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HomeMy WebLinkAboutNCG060413_MRO Copy MONITORING REPORT_20210223M NCDEQ Division of Energy, Mineral and Land Resources Co T Stormwater Discharge Monitoring Report (DMR) Form for N0006000'v, f� C) (0 G U Food and Kindred CP Lc (n Click here for instructions `o g r Complete, sign, scan and submit the DMR via the Stormwater NPDES Permit_ Data Monitoring Report (DMR) 46ad form within 30 days of receiving sampling results. Mail the original, signed hard copy of the DMR to the appropriate DEMA Regional Office. Certificate of Coverage No, NCG06 0 4 1 Facility Name: Amazon.com Services LLC - DLT3 Person Collecting Samples: Parker Cliatt Laboratory Name: EurofinsTestAmerica Facility County: Cabarrus Laboratory Cert. No.: 269 Discharge during this period: ❑■ Yes ❑ No (if no, skip to signature and dote) Has your facility implemented mandatory Tier response actions for any benchmark exceedances? ❑ Yes N No If so, which Tier (I, II, or III)? Part A: Analytical Monitoring Requirements for Outfalls with Industrial Activities— Benchmarks in (Rod) Parameter Code Parameter Outfall01 Outfall02 Outfall03 Outfall Outfall N/A Receiving Stream Class C C C N/A Date Sample Collected MM/DD/YYYY 01/25/2021 01/25/2021 01/25/2021 46529 24-Hour Rainfall in inches 0.6 0.6 0.6 00556 Oil & Grease in mg/L (30) < 1.4 < 0.56 3.5 C0530 TSS in mg/L (100 or 50*) < 2.5 < 5 7.9 00400 pH in standard units (6.0 •- 9.0) 7.58 7.94 7.13 31616 Fecal Coliform per 100 ml of N/A N/A N/A freshwater (.i.Eifit)) 61211 Enterococci per 100 ml of saltwater N/A N/A N/A 700340 Chemical Oxygen Demand in mg/L < 5 < 5 150 Part B: Vehicle & Equipment Maintenance Areas — Benchmarks in (Red) Parameter Code Parameter Outfall Outfall Outfall Outfall Outfall N/A Receiving Stream Class N/A Date Sample Collected MM/DD/YYYY 00552 1 Non -Polar Oil & Grease in mg/L (:15) New Motor/Hydraulic Oil Usage in NCOIL gal/month T___7 Outfalls to Outstanding Resource Waters (ORW), High Quality Waters (HOW), Trout Waters (Tr) and Primary Nursery Areas (PNA) have a benchmark TSS limit of F;u rn '/L. All other water classifications have a benchmark of 1.00 rng/I . Notes (optional): "I certify by my signature below, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for know re of Permittee or Delegated Authorized Individual L:: 2 J_//— i Date DocuSign Envelope ID: 11OECCCC-4COB-4164-917A-E418C922A295 AMAZON.COM SERVICES LLC DELEGATION OF AUTHORITY (Boese, Nickens, Wilson, Vijaykumar, Sanches) I, Michael D. Deal, being the duly elected, qualified and acting President, Treasurer and Secretary of Amazon.com Services LLC (the "Company"), and having been authorized by resolutions duly adopted by the Board of the Company, do hereby sub -delegate my authority as follows: DELEGATION OF AUTHORITY 1. Effective September 10, 2020, authority is hereby delegated to Michael Boese, Amber Nickens, Paul Wilson, Vimal Vijaykumar, and Debora Sanches ("Authorized Representatives") to act on behalf of the Company and in its name and place to execute and file environmental and permitting applications, and related documents with government authorities. This Delegation of Authority shall not include any authority to commit spend on behalf of the Company. SUBDELEGATION 2. The Authorized Representatives are not authorized to subdelegate the authority granted to them in this delegation. TERM OF DELEGATION 3. The authority delegated hereby shall terminate upon the earlier of: (i) when revoked by the Company, the undersigned, any successor in responsibility to the undersigned, or any person to whom the undersigned reports; or (ii) immediately upon the cessation of the Authorized Representative's employment by Amazon.com, Inc. ("Amazon"), the Company, and Amazon's affiliates. 