NCS000329_MONITORING INFO_20190819

m,711,10
STORMWATER DIVISION CODING SHEET
NCS PERMITS
PERMIT NO.
(�I
�v
DOC TYPE
❑FINAL PERMIT
MONITORING REPORTS
❑ APPLICATION
❑ COMPLIANCE
❑ OTHER
DOC DATE
❑ �b I � �1 �'
YYYYMMDD

44-ATI
August 9, 2019
Attn: Central Files
N.C. Division of Water Quality
1617 Mail Service Center
Raleigh, NC 27699-1617
Central Files:
REECEIVED
AUG 19 2019
CEN t W` L FILES
DWR SECTION
P.O. Box 5030
2021) Ashcrafi A,C1WC
Monroe. NC 281 11-5030
Phone: [phone]
Fax: [phone]
Ismail: tyler.nierccr@aliineta[s.cnrn
Attached, please find stormwater monitoring data for Permit No NCS000329. The originals and
one copy are included. The monitoring data is for the following monitoring schedule:
monitoring Period
Sample Number
Start
End
Year 10 — Period 1
19
March 1, 2019
August 3 l , 2019
Analytical monitoring includes:
• Outfall #01 (13), commingled stormwater
• Outfall #02 (13), non -commingled stormwater
• Outfall #03 (13), non -commingled stormwater
• Non -Contact Cooling Water #1 - #8
If you have any questions or need additional information, please contact me at 704-289-451 1.
Thank you.
Sincerely,
Tyler Mercer
Manager, EH&S

Ativae - Bakers Plant��� �� �t�tv�c
Stvrmwater Monitoring Report Foim
Sample Elate: 7 -046 /1
Sample Location -
Person Collecting Samples:
Laboratory Performing Analysis:
Analytical Techniques and Methods:
Results of Sample Analysis:
Sample Time: !l-'D�'Q....
Stormwater Discharge Outfall #01 (Commingled)
Drainage Area = 2 915,470s . ft. = 69 acres
% Impervious = 34%
40 CFR Part 136
Parameter
Results (mg/1)
Benchmark Values (mg/1)
BOD
30
COD
7 D
120
TSS
100
Cadmium
0.001
Chromium, total recoverable
1
Copper, total recoverable
0.007
Nickel, total recoverable
�.
0.26
Zinc, total recoverable
©
0.067
Oil and Grease
20
Temp (receiving stream)
(deg C)
32 (deg C)
Total Residual Chlorine
0.017
pH
(std units)
6-9 (std Units)
Storm Date: 7 o?3 19 Storm Duration: % a (Hrs.) Inches of Rainfall: 6.35'
Duration of time preceding rain event exceeding 0.111: 9.R (Hrs.)
Estimated Flow C'aiculation:
Q=CIA
Q(Total) = Q(Pervious Area) + Q(Impervious Area)
Q(tot., cfs) _ (A x inches rain/12 inches/ft. x 69 acres x .66) + .9 x inches raut/I2inehes/ft. x 69 x .34)
Q(Total, cfs) = 1.5 l80 x O. ' j` (Inches of rain) + 1.7595 x D , 3.r (Inches of rain)

aceAnalytical
WW..Pecelsba.WM
August 02, 2019
Scott Ryan
Allvac
Monroe, NC
RE: Project: SW Outfall#01(B)
Pace Project No.: 92438396
Dear Scott Ryan:
Pace Analytical Services, LLC
9800 Kircey Ave, Suite 100
Huntersville, NC 28078
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on July 24, 2019. The
results relate only to the samples included in this report. Results reported herein conform to the most
current, applicable TNUNELAC standards and the laboratory's Quality Assurance Manual, where
applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Matthew Brainard
[e-mail]
[phone]
Project Manager
Enclosures
cc: Larry Allen, Allvac
Tyler Mercer, ATI Specialty Materials
David Pope, Ailvac
pCCRF4
TN
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
Page 1 of 15

�;a'neAnalj4ica(
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Project: SW Outfall#01(8)
Pace Project No.: 92438396
Charlotte Certification iDs
9800 Kincey Ave. Ste 100, Huntersville, NC 2BO78
Louisiana/NELAP Certification # t.A170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NCO30
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
South Carolina Certification #: 99006001
FloridalNELAP Certification #: E87627
Kentucky UST Certification #: 84
VirginiaNELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
VirginiaNELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
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SAMPLE ANALYTE COUNT
Project: SW Outfall#01(13)
Pace Project No.: 92438396
Paco Analytical Services, LLC
9800 Kincey Ave. Suite 100
HuntersvIle, NC 28078
[phone]
Lab ID Sample ID Method
Analysts
Analytes
Reported
Laboratory
92438396001 SW OUTFALL #01 (B) EPA 1664E
JMS
1
PASI-C
EPA 200.7 Rev 4.4 1994
SH1
5
PASI-A
SM 254OD-2011
MJP
1
PASI-A
SM 4500-CI G-2011
GC
1
PASI-A
SM 521OB-2011
JP1
1
PASI-A
SM 5220D-2011
GC
1
PASI-A
REPORT OF LABORATORY ANALYSIS
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Pace Analytical Services, LLC
�'"
;acmnalytical 9800 Kincey Ave. Suite 100
Huntersville, NC 28078
www.pacefabs.com [phone]
f
ANALYTICAL RESULTS
Project: SW Outfall*01(B)
Pace Project No.: 92438396
Sample: SW OUTFALL #01 (B) Lab ID: 92438396001 Collected: 07/23/19 16:12 Received: 07/24/19 11:45 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qua]
Field Data
Analytical Method:
Collected By
DPJ
1
07/23/19 16:27
Collected Date
07/23/19
1
07/23/19 16:27
Collected Time
16:15
1
07/23/19 16:27
pH
6.9 Sid, Units
0.10
1
07123/19 16:27
Temperature
28.1 deg C
0.50
1
07/23/19 16:27
HEM, Oil and Grease
Analytical Method: EPA 1664E
Oil and Grease
ND mg1L
5.0
1
07/31/19 05:43
200.7 MET ICP
Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994
Cadmium
ND ug1L
1.0
1
07/31/19 13:56 08/01119 21:55 7440-43-9
Chromium
ND ug1L
5.0
1
07/31/19 13:56 08/01/19 21:55 7440-47-3
Copper
30.2 ug1L
5.0
1
07/31119 13:56 08/01/19 21:55 7440-50-8
Nickel
5.0 ug1L
5.0
1
0713l/19 13:56 08/01/19 21:55 7440-02-0
Zinc
10.5 ug1L
10.0
1
07/31/19 13:56 08/01/19 21:55 7440-66-6
2540D Total Suspended Solids
Analytical Method: SM 2540D-2011
Total Suspended Solids
7.2 mg1L
4.2
1
07/29/19 13:06
4500CL G Chlorine, Residual
Analytical Method: SM 4500-CI G-2011
Chlorine, Total Residual
0.16 mg1L
0.024
1
07/29/19 18:48 7782-50-5 H3
5210E BOD, 5 day
Analytical Method: SM 5210B-2011
BOD, 5 day
10.4 mg1L
2.0
1
07/25/19 03:10 07/30/19 04:33
5220D COD
Analytical Method: SM 5220D-2011 Preparation Method: SM 5220D-2011
Chemical Oxygen Demand
67.0 mg1L
25.0
1
07/26/19 15:30 07/29/19 17:10
REPORT OF LABORATORY ANALYSIS
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ace Analytical
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Project: SW Outfall#01(B)
Pace Project No.: 92438396
QC Batch: 489444
QC Batch Method: EPA 1664E
Associated Lab Samples: 92438396001
METHOD BLANK: 2641152
Associated Lab Samples: 92438396001
Parameter Units
Oil and Grease mg/L
LABORATORY CONTROL SAMPLE: 2641153
Parameter Units
Oil and Grease mg/L
Pace Analytical Services, LLC
9800 Ki ncey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Analysis Method: EPA 1664B
Analysis Description: 1664 HEM, Oil and Grease
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 4.8 07/31/19 05742
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
38.5 37.0 96 78-114
Results presented on this page are in the units indicated by the "Units" column except where an altemate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 08/02/2019 11:30 AM without the written consent of Pace Analytical Services, LLC.
Page 5 of 15

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J
Project: SW Outfall#01(B)
Pace Project No.: 92438396
QC Batch: 489431
QC Batch Method: EPA 200.7 Rev 4.4 1994
Associated Lab Samples: 92438396001
METHOD BLANK: 2641114
Associated Lab Samples: 92438396001
Parameter
Units
Cadmium
ug/L
Chromium
ug/L
Copper
ug/L
Nickel
ug/L
Zinc
ug1L
QUALITY CONTROL DATA
Analysis Method:
Analysis Description:
Matrix: Water
EPA 200.7 Rev 4.4 1994
200.7 MET
Blank
Result
Reporting
Limit
Analyzed
ND
1.0
08/01/19 21:11
ND
5.0
08/01119 21:11
ND
5.0
08/01/19 21:11
ND
5.0
08/01/19 21:11
ND
10.0
08/01/19 21:11
Qualifiers
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28076
[phone]
LABORATORY CONTROL SAMPLE:
2641115
Spike
LCS
LCS
% Rec
Parameter
Units
Cone.
Result
% Rec
Limits Qualifiers
Cadmium
ug/L
500
489
98
85-115
Chromium
ug/L
500
494
99
85-115
Copper
ug/L
500
494
99
85-115
Nickel
ug/L
500
492
98
85-115
Zinc
ug/L
500
497
99
85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2641116
MS
92437770001
Spike
Parameter
Units
Result
Cone.
Cadmium
ug/L
ND
500
Chromium
ug/L
ND
500
Copper
ug/L
22.4
500
Nickel
ug1L
ND
500
Zinc
ug/L
133
500
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2641118
MS
92438403001
Spike
Parameter
Units
Result
Conc.
Cadmium
ug/L
ND
500
Chromium
ug/L
NO
500
Copper
ug/L
53.0
500
Nickel
ug/L
5.4
500
Zinc
ug/L
45.9
500
2641117
MSD
Spike
MS
MSD
MS
MSD
% Rec
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
500
503
499
101
100
70-130
1
500
503
497
100
99
70-130
1
500
517
516
99
99
70-130
D
500
500
493
99
98
70-130
1
500
640
632
101
100
70-130
1
2641119
MSD
Spike
MS
MSD
MS
MSD
% Rec
Conc.
Result
Result
% Rec
% Rec
Limits RPD
500
502
504
100
101
70-130 1
500
502
512
100
102
70-130 2
500
547
555
99
100
70-130 1
500
496
502
98
99
70-130 1
500
544
551
100
101
70-130 1
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full.
Date: 08/02/2019 11:30 AM without the written consent of Pace Analytical Services, LLC.
Qual
Qual
Page 6 of 15

