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HomeMy WebLinkAboutNCS000303_COMPLETE FILE - HISTORICAL_201902185TORMWATER DIVISION CODING SHEET ---- RESCISSIONS . PERMIT NO.. �r � S 00 D. � U 3 �v DOC TYPE Iff COMPLETE FILE'- HISTORICAL DATE OF RESCISSION YYYYMMDD Craig Fulcher Environmental, Health & Safety Manager SPX Transformer Solutions, Inc. craig.fulcher@spx.com T 919 288 8378 January 9, 2019 FEB 18 ZGI1 CENTRAL FILF,c, Division of Water Quality GINR IE-CTIONI Attn: Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 RE: Discharge Monitoring Report for SDO-001 for December 2018 To Whom it May Concern: Please find enclosed SPX Goldsboro's completed Discharge Monitoring Report (DMR) for December 2018. This fulfils the requirement of the Stormwater Permit NCS000303, Tier 11 monthly reporting. Please feel free to contact me at (919) 581-1677 if you have any questions or require any additional information. Sincerely, Craig Fulcher Environmental, Health & Safety Manager SPX Transformer Solutions, Inc. 2701 US Highway 117 South, Goldsboro, NG 27530 www.spxtransformeTsolutions.com STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT Permit Number NCS000303 SAMPLES COLLECTED DURING CALENDAR YEAR: 2018 (This monitoring report shall be received by the Division no later than 30 days from the date the facility receives the sampling results from the laboratory.) FACILITY NAME SPX Goldsboro COUNTY Wavne PERSON COLLECTING SAMPLE(S) Sara Lorette/AECOM PHONE NO.919-581-1677 CERTIFIED LABORATORY(S) Pace Analytical Services, LLC Lab. Cert. #12, 5342, 37706 Part A: Specific Monitoring Requirements Outfall No. Date Sample Collected pH Total Rainfall mo/dd/ r S.U. Inches SDO 001 12/01/18 7.48 1.51" ND = Non Detect Outfall No. Date Sample Collected TSS Oil & Grease mo/dd/yr m /L m IL SDO 001 12/01/18 18.6 ND ND = Non Detect Outfall No. Date Sample Collected PCBs Total Nitrate mo/dd/vr m /L mgfL SDO 001 12/01/18 ND 2.4 ND = Non Detect E GNATURE OF PERMITTEE OR DESIGNEEEQUIRED ON PAGE 2. Note: Monthly monitoring is in effect due to the current Tier II status. Permit Number NCS000303 Form SWU-247, last revised 21212012 Page 1 of 2 Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? _ yes X no (if yes, complete Part B) Part B: Vehicle Maintenance Activity Monitoring Requirements outfall Date 50050 00556 00530 00400 Total Flow Total Oil & Grease Non -polar Total pH New Motor No. Sample Collected (if applicable) Rainfall (if appl.) O&GITPH Suspended Oil Usage (Method 1664 Solids SGT-HEM), if appi. molddlvr I MG linches I m h I m Il unit I gal/mo STORM EVENT CHARACTERISTICS: Date 12/ 1 /18 Total Event Precipitation (inches): 1.51 inches Event Duration (hours): (only if applicable — see permit.) (if more than one storm event was sampled) Date Total Event Precipitation (inches): Event Duration (hours): (only if applicable — see permit.) Mail Original and one copy to: Division of Water Quality Attn: Central Files 1617 Mail Service Center Raleigh, North Carolina 27644-1617 "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines altd imprisonment for knowing violations." (Signature of Perm (Date) Permit Number NCS000303 Form SWU-247, last revised 21212012 Page 2 of 2 NCDENR Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report Forguidance on filling out this form, please visit: Permit No.: a /3/0 /3 / or Certificate of Coverage No.: Facility Name: SPX (n)lSSb3(V _ County: 47A+NC Phone No. _q i Inspector: (LA Z-oae-rrC _ Date of Inspection: 0 t -Zp! k Time of Inspection: _ 3 ! PA Total Event Precipitation (inches): 1 - S- i Was this a "Representative Storm Event" or "Measureable Storm Event" as defined by the permit? (See information below.) Yes ❑ No Please verify whether Qualitative Monitoring must be performed during a "representative storm event" or "measureable storm event" (requirements vary, depending on the permit). Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be performed during a "representative storm event" or during a "measureable storm event." However, some permits do not have this requirement. Please refer to these definitions, if applicable. A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. A "measurable storm event" is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DWQ Regional Office. By this signature, I certify, that t�is report is accurate and complete to the best of my knowledge: (Signature of Permitteee or Designee) Pagel of 2 SWU-242, Last modified 7/31/2013 1. Outfall Description: Outfail No. 00t Structure ( ipe, ditch, etc.) Receiving Stream: UMictly.2 t 0,J Describe the industrial activities that occur within th i T1' drainage area: 2. Color: Describe the color of the dischusing basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: Ito (D 1 d r _ 3. Odor: Describe any distinct odors that p the discharge may have (i.e., smells strongly of oil, a weak chlorine odor, etc.): O o o o-r 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 1 2 3 4 S 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: 1 2 0 4 5 b. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 1 2 0 4 5 7. Is there any foam in the stormwater discharge? Yes No 8. Is there an oil sheen in the stormwater discharge? & No 9. Is there evidence of erosion or deposition at the outfall? Yes No 10. Other Obvious Indicators of Stormwater Pollution: List and describe cy"kA P i u W &3 air^os-� e' k TC (,t;i, Uf\�vu a,Vr. 0r- Ur` t hn,. r— Ain Us hiJi' 51��Alii� M, ne,bv- � kJe 14? 1.0'V DCPt.tJJCILi An, a.lA1n.T 41 A" N 1 ti i 0L t 1 CL S 62r .. r ce ,n <,,U r` W A S I f\' Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 SWU-242, Last modified 7/31/2013 aceAnalytrcal o www,pacefabs.c= December 12, 2018 Craig Fulcher SPX Transformer Solutions, Inc. 2701 Highway 117 South Goldsboro, NC 27530 RE: Project: Stormwater Pace Project No.: 92409147 Dear Craig Fulcher: Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersviile, NC 28078 (704)875-9092 Enclosed are the analytical results for sample(s) received by the laboratory on December 03, 2018, The results relate only to the samples included in this report. Results reported herein conform to the most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. If you have any questions concerning this report, please feel free to contact me. Sincerely, Nicole Gasiorowski nicole.gasiorowski@paceiabs.com (704)875-9092 Project Manager Enclosures cc: Jennifer Jones, AECOM Jennifer Wheat, AECOM t 9B��pQ�s REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 14 aceAnalytrcal" www-paceMbs-corn CERTIFICATIONS Project: Stormwater Pace Project No.: 92409147 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 106 Huntersville, NC 28078 (704)875-9092 Charlotte Certification IDs 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 South Carolina Certification #: 99006001 Louisiana/NELAP Certification # LA17002B FloridalNELAP Certification #. E87627 North Carolina Drinking Water Certification #: 37706 Kentucky UST Certification #: 84 North Carolina Field Services Certification #: 5342 VirginiafVELAP Certification #: 460221 North Carolina Wastewater Certification #: 12 Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 FloridalNELAP Certification #: E87648 Massachusetts Certification #: M-NC030 North Carolina Drinking Water Certification #: 37712 Eden Certification IDs 205 East Meadow Road Suite A, Eden, NC 27288 North Carolina Drinking Water Certification #: 37738 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 VirginiafVELAP Certification #: 460222 North Carolina Wastewater Certification #: 633 VirginiafVELAP Certification #: 460025 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 14 aceAnalytical. www.pacelatrs.