4. The authority delegated herein shall remain in full force and effect until terminated in accordance with Section 3 of this Delegation of Authority regardless of the appointment status of the undersigned with the Company. DATED: September 10, 2020 Docusigned by: PL41 Pd -=-WFJeDG4 Michael D. Deal President, Treasurer and Secretary eurofins Environmen'tTesting America Eurofins TestAmerica, Savannah 5102 LaRoche Avenue Savannah, GA 31404 Tel: (912)354-7858 Laboratory Job IU: 680-194358-1 Client Project/Site: Storm Water - Amazon Warehouses (ULT3) For: ERM-West 1920 Main Street Suite 300 Irvine, California 92614 . Attn: Doug J Wade VO G j Authorized for release by: 21912021 7:58: 90 AM Lauren Evans, Project Manager 1 (615)301-5034 Lauren. Evans@Eurofinset.com The test results in this report meet all 2003 NELAC, 2009 TNI, and 2016 TNI requirements for accredited parameters, exceptions are noted in this report. This report may not be reproduced except in full, and with written approval from the laboratory. For questions please contact the Project Manager at the e-mail address or telephone number listed on this page. This report has been electronically signed and authorized by the signatory. Electronic signature is intended to be the legally binding equivalent of a traditionally handwritten signature. Results relate only to the items tested and the sample(s) as received by the laboratory. Deeo`ilroKi,i on ,/6 os navy Client: ERM-West Project/Site: Storm Water - Amazon Warehouses (DLT3) Dualifiers General Chemistry Qualifier Qualifier Description J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value. Abbreviation These commonly used abbreviations may or may not be present in this report. a Listed under the "D" column to designate that the result is reported on a dry weight basis %R Percent Recovery CFL Contains Free Liquid CFU Colony Forming Unit CNF Contains No Free Liquid DER Duplicate Error Ratio (normalized absolute difference) Dil Fac Dilution Factor DL Detection Limit (DoD/DOE) DL, RA, RE, IN Indicates a Dilution, Re -analysis, Re -extraction, or additional Initial metals/anion analysis of the sample DLC Decision Level Concentration (Radiochemistry) EDL Estimated Detection Limit (Dioxin) LOD Limit of Detection (DoD/DOE) LOQ Limit of Quantitation (DoD/DOE) MCL EPA recommended "Maximum Contaminant Level' MDA Minimum Detectable Activity (Radiochemistry) MDC Minimum Detectable Concentration (Radiochemistry) MDL Method Detection Limit ML Minimum Level (Dioxin) MPN Most Probable Number MQL Method Quantitation Limit NC Not Calculated ND Not Detected at the reporting limit (or MDL or EDL if shown) NEG Negative / Absent POS Positive / Present PQL Practical Quantitation Limit PRES Presumptive QC Quality Control RER Relative Error Ratio (Radiochemistry) RL Reporting Limit or Requested Limit (Radiochemistry) RPD Relative Percent Difference, a measure of the relative difference