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aceAnapical
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Pace Analytical Services, LLC
9800 KinceyAve. Suite too
Huntersville, INC 28078
[phone]
QUALITY CONTROL DATA
Project: SW Outfall#01(8)
Pace Project No.: 92438396
QC Batch: 488845 Analysis Method: SM 25400-2011
QC Batch Method: SM 2540D-2011 Analysis Description: 2540D Total Suspended Solids
Associated Lab Samples: 92438396001
METHOD BLANK: 2638666
Associated Lab Samples: 92438396001
Parameter
Units
Total Suspended Solids
mg1L
LABORATORY CONTROL SAMPLE:
2638667
Parameter
Units
Total Suspended Solids
mg/L
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 2.5 07129/1913:04
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
250 250 100 90-110
SAMPLE DUPLICATE: 2639441
92438421003
Dup
Parameter
Units
Result
Result
Total Suspended Solids
mg/L
58.7
57.3
SAMPLE DUPLICATE: 2639442
92438506002
Dup
Parameter
Units
Result
Result
Total Suspended Solids
mg1L
440
444
RPD Qualifiers
2
RPD Qualifiers
i
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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QUALITY CONTROL DATA
Project: SW 0utfall#01(B)
Pace Project No.: 92436396
QC Batch: 489113 Analysis Method: SM 4500-CI G-2011
QC Batch Method: SM 4500-CI G-2011 Analysis Description: 4500CL G Chlorine, Total Residual
Associated Lab Samples: 92438396001
METHOD BLANK: 2639819
Associated Lab Samples: 92438396001
Parameter Units
Chlorine, Total Residual mg/L
SAMPLE DUPLICATE: 2639820
Parameter Units
Chlorine, Total Residual mg/L
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 0.024 07129/1918:44
92438396001 Dup
Result Result RPD Qualifiers
0.16 0.16 4 H3
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, INC 28078
[phone]
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date'. 08102/2019 11:30 AM without the written consent of Pace Analytical Services, LLC.
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aceAnalyticaJ0
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QUALITY CONTROL DATA
Project: SW Outfall#01 (B)
Pace Project No.: 92438396
QC Batch: 488319 Analysis Method: SM 521OB-2011
QC Batch Method: SM 521OB-2011 Analysis Description: 5210B BOD, 5 day
Associated Lab Samples: 92438396001
METHOD BLANK: 2636157
Associated Lab Samples: 92438396001
Parameter Units
BOD, 5 day mg/L
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 2.0 07/30/19 03:34
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
hiuntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE:
2636158
Spike LCS LCS
% Rec
Parameter
Units
Conc. Result % Rec
Limits Qualifiers
BOD, 5 day
mg/L
198 203 103
84.6-115
SAMPLE DUPLICATE: 2636160
92438416001 Dup
Parameter
Units
Result Result RPD
Qualifiers
BOD, 5 day
mg/L
ND ND
Results presented on this page are In the units Indicated by the "units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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QUALITY CONTROL DATA
Project: SW Outfall#01(B)
Pace Project No.: 132438396
QC Batch: 488767 Analysis Method: SM 5220D-2011
QC Batch Method: SM 5220D-2011 Analysis Description: 5220D COD
Associated Lab Samples: 92438396001
METHOD BLANK: 2638169
Associated Lab Samples: 92438396001
Parameter Units
Chemical Oxygen Demand mg/L
LABORATORY CONTROL SAMPLE: 2638170
Parameter Units
Chemical Oxygen Demand mg1L
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 25.0 07/2911917:06
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
750 738 98 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 26313171 2638172
MS MSD
92438348001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RP❑ Qual
Chemical Oxygen Demand mg/L 3010 100 100 3090 3100 85 95 90.110 0 M1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2638173 2638174
MS MSD
92438402001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RP❑ Qual
Chemical Oxygen Demand mg/L ND 100 100 119 121 99 102 90-110 2
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 08102/2019 11:30 AM without the written consent of Pace Analytical Services, LLC.
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QUALIFIERS
Project: SW Outfall#01(B)
Pace Project No.: 92438396
DEFINITIONS
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL-Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis ofAcrolein and Acrylonitrile by EPA
Method 8260,
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services -Asheville
PAS!-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
H3 Sample was received or analysis requested beyond the recognized method holding time.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
REPORT OF LABORATORY ANALYSIS
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QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: SVVOulfall#01(B)
Pace Project No.: 92438396
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersviile, NC 28078
[phone]
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Analytical
Batch
92438396001
SW OUTFALL #01 (B)
92438396001
SW OUTFALL #01 (B)
EPA 1664B
489444
92438396001
SW OUTFALL #01 (8)
EPA 200.7 Rev 4.4 1994
489431
EPA 200.7 Rev 4.4 1994
489630
92438396001
SW OUTFALL #01 (8)
SM 254OD-2011
488845
92438396001
SW OUTFALL #01 (B)
SM 4500-CI G-2011
489113
92438396001
SW OUTFALL #01 (B)
SM 521OB-2011
488319
SM 521 OB-2011
488349
92438396001
SW OUTFALL #01 (B)
SM 5220D-2011
488767
SM 5220D-2011
489096
Date: 08/02/2019 11:30 AM
REPORT OF LABORATORY ANALYSIS
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Page 12 of 15

Document Name:
Document Revised: February 7, 2018
2
r�CBf�f?81�alCc?rra
y`
Sample Condition Upon Recel t SCUR
Page 1 of 2
Document No.:
issuing Authority:
F•CAR•CS-033-Rev.06
Pace Carolinas Quality Office
Laboratory receiving samples.
Asheville ❑ Eden[—]
Client Name:
Greenwood ❑ Huntersville ❑ Raleigh❑ Mechanicsville❑
WQ#:92438396
I 'S C' Project g:
,i�, .� ���-1��ry;_...__.__..____. 11111111111111 III i III
Courier; ❑Fed Ex ❑UPS ❑U5P5 ❑Client
❑ Commercial ❑. Pace ❑Other: 92438396
Custody Seat Present? ❑Yes Oft Seals Intact? ❑Yes 0
Dattlrnilials Person Examining Contents`. %u- L1
Packing Material: []Bubble Wrap ❑Bubble Bags ❑None ❑ Other Biological Tissue Frozen?
Thermometer: ❑Yes ❑❑ No N/A
E1,1A Gun tD: 92T O48 Type of ice: i❑wet ❑Blue ❑None
Cooler Temp ('C). Z • tl Correction Factor: Add/Subtract ('C) 0.0
� Temp should be above freezing to 6'C
4
Cooler Temp Corrected ('C): ❑Samples out of temp criteria. Samples on ice, cooling process
has begvn
USDA Regulated Sail ((D'N/A, water sample]
Did samples originate in a quarantine zone within the United States: CA. NY, or SC (check maps)? Old samples originate from a foreign source (iniernatianaliV,
MVPs MNn ineludina Hawaii and Puerto Rice l? f-lYe..s RNo
Comments/Discre panc :
Chain of Custody Present?
• Yes
Na
N/A
1.
Samples Arrived within Hold Time?
DY/es
ONO
❑N/A
2.
Short Hold Time Analysis e72 hr.)?
i ves
ONO
N A
3.
Rush Turn Around Time Requested?
❑vas
M No
NIA
4,
Sufficient Volume?
; Yes
No
NJA
S.
Correct Containers Used?
Ves
❑No
❑N/A
6.
-Pace Containers Used?
dYes
ONo
UNIA
Containers Intact?
Dyes
No
N/A
7.
Dissolved analysis: Samples Field Filtered?
❑Yes
[]NO
JBN/A
S.
$ample Labels Match COC?
QYes
❑No
❑N/A
9.
-Includes Date/Time/ID/Analysis Matrix:
i
Headspace in VOA Vials (s5-6mm)?
OYes
No
H/A
10,
Trip Blank Present?
❑Yes
ONO
EINIA
11.
Trip Blank Custody Seals Present?
Yes
No
N/A
COMMENTS/SAMPLE DISCREPANCY
Lot ID of split containers:
CLIENT NOTIFiCATICINJRESOLUTiON
Field Data Required) [:]Yes [:]NO
Person contacted: Date/Time:
Project Manager SCURF Review: /%,/ Date: �� �. H i
Project Manager SRF Review: (. Date:
Page 13 of 15

Document Name:
Document Revised: February 7, 2013
Sample Condition Upon Receipt(SCi1R)
Page 1 of 2
Document No.:
Issuing Authority:
F-CAR-CS.033-Rev.06
Pace Carolinas Quality Office
"Check mark top half of box if pH and/or dechlorination is
verified and within the acceptance range for preservation
samples.
Exceptions: VOA, Coliform, TOC, Olf and Grease, DF10/8015 (water) DOC, LLHg
*"Bottom half of box is to list number of bottle
Project
WO#:92439396
p": MWB Due Date: 08/02/19
CLIENT: 92—Rllvac NC
E
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11
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pH Adjustment Log for Preserved Samples
sample 10
Type of Preservative
pH upon receipt
Date preservatlon adjusted
Time preservation
adjusted
Amount of Preservative
added
lot a
Note: whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form wll! be sent to the North Carallna D HfVft Certification Office ji.e.
Out of hold, incorrect preservative, out of temp, incorrect containers.
Page 14 of 15

Stormwater Monitorin
Chain of Custody Record
Project Number/Nance:
SW Outfall #01(13)
jProject Location: AT1 SM - Bakers
Sample -'s Signature:
Date: 3- 9
v
a
o
�
F
T
a U
L
Requested Test Parameters
I .t
(U
rr
3.
S'
G
G /Q
HNO3
Y
Total Recoverable: Chromium, Nickel. Copper. Zinc
Q
G
G /m
HNO3
Y
Cadmitim +
G
/ i'
HCL
Y
Oil & Grease
G
G /0
112SO4
Y
COD
O///o
G
G /©
Nonc
Y
BOD
G
G /(�3
None
Y
TSS
G
G /®
None
Y
Residual Chlorine
Onsite , ield
p1l Analysis
Onsite Field rem erature Analysis
pH: �._9 (s.u.)
Sample Time:
Temp: B.I (0C) Sampic TEmc:
_
Analysis "rune:
Analysis 'rime:
Meter Calibrated: e
Thermometer Calibrated: / N
amptin g and field analysis completed by:
ReEincluishccl By:
Received Brl
Date:
Tin1c: 6 Q.
Datc:
Relinquished By: ' f
'
Received By:
Date: 7/,,IL '
-Time-, 'fl
Date: / 21, Timc: �
EHS-SW-Chain of Costody Outfa€I 01-Rev 001
Page 15 of 15

