
D STRICKLAND
Region:
FRO
Sample Matrix:
Surfacewater
Lac. Type;
RIVERISTREAM
Emergency Yes/No YES
COC YeslNo
YES
DENR FRO
FEB 12 2008
DW Q
VisitlD
Loc. Descr.: LICK CREEK 0- US 220 (616k4457�� )
Sample ID:
AB26499
PO Number#
8W0950
Date Received:
02/08/2008
Time Received:
12:40
Labworks LoginlD
MMATHIS
Date Reported:
2/21/08
Report Generated: 02/21/2008
I Location ID: FROSPNLC I Collect Date: 02r0812008 I Collect Tme:: 10:20 I Sample Depth
Sample Qualifiers and Comments
Routine Qualifiers
For a more detailed description of these qualifier codes refer to www.dwglab.org under Staff Access
A -Value reported is the average of two or more determinations
N3-Estimated concentration is < PQL and >MDL
St -Countable membranes with <20 colonies; Estimated
NE -No established PQL
B2- Counts from all filters were zero.
B3- Countable membranes with more than 60 or $0 colonies; Estimated P-Elevated PQL due to matrix interference and/or sample dilution
B4-Filters have counts of bath >60 or 80 and < 20; Estimated 01-Holding time exceeded prior to receipt at lab.
65-Too many colonies were present; too numerous to count (TNTC) 02- Holding time exceeded following receipt by lab
J2-Reported value failed to meet QC criteria for either precision or accuracy; Estimated PQL- Practical Quantitation Limit -subject to change due to instrument sensitivity
U- Samples analyzed for this compound but not detected
J3-The sample matrix interfered with the ability to make any accurate determination; Estimated
Xi - Sample not analyzed for this compound
J6-The lab analysis was from an unpreserved or improperly chemically preserved sample; Estimated
Ni-The component has been tentatively identified based on mass spectral library search and has an estimated value
LAB
Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 1919) 733-3908 Page 1 of 2

WC IDWQ Laboratory Section Results Sample ID A326499
Location ID: FROSPNLC Collect Date: 02108/2008
Loc. Descr.: LICK CREEK @ US 220 Collect Time:: 10.20
Visit ID
Anatyte Name PQL Result Qualifier Units AnalystfDate Approved By Rate
Method Reference 2/8108 218108
MIC
BOD, 5-Day In Iiqutd 2.0 2 U G5 mg1L ADEXTER MOVERIa1AN
Method Reference APHAS210B M8 2/15108
Turbidity 1.0 23 NTU BSWANSON MOVERMAN
Method Reference APHA213013-20th 2/M8 2111108
WET
Residue Suspended In liquid
6.2
6.2
U
mg&
AWILLIAMS
MOVERMAN
Method Reference
APHA2540D-20th
2/11/W
2114108
Grease and Oil In Oquid
10
10
U
mg1L
MIBRAHIMI
MOVERMAN
Method Reference
EPA1664A
2112/08
2114/08
MET
7440-22A
AgbylCPMS
5.0
5.0
U
ug1L
PGALITHIER
ESTAFFORD
Method Reference
EPA 200.8
2112108
2120108
7429-90-5
AI by ICP
50
1300
ug1L I `
DSTANLEY
ESTAFFORD