between two points TEF Toxicity Equivalent Factor (Dioxin) TEQ Toxicity Equivalent Quotient (Dioxin) TNTC Too Numerous To Count Job ID: 680-194358-1 Eurofins TestAmerica, Savannah Page 2 of 16 2/9/2021 ��u��c�� ��U0linar)f Client: ERM-West Project/Site: Storm Water - Amazon Warehouses (DLT3) Lab Sample ID Client Sample ID Matrix 680-194358-1 DLT3_Sample_Point 01_20210125 Water 680-194358-2 DLT3_ Sample_ Point_02_20210125 Water 680-194358-3 DLT3_Sample_Point 03_20210125 Water Job ID: 680-194358-1 Collected Received Asset ID 01/25/2108:53 01127/2 009,40 01/25/21 08:27 01/27/21 09:40 01/25/2110:26 01/27/2109:40 Eurofins TestAmerica, Savannah Page 3 of 16 2/0/2021 Case Narrative Client: ERM-West Project/Site: Storm Water - Amazon Warehouses (DLT3) Job ID: 680-194358-1 Laboratory: Eurofins TestAmerica, Savannah Narrative Job Narrative 680-194358-1 Comments No additional comments. Job ID: 680-194358-1 Receipt The samples were received on 1/27/2021 9:40 AM; the samples arrived in good condition, and where required, properly preserved and on ice. The temperature of the cooler at receipt was 0.50 C. General Chemistry Method SM 2540D: Insufficient sample volume was provided to produce results within the specifications of SM 2540D which requires at least 2.5 mg dried residue with a sample volume not to exceed 1 L. A sample volume less than 1 L, that yielded less than 2.5 mg dried residue, was provided for the following sample: DLT3_Sample_Point_02_20210125 (680-194358-2). Methods SM 2540D: The sample duplicate precision for the following sample associated with analytical batch 680-653748 was outside control limits: (680-194340-C-3 DU). The associated Laboratory Control Sample / Laboratory Control Sample Duplicate (LCS/LCSD) precision met acceptance criteria. Methods 16648: Insufficient sample volume was available to perform a matrix spike/matrix spike duplicate/sample duplicate (MS/MSD/DUP) associated with preparation batch 680-654887. Methods SM 5220D: COD results may be biased high due to chloride interference for the following sample: DLT3_Sample_Point_03_20210125 (680-194358-3). No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page. Eurofins TestAmerica, Savannah Page 4 of 16 2/9/2021 Gfiv ate SarnpAe Resufts Client: ERM-West Project/Site: Storm Water - Amazon Warehouses (DLT3) Client Sample ID: DLT3_Sample_Point_01_20210125 Date Collected: 01/25/21 08:53 Date Received: 01/27/21 09:40 General Chemistry Analyte Result Qualifier RL Oil & Grease (HEM) <1.4 5.0 Chemical Oxygen Demand <5.0 10 Total Suspended Solids <2.5 2.5 Job ID: 680-194358-1 Lab Sample ID: 680-194358-1 Matrix: Water MDL Unit D Prepared Analyzed Dil Fac 1.4 mg/L 02/08/21 08:06 02/08/2110:36 1 5.0 mg/L 02104/2113:59 1 2.5 mg/L 01/28/2114:44 1 Eurofins TestAmerica, Savannah Page 5 of 16 2/9/2021 Gfie 'c Sample Results Client: ERM-West Job ID: 680-194358-1 Project/Site: Storm Water - Amazon Warehouses (DLT3) Client Sample ID: DLT3_ Sam ple_Point_02_20210125 Lab Sample ID: 680-194358-2 Date Collected: 01/25/21 08:27 Matrix: Water Date Received: 01/27/21 09:40 General Chemistry _ Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Oil & Grease (HEM) <0.56 2.0 0.56 mg/L 02/08/21 08:06 02/08/21 10:36 1 Chemical Oxygen Demand <5.0 10 5.0 mg/L 02/04/21 13:59 1 Total Suspended Solids <5.0 5.0 5.0 mg/L 01/28/21 14:44 1 Eurofins TestAmerica, Savannah