3". 1 A
- T
Allvac
Ativ c m Bakes Plant
Stormwater Mgt rnutori.n Re ort Form
Sample Date: _ % a3 /4
Sample Location:
Person Collecting Samples:
Laboratory Performing Analysis:
AnalyticalTechniques and Methods:
Results of Sample Analysis:
Sample Time: =1/S
Stormwater Dischar a Out
fA11 #02 (Non -Commingled)
Drainage Area = 212 952s . ft. = 4.9 acres
% Impervious =12%
40 CFR Part 1.36
Parameter
Results (mg/1)
Benchmark Values (mg/l)
BOD
30
COD
120
TSS
,7
100
Cadmium
Al'p
0.001
Chromium, total recoverable
ND
1
Copper, total recoverable
®, � .�
0.007
Nickel, total recoverable
0.60$-
0.26
Zinc, total recoverable
D Y6
0.067
pH
7 f (std units)
6-9 (std units)
Stem Date: :7 2j :ZQ Stormu Duration: 4-,Rjf (His.) Inches of RaWhil:
Duration of time precedtng rain event exceeding 0.111: �a — (Hrs.)
Estimated Flow Calculation:
Q = CIA
Q(Total) = Wervious Area) + Q(Impervious .tea)
Q(tot., efs) = (.4 x inches rain/12 inches/ft. x 4.9 acres x .88) + .9 x inches rain/12inches/ft. x 4.9 x. 12)
Q(Tota1, cfs) = 0.1437 x D. 3S (Inches of rain) + 0.0441 x
= . 196 1-6 cfs
O. 3S (Inches of rain)

acanalytical
www.pacelehs.cam
August 02, 2019
Scott Ryan
Allvac
Monroe, NC
RE: Project: SW Outfall #02 (B)
Pace Project No.: 92438403
Pace Analytical Services, Lill
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Dear Scott Ryan:
Enclosed are the analytical results for sample(s) received by the laboratory on July 24, 2019. The
results relate only to the samples included in this report. Results reported herein conform to the most
current, applicable TNIINELAC standards and the laboratory's Quality Assurance Manual, where
applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Matthew Brainard
[e-mail]
[phone]
Project Manager
Enclosures
cc: Larry Allen, Allvac
Tyler Mercer, ATI Specialty Materials
David Pope, Allvac
pCCAg��
I
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 13

aceAnalytical
wwwpacelabs.wm
Project: SW Outfall #02 (13)
Pace Project No.: 92438403
Pace Analytical Services, LLC
9800 KinceyAve . Suite 100
Huntersville, NC 28078
[phone]
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
VirginiaNELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
VirginiaNELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not he reproduced, except in full,
without the written consent of Pace Analytical Services, UC. Page 2 of 13

laceAnalyficalo
wwwpacelabs.mn
SAMPLE ANALYTE COUNT
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 1 OD
Huntersville, NC 28078
[phone]
Project:
Pace Project No.:
SW Outfall #02 (B)
92438403
Analytts
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92438403001
SW OUTFALL #02 (B)
EPA 200.7 Rev 4.4 1994
SH1
5
PASI-A
SM 2540D-2011
MJP
1
PASI-A
SM 521OB-2011
JP1
1
PASI-A
SM 5220D-2011
GC
1
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LAC- Page 3 of 13

leAnalytical"
www.pacelabs.corn
ANALYTICAL RESULTS
r
Pace Analytical Services, LLC
9800 KinceyAve_ Suite 100
Huntersville, NC 28078
[phone]
Project: SW Outfal1 #02 (B)
Pace Project No.: 92438403
Sample: SW OUTFALL #02 (B) Lai) ID: 92438403001 Collected: 07/23/19 15:50 Received: 07/24119 11A5 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Field Data
Analytical Method:
Collected By
DPJ
1
07/23/19 15:58
Collected Date
07/23/19
1
07/23/19 15:58
Collected Time
15:51
1
07/23/19 15:58
pH
7.1 Sid. Units
0.10
1
07/23/19 15:58
Temperature
23.5 deg C
0.50
1
07/23/19 15:58
200.7 MET ICP
Analytical Method: EPA200.7 Rev 4.4 1994 Preparation Method: EPA200.7
Rev 4.4 1994
Cadmium
ND ug1L
1 A
1
07/31/19 13:56
08/01/19 22:01
7440-43-9
Chromium
ND uglL
5.0
1
07/3111913:56
08/01/1922:01
7440-47-3
Copper
53.0 uglL
5.0
1
07/3111913:56
08/01/1922:01
7440-50-8
Nickel
5.4 uglL
5.0
1
07/31/19 13:56
08/01/19 22:01
7440-02-0
Zinc
45.9 uglL
10.0
1
07/3111913:56
08101/1922:01
7440-66-6
2540D Total Suspended Solids
Analytical Method: SM 25400-2011
Total Suspended Solids
26.7 mg/L
2.5
1
07129/19 13:06
5210B BOD, 5 day
Analytical Method: SM 521 OB-2011
BOD, 5 day
4.6 my/L
2.0
1
07/25/19 03:10
07/30/19 04:30
B2
5220D COD
Analytical Method: SM 5220D-2011
Preparation
Method: SM 5220D-2011
Chemical Oxygen Demand
45.8 mg1L
25.0
1
07/26/19 15:3D
07129119 17:11
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/02/2019 11:30 AM without the written consent of Pace Analytical Services, LLC, Page 4 of 13

acMnalytrcal
www.pscelabs.wm
QUALITY CONTROL DATA
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Project: SW Outfall #02 (8)
Pace Project No.: 92438403
QC Batch: 489431
Analysis Method:
EPA 200.7 Rev 4.4 1994
QC Batch Method: EPA 200.7 Rev 4A 1994
Analysis Description:
200.7 MET
Associated Lab Samples: 92438403001
METHOD BLANK: 2641114
Matrix:
Water
Associated Lab Samples: 92438403001
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Cadmium
ug1L
ND
1.0 08/01/19 21:11
Chromium
ug/L
ND
5.0 08/01/19 21:11
Copper
ug/L
ND
5.0 08/01/19 21:11
Nickel
uglL
ND
5.0 08/01/19 21:11
Zinc
uglL
ND
10.0 08/01/19 21:11
LABORATORY CONTROL. SAMPLE: 2641115
Spike
LCS
LCS % Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
Cadmium
ug/L
500
489
98 85-115
Chromium
uglL
500
494
99 85-115
Copper
ug/L
500
494
99 85-115
Nickel
ug/L
500
492
98 85-115
Zinc
ug/L
500
497
99 85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2641116
MS
92437770001
Spike
Parameter
Units
Result
Conc.
Cadmium
ug/L
ND
500
Chromium
ug/L
ND
500
Copper
ug/L
22.4
500
Nickel
uglL
N❑
500
Zinc
uglL
133
500
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2641118
MS
92438403001
Spike
Parameter
Units
Result
Conc.
Cadmium
ug/L
ND
500
Chromium
uglL
ND
500
Copper
uglL
53.0
500
Nickel
uglL
5.4
500
Zinc
ug/L
45.9
500
2641117
MSD
Spike MS MSD MS MSD % Rec
Conc. Result Result % Rec % Rec Limits RPD
500 503 499 101 100 70-130 1
500 503 497 100 99 70-130 1
500 517 516 99 99 70-130 0
500 500 493 99 98 70-130 1
500 640 632 101 100 70-130 1
2641119
MSD
Spike
MS
MSD
MS
MSD
% Rec
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
500
502
504
100
101
70-130
1
500
502
512
100
102
70-130
2
500
547
555
99
100
70-130
1
500
496
502
98
99
70-130
1
500
544
551
100
101
70-130
1
Results presented on this page are In the units indicated by the "Units" column except where an aitemate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08102/2019 11:30 AM without the written consent of Pace Analytical Services, LLC.
Qual
Qual
Page 5 of 13

leAnalytical
»,vw.paeeJahs.cotb
QUALITY CONTROL DATA
Pace Analytical Services, LLC
9800 Kincey Ave, Suite 100
Huntersville, NC 28078
[phone]
Project: SW Outfall #02 (B)
Pace Project No.: 92438403
QC Batch: 488845
Analysis Method:
SM 25400-2011
QC Batch Method: SM 254OD-2011
Analysis Description:
2540D Total Suspended Solids
Associated Lab Samples: 92438403001
METHOD BLANK: 2638666
Matrix: Water
Associated Lab Samples: 92438403001
Blank Reporting
Parameter
Units
Result Limit
Analyzed Qualifiers
Total Suspended Solids
mg/L
ND
2.5 07/29/19 13:04
LABORATORY CONTROL SAMPLE: 2638667
Spike, LCS
LCS % Rec
Parameter
Units
Conc. Result
% Rec Limits Qualifiers
Total Suspended Solids
mg1L
250 250
100 90-110
SAMPLE DUPLICATE: 2639441
92438421003 Dup
Parameter
Units
Result Result
RPD Qualifiers
Total Suspended Solids
mg/L
58.7
57.3 2
SAMPLE DUPLICATE: 2639442
92438506002 Dup
Parameter
Units
Result Result
RPD Qualifiers
Total Suspended Solids
mg1L
440
444 1
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/02/2019 11:30 AM without the written consent of Pace Analytical Services, LLC. Page 6 of 13

lacieAnalyticalo
www.petefaftcortl
Project: SW Outfall #02 (B)
Pace Project No.: 92438403
QC Batch: 488319
QC Batch Method: SM 521 OB-2011
Associated Lab Samples: 92438403001
METHOD BLANK: 2636157
Associated Lab Samples: 92438403001
Parameter Units
600, 5 day mg/L
LABORATORY CONTROL SAMPLE: 2636158
Parameter Units
1301), 5 day mg1L
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NO 28078
[phone]
QUALITY CONTROL DATA
Analysis Method: SM 521OB-2011
Analysis Description: 5210B BOD, 5 day
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 2.0 07/30/19 03:34
Spike LCS LCS % Rec
Conc. Result % Rec. Limits Qualifiers
198 203 103 84.6-115
SAMPLE DUPLICATE: 2636160
92438416001 Dup
Parameter Units Result Result
BOD, 5 day mg1L ND ND
RPD Qualifiers
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/02/2019 11:30 AM without the written consent of Pace Analytical Services, LLC. Page 7 of 13