Method Reference
EPA 200.7
r r we
2112/08
2/20108
7440-43-9
Cd by ICPMS
1.0
1.0
U
ug1L
PGAUTHIER
ESTAFFORD
Method Reference
EPA 200.8
2112=
2/20M
744047-3
Or by ICPtu1S
10
10
U
U911-
DSTANLEY
ESTAFFORD
Method Reference
EPA 200.8
211201
2120=
7440-50-8
CU by ICPMS
2.0
7.1
U91L ! D 1�7+ �` DSTANLEY
ESTAFFORD
EPA200.8
2112/08
212OMS
Method Reference
7440-08-4
Fe by ICP
50
1000
ug/L /
DSTANLEY
ESTAFFORD
Method Reference
EPA200.7
2112/08
2120/08
7439-96-5
Mn by ICPMS
10
30
ug1L
DSTANLEY
ESTAFFORD
Method Reference
EPA 200.8
2112M
2120/08
7440-02-0
Ni by ICPMS
10
10
U
u9fL
DSTANLEY
ESTAFFORD
Method Reference
EPA200.8
2/12MB
2120108
7439-92-1
Pb by ICPMS
10
10
U
u9fL
DSTANLEY
ESTAFFORD
Method Reference
EPA 200.8
2112/08
2/20/08
7440-66-6
Zn by ICPMS
10
45
ugll-
DSTANLEY
ESTAFFORD
Method Reference
EPA 200.8
2/12MB
2/20/08
Laboratory Section?> 1623 Mail Service Center, Raleigh, NC 27699-1623 [phone] Page 2 of 2

COUNTY -rtMef
RIVER BASIN: ('gyp
REPORTTO Regional Office
Other :
COLLECTOR(S)
DIVISION OF WATER QUAL Y
Chemistry Laboratory Report IWater ■lity
SAMPLE TYPE
(�
n\
PR1
AMBIENT QA Q STREAM
EFFLUENT
❑ COMPLIANCE CHAIN OF CUSTODY
LAKE
INFLUENT
EMERGENCY VISIT ID ESTUARY
R-1
r
I Receber .0S0a& Ispate Receives : Tiiue Received . 1 rl (,(D
Received By : y"
Data Released :
Date Repaded :
Estimated BOD Range-. Station Location:
Seed: Chlorinated: Remarks:
Siodon #/Location Code Date Begla (yy/mmldd) Date End (yylmmldd) Time Begin I Time End Depth - DM, DB, DBM Value Type - A, H, L Composite-T, S, B Sample Type
BOD 310 nWL
COD High 340 malL
COD Low 335 MOIL.
Coliform: MF Fecal 31616 A00ml
Colifurm: MF Total 31504 110011111
Coliform: tube Fecal 31615 1100mi
Caliform: Feral Strep 31673 II00m1
Residue: Total 500 mgrL.
Volatile 505 mg/L
Fixed 510 mnglL
Residue: Suspended 530 mwL
Volatile 535 F*L
Fixed 540 mg/l.
pH 403 units
Acidity to pH 4.5 436 mg1L
Acidity to pH 8.3 435 mg/L
Alkalinity to pH 8.3 415 mg/L
Alkalinity to pH 4.5 410 - mgrL
IOC 680 ma(L
Turbidity 76 NTU
Coliforrrr Total Tube 1100 ml
COMMENTS:
Chloride 940 -g/L.
Chlorophyll a EPA 445.0 modified option ugmL
Color: True 80 c.u-
Color: (pH) 83 pH= C.U.
Color: pH 7.6 82 c.u.
Cyanide 720 nwL
Fluoride 951 mo(L
Formaldehyde 71880 UWL
Cease and Oils 556 MWL.
Hardness Total900 mg)L
Specific Cond. 95 umhoslcm
MBAS 39260 mg/L
Phenols 32730 uglL
Sulfate 945 nwL
Sulfide 745 mg(l,
Boron
Tannin & Ligtin ug(L
Hexavalent Chromium uglL
Bicarbonate mg'L.
Carbonate MIA
Total Dissolved Solids mall,
NH3 as N 610 m91L.
TKN an N 625 miVL
NO2 plus NO3 as N 630 mg/l,
P: Total as P 665 mg/L
PO4 as P 70507 mgmL.
P: Dissolved as P 666 mg/I,
K-Potassium mg L
Cd- Cadmium 1027 ug/L.