Page 6 of 16 2/9/2021 Client: ERM-West Project/Site: Storm Water - Amazon Warehouses (DLT3) Client Sample ID: DLT3_ Sample_Point_03_20210125 Date Collected: 01/25/21 10:26 Date Received: 01/27/21 09:40 General Chemistry Analyte Oil & Grease (HEM) Chemical Oxygen Demand Total Suspended Solids Job ID: 680-194358-1 Lab Sample ID: 680-194358-3 Matrix: Water Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac 3.5 J 8.7 2.4 mg/L 02/08/2108:06 02/08/2110:36 1 150 100 50 mg/L 02/08/2109:09 10 7.9 2.5 2.5 mg/L 01/28/21 11:30 1 Eurofins TestAmerica, Savannah Page 7 of 16 2/9/2021 CSC sarfipe Gym-*s Client: ERM-West Project/Site: Storm Water - Amazon Warehouses (DLT3) Method: 1664B - HEM and SGT-HEM Lab Sample ID: MB 680-654887/1-A Matrix: Water Analysis Batch: 654937 Job ID: 680-194358-1 Client Sample ID: Method Blank Prep Type: TotalINA Prep Batch: 654887 MB MB Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Oil & Grease (HEM) <1.4 5.0 1.4 mg/L 02/08/21 08:06 02/08/21 10:36 1 e Lab Sample ID: LCS 680-654887/2-A Client Sample ID: Lab Control Sample Matrix: Water Prep Type: TotalINA Analysis Batch: 654937 Prep Batch: 654887 Spike LCS LCS %Rec. Analyte Added Result Qualifier Unit D %Rec Limits Oil & Grease (HEM) 40.0 33.40 mg/L 84 78 -114 Lab Sample ID: LCSD 680-654887/3-A Client Sample ID: Lab Control Sample Dup Matrix: Water Prep Type: TotalINA Analysis Batch: 654937 Prep Batch: 654887 Spike LCSD LCSD %Rec. RPD Analyte Added Result Qualifier Unit D %Rec Limits RPD Limit Oil & Grease (HEM) 40.0 35.00 mg/L 88 78 - 114 5 18 Method: 5220D-2011 - Chemical Oxygen Dernand Lab Sample ID: MB 680-65464113 Client Sample ID: Method Blank Matrix: Water Prep Type: Total/NA Analysis Batch: 654641 MB MB Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Chemical Oxygen Demand <5.0 10 5.0 mg/L 02/04/21 13:59 1 Lab Sample ID: LCS 680-654641/4 Client Sample ID: Lab Control Sample Matrix: Water Prep Type: Total/NA Analysis Batch: 654641 Analyte Chemical Oxygen Demand Lab Sample ID: 680-194358-2 MS Matrix: Water Analysis Batch: 654641 Sample Sample Analyte Result Qualifier Chemical Oxygen Demand <5.0 Lab Sample ID: 680-194358-2 MSD Matrix: Water Analysis Batch: 654641 Analyte Chemical Oxygen Demand Sample Sample Result Qualifier ------------------ <5.0 Spike LCS LCS %Rec. Added Result Qualifier Unit D %Rec Limits 60.0 49.7 mg/L 99 90 -110 Client Sample ID: DLT3_Sample_Point_02_20210125 Prep Type: TotalINA Spike MS MS %Rec. Added Result Qualifier Unit D %Rec Limits 50.0 50.7 mg/L 101 90 - 110 Client Sample ID: DLT3_Sample_Point_02_20210125 Prep Type: Total/NA Spike MSD MSD %Rec. RPD Added Result Qualifier Unit D %Rec Limits RPD Limit 50.0 49.0 mg/L 98 90 - 110 3 30 Eurofins TestAmerica, Savannah Page 8 of 16 2/9/2021 CSC Sample Results Client: ERM-West Job ID: 680-194358-1 Project/Site: Storm Water - Amazon Warehouses (DLT3) Method: 5220D-2011 - Chemical Oxygen Demand (Continued) Lab Sample ID: MB 680-654899/3 Client Sample ID: Method Blank Matrix: Water Prep Type: Total/NA Analysis Batch: 654899 MB MB Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Chemical Oxygen Demand <5.0 10 5.0 mg/L 02/08/21 09:09 1 3 Lab Sample ID: LCS 680-664899/4 Client Sample ID: Lab Control Sample Matrix: Water Prep Type: Total/NA Analysis Batch: 654899 Spike LCS LCS %Rec. Analyte Added Result Qualifier Unit D %Rec Limits