leAnalXical
wtMvpacelabs.com
Project: SW Outfall #02 (B)
Pace Project No.: 92438403
QC Batch: 488767
QC Batch Method: SM 5220D-2011
Associated Lab Samples: 92438403001
METHOD BLANK: 2638169
Associated Lab Samples: 92438403001
Parameter Units
Chemical Oxygen Demand mg1L
LABORATORY CONTROL SAMPLE: 263BI70
Parameter Units
Chemical Oxygen Demand mg/L
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Analysis Method: SM 5220D-2011
Analysis Description: 5220D COD
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 25.0 0712911917:06
Spike LCS LCS % Rec
Cone. Result % Rec Limits Qualifiers
750 738 98 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2638171 2638172
MS MSD
92438348001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual
Chemical Oxygen Demand mg/L 3010 100 100 3090 3100 85 95 90-110 0 M1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2638173 2638174
MS MSD
92438402001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Cone. Cone. Result Result % Rec %6 Rec Limits RPD Qual
Chemical Oxygen Demand mg/L ND 100 100 119 121 99 102 90-110 2
Results presented on this page are in the units indicated by the "Unite" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08102/2019 11:30 AM without the written consent of Pace Analytical Services, LLC.
Page 8 of 13

laceAnalytical
www.pscelab&c=
QUALIFIERS
Project: SW Outfall #02 (2)
Pace Project No.: 92438403
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL- Adjusted Method Detection Limit.
Pace Analytical Services, LLC
9800KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyse in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis ofAcrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services -Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
B2 Oxygen usage is less than 2.0 for all dilutions set. The reported value is an estimated less than value and is calculated
for the dilution using the most amount of sample.
M1 Matrix spike recovery exceeded OC limits. Batch accepted based on laboratory control sample (LCS) recovery.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/02/2019 11:30 AM without the written consent of Pace Analytical Services, LLC. Page 9 of 13

ac6Analyiical
wwwDM10h3-c ro
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: SW Outfall #02 (B)
Pace Project No.: 92438403
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, INC 28078
[phone]
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Analytical
Batch
92438403001
SW OUTFALL #02 (B)
92438403001
SW OUTFALL #02 (B)
EPA 200.7 Rev 4.4 1994
489431
EPA 200.7 Rev 4.4 1994
489630
92438403001
SW OUTFALL #02 (13)
SM 254OD-2011
488845
92438403001
SW OUTFALL #02 (B)
SM 521OB-2011
488319
SM 521OB-2011
488349
92438403001
SW OUTFALL #02 (B)
SM 5220D-2011
488767
SM 52200-2011
489096
Date: G810212019 11:30 AM
0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 10 of 13

Document Name:
pocument Revised: February 7, 201a
a
.aceAnarytfea!
Sample Condition Upon Recei i(SCUR
Page 1 of 2
Document No,;
Issuing Authority:
F-CAR-CS-0334Rev.06
Pace Carolinas Quailly Office
Laboratory receiving samples:
Asheville ❑ Eden[] Greenwood ❑ Huntersville 12/ Raleigh[] Mechanicsville[]
Client Name: Project #; W0 : 92438403
Courier: ❑Fed Ex� 1- ❑UPS 1, ❑USPS []Client
❑ Commercial Pace ❑Other: 92436403
Custody Seal Present? []Yes []No Seals Intact? ❑Yes ❑No
DatellnitialsPersonExamining Contents:
Parking Material: ❑Bubble Wrap []Bubble Bags QNone ❑ Other Biological Tissue Frozen?
Thermometer- ,Guy Ip: []Yeses []No ❑1 14/A
©tR
j 92TO48 Type of ice: ❑%ket [)Blue []None
__ Correction Factor: Add/Subtract {°C) q Q Cooler Temp (°C): I Y
1 L Temp should be above freezing to VC
Cooler Temp Corrected ('CI; I []samples out of temp criteria. Samples on ice, cooling process
has begun
USDA Regulated Sail ((2/M/A, water sample)
Did samples originate in a quarantine zone within the United Slates: CA, NY, or SC (check maps)? Did samples originate from a foreign source Iinternationally.
l—lyes nNn inrludinrt Hawaii and Pcsertn Rlcol7 i—IYnc MNn
Cam ments/Discre anc :
Chain of Custody Present?
es
No
N/A
1.
Samples Arrived within Hold Time?
Myles
ONO
❑N/A
2,
Short !fold Time Analysis <72 hr.)?
Yes
No
NJA
3.
Rush Turn Around Time Requested?
Yes
oio
(]NJA
4.
Sufficient volume?
Yei
Na
aN A
S.
Correct Containers Used?
-Pace Containers Used?
QYes
43
ONO
ONO
❑NIA
N/A
6.
Containerslntact?
QYes
QNo
NJA
7.
Dissolved analysis: Samples Field Filtered?
Oyes.
©No
NJA
g.
Sample Labels Match COC?
-Includes Date/Time/ID/Analysis Matrix:
©Yes
ON.
❑NJA
4.
Heads ace In VOA Vials (>5-6rnm)?
Yes
❑No
j]N A
10.
Trip Blank Present?
Tri Blank Custody Seals Presents
QYes
Yes
©No
Na
Cgv/A
tuJA
11.
COMMENTS/SAMPLE DISCREPANCY Field data Required? ❑Yes ❑No
Lot ID of split Containers:
CLIENT N01IF1CATi0NJRE5OLtiTION
Person contacted: /1 Date/Time:
Project Manager SCURF Review: iL /) Rate: 7 L 4 C
�.. r }
Protect Manager SRF Review: r Date: -? ,) {
Page 11 of 13

DOcilment Name,.
Document Revised: February7, 2018
c?CBAnalXICdf
Sample Condition Upon Recei t(SCUR)
Page 1 of 2
Document No.:
Issuing Authority:
F-CAR-CS•033-Rev.06
Pace Carolinas Quality Office
'Check (nark top half of box If pH and/or dechiorination Is
verified and within the acceptance range for preservation
samples.
EMcepbans: VOA, Coliform, TOC, 011 and Grease, ORO/8015 (water) DOC, LLHg
"Bottom half of box is to list number of bottle
Project # W0 : 92433403
PM: MWB Due Date: 08/02/19
CLIENT: 92-Aiivae NC
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pH Adjustment Log for Preserved Samples
Sample ID
Type of Preservative
pH upon receipt
Date pfeservatlon adjusted
Time preservatlan
adjusted
amount of Preservative
added
Lai 4
Now Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this farm will be sent to the Borth Carallna DEHNR Certification Office (i.e.
Out of hold, incorrect preservative, out of temp, incorrect contafners.
Page 12 of 13

Stormwater Monit�rill�
Chain of Custody Record
Project Number/Nance:
W Out fall #02 B
Pr gjcct Location: A-l'1 SM - Bakers
Sample 's Si nature:
Date: %- 3
Requested Test Parameter's
+
D
�r G)
v
- 3 Id
G
G /d
f-fNO3
Y
Total Recoverable: Chronlirim, Ni • el COp per. Lii}c
G
G /O
HNO3
Y
Cadmium
y
G
G /m
1-12SO4
Y
COD
G
G AP
None
Y
BOD
3•'
G
G /0
None
Y
TSS
Onsite Field
ell Analysis
Onsite Field Temperature Analysis
pl-1: 7• / (s.u.)
Sample Time:
Temp: aMs- (T) Sample Timc: ,3 �
Analysis Time:
Analysis'limc: , y_7
Meter Calibrated: Yes
f hermometer Calibratcd: (55 / N
Samplinp, and field analysis completed by:
Relinquished B
Recelvccl K t y tvy.�
Date: -Z9
a
Dine:
ITituctl
Rclin uisl cd B G
Received B
Date: L
Time:
L 1
Date: - / )1
Time: 5 4
EHS-SW-Chain of Coslody Oulfall 02-Rev 009
Page 13 of 13

ear
'1Allvac
Afivac ® Bakers Plant
Storrnwater Mortitorineport Farm
Sample Date: ;"- 3
Sample Location:
Person Collecdag Samples:
Laboratory Performing Analysis:
Analyftcal Techniques and Methods:
Results of Swale Analvsis:
Samppe Time: _ 9 .
Stormwater QiscljAr e Outfall #03 on -Comm led
Drainage Area = 336,590sg. ft. = 7.8 acres
% Impervious = 15%
40 CFR Part 136
I
Parameter
Results (mg/1)
Benchmark Values (mg/1)
BOB
a
30
COI?
120
TSS
19.9
100
Cadmium
/VP
0.001
Chromium, total recoverable
D
1
Copper, total recoverable
. D 7
0.007
Nickel, total recoverable
0.26
Zinc, total recoverable
�Q f
0.067
pH
7 a (std units)
6-9 (std units)
Storm Date: Z23YI Storm Duration: 2. 4� (Hxs.) Inches of Rainfall:
Duration of time preying rain event exceeding 0.1 `°: - 6--_2 - — (l-Irs.)
Estimated Flow Calculation:
Q=CIA
Q(Total) = Q(Pervious Area) + Q(7mpervious ,area)
Q(tot., cfs) = (.4 x inches rain/i 2 inches/ft. x 7.8 acres x .&5) + .9 x inches rain/121nches/ft. x 7.8 x. 15)
Q(Total, cfs) = 0.2210 x (Inches of rain) + 0.0878 x 0. W (Inches of rain)
_ , & zpm ,.__ _ cfs

0
aceAnalytical
www.paceiabs.com
August 02, 2019
Scott Ryan
Allvac
Monroe, NC
RE: Project: SW Outfall #03 (B)
Pace Project No.: 92438402
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Dear Scott Ryan:
Enclosed are the analytical results for sample(s) received by the laboratory on July 24, 2019. The
results relate only to the samples included in this report. Results reported herein conform to the most
current, applicable TNIINELAC standards and the laboratory's Quality Assurance Manual, where
applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Matthew Brainard
[e-mail]
[phone]
Project Manager
Enclosures
cc: Larry Allen, Allvac
Tyler Mercer, ATI Specialty Materials
David Pope, Allvac
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 13

leAnalytr'ca!
www.pecera63.com
Project: SW Outfall #03 (B)
Pace Project No.: 92438402
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville. NC 28078
[phone]
Charlotte Certification IDS
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
LouisianalNELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87646
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
VrginiaNELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, L.L.C. Page 2 of 13