Cr-Chromium:Total 1034 ug/L
Cu- Copper 1042 uSIL
Ni-Nickel 1067 ug/L
Pb- Lead 1051 uWL
Zn- Zinc 1092 ug/L
V-Vanadmm uWL
Ag- Silver 1077 ug/L
Al- Aluminum 1105 ug/L
Be- Beryllium 1012 ug/L
Ca- Calcium 916 mgrL
Co- Cobalt 1037 ug/L
Fe- Iron 1045 ug/L
Mo-Molybdenum ug(L
Sb-Antimony ug/L
Sn-Tin ug/L
TI-Thallium ug1L.
TrTttaaum ug%L
141-1631 ng7L
Li -Lithium 1132 ugrL
Mg- Magnesium 927 rr;WL
Mn-Manganese 1055 ug'L
Na- Sodium 929 mc-jl-
Arsenie:Tntal1002 ug/L
Se- Selenium 1147 ug(L
Hg- Mercury 71900 ug/L
Ds -Barium ug'L,
Organochlorine Pesticides
Organophosphoms Pesticides
Organonitrogen Pesticides
Acid Herbicides
Base/Neutraf&Acid Extractable Organics
TPH Diesel Range
Purgeable Organics (VOA bottle req'd)
TPH Gasoline Range
TPH/BTEX Gasoline Range
Phytoplankton
Temperature on arrival (eC):
k.i r: 1

Report to: _FRO .
Sample Anomaly Report (SAR)
Lab Number: Ab26499
Station Location: Lick Creek @ US
220
Sample ID:
County: Montgomery Region
Sample Type: Stream Priority: Emergency Collector:
Date collected: 2/8/08 Date received: 2/8108 Date analyzed
Affected Parameter(s):
BOD
Analytical Area (check one):
❑ W CH ❑ METALS
❑ NUT ®MICRO
The following anomalies occurred (check all that apply):
❑Samples
❑improper container used
❑VOA vials with headspace
❑Sulfide samples with headspace
❑Samples not received, but listed on fieldsheet
❑Samples received, but not listed on fieldsheet
❑Mislabeled as to tests, preservatives, etc.
❑Holding time expired
❑Prior to receipt in lab
❑After receipt in lab
❑Insufficient quantity for analysis
El Sample exhibits gross non -homogeneity
❑Sam le not chemically preserved properly
�PH out of range (record pH):
❑Improper chemical
❑Residual chlorine present in sample
❑Color interference
❑Heavy emulsion formed during extraction
❑Sample bottle broken in lab - no reportable results
El Other (specify):
Fayetteville
D. Strickland
2/8/08
❑VOA ❑SVOA
❑PEST
®Quality Control
❑Instrument failure — no reportable results
❑Analyst error — no reportable results
❑Surrogates
❑None added
❑Recovery outside acceptance limits
El Spike recovery
❑None added
❑Recovery outside acceptance limits
❑Failed to meet criteria for precision
❑Internal standards
❑Blank contamination
®QC data reported outside of controls (e.g., QCS, LCS)
❑Incorrect procedure used
❑SOP intentionally modified with QA and Branch Head
a proval
Invalid instrument calibration
❑Elevated detection limits due to:
❑Insufficient sample volume
Comments: Both of the two glucose glutamic acid standards were below the acceptable range of 167.5 to 228.8 mg/L at 159.7mg/L
and 152.2mg/L. Sample was not seeded.
Corrective Action:Ongoing investigation to determine the cause of low GGA standard results.
[]Samples were rejected by DWQ Lab. Authorized by: Date:
❑Accepted and analyzed after notifying the collector or contact person and determining that another sample could not be secured.
❑Sample(s) on hold until:
®Sample reported with qualification. Data qualification code used:G5
❑Other (explain):
Notification Required? ❑ Yes ❑ No
Person Contacted: Date:
Form completed by: ela Dexte Date: 2/15/2008
Lead Chemist Review (initial):
WBiOCHEM m,,O
❑Mir PALS
❑ PEST
❑ VOA
Branch Head Review (initial /;" Jf •0 T
QAIQC Review (initi C
vlo-e
ZATo mi s%Laba rat n ry\S AR
❑SVOA
Logged into database by (initial):
Mrn/Qldbs
A