Chemical Oxygen Demand 50.0 54.1 mg/L 108 90-110 Method: SM 2540D - Solids, Total Suspended (TSS) FLab Sample ID: MB 680-653706/1 Client Sample ID: Method Blank Matrix: Water Prep Type: Total/NA Analysis Batch: 653706 MB MB Analyte Result Qualifier Total Suspended Solids <2.5 Lab Sample ID: LCS 680-653706/2 Matrix: Water Analysis Batch: 653706 Analyte Total Suspended Solids Lab Sample ID: LCSD 680-653706/3 Matrix: Water Analysis Batch: 653706 Analyte Total Suspended Solids Lab Sample ID: MB 680-663748/1 Matrix: Water Analysis Batch: 653748 MB MB Analyte Result Qualifier Total Suspended Solids <2.5 Lab Sample ID: LCS 680-653748/2 Matrix: Water Analysis Batch: 653748 Analyte Total Suspended Solids RL MDL Unit D Prepared Analyzed oil Fac 2.5 2.5 mg/L 01/28/21 11:30 1 Client Sample ID: Lab Control Sample Prep Type: Total/NA Spike LCS LCS %Rec. Added Result Qualifier Unit D %Rec Limits 951 874 mg/L 92 80 - 120 Client Sample ID: Lab Control Sample Dup Prep Type: Total/NA Spike Added 951 Spike Added 951 LCSD LCSD Result Qualifier Unit 952 mg/L %Rec. RPD D %Rec Limits RPD Limit 100 80-120 9 25 Client Sample ID: Method Blank Prep Type: Total/NA RL MDL Unit D Prepared Analyzed Dil Fac 2.5 2.5 mg/L 01/28/2114:44 1 Client Sample ID: Lab Control Sample Prep Type: Total/NA LCS LCS Result Qualifier Unit 976 mg/L %Rec. D %Rec Limits 103 80-120 Eurofins TestAmerica, Savannah Page 9 of 16 2/9/2021 Client: ERM-West Job ID: 680-194358-1 Project/Site: Storm Water - Amazon Warehouses (DLT3) Method: SM 2540D - Solids, Total Suspended (TSS) (Continued) Lab Sample ID: LCSD 680-663748/3 Client Sample ID: Lab Control Sample Dup Matrix: Water Prep Type: Total/NA Analysis Batch: 653748 Spike LCSD LCSD %Rec. RPD Analyte Added Result Qualifier Unit D %Rec Limits RPD Limit Total Suspended Solids 951 968 mg/L 102 80 -120 1 25 Eurofins TestAmerica, Savannah Page 10 of 16 2/9/2021 Client: ERM-West Project/Site: Storm Water - Amazon Warehouses (DLT3) General Chemistry Analysis Batch: 663706 Job ID: 680--194358-1 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 680-194358-3 DLT3_Sample_Point_03_20210125 Total/NA Water SM 2540D MB 680-653706/1 Method Blank Total/NA Water SM 2540D LCS 680-653706/2 Lab Control Sample Total/NA Water SM 2540D LCSD 680-65370613 Lab Control Sample Dup Total/NA Water SM 2540D Analysis Batch: 663748 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 680-194358-1 DLT3_Sample_Point 01_20210125 Total/NA Water SM 2540D 680-194358-2 DLT3_Sample_Point_02_20210125 Total/NA Water SM 2540D MB 680-653748/1 Method Blank Total/NA Water SM 2540D LCS 680-65374812 Lab Control Sample Total/NA Water SM 2540D LCSD 680-653748/3 Lab Control Sample Dup Total/NA Water SM 2540D Analysis Batch: 654641 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 680-194358-1 DLT3_ Sample_ Point _01_20210125 Total/NA Water 5220D-2011 680-194358-2 DLT3_Sample_Point 02_20210125 Total/NA Water 5220D-2011 MB 680-654641/3 Method Blank Total/NA Water 5220D-2011 LCS 680-654641/4 Lab Control Sample Total/NA Water 5220D-2011 680-194358-2 MS DLT3_ Sample_ Point _02_20210125 Total/NA Water 5220D-2011 680-194358-2 MSD DLT3_Sample_Point_02_20210125 Total/NA Water 5220D-2011 Prep Batch: 654887 Lab Sample ID Client Sample ID Prep Type 680-194358-1 DLT3_ Sample_Point_01_20210125 Total/NA 680-194358-2 DLT3_Sample_Point_02_20210125 Total/NA 680-194358-3 