� K
ace Analytical
www.petelabs.eam
Project: SW Outfall #03 (B)
Pace Project No.: 92438402
Lab ID Sample ID
92438402001 SW OUTFALL #03 (13)
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE ANALYTE COUNT
Method
Analysts
Analysts
Reported
Laboratory
EPA 2007 Rev 4.4 1994
SW
5
PASI-A
SM 254OD-2011
MJP
1
PASI-A
SM 52106-2011
JP1
1
PASI-A
SM 5220D-2011
GC
1
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 3 of 13

aceAnalytical
w6wPacelaLs.eom
ANALYTICAL RESULTS
I. ..M 4
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Project: SW Outfall #03 (B)
Pace Project No.: 92438402
Sample: SW OUTFALL #03 (e) Lab ID: 92438402001 Collected: 07/23/19 15:33 Received: 07/24/19 11:45 Matrix: Water
Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual
Field Data
Analytical Method:
Collected By
DPJ
1
07/23/19 15:38
Collected Date
07/23/19
1
07123M9 16:38
Collected Time
15:26
1
07/23/19 15:38
pH
7.2 Std. Units
0.10
1
07/23/1915:38
Temperature
23.8 deg C
0.50
1
07/23119 15:58
200.7 MET ICP
Analytical Method: EPA 200.7 Rev 4.4
1994 Preparation
Method: EPA200.7 Rev 4.4 1994
Cadmium
ND ug/L
1.0
1
07/31/19 13:56 08/01/19 21:58
7440-43.9
Chromium
ND ug/L
5.0
1
07/31/19 13:56 08/01/19 21:58
7440-47-3
Copper
17.8 ug1L
5.0
1
07/31/19 13:56 08/01/19 21:58
7440-50-8
Nickel
ND ug1L
5.0
1
0713111913:56 08101/19 21 ;58
7440-02-0
Zinc
16.8 ug1L
10.0
1
07/31/19 13:56 08/01/19 21:58
7440-66-6
2540D Total Suspended Solids
Analytical Method: SM 254OD-2011
Total Suspended Solids
19.8 mg/L
5.0
1
07/29/19 13:06
5210B BOD, 5 day
Analytical Method: SM 521OB-2011
BOD, 5 day
2.2 mg1L
2.0
1
07/25/19 03:10 07/30/19 04:29
5220D GOD
Analytical Method: SM 5220D-2011
Preparation Method: SM 5220D-2011
Chemical Oxygen Demand
ND mg/L
25.0
1
07/26/19 15:30 07/29/19 17:10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/02/2019 11:30 AM without the written consent of Pace Analytical Services, LLC.
Page 4 of 13

aceAnalytical
www pacelabs. cm
QUALITY CONTROL DATA
Project: SW Outfall #03 (B)
Pace Project No.: 92438402
QC Batch: 489431 Analysis Method: EPA 200.7 Rev 4.4 1994
QC Batch Method: EPA 200.7 Rev 4.4 1994 Analysis Description: 200.7 MET
Associated Lab Samples: 92438402001
METHOD BLANK: 2641114
Matrix:
Water
Associated Lab Samples: 92438402001
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Cadmium
ug1L
N❑
1.0
08/01119 21:11
Chromium
uglL
ND
5.0
08/01119 21:11
Copper
uglL
ND
5.0
08/01119 21:11
Nickel
ug1L
ND
5.0
08/01119 21:11
Zinc
ug1L
ND
10.0
08/01/19 21:11
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huniersville, NC 2807E
[phone]
LABORATORY CONTROL SAMPLE:
2641115
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits Qualifiers
Cadmium
U91L
500
489
98
85-115
Chromium
ug1L
500
494
99
85-115
Copper
uglL
500
494
99
85-115
Nickel
uglL
500
492
98
85-115
Zinc
uglL
500
497
99
85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2641116
2641117
MS
MSD
92437770001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
Cadmium
ug1L
ND
500
500
503
499
101
100
70-130
1
Chromium
ug1L
NO
500
500
503
497
100
99
70-130
1
Copper
ug1L
22.4
500
500
517
516
99
99
70-130
0
Nickel
ug1L
NO
500
500
500
493
99
98
70-130
1
Zinc
ug1L
133
500
500
640
632
101
100
70-130
1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2641118
MS
92438403001
Spike
Parameter
Units
Result
Conc.
Cadmium
uglL
ND
500
Chromium
uglL
ND
500
Copper
uglL
53.0
500
Nickel
uglL
5.4
500
Zinc
uglL
45.9
500
2641119
MSD
Spike
MS
MSD
MS
MSD
% Rec
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
500
502
504
100
101
70-130
1
500
502
512
100
102
70-130
2
500
547
555
99
100
70-130
1
500
496
502
98
99
70-130
1
500
544
551
100
101
70-130
1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right or the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/0212019 11:30 AM without the written consent of Pace Analytical Services, LLC.
Qual
Qual
Page 5 of 13

aceAnalytical
www.pacefabs.cam
QUALITY CONTROL DATA
Project: SW Outfall #03 (B)
Pace Project No.: 92438402
QC Batch: 4BBB45 Analysis Method: SM 2540D-2011
QC Batch Method: SM 2540D-2011 Analysis Description: 2540D Total Suspended Solids
Associated Lab Samples: 92438402001
METHOD BLANK: 2638666
Associated Lab Samples: 92438402001
Parameter Units
Total Suspended Solids
mg/L
LABORATORY CONTROL SAMPLE:
Parameter
2638667
Units
Total Suspended Solids
mg/L
SAMPLE DUPLICATE: 2639441
Parameter
Units
Total Suspended Solids
mg1L
SAMPLE DUPLICATE: 2639442
Parameter
Units
Total Suspended Solids
mg1L
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 2.5 0712911913:04
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
250 250 100 90-110
92438421003 Dup
Result Result
58.7 57.3
92438506002 Dup
Result Result
440 444
RPD Qualifiers
2
RPD Qualifiers
1
Results presented on this page are In the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date'. 08/02/2019 11:30 AM without the written consent of Pace Analytical Services, LLC. Page 6 of 13

aceAnaIX cal
www porelabs. com
QUALITY CONTROL DATA
Project: SW Outfal1 #03 (B)
Pace Project No.: 92438402
QC Batch: 488319 Analysis Method: SM 52108-2011
QC Batch Method: SM 521OB-2011 Analysis Description: 5210B BOD, 5 day
Associated Lab Samples: 92438402001
METHOD BLANK: 2636157
Associated Lab Samples: 92438402001
Parameter Units
BOD, 5 day mg1L
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 2.0 07/30/19 03:34
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE:
2636158
Spike LCS LCS
% Rec
Parameter
Units
Conc. Result % Rec
Limits Qualifiers
BOD, 5 day
mglL
198 203 103
84.6-115
SAMPLE DUPLICATE: 2636160
92438416001 Dup
Parameter
Units
Result Result RPD
Qualifiers
BOD, 5 day
mg1L
ND ND
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the fight of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/02/2019 11:30 AM without the written consent of Pace Analytical Services, LLC. Page 7 of 13

aceAnalytical"
www.pacelabs.com
Project: SW Outfall #03 (B)
Pace Project No.: 92438402
QC Batch: 488767
OC Batch Method: SM 5220D-2011
Associated Lab Samples: 92438402001
METHOD BLANK: 2638169
Associated Lab Samples: 92438402001
Parameter Units
Chemical Oxygen Demand mglL
LABORATORY CONTROL SAMPLE: 2638170
Parameter Units
Chemical Oxygen Demand mg/L
Pace Analytical Services, LLC
98D0 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Analysis Method: SM 5220D-2011
Analysis Description: 5220D COD
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 25.0 07/29/1917:06
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
750 738 98 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2638171 2638172
MS MSD
92438348001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Chemical Oxygen Demand mg/L 3010 100 100 3090 3100 85 95 90-110 0 M1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2638173 2638174
MS MSD
92438402001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qua)
Chemical Oxygen Demand mglL ND 100 100 119 121 99 102 90-110 2
Results presented on this page are In the unlls Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/02/2019 11:30 AM without the written consent of Pace Analytical Services, LLC.
Page 8 of 13

aceAnalytical
www.pacefe6s.wm
QUALIFIERS
Project: SW Outfall #03 (B)
Pace Project No.: 92438402
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
Pace Analytical Services, LLC
9800 Kincey Ave, Suite 100
Huntersville, NC 26078
[phone]
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix,
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azubenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosod iphenyla mine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
PASI-A Pace Analytical Services -Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/02/2019 11:30 AM without the written consent of Pace Analytical Services, LLC, Page 9 of 13

aceAnalytical
w"..pacelab& Wn
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: SW Outfall #03 (B)
Pace Project No.: 92438402
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method.
Batch
92438402001
SW OUTFALL #03 (B)
92438402001
SW OUTFALL #03 (B)
EPA 200.7 Rev 4.4 1994
489431
EPA 200.7 Rev 4.4 1994
489630
92438402001
SW OUTFALL #03 (B)
SM 2540D-2011
488845
92438402001
SW OUTFALL#03 (B)
SM 521OB-2011
488319
SM 521OB-2011
488349
9243B402001
SW OUTFALL #03 (B)
SM 5220D-2011
488767
SM 5220D-2011
489096
Date: 081D212019 11;30 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 10 of 13

Document Name:
Document Revised: February 7, 2018
a
�aceAnaOcal
Sam le Condition Upon Recei t SCUR
Page 1 of 2
Document No.:
Issuing Authority:
F-CAR•CS-033•Rev.06
pace Carolinas Quality office
Laboratory receiving samples:
Asheville ❑ Eden❑ Greenwood ❑ Huntersviile ❑tr Ralelgh❑ Mechanicsville[]
• ». J#
Client Name: Wo# : 92438402
nowrm-amm _ Project R
L
Courier. []Fed Ex ❑UPS ❑LISPS ❑Client
❑ Commercial ❑Pace ❑Other: 92438402
Custody Seal Present? ❑Yes ❑No Seals Intact? ❑Yes fNo 1
Date/lniiials Person Examining Contents:
Packing Material: []Bubble Wrap ❑8ubble Bags None ❑ Other Biological Tissue Frozen?
Thermometer: []Yes❑No [] /A
❑IR Gun ID: 92TO48 Type of Ice: [DWet ❑Blue ❑None
Cooler Temp ('C): 2-,01 Correction Factor. Add/Subtract ('C) 0,0
Temp should be above freezing to 5'C
Cooler Temp Corrected ('C): ❑samples out of temp criteria. Samples on ice, tooling process
has begun
USDA Regulated Sail (Ef N/A, water sample)
Did samples originate in a quarantine zone within the United States: CA, NY, or SC{check maps)? Did samplesorlginate From a foreign source (internationally,
mv.. mnl inrludinv Hawaii and AuPhn Rlenl? FIVnc f-iNn
Comment s/0lscrepant :
Chain of Custody Present?
' le,
ON.
❑NJA
1.
Samples Arrived within Hold Time?
4s
ONO
❑N/A
2,
Shot Hold Time Analysis 02 hr.)?
Yes
No
N A
3.
Rush Turn Around Time Requested?
❑Yes
M No
❑N/A
q.
Sufficient Volume?
• Yes
No
N/A
5.
Correct Containers Used?
-Pace Containers Used?
Qyes
0i es
[:)No
No
❑N/A
NIA
6.
Containers Intact?
©Yes
No
N//A
7.
Dissaived analysis: Samples Field Filtered?
❑Yes
❑No
N/A
8.
Sample Labels Match CDC?
-Includes Date/Time/ID/Anatysis Matrix:
©Its
❑No
❑N/A
9.
Headspace in VOA Vials (>5-6mm)?
Yes
ONO
❑N/A
10.
Trip Blank Present?
Trip Blank Custody Seals Present?
❑Yes
oYes
[)ND
0 Na
041A
N/A
11.
COMMENTS/SAMPLE DISCREPANCY Field Data Required? Des []No
Lot ID of split containers:
CUENT NOTIFICATION/RESOLUTION
Person contacted: Date/Time:
Project Manager SCURF Review: l/., Date:.
Project Manager SRF Review: % < Date:
Page 11 of 13