=n SAMPLE ANALYTE COUNT Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: Pace Project No.: Stormwater 92409147 Analytes Lab ID Sample to Method Analysts Reported Laboratory 92409147001 001 SM 254OD-2011 SOB 1 PASI-E EPA 1664B JMS 1 PASI-C EPA 608.3 SEM 9 PASI-C TKN+NO3+NO2 Calculation EWS 1 PASI-A EPA 351.2 Rev 2.0 1993 MFO 1 PASI-A EPA 353.2 Rev 2.0 1993 KDF1 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 14 Pace Analytical Services, LLC Analytical 9B00HuntersvIle, NCi2B 08lace wwwpacWabscom (704)875-9092 ANALYTICAL RESULTS Project: Stormwater Pace Project No.: 92409147 Sample: 001 Lab ID: 92409147001 Collected: 12/01/18 15:30 Received: 12/03/18 09:24 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed GAS No. Qual 2540D Total Suspended Solids Analytical Method: SM 254OD-2011 Total Suspended Solids 18.6 mglL 5.0 1 12/04/18 10:41 D6,L1 HEM, Oil and Grease Analytical Method: EPA 1664B Oil and Grease ND mglL 4.8 1 12/08/18 19:31 608 PCB Pest RVE Analytical Method: EPA 608.3 Preparation Method: EPA 608.3 PCB-1016 (Aroclor 1016) ND ug/L 0.50 1 12/05/18 13:56 12/11/18 21:59 12674-11-2 PCB-1221 (Aroclor 1221) ND ug/L 0.50 1 12/05/18 13:56 12/11/18 21:59 11104-28.2 PCB-1232 (Aroclor 1232) ND ug/L 0.50 1 12/05/18 13:56 12/11/18 21:59 11141-16-5 PC8-1242 (Aroclor 1242) ND ug/L 0.50 1 12/05/18 13:56 12/11/18 21:59 53469-21-9 PCB-1248 (Aroclor 1248) ND ug/L 0.50 1 12/05/18 13:56 12/11/18 21:59 12672-29-6 PC8-1254 (Aroclor 1254) ND ug/L 0.50 1 12/05/18 13:56 12/11/18 21:59 11097-69-1 PCB-1260 (Aroclor 1260) ND ug/L 0.50 1 12/05/18 13:56 12/11/18 21:59 11096-82-5 Surrogates Tetrachioro-m-xylene (S) 77 % 60-140 1 12/05/18 13:56 12/11/18 21:59 877-09-8 Decachlorobiphenyl (S) 108 % 60-140 1 12/06/16 13:56 12/11/18 21:59 2051-24-3 Total Nitrogen Calculation Analytical Method: TKN+NO3+NO2 Calculation Total Nitrogen 1.4 mg/L 0.52 1 12/07/18 17:48 351.2 Total Kjeldahl Nitrogen Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993 Nitrogen, Kjeldahl, Total ND mg/L 0.50 1 12/06/18 01:26 12/07/18 05:51 7727-37-9 353.2 Nitrogen, N021NO3 Ares. Analytical Method: EPA 353.2 Rev 2.0 1993 Nitrogen, NO2 plus NO3 1.0 mg/L 0.020 1 12/05/18 09:05 Date: 12/12/2018 12:47 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 4 of 14 aceAnalytical www.pscefabs.WM QUALITY CONTROL DATA Project: Stormwater Pace Project No.: 92409147 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QC Batch: 445458 Analysis Method: SM 254OD-2011 QC Batch Method: SM 254OD-2011 Analysis Description: 2540D Total Suspended Solids Associated Lab Samples: 92409147001 METHOD BLANK: 2441919 Matrix: Water Associated Lab Samples: 92409147001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mg/L ND 2.5 12/04/18 10:40 LABORATORY CONTROL SAMPLE: 2441920 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Suspended Solids mg/L 250 278 111 90-110 L1 SAMPLE DUPLICATE: 2441921 92409147001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg1L 18.6 20.8 11 D6 SAMPLE DUPLICATE: 2441922 92409226001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 25.0 27.5 10 D6 Results presented on this page are In the units indicated by the -Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/12/2018 12:47 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 14 (�Iacmnalj&alo www.pecelabs.com QUALITY CONTROL DATA Project: Stormwaler Pace Project No.: 92409147 QC Batch: 446596 Analysis Method: EPA 1664E QC Balch Method: EPA 16646 Analysis Description: 1664 HEM, Oil and Grease Associated Lab Samples: 92409147D01 METHOD BLANK: 2447681 Associated Lab Samples: 92409147001 Parameter Units Oil and Grease mglL Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers NO 4.8 12/08/1819:20 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28076 (704)875-9092 LABORATORY CONTROL SAMPLE: 2447682 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Oil and Grease mglL 38.5 37.3 97 78-114 MATRIX SPIKE SAMPLE: 2447683 92408693004 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Oil and Grease mglL ND 38.5 42.4 107 78-114 Results presented on this page are In the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/12/2018 12:47 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 14 aceAnalytical www.p"labs.com QUALITY CONTROL DATA Project: Stormwater Pace Project No.: 92409147 QC Batch: 445740 Analysis Method: EPA 608.3 QC Batch Method: EPA608.3 Analysis Description: 608 PCB Pest Red Vol Associated Lab Samples: 92409147001 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 METHOD BLANK: 2443338 Matrix: Water Associated Lab Samples: 92409147001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers PCB-1016 (Aroclor 1016) ug1L ND 0.50 12/11/18 23:03 PCB-1221 (Aroclor 1221) ug/L ND 0.50 12/11/18 23:03 PCB-1232 (Aroclor 1232) ug/L ND 0.50 12/11/18 23:03 