DLT3_ Sample_ Point_03_20210125 Total/NA MB 680-654887/1-A Method Blank Total/NA LCS 680-654887/2-A Lab Control Sample Total/NA LCSD 680-654887/3-A Lab Control Sample Dup Total/NA Analysis Batch: 654899 Matrix Method Prep Batch Water 1664E Water 1664E Water 1664B Water 1064B Water 1664E Water 1664B Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 680-194358-3 DLT3_Sampie_Point_03_20210125 Total/NA Water 5220D-2011 MB 680-654899/3 Method Blank Total/NA Water 5220D-2011 LCS 680-654899/4 Lab Control Sample Total/NA Water 5220D-2011 Analysis Batch: 654937 Lab Sample ID Client Sample ID 680-194358-1 DLT3_Sample_Point_01_20210125 680-194358-2 DLT3_ Sample_Point_02_20210125 680-194358-3 DLT3_Sample_Point_03_20210125 MB 680-654887/1-A Method Blank LCS 680-654887/2-A Lab Control Sample LCSD 680-654887/3-A Lab Control Sample Dup Prep Type Matrix Total/NA Water Total/NA Water Total/NA Water Total/NA Water Total/NA Water Total/NA Water Method Prep Batch 1664B 654887 1664B 654887 1664B 654887 1664B 654887 1664E 654887 1664B 654887 Eurofins TestAmerica, Savannah Page 11 of 16 2/9/2021 Lab Chronid Client: ERM-West Project/Site: Storm Water - Amazon Warehouses (DLT3) Client Sample ID: DLT3_Sample_Point_01_20210125 Date Collected: 01/25/21 08:53 Date Received: 01/27/21 09:40 Batch Batch Dil Initial Prep Type Type Method Run Factor Amount Total/NA Prep 16646 497 mL Total/NA Analysis 1664B 1 Instrument ID: NOEQUIP Total/NA Analysis 5220D-2011 1 2 mL Instrument ID: SPC7 Total/NA Analysis SM 2540D 1 1000 mL Instrument ID: NOEQUIP Client Sample ID: DLT3_ Sam ple_Point_02_20210125 Date Collected: 01/26121 08:27 Date Received: 01/27/21 09:40 Batch Batch Dil Initial Prep Type Type Method Run Factor Amount Total/NA Prep 1664B 1246 mL Total/NA Analysis 1664B 1 Instrument ID: NOEQUIP Total/NA Analysis 5220D-2011 1 2 mL Instrument ID: SPC7 Total/NA Analysis SM 2540D 1 500 mL Instrument ID: NOEQUIP Client Sample ID: DLT3_ Sam ple_Point_03_20210125 Date Collected: 01/26/21 10:26 Date Received: 01/27/21 09:40 Batch Batch Dil Initial Prep Type Type Method Run Factor Amount Total/NA Prep 1664B 286 mL Total/NA Analysis 1664B 1 Instrument ID: NOEQUIP Total/NA Analysis 5220D-2011 10 2 mL Instrument ID: SPC7 Total/NA Analysis SM 2540D 1 1000 mL Instrument ID: NOEQUIP Job ID: 680-194358-1 Lab Sample ID: 680-194358-1 Matrix: Water Final Batch Prepared Amount Number or Analyzed Analyst Lab 500 mL 654887 02/08/21 08:06 JAS TAL SAV 654937 02/08/21 10:36 JAS TAL SAV 2 mL 654641 02/04/21 13:59 ALG TAL SAV ©' 1000 mL 653748 01/28/21 14:44 MS TAL SAV Lab Sample ID: 680-194358-2 Matrix: Water Final Batch Prepared Amount Number or Analyzed Analyst Lab 500 mL 654887 02/08/21 08:06 JAS TAL SAV 654937 02/08/21 10:36 JAS TAL SAV 2 mL 654641 02/04/21 13:59 ALG TAL SAV 1000 mL 653748 01/28/21 14:44 MS TAL SAV Lab Sample ID: 680-194358-3 Matrix: Water Final Batch Prepared Amount Number or Analyzed Analyst Lab 500 mL 654887 02/08/21 08:06 JAS TAL SAV 654937 02/08/21 10:36 JAS TAL SAV 2 mL 654899 02/08/21 09:09 ALG TAL SAV 1000 mL 653706 01/28/21 11:30 MS TAL SAV Laboratory References: TAL SAV = Eurofins TestAmerica, Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL (912)354-7858 Eurofins TestAmerica, Savannah Page 12 of 16 2/9/2021 Accreditation/Certification Summary Client: ERM-West Job ID: 680-194358-1 Project/Site: Storm Water - Amazon