Document Name:
Document Revised: February 7, 2018
aceAnalAMI
Sample Condition Upon Recei tISCURI
Page 1 of 2
Document No.:
issuing Authority:
F-CAR-0-033-Rev.06
Pace Carolinas Quality Office
`Check mark tap half of box if pH and/or dechlorination is
verified and within the acceptance range for preservation
samples.
Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/8015 (water) DOC, LLHg
"Bottom half of box Is to list number of bottle
Project # WO : 92433402
PM: MW8 Due Date: 06/02/19
CLIENT: 92-Allva. NC
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pH Adjustment Log for Preserved Samples
Sam pie 10
Type of preservative
pit upon receipt
pate preservatlon adJusted
Time preservation
adjusted
Amount of Preservative
added
Lot u
Note: Whenever there is a discrepancy affecting NorthCarolina compliance samples, a tapy of this farm will be sent to the North Carolina DEFINR Certification Office [i.e.
Out of hold, incarmtt preservative, out of ternp,'mcerrect containers.
Page 12 of 13

Stormwater Monitorin
Chain of Custody Record
Project Number/Name:
SW Outfall #03 B
Pra'ect Location: AT1 SM - Bakers
Sample 's Si mature:
Date: "a?3-
F
E
o
a�
CL
a,
o tI
V
F
Requested `Pest Parameters
6.
/
a8
G
G /(D
f-1NO3
Y
Total Recoverable: Chromium, Nickel, Co > > qr %mc
$
G
G /0
HNO3
Y
Cadmium L-Y
:3
G
G /d)
1-12SO4
Y
COD
G
G /Q
None
Y
BOD
.3:
3
G
G /
None
Y
TSS
Otlsite Vield
11-1 Analysis
Onsite Fiel(! Tens eraturc Analysis
pli:via (s.u.)
Sampi Tine:
756
Temp: °c) Sample Tinic: 3
AnalysIS
1'Irne:
I
I Analysls 1'mle:
Meter Calibrated.
Thcrliiomet •r Calibrated:C / N
Sam iirl ;Intl field analysis co>nt letedl b ,:
Rel i11 t. khed B :
Receives
Date:
l 1 c:
%1J
Date:
Reline uished By:
`� "
Received B �-
Date: ` �I
f'in�c :
1(.
Datc:
JTimc:
EI-IS-SW-Chain of Costody Outfalt 03-Rev 001
Page 13 of 13

Allvac - Bakers Plant
Stormwater Monitoring Report Form
Sample Location:
Person Collecting Samples:
Laboratory Performing Analysis:
Analytical Techniques and Methods:
Results of Sample Analysis:
Non-ContactCooling Wastewater
p4.,w Popp Vie. 1A4 �z
40 CFR Part 136
OATI
Non- I
Contact
Cooling
Water # ,
Sampling
Date
Sampling
Time
Estimated
Flow(MGD)
Total
Residual
Chlorine
Temperature
pH (std. units)
Effluent
Downstream
Upstream
-sue
0 00v3
°e
gy
aV!
7 a
3
6-%-
.00ag
NP
9 °`
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4
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9 _
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013..a`'`
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.0036
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7.7
8
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0 : -;5
0. O l aO
a?a�• 4 °�
�3 a'`
0?3. °`
7 $1

acmnalytical
www.pscelaumm
June 26, 2019
Scott Ryan
Allvac
Monroe, NC
RE: Project: NONCONTACT COOLING WATER
Pace Project No.: 92433143
T . t
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersviile, NC 28078
[phone]
Dear Scott Ryan:
Enclosed are the analytical results for sample(s) received by the laboratory on June 14, 2019. The
results relate only to the samples included in this report. Results reported herein conform to the most
current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where
applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Matthew Brainard
[e-mail]
[phone]
Project Manager
Enclosures
cc: Tyler Mercer, ATI Specialty Materials
David Pope, Allvac
ACCRfO
q�a�!
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 19

aceAnalytical
wNwpecelabs.snm
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704 )875-9092
Project: NONCONTACT COOLING WATER
Pace Project No.: 92433143
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
LouisianalNEI-AP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky LIST Certification #: 84
VrginiaNELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
VirginiaNELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consentof Pace Analytical Services, LLC. Page 2 of 19

aceAnalytical
www.pecelaft com
SAMPLE ANALYTE COUNT
Pace Analytical Services, LLC
9600 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Project:
Pace Project No.:
NONCONTACT COOLING WATER
92433143
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92433143001
NON-CONTACT#1
EPA 1664E
JMS
1
PASI-C
SM 4500-CI G-2011
GC
1
PASI-A
92433143002
NON-CONTACT#2
EPA 1664E
JMS
1
PASI-C
SM 4500-CI G-2011
GC
1
PASI-A
92433143003
NON-CONTACT#3
EPA 1664E
JMS
1
PASI-C
SM 4500-CI G-2011
GC
1
PASI-A
92433143004
NON-CONTACT04
EPA 1664E
JMS
1
PASI-C
SM 4500-CI G-2011
GC
1
PASI-A
92433143005
NON-CONTACT#5
EPA 1664B
JMS
1
PASI-C
SM 4500-CI 0-2011
GC
1
PASI-A
92433143006
NON-CONTACT#6
EPA1664B
JMS
1
PASI-C
SM 4500-CI G-2011
GC
1
PASI-A
92433143007
NON-CONTACT#7
EPA 1664B
JM5
1
PASI-C
SM 4500-CI G-2011
GC
1
PASI-A
92433143008
NON-CONTACT#8
EPA 1664E
JMS
1
PASI-C
SM 4500-CI G-2011
GC
1
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 3 of 19

aceAnalytical
www.pacelabs wm
ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Hunlersville, INC 28078
[phone]
Project: NONCONTACT COOLING WATER
Pace Project No.: 92433143
Sample: NON-CONTACT#1 Lab ID: 92433143001 Collected: 06/13119 07:50 Received: 06/14/19 10:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
HEM, Oil and Grease
Oil and Grease
4500CL G Chlorine, Residual
Chlorine. Total Residual
Date: 06/26/2019 02:40 PM
Analytical Method: EPA 1664B
ND mglL 5.0 1 06/26/19 06:43
Analytical Method: SM 4500-CI G-2011
ND mg/L 0.024 1 06/1811917:57 7782-50-5 H3
REPORT OF LABORATORY ANALYSIS
This report shall riot he reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 4 of 19

m
aceAnalytical
»ww.paCefab&wM
ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 KinceyAve. Suite too
Huntersville, NC 2807E
[phone]
Project: NONCONTACT COOLING WATER
Pace Project No.: 92433143
Sample: NON-CONTACT#2 Lab ID: 92433143002 Collected: 06/13/19 08:15 Received: 06/14/19 10:00 Matr"ix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Oual
HEM, Oil and Grease Analytical Method: EPA 1664B
Oil and Grease ND mg/L 5.0 1 06/26/19 06:43
4500CL G Chlorine, Residual Analytical Method: SM 4500-CI G-2011
Chlorine, Total Residual ND mg1L 0.024 1 06/18/19 17:57 7782-50-5 H3
Date. 06I2612019 02:40 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written Consent of Pace Analytical Services, LLC.
Page 5 of 19

aceAnalytical
WWW.PM)8bS.WM
ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave, Suite 100
Huntersville, NO 28078
[phone]
Project: NONCONTAC I COOLING WATER
Pace Project No.: 92433143
Sample: NON-CONTACT#3 Lab ID: 92433143003 Collected: 06/13119 08:40 Received: 06/14119 10:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
HEM, Oil and Grease Analytical Method: EPA 1664B
Oil and Grease ND nri 5.0 1 06/26/19 06:43
4500CL G Chlorine, Residual Analytical Method: SM 4500-CI G-2011
Chlorine, Total Residual ND mg/L 0,024 1 06/18/19 17:57 7782-50-5 H3
Date: 06/26/2019 02:40 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 6 of 19

(�IacleAnalyfical"
wxwpacelebs.c=
ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 KinceyAve, Suite 100
Huntersville, NC 28078
[phone]
Project: NONCONTACT COOLING WATER
Pace Project No.: 92433143
Sample: NON-CONTACT#4 Lab IA: 92433143004 Collected: 06113119 09:00 Received: 06/14/19 10:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
HEM, Oil and Grease Analytical Method: EPA 1664B
Oil and Grease ND mg/L 5.0 1 06/26/19 06:44
4500CL G Chlorine, Residual Analytical Method: SM 4500-CI G-2011
Chlorine, Total Residual ND mg/L 0.024 1 06/18/19 17:57 7782-50-5 H3
Date: 06/26/2019 02:40 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 7 of 19

aceAnalytical
www.pacelabs.com
ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave, Suite 100
Huntersville. NC 28078
[phone]
Project: NONCONTACT COOLING WATER
Pace Project No.: 92433143
Sample: NON-CONTACT#5 Lab ID: 92433143005 Collected: 0611311909:25 Received: 06/14/1910:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
HEM, Oil and Grease Analytical Method: EPA 1664E
Oil and Grease ND mg/1- 5.0 1 06126/19 06:44
4500CL G Chlorine, Residual Analytical Method: SM 4500-CI G-2011
Chlorine, Total Residual ND mg/L 0.024 1 06/18/19 17:57 7782-50-5 H3
Date: 06126/2019 02:40 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 8of19

aeeAnalytical
www.pacelabs eom
ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Project: NONCONTACT COOLING WATER
Pace Project No.: 92433143
Sample: NON-CONTACT#6 Lab ID: 92433143006 Collected: 06113119 09:45 Received: 06/14/19 10:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
HEM, Oil and Grease Analytical Method: EPA 1664B
Oil and Grease ND mg/L 5.0 1 06126I19 06:44
4500CL G Chlorine, Residual Analytical Method: SM 4500-CI G-2011
Chlorine, Total Residual ND mg/L 0.24 10 06/18/19 17:57 7782-50-5 H3
Date: 06/26/2019 02:40 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC,
Page 9 of 19