PCB-1242 (Aroclor 1242) ug/L NO 0.50 12/11/18 23:03 PCB-1248 (Aroclor 1248) ug/L NO 0.50 12/11/18 23:03 PCB-1254 (Aroclor 1254) ug/L NO 0.50 12/11/18 23:03 PCB-1260 (Aroclor 1260) ug/L NO 0.50 12/11/18 23:03 Decachlorobiphenyl (S) % 95 60-140 12/11/18 23:03 Tetrachloro-m-xylene (S) % 64 60-140 12111/18 23:03 LABORATORY CONTROL SAMPLE: 2443339 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Decachlorobiphenyl (S) % 91 60-140 Tetrachloro-m-xylene (S) % 62 60-140 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2443341 2443340 MS MSD 92409458001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Decachlorobiphenyl (S) % 64 74 60-140 Tetrachloro-m-xylene (S) % 31 54 60-140 S2 Results presented on this page are In the units Indicated by the "units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/12/2018 12:47 PM without the written consent of Pace Analytical Services, LLC. Page 7of14 aceAnalytical www.pacelebs-=n QUALITY CONTROL DATA Project: Stormwater Pace Project No.: 92409147 QC Batch: 445902 Analysis Method: EPA 351.2 Rev 2.0 1993 QC Batch Method: EPA 351.2 Rev 2.0 1993 Analysis Description: 351.2 TKN Associated Lab Samples: 92409147001 METHOD BLANK: 2444299 Matrix: Water Associated Lab Samples: 92409147001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Nitrogen, Kjeldahl, Total mg/L ND 0.50 12/07/18 05:49 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 2444300 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Nitrogen, Kjeldahl, Total mglL 10 10.1 101 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2444301 2444302 MS MSD 92409147001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc, Conc. Result Result %Rec % Rec Limits RP❑ Qual Nitrogen, Kjeldahl, Total mglL ND 10 10 9.6 9.9 92 95 90-110 3 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2444303 2444304 MS MSD 92409401001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Kjeldahl, Total mg1L 2.3 10 10 12.1 11.8 98 95 90-110 3 Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/12/2018 12:47 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 14 acmnalytical` www.pec@Wbs,com Project: Stormwater Pace Project No.: 92409147 QC Batch: 445641 QC Batch Method: EPA 353.2 Rev 2,0 1993 Associated Lab Samples: 92409147001 METHOD BLANK: 2442921 Associated Lab Samples: 92409147001 Parameter Units Nitrogen, NO2 plus NO3 mglL QUALITY CONTROL DATA Analysis Method: EPA 353.2 Rev 2.0 1993 Analysis Description: 353.2 Nitrate + Nitrite, preserved Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers NO 0,020 12/05/18 08:50 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 2442922 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Nitrogen, NO2 plus NO3 mglL 2.5 2.5 100 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2442923 2442924 MS MSD 92409232001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, NO2 plus NO3 mglL NO 2.5 2.5 2.5 2.5 101 101 75-125 0 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2442925 2442926 MS MSD 92409232002 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, NO2 plus NO3 mglL ND 2.5 2.5 2.6 2.6 103 104 75-125 0 Results presented on this page are In the units Indicated by the-ttnits- column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/12/2018 12:47 PM without the written consent of Pace Analytical Services, LLC, Page 9 of 14 laxAnalytical" www. pacelabs corn QUALIFIERS Project: Stormwater % Pace Project No.: 92409147 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersvilte, NC 28078 {704)875-9092 PQL - Practical Quantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4.5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC institute. LABORATORIES PASI-A Pace Analytical Services - Asheville PASI-C Pace Analytical Services - Charlotte PASI-E Pace Analytical Services - Eden ANALYTE QUALIFIERS D6 The precision between the sample and sample duplicate exceeded laboratory control limits. L1 Analyte recovery in the laboratory control sample (LCS) was above QC limits. Results for this analyte in associated samples may be biased high. 52 Surrogate recovery outside laboratory control limits due to matrix interferences (confirmed by similar results