Warehouses (DLT3) Laboratory: Eurofins TestAmerica, Savannah The accreditations/certifications listed below are applicable to this report. Authority Program Identification Number North Carolina (WW/SW) State 269 Expiration Date 12-31-21 Eurofins TestAmerica, Savannah Page 13 of 16 2/9/2021 Method Summary Client: ERM-West Project/Site: Storm Water - Amazon Warehouses (DLT3) Job ID: 680-194358-1 Method Method Description Protocol Laboratory 1664B HEM and SGT-HEM 1664B TAL SAV 5220D-2011 Chemical Oxygen Demand SM TAL SAV SM 2540D Solids, Total Suspended (TSS) SM TAL SAV 1664B HEM and SGT-HEM (Aqueous) 1664B TAL SAV Protocol References: 1664B = EPA-821-98-002 SM = "Standard Methods For The Examination Of Water And Wastewater" Laboratory References: TAL SAV = Eurofins TestAmerica, Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL (912)354-7858 Eurofins TestAmerica, Savannah Page 14 of 16 2/9/2021 0 m M m ONc�£ gg �� aa z 0 o c N �ZQ z2 S�Q� U C SS Epp �20n.da NNr7>?iN O 2 C cEc C U c 6 m ^ C m o e c� O (0 a Z UUO 5ryry�� ��❑qG y IZNilZ N b� LL .1` am UOW 2 a) c u ,- suulquoo jo jsywnN 1+401 r d z 0. 1Ep a n a o a C N J tz O n Q q� U ate+ Q cD LC Yl y�j a q N (A > A Q •sue a o a Ll b E i E a � 3i U m C w o U U m (SU) s011oS popuedenS lgol - OCV9Z — — N E m c (000) puew*0 w0Ax0 teo1-40.00M — — Ur� ol cD; Qu N (es-0 y 110) 613H - 869% rq q4 K (ON Jo a+A) OSIYJSNI u++oiIad V� m E (ON Jo s*AJ sldweS PvNlld Pl+ld Xr > > °p _ m J 7 W U y Qa C g ° m o ° Eo U � � g E Q a m E r u° o r 11 II CD v ' v) U a ti e E r . ) i= a ` 0 r ° � a � D O s m c cu m u a # c a o E d u o 0 d -- l p a C c o d Q �1 T o o a S + 1 u m= ^ U .2 r S EEo o d a a u o Z c � @ o (c71 v7 ? J t ` 1 a c I - 1 2 -,lug 3 o�"i nN NqS� N .. is�C G y pN z v Y �, "> Ot, N H �ch (� y a g 7 V U OV w3 (A Q f1 9 MV GE 7 W 2m �48 Page 15 of 16 2/9/2021 Login Sample Receipt Checklist Client: ERM-West Job Number: 680-194358-1 Login Number: 194358 List Number: 1 Creator: Sims, Robert D Question List Source: Eurofins TestAmerica, Savannah Answer Comment Radioactivity wasn't checked or is </= background as measured by a survey _ N/A meter. The cooler's custody seal, if present, is intact. True Sample custody seals, if present, are intact. True The cooler or samples do not appear to have been compromised or True tampered with. Samples were received on ice. True Cooler Temperature is acceptable. True Cooler Temperature is recorded. True COC is present. True COC is filled out in ink and legible. True COC is filled out with all pertinent information. True Is the Field Sampler's name present on COC? True There are no discrepancies between the containers received and the COC. True Samples are received within Holding Time (excluding tests with immediate True HTs) Sample containers have legible labels. True Containers are not broken or leaking. True Sample collection date/times are provided. True Appropriate sample containers are used. True Sample bottles are completely filled. True Sample Preservation Verified. N/A There is sufficient vol. for all requested analyses, incl. any requested True MS/MSDs Containers requiring zero headspace have no headspace or bubble is True <6mm (1/4"). Multiphasic samples are not present. True Samples do not require splitting or compositing. True Residual Chlorine Checked. N/A Eurofins TestAmerica, Savannah Page 16 of 16 2/9/2021