aceAnalytical
www.pacelab&C=
ANALYTICAL RESULTS
Project: NONCONTACT COOLING WATER
Pace Project No.: 92433143
Pace Analytical Services, LLC
9600 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: NON-CONTACT#7 Lab ID: 92433143007 Collected: 06/13119 10:10 Received: 06114119 10:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed GAS No. Qual
HEM, Oil and Grease Analytical Method: EPA 1664B
Oil and Grease ND mg1L 5.0 1 06/26/19 06:45
4500CL G Chlorine, Residual Analytical Method: SM 4500-CI G-2011
Chlorine, Total Residual ND mg1L 0.024 1 06/18/19 17:57 7782-50-5 H3
Date: 06/26/2019 02:40 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 10 of 19

aceAnalytical
www.pecelabs.com
ANALYTICAL RESULTS
Pace Analytical Services, LLC
9600 Kincey Ave, Suite 100
Huntersville, NC 28078
[phone]
Project: NONCONTACT COOLING WATER
Pace Project No.: 92433143
Sample: NON-CONTACT#8 Lab ID: 92433143008 Collected: 06/13/19 10:35 Received: 06/14/19 10:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
HEM, Oil and Grease Analytical Method: EPA 1664B
Oil and Grease ND mg/L 5.0 1 06/26/19 06:45
4500CL G Chlorine, Residual Analytical Method: SM 4500-CI G-2011
Chlorine, Total Residual ND mg1L 0.024 1 06118/19 17:57 7782-50-5 H3
Date: 06/26/2019 02:40 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 11 of 19

aceAnalyfical
www.pacelabs.com
QUALITY CONTROL DATA
Project: NONCONTACT COOLING WATER
Pace Project No.: 92433143
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QC Batch: 483277 Analysis Method: EPA 1664B
QC Batch Method: EPA 1664E Analysis Description: 1664 HEM, Oil and Grease
Associated Lab Samples: 92433143001, 92433143002, 92433143003, 92433143004, 92433143005, 92433143006, 92433143007,
92433143008
METHOD BLANK: 2612203 Matrix: Water
Associated Lab Samples: 92433143001, 92433143002, 92433143003, 92433143004, 92433143005, 92433143006, 92433143007,
92433143008
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Oil and Grease mg/L NO 4.8 06/26/19 06:42
LABORATORY CONTROL SAMPLE:
2612204
Spike LCS
LCS
% Rec
Parameter
Units
Conc. Result
% Rec
Limits
Qualifiers
Oil and Grease
mg/L
38.5 38.5
100
78-114
MATRIX SPIKE SAMPLE:
2612205
92433576001 Spike
MS
MS
% Rec
Parameter
Units
Result Conc.
Result
% Rec
Limits Qualifiers
Oil and Grease
mg/L
ND 38.5
37.2
97 78-114
Results presented on this page are in the units Indicated try the "Unite" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/26/2019 02:40 PM without the written consent of Pace Analytical Services, LLC.
Page 12 of 19

lacmnalyfical*
www.peceleb&com
QUALITY CONTROL DATA
Project: NONCONTACT COOLING WATER
Pace Project No.: 92433143
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
OC Batch: 481875 Analysis Method: SM 4500-CI G-2011
OC Batch Method: SM 4500-CI G-2011 Analysis Description: 4500CL G Chlorine, Total Residual
Associated Lab Samples: 92433143001, 92433143002, 92433143003, 92433143004, 92433143005, 92433143006, 92433143007,
92433143008
METHOD BLANK: 2605891 Matrix: Water
Associated Lab Samples: 92433143001, 92433143002, 92433143003, 92433143004, 92433143005, 92433143006, 92433143007,
92433143008
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Chlorine, Total Residual mg/L ND 0.024 06/18/19 17:57
SAMPLE DUPLICATE: 2605892
92432727001 Dup
Parameter Units Result Result RPD Qualifiers
Chlorine, Total Residual mg/L NO ND H3
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/26/2019 02:40 PM without the written consent of Pace Analytical Services, LLC.
Page 13 of 19

accAnalytical
wwwpacelebs.com
QUALIFIERS
Project: NONCONTACT COOLING WATER
Pace Project No.: 92433443
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
I.CS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosod iphenyla mine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services -Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
H3 Sample was received or analysis requested beyond the recognized method holding time.
REPORT OF LABORATORY ANALYSIS
Thls report shall not be reproduced, except in full,
Date: 06/26/2019 02:40 PM without the written consent of Pace Analytical Services, LLC. Page 14 of 19

laoAnalyficalo
www.pecelabs.cam
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: NONCONTACT COOLING WATER
Pace Project No.: 92433143
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
92433143001
NON-CONTACT#1
EPA 16646
483277
92433143002
NON-CONTACT#2
EPA 1664B
483277
92433143003
NON-CONTACT#3
EPA 1664B
483277
92433143004
NON-CONTACT#4
EPA 1664B
483277
92433143005
NON-CONTACT#5
EPA 1664B
483277
92433143006
NON-CONTACT#6
EPA 1664B
483277
92433143007
NON-CONTACT#7
EPA 1664B
483277
92433143008
NON-CONTACT0
EPA 1664B
483277
92433143001
NON-CONTACT#1
SM 4500-CI G-2011
481875
92433143002
NON-CONTACT#2
SM 4500-CI G-2011
481875
92433143003
NON-CONTACT#3
SM 4500-C1 G-2011
481875
92433143004
NON-CONTACT#4
SM 4500-CI G-2011
481875
92433143005
NON-CONTACT#5
SM 4500-CI G-2011
481875
92433143006
NON-CONTACT#6
SM 4500-CI G-2011
481875
92433143007
NON-CONTACT#7
SM 4500-CI G-2011
481875
92433143008
NON-CONTACT#8
SM 4500-CI G-2011
481875
Date: 06126l2019 02:40 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Analytical
Batch
I
Page 15 of 19

Document Name:
{Document Revised: February 7, 2018
- .aceAnalyfrcal e
Sample Conditlon Upon Recei t(SCUR)
Page 1 of 2
Document No.:
Issuing Authority:
F-CAR-CS-033-Rev.06
Pace Carolinas Quality Office
Laboratory receiving samples:
Asheville ❑ Eden[] Greenwood ❑ Huntersville p�Z Raleigh[] Mechanicsville❑
Client Narne: Project Wot• ; 92433143
,2�4L
Courier: ❑Fed Ex� ❑UPS CUSPS ❑Client
❑ Commercial .QFace ❑Other:
924331 43 �
Custody Seal Present? --- ❑Yes--. ❑No Seals intact? ❑Yes [IN'o t!%% f
Date/initials Person Examining Contents: � l
Packing Material: []Bubble Wrap 08ubble Bags ❑None ❑ Other Biological Tissue Frozen?
❑Yes QNo ❑N/A
Thermometef
QIR Gun 1E7: 921'048 Type of ice: [20 et ❑Blue ❑None
r� r
Cooler Ternp ('C): t • CY i-9 Correction Factor: Add/Subtract ('C) 0.0
Temp should be above freezing to 6'C
Cooler Temp Corrected ('C): ❑samples out of temp criteria. Samples on ice, cooling process
f/ has begun
USDA Regulated Sall (M N/A, water sample)
Did samples originate in a quarantine zone within the United States: CA, NY, or SC (check maps)? Old samples originate from a foreign source (internationally,
nYes A13 includine Hawaii and Puerto Ricol? MYes RNo
Comments/Discre ant :
/
Chain of Custody Present?
04s
No
❑N/A
1.
Samples Arrived within Hold Time?
Yc
❑No
❑N/A
2.
Short Hold Time Analysis <72 hr.)?
Yes
Na
N/A
3.
Rush Turn Around Time Requested?
Y,�cs
No
❑N/A
4.
Sufficient Volume?
. Y
,es
No
N/A
5.
Correct Containers Used?
❑Yes
©Na
❑NIA
6.
-Pace Containers Used?
weer
No
NIA
Containers Intact?
0ie�s
QNo
Q N/A
7.
Dissolved analysis: Samples Field Filtered?
❑Ycs-
❑No
❑N/A
B.
Sample Labels Match CDC?
QYes
[)NO
❑N/A
9.
-Includes Date/Time/ID/Analysis Matrix:
Headspace in VOA Vials (>5-6mm)?
Des
ON
N A
10,
Trip Blank Present?
❑Ycs
QNo
❑N/A
11,
N
Ttie Blank CustoL Seats Present?
Uyes
CINO
" A/
COMMENT;/SAMPLE DISCREPANCY
Lot ID of split containers:
CLIENT NOTIFICATION/RESOLUTION
Field Data Required? []Yes ONO
Person contacted: oateMme:
Project Manager SCURF Review: fj/ Dater
Project Manager SRF Review: L Date:
Page 16 of 19

Document Name:
Document Revised: February 7, 2018
�-Uce �if?�3�IGc3j
Sample Condition Upon Recei t(SCURj
Page 1 of 2
Document No.:
Issuing Authority:
f.CAR-0-033•Rev.Ofi
Pace Carolinas Quality Office
'Check mark top half of box If pH and/or dechlorination Is
verified and within the acceptance range for preservation
samples.
Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/9015 (water) DOC, LLHg
`*bottom half of box is to list number of bottle
Project t# " : 92433143
—� puc Daiet 0 /28/19
pp : MW43
2�Al_ivac VIC .�.._.�
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pH Adjustment Log for Preserved Samples
Sample IO
Type of Preservative
pH upon recelpt
Date preservation ad)uited
Time preservation
adlusted
Amount of Preservative
added
Lot rr
Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office Ii.e.
Out of hold, incorrect preservative, out of temp, incorrect containers.
Page 17 of 19

t
ATI
Slreeialq• Efalr.rials
Storm Dater monitoring
(NON CONTACT)
Bakers North
Chain of Custody Record
page 41
Project Number/Name: NonContact Cooling Water Project Location: ATI SM
- Bakers
Sampler's Signature:
Date:6
3
u
dL
E
M
a
to
a
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a
a
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u
tc
M
�,
Requested Test
A
i=
0
a
CL
Parameters
a,'
4�CL
O
a
F
L
a
W
a
SA
°
aZ�331
0
G
G
None
Y
'J, J
Residual Chlorine
so,,-
G
G,db
None
Y
j
Residual Chlorine
G
GAP
None
Y
Residual Chlorine
Co4,_-t#j
G
G/(0
None
Y
Residual Chlorine
O4_C �}
•-,r,
G
Gla
None
Y
b
Residual Chlorine
Mal-CpA+t't+*6
flf,.,
G
G/a
None
Y
,9
Residual Chlorine
A/0,1 ae
•/0,
G
G/(D
None
Y
Residual Chlorine
Gin-Cr+ti�fac 8
D '3S�
G
G/e
None
I Y
y
Residual Chlorine
Meter Calibrated: / N IThermorneter Calibrapd— N
Sampling and Field analysis completed by:
Relinquished By:
Received By: a�G
Date : Time:
Date: 111 -Iq Time: jp;«.�..�,v.
Relinquished By: '
Received By : ",,:tj. 1, Y "
Date y -1
Time: j ; ,,,,`.
Date:(,")
"rime: It �1
EHS Baker South SW REV 9 2 5/10/2016
Page 18 of 19