from sample re -analysis). REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/12/2018 12i47 PM without the written consent of Pace Analytical Services, LLC. Page 10 of 14 Pace Analytical Services, LLC acEAnalyircal 98D0 4(incey Ave. Suite 100 Huntersvdie, NC 28078 www.pecelebs.cam (704)875-9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Stormwater Pace Project No.: 92409147 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92409147001 001 SM 2540D-2011 445458 92409147001 001 EPA1664B 446596 92409147001 001 EPA608.3 445740 EPA608.3 446614 92409147001 001 TKN+NO3+NO2 446439 Calculation 92409147001 001 EPA 351,2 Rev 2.0 1993 445902 EPA 351.2 Rev 2.0 1993 446217 92409147001 001 EPA 353.2 Rev 2.0 1993 445641 Date: 12/12/2018 12:47 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 11 of 14 Document Name: Document Revised: February 7, 2018 Sample Condition Upon Recei t(SCUR) Page 1 of 2 C$�fialCBr+ ` Document No.: Issuing Authority: F-CAA-CS.033-Rev.06 Pace Carolinas Quality Office Laboratory receiving samples: Asheville ❑ Eden[] Greenwood D Huntersville ❑ Raleigh❑ Mechanicsville(] Client Name: Project #: !(/ WO# : 92409 1 47 Courier: ❑Fed>=x ❑UPS V❑USPS [Glicnt I��I� i fl.�Ili �If!� 011 ❑ Commercial []Pace ❑Other: 2409147 i Custody Seat Present? ❑Yes &Ko Seals Intact? Des ®No Date/initials Person Examining Content Packing Material: ❑Babble Wrap ❑Bubble Hags = done ❑ Other Biological Tissue Frrs:en? Thermometer: [)Yes ❑No QN/A ❑iR C{un ID: q;T�C.5 Type of Ice: �et ❑Biue ❑None Cooler Temp ('C): IV , t Correction Factor; Add/Subtract ('C) r 4 � Temp should be above freezing to VC Cooler Temp Corrected (. C): �- ❑Sarnp.es out of temp criteria. samples on ice, cooling process has begun USDA Regulated Soil (E] N/A, water sample) Did samples origi5jUe in a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate frum a fareign source (internati Ily, F-iYps Tnrkiriino Havall anrd Puprtn Rirn17 I-lYes F< Comments/Discrepancy: Chain of Custody Present? ©No ❑NYA 1. - Sa moles Arrived within Hold Time? Wes ❑Np ❑V/A 2. Short Hold Time Analysis (02 hr.)? ❑4'es Bo ❑rf/A 3. Rush Turn Around Time Requested? ElYes 4, Sufficient Vaiume? ElYes ❑N❑ ❑N/A 5. Correct Containers Used? -Pace Containers Used? E res cs ONo ❑Na ❑N/A ❑N/A 6. Containers Intact? [:IN. El WA 7. Dissolved analysis:5amples Field Filtered? EJY. Sample Labels Match COC? -includes Date/Time/ID/Analysis Matrix: W es [:)No ❑N/A 9. Neadspace in VOA Viats (>5-6mm)? ❑Yes ❑No 2N/A 10. Trip Blank Present? Trip Blank Custody 5eais Present? []Yes ❑Yes ❑Na []NO Q(,IJA LV%A 11. CONVYIENTSAAMPLE DISCREPANCY CLIENT NOTIFICATION/RESOLUTION Person contacted: Project Manager SCURF Review: Project Manager SRF Review: it! i!V b Oki Date/Time: Field Data Required? []Yes [-]Flo Lot ID of split containers: Date: �Z � Date: IQ I V Page 12 of 14 M Iterno BP4U-125 mL Plastic Unpreserved (N/A) (CI-) AP3U-250 mL Pi4stic Unpreserved (N/A) Bp2U-5Q0 mL Plestic Unpreserved (N/A) 9P1U-1 liter Plustit Unpreserved (N/A) BP45-125 mL Plastic H2SO4 (pH < 2) (Cl-) 0P3N-250 mL PlastlC HNO3 (pH < 2) eP4Z-17S mL Plastic 2N Acetate & NaOH (>9) 9P4C-225 mL Plastic tVaDH (pH: 12) (Ci-) WGFU-Wide-mouthed Glass'a r Unpreserved AG1U-1 IkCr Amber Unpreserved (N/A) (CI-) AG1Fi-1 liter Amber HCI (pH 2) AUBU-250 mL Amber Unpreserved (N/A) (Cl-) AGSS-1 ilterAmber H2SO4 (pH <2) AG35-25n mL Amber H2SO4 [PH c 2) AMA(QG3A)-2SO mL Amber NH4C] (N/A)(Ci-) D69H-40 mL VOA HCI (N/A) VG9T.40 mL VOA Na2S203 (N/A) VG9U-40 mL VOA Unix (N/A) DGDP-40 mL VOA H3PO4 (N/A) - VDAK (G vWls Per kit)-5035 kit (N/A) V/GK (3 vials Perklt)-VPH/Gas kit (N/A) SPST-125 mL Sterile Plastic (N/A— iab) SP2T-250 mL Sterile Plastic (N/A — lab) IIPBA-750 mL Plastic (NH2)zSD4 (9.3-9,7) lam'" AGOU-100 mL Amber Unpreserved vials (N/A) f VSUU-20 mLSclntlliatlon vials (N/A) Dp9U-40 mL Amber Unpreserved vials (N/A) W O ♦ n M C 7C- In Dcr O iti D o o X u; a ro o O n tT x :3 CL r a n 2 C rA w ti -D w t:7- O ra O O 6 O 4 M d 7 0 2 nzu � H r 3 H .. M N I X 0 O_ C 1D Q- N O IN ram' M CID N D 1^^• D rbr �8 A v O v C NAl N-OF-CUSTODY / 7hs Qwlr-al-Llnlody to a LEGAL C :a! Request Document NI retevam fields must be carrtPkftd 8=MtNY• ISP .� all= M ■ra■©■0 r■ ©©©r■■■■r■■■ ■■■■MMrr■i■■i■■3 ■r■■■■r■■r■■ ■■M■■MMrrrrr■Mr■■ ■■r■■r■■■■■■ ■■■r■■�r■■■rr■■■■■ ■r■■r■r■rrrr iiiii■�iiiiii�i�ii iiiiiri��iii ■■■�■■�■■r■■r■■r■ r■rr■rr■rrr■ ■r■�r�■■■■r■rrrr■�r■ ■■■■■r■rr■■■ ■r■■_ err■■■■■_ ■ f4. 4ySC16.� _TTT__y C:�-^.•, i�--.]l`k![F T■'.■■�■r■■■■r■■■■r�r■ �:';y'F+' ••�: 1• _ ;.b :• ��TTr',rel. .: _ .. ...w '. _ C"KAW96 Craig Fulcher Environmental, Health & Safety Manager SPX Transformer Solutions, Inc. craig.fulcher@spx.com T 919 288 8378 December 5, 2018 Division of Water Quality Attn: Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 ,o\l eo ,� zoti� �WR S�C�`O� RE: Discharge Monitoring Report for SDO-001 for November 2018 To Whom it May Concern: WAU KESHA 71 Please find enclosed SPX Goldsboro's completed Discharge Monitoring Report (DMR) November 2018. Due to the lack of flow for the month of November this was a "No Flow" event and the DMR is filled out accordingly. This fulfils the requirement of the Storinwater Permit NCS000303, Tier II monthly reporting. Please feel free to contact me at (919) 581-1677 if you have any questions or require any additional information. Sincerely, Z 1, e�A e-27' Craig Fulcher Environmental, Health & Safety Manager SPX Transformer Solutions, Inc. 2701 US Highway 117 South, Goldsboro, NC 27530 www.spxtransformersolutions.com STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT Permit Number NCS000303 SAMPLES COLLECTED DURING CALENDAR YEAR: 2018 (This monitoring report shall be received by the Division no later than 30 days from the date the facility receives the sampling results from the laboratory.) FACILITY NAME SPX Goldsboro COUNTY Wavne PERSON COLLECTING SAMPLE(S) Sara Lorette/AECOM PHONE NO.919-581-1677 CERTIFIED LABORATORY(S) Pace Analytical Services, LLC Lab. Cert. #12, 5342, 37706 Part A: Specific Monitoring Requirements Outfall No. Date Sample Collected pH Total Rainfall mo/dd/yr S.U. inches SDO 001 1 NO FLOW ND = Non Detect Outfall No. Date Sample Collected TSS Oil & Grease mo/dd/yr m m /L SDO 001 NO FLOW ND = Non Detect Outfall No. Date Sample Collected PCBs Total Nitrate mo/dd/ yr m /L m IL SDO 001 NO FLOW ND = Non Detect SIGNATURE OF PERMITTEE OR DESIGNEE REQUIRED ON PAGE 2. Note: No Flow was available in November 2018. Monthly monitoring is in effect due to the current Tier II status. Permit Number NCS000303 Form SWU-247, last remised 21212012 Page 1 of 2 Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month?_ yes X no (if yes, complete Part B) Part B: Vehicle Maintenance Activity Monitoring Requirements Outfall Date 50050 00556 OOS30 .00400 Total Flow (if applicable) Total Rainfall Oil & Grease (if appl.) Non -polar O&GITPH Total Suspended pH New Motor Oil Usage No. Sample Collected (Method 1664 Solids SGT-HEM), if appl. mo/dd/ r MG inches m /l m Il unit al/mo STORM EVENT CHARACTERISTICS: Date Total Event Precipitation (inches): Event Duration (hours): (only if applicable — see permit.) (if more than one storm event was sampled) Date Total Event Precipitation (inches): Event Duration (hours): (only if applicable — see permit.) Mail Original and one copy to: Division of Water Quality Attn: Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there ar`e significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature /..- S- f? (Date) Permit Number NCS000303 Form SWU-247, last revised 21212012 Page 2 of 2 Craig Fulcher Environmental, Health & Safety Manager SPX Transformer Solutions, Inc. craig.fulcher@spx.com T 919 288 8378 WAUKESHA 71 December 5, 2018 Division of Water Quality Attn: Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 RE: Discharge Monitoring Report for SDO-001 for October 2018 To Whom it May Concern: Please find enclosed SPX Goldsboro's completed Discharge Monitoring Report (DMR) for October 2018. No parameters were recorded over the benchmarks. The facility is still under monthly monitoring due to the Tier 11 status of previous months. This fulfils the requirement of the Stormwater Permit NCS000303, Tier II monthly reporting. Please feel free to contact me at (919) 581-1677 if you have any questions or require any additional