�ATI
S�BGi,3ity h4ateriala
Storm Water Monitoring
(NON CONTACT)
Bakers North
Chain of Custody Record
oa¢e B2
Project Number/Name: NonContact Cooling Water
project Location: ATI SM - Bakers
Sampler's Signature:
Date:
a
E
fa
oCL
d
Q
U
C
I— •y
�,
Cp
i .
?
U
V
9
a..
f13
E
LJ
c
°
Requested Test
Parameters
'J
-IL
� f L
G
G
HCL
Y
f
Oil & Grease
& eAS�
G
G
HCL
Y
Oil & Grease
DA-CbR
r}�
G
G
HCL
Y
U. q
Oil & Grease
lVjA - CM�04 # q(Xj„r
G
G
HCL
Y
Oil &Grease
3
,,_
G
G
HCL
Y
Oil & Grease
per- bq
.1w,
G
G
HCL
Y
Oil & Grease
M iQ Ae1
' Q
G
G
HCL
Y
Oil & Grease
O',-Comma 8
/0 Ste-
G
G
HCL
Y
Oil & Grease
Meter Calibrated: / N
lThermometer Calibrated: / N
Sampling and Field analysis completed by:
Relinquished By:
Relinquished By: l
Date :
Time:
Date :01 11 I `I
Time:
Relinquished By:
:Relinquished By:
Date : 0J -/ y-(e
Time: !!l S.:,
Date : r �- c� ; `
Time:
EHS Baker South SW REV 9 2 5/10/2016
Page 19 of 19

STORMWATER DISCHARGE OUTFALL (SDO)
MONITORING REPORT
Permit Number NCS ODD 3v2 9
FACILITY NAME 412-Y- l✓Ae,— Vf&-s
PERSON COLLECTING SAMPLE S) oh, TR.
CERTIFIED LABORATORY(S) aae Lab #
Lab #
Part A: Specific Monitoring Requirements
SAMPLES COLLECTED DURING CALENDAR YEAR: aW
(This monitoring report shall be received by the Division no later than 30 days from
the date the facility receives the sampling results from the laboratory.)
COUNTY 1 ,L.;t,
PHONE NO. if dy) "9-44-r//
SIGNATURE OF PERMITTEE OR DESIGNEE
REQUIRED ON PAGE 2.
•
Date
Sample
Collected
Total
Rainfall
Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month?
(if yes, complete Part B)
Part B: Vehicle Maintenance Activity Monitoring Requirements
yes _no
Outfall
No.
Date
Sample
Collected
50050
00556
00530
00400
Total Flow
(if applicable)
Total
Rainfall
Oil & Grease
(if appl.)
Non -polar
O&GITPH
(Method 1664
SGT-HEM), if
appl.
Total
Suspended
Solids
pH
New Motor
Oil Usage
moldd/vr
MG
inches
mgA
m
unit
al/mo
Form SWU-247, last revised 21212012
Page 1 of 2

STORM EVENT CHARACTERISTICS: Mail Original and one copy to:
Division of Water Quality
Date 7 93 /? Attn: Central Files
Total Event Precipitation (inches): 9 3S 1617 Mail Service Center
Event Duration (hours): /.as (only if applicable — see permit.) Raleigh, North Carolina 27699-1617
(if more than one storm event was sampled)
Date
Total Event Precipitation (inches):
Event Duration (hours): (only if applicable — see permit.)
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a
system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person
or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the
best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations."
9=.PA_ g-9-1!p
(Signature of Permifte (Date)
Form SWU-247, last revised 21212012
Page 2 of 2

Enutonmcnral
Qualrr,v
Stormwater Discharge Outfall (SDO)
Qualitative Monitoring Report
For guidance on filling oul this form, please visit https://deg.nc.Y v/about/divisions/enerQY-mineral-tand-
resourceslenergy-mineral-land-permits./stormwater-permitslnpdes-industrial-sw#tab-4
Pennit No.: or Certificate of Coverage No.: NIC/GI_I_I_I_I_I_I
Facility Name: Aweel_-r
Connty, a/t. /0a Phone Nn. 7,0 y-a8 9 —17/ 11
Inspector: DGt l B J&,
Date of Inspection: % a,; Yq
Time of Inspection: Y"em
Total Event Precipitation (inches): 40. 55—
All permits require qualitative monitoring to be perforined during a "measurable storm event."
A "measurable storm event" is a storin event that results in an actual discharge from the pernitted site
outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm
interval does not apply if the pennittee is able to document that a shorter interval is representative for
local storm events during the sampling period, and the pennittee obtains approval from the local DEMLR
Regional Office.
By this signature, I certify that this report is accurate and complete to the best of my knowledge:
(Signature of
1. Outfall Description:
Outfall No. $5kyol Structure (pipe, ditch, etc.):
Receiving Stream:
Describe the industrial activities that occur within the outfall drainage area:
Page 1 of 2
SWU-242, last modiGed07125/2617

2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint
(light, medium, dark) as descriptors: a/ea.,-
3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak
chlorine odor, etc.): IL4/+-'e
4. Clarity: Choose the number which best describes the clarity of the discharge, where I is clear
and 5 is very cloudy:
(P 2 3 4 5
5. Floating Solids: Choose the number which best describes the amount of floating solids in the
stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids:
2 3 4 5
6. Suspended Solids: Choose the number which best describes the amount of suspended solids in
the stormwater discharge, where 1 is no solids and 5 is extremely muddy:
6) 2 3 4 5
VA
8.
9.
Is there any foam in the stormwater discharge? O Yes ®No.
Is there an oil sheen in the stormwater discharge? OYes (g)No.
Is there evidence of erosion or deposition at the outfall? o Yes ®No.
10. Other Obvious Indicators of Stormwater Pollution:
List and describe N42 t?
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be
indicative of pollutant exposure. These conditions warrant further investigation.
Page 2 of 2
5wU-242. Last modified 07/2812017

K,,.,r,a-
Environmental
Quality
Stormwater Discharge Outfall (SDO)
Qualitative Monitoring Report
For guidance on filling out this fol7n, please visil httns://den.nc.gov/about/divisions/enerey-mineral-Iand-
resources/energy-mineral-land-permits/stormwater-permitslnpdes-industrial-sw#tabA
Permit No.: N/Cl,�(O 1010/31�1�1 or Certificate of Coverage No.: NIC/GI_l—l—1 l—1 l
Facility Name: 8axe/--r
County: &it1en Phone No.
Inspector: D4W,.0 Idd� -
Date of Inspection:
Time of Inspection:
Total Event Precipitation (inches): 0-36­
All permits require qualitative monitoring to be performed during a "measurable storm event."
A "measurable storm event" is a storm event that results in an actual discharge from the permitted site
outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm
interval does not apply if the permittee is able to document that a shorter interval is representative for
local storm events during the sampling period, and the permittee obtains approval from the local DEMLR
al Office.
By this signature, i certify that this report is accurate and complete to the best of my knowledge:
(Signature of Permittee or'besignee)
1. Outfall Description:
Outfall No. ,BSWU Structure (pipe, ditch, etc.)
Receiving Stream: _
Describe the industrial activiftips tl)at occur within the outfall drainage area:
Page I of 2
SWU-242, Last modified M812011

2. Color: Describe the color of the discharge using basic colors (red,
(light, medium, dark) as descriptors: QZe�z f q4!�
blue, etc.) and tint
3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak
chlorine odor, etc.): .A AI[LP _
4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear
and 5 is very cloudy:
1 ® 3 4 5
5. Floating Solids: Choose the number which best describes the amount of floating solids in the
stonnwater discharge, where 1 is no solids and 5 is the surface covered with floating solids:
m 2 3 4 5
6. Suspended Solids: Choose the number which best describes the amount of suspended solids in
the stormwater discharge, where 1 is no solids and 5 is extremely muddy:
d 2 3 4 5
7. Is there any foam in the stormwater discharge? O Yes dnNo.
8. Is there an oil sheen in the stonnwater discharge? OYes (!�DNo.
9. Is there evidence of erosion or deposition at the outfall? O Yes CNo.
10. Other Obvious Indicators of Stormwater Pollution:
List and describe ZLZ
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be
indicative of pollutant exposure. These conditions warrant further investigation.
Page 2 of 2
SWi3.242, Last modified o7/28/2017

Environmental
Quality
Stormwater Discharge Outfall (SDO)
Qualitative Monitoring Report
Forguidance onfrlling out thisform, please visit https://deg.nc.gov/about/divisionVenergy-mineral-land-
resources/energy--mineral-I_and-permits/stormwater-permits/npdes-ind ustrial-sw#tab-4
Permit No.: NICISIOIOIQ/.IIor Certificate of Coverage No.: NICIGITI�hI_hl l
Facility Name
County:
7� � v� - ��.r
Phone No.
Inspector: �D~d /�ypG 31�.
Date of Inspection: :r�
Time of Inspection: .3
Total Event Precipitation (inches): P • 3-1-
All permits require qualitative monitoring to be performed during a "measurable storm event."
A "measurable storm event" is a storm event that results in an actual discharge from the pennitted site
outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm
interval does not apply if the penmittee is able to document that a shorter interval is representative for
local stone events during the sampling period, and the permittee obtains approval from the local DEMLR
Regional Office.
By this signature, I certify that this report is accurate and complete to the best of my knowledge:
(Signature of Permittee or Des gnee)
1. Outfall Description:
Outfall No. 185WO Structure (pipe, ditch, etc.)
Receiving Stream:
Describe the industrial activities
P1Q e- /yi VG k
wilhin the outfall drainage area:
Page I of 2
SWU-242, Lase modified 07/28/2017

2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint
(light, medium, dark) as descriptors: Z49!.-- _
3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak
chlorine odor, etc.):,y®
4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear
and 5 is very cloudy:
© 2 3 4 5
5. Floating Solids: Choose the number which best describes the amount of floating solids in the
stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids:
6 2 3 4 5
6. Suspended Solids: Choose the number which best describes the amount of suspended solids in
the stormwater discharge, where I is no solids and 5 is extremely muddy:
© 2 3 4 5
7. Is there any foam in the stormwater discharge? O Yes �ia.
8. Is there an oil sheen in the stormwater discharge? OYes (9,10.
9. Is there evidence of erosion or deposition at the outfall? O Yes (5ko.
10. Other Obvious Indicators of Stormwater Pollution:
List and describe /1171 �
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosionldeposition may be
indicative of pollutant exposure. These conditions warrant further investigation.
Page 2 of 2
S W U-242, Last modified 07/28/2017