information. Sincerely, Craig Fulcher Environmental, Health & Safety Manager SPX Transformer Solutions, Inc. 2701 US Highway 117 South, Goldsboro, NC 27530 www.spxtransformersolutions.com STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT Permit Number NCS000303 SAMPLES COLLECTED DURING CALENDAR YEAR: 2018 (This monitoring report shall be received by the Division no later than 30 days from the date the facility receives the sampling results from the laboratory.) FACILITY NAME SPX Goldsboro COUNTY Wayne PERSON COLLECTING SAR'IPLE(S) Sara Lorette/AECOM PHONE NO. 919-581-1677 CERTIFIED LABORATORY(S) Pace Analytical Services, LLC Lab. Cert. #12, 5342, 37706 Part A: Specific MonitoringRe uirements Outfall No. Date Sample Collected pH Total Rainfall mo/ddl r S.U. Inches SDO 001 10/10/2018 7.92 0.25 ND = Non Detect Outfall No. Date Sample Collected TSS Oil & Grease moldd/ r m /L m /L SDO 001 10/10/2018 34.9* <4.8* ND = Non Detect Outfall No. Date Sample Collected PCBs Total Nitrate moldd/ r m L m IL SDO 001 10/10/2018 <0.0005* 2.6* ND = Non Detect SIGNATURE OF PERMITTEE OR DESIGNEE REQUIRED ON PAGE 2. Note: Monthly monitoring is in effect due to the current Tier II status. *Samples requiring thermal preservation were received outside of recommended temperature limits of 0-6 degrees Celsius. Permit Number NCS000303 Form SWU-247, last revised 21212012 Page 1 of 2 Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month?_ yes X no (if yes, complete Part B) Part B: Vehicle Maintenance Activity Monitoring Requirements Ontfall Date 50050 00556. 00530 00400 No. Sample Total Flow Total Oil & Grease Non -polar Total pH New Motor Collected (if applicable) Rainfall (if appl.) O&GITPH Suspended Oil Usage (Method 1664 Solids SGT-HEM), if appl. molddlvr MG inches m Il mg/1 unit al/mo STORM EVENT CHARACTERISTICS: Date 10/10/2018 Total Event Precipitation (inches): 0.25 inches Event Duration (hours): (only if applicable — see permit.) (if more than one storm event was sampled) Date Total Event Precipitation (inches): Event Duration (hours): (only if applicable — see permit.) Mail Original and one copy to: Division of Water Quality Attn: Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Permi 12r!-1Z (Date) Permit Number NCS000303 Form SWU-247, last revised 21212012 Page 2 of 2 NCDENR Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report Forguidance on filling out this form, please visit- bttl2vllpQrtal.nc:denE.org/wgbllrinpdes-stormwate Permit No.: j�/�/�/_/_ _/ �/� // or Certificate of Coverage No.: Facility Name: SPX f o 14 Sbar-o County: w aA rye, Phone No. 9 11 ` 73q — 9a o Inspector &,,& Lo r-e_ Date of Inspection: _ 10 I D `" I iK Time of Inspection- la SD PM Total Event Precipitation (inches):y ` [ - Was this a 'Representative Storm Event" or "Measureable Storm Event" as defined by the permit? (See information below.) es ❑ No Please verify whether Qualitative Monitoring must be performed during a "representative storm event" or "measureable storm event" (requirements vary, depending on the permit). Qualitative monitoring requirements vary. Most permits require qualitativeto be - performed during a "representative storm event" or during a "measureable storm event." However, some permits do not have this requirement. Please refer to these definitions, if applicable. A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. A "measurable storm event" is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DWQ_Regional Office. By this signature, I certify that this repgrt is accurate and complete to the best of my knowledge: (Signature of'hermittee or Wignee) Pagel of 2 5WU-242, Last modified 7/31/2013 1. Outfall Description: Outfall No. '500 — I Struc re (pipe, ditch, etc.) Receiving Stream: UIR A& +-V�6u J1. LL►y[S N� Describe the industrial activities that occur witbin the outfali drainage area: 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: k4�i u�: i DI�u.W 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): A Wyk. 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 1 2 3 � 5 S. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: 1 2 (3) 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is noosolids and 5 is extremely muddy: 1 2 C3 J 4 S 7. Is there any foam in the stormwater discharge? Yes CN q) 8. Is there an oil sheen in the stormwater discharge? Yes (No 9. Is there evidence of erosion or deposition at the outfall? Yes No 10. Other Obvious Indicators of Stormwater Pollution: Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 SWU-242, Last modified 7/31/2013 aceAnalytical www.pecehbs =n October 23, 2018 Craig Fulcher SPX Transformer Solutions, Inc. 2701 Highway 117 South Goldsboro, NC 27530 RE: Project: Stormwater Pace Project No.: 92403015 Dear Craig Fulcher: Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 Enclosed are the analytical results for sample(s) received by the laboratory on October 11, 2018. The results relate only to the samples included in this report. Results reported herein conform to the most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. If you have any questions concerning this report, please feel free to contact me. Sincerely, Nicole Gasiorowski nicole.gasiorowski@pacelabs.com (704)875-9092 Project Manager Enclosures cc: Jennifer Jones, AECOM Jennifer Wheat, AECOM PCB° REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. (704)875-9092 Page 1 of 15 lacceeAnalytical www.paoelab&mn Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 CERTIFICATIONS Project: Stormwater Pace Project No.: 92403015 Charlotte Certification IDS 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 South Carolina Certification #: 99006001 LouisianalNELAP Certification # LA170028 FloddalNELAP Certification #: E87627 North Carolina Drinking Water Certification #: 37706 Kentucky UST Certification #: 84 North Carolina Field Services Certification #: 5342 VirginiaNELAP Certification #: 460221 North Carolina Wastewater Certification #: 12 Asheville Certification IDS 2225 Riverside Drive, Asheville, NC 28804 North Carolina Wastewater Certification #: 40 FloridalNELAP Certification #: E87648 South Carolina Certification #: 99030001 Massachusetts Certification #: M-NC030 VirginiaNELAP Certification #: 460222 North Carolina Drinking Water Certification #: 37712 Eden Certification IDS 205 East Meadow Road Suite A, Eden, NC 27288 North Carolina Drinking Water Certification #: 37738 North Carolina Wastewater Certification #: 633 VirginiaNELAP Certification #: 460025 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 15 Pace Analytical Services, LLC aceAnalytrcal0 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 www.peookftcorn (704)875-9092 SAMPLE ANALYTE COUNT Project: Stormwater Pace Project No.: 92403015 Analyses Lab ID Sample ID Method Analysts Reported Laboratory 92403015001 SDP-001 SM 2540D-2011 SOB 1 PASI-E EPA 1664B JMS 1 PASI-C EPA608.3 SEM 9 PASI-C TKN+NO3+NO2 Calculation KDF1 1 PASI-A EPA 351.2 Rev 2.0 1993 MFO 1 PASI-A EPA 353.2 Rev 2.0 1993 KDF1 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page.3 of 15 (�Iacmnalyfical* www.pecelabs ccm ANALYTICAL RESULTS Project: Stormwater Pace Project No.: 92403015 Pate Analytical Services, LLG 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: SDP-001 Lab ID: 92403015001 Collected: 10/10/18 23:30 Received: 10/11118 10:40 Matrix: Water Comments: • Samples requiring thermal preservation were received outside of recommended temperature limits of 0-6 degrees Celsius. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 2540D Total Suspended Solids Analytical Method: SM 2540D-2011 Total Suspended Solids 34.9 mglL 3.6 1 10/15/18 08:58 HEM, Oil and Grease Analytical Method: EPA 1664E Oil and Grease ND mg1L 4.8 1 10/22/18 00:10 608 PCB Pest RYE Analytical Method: EPA608.3 Preparation Method: EPA608.3 PCB-1016 (Aroclor 1016) ND uglL 0.50 1 10/15118 11:37 10/16/18 12:55 12674-11-2 PCB-1221 (Aroclor 1221) ND ug1L 0.50 1 10/15/18 11:37 10/16/18 12:55 11104-28-2 PCB-1232 (Aroclor 1232) NO ug1L 0.50 1 10/15/18 11.37 10/16/18 12.55 11141-16-5 PC13-1242 (Aroclor 1242) ND ug/L 0.50 1 10/15/18 11:37 10/16/18 12:55 53469-21-9 PCB-1248 (Aroclor 1248) ND uglL 0.50 1 10/15/18 11:37 10/16/18 12:55 12672-29-6 PCB-1254 (Aroclor 1254) NO uglL 0.50 1 10/15/18 11:37 10116/18 12:55 11097-69-1 PCB-1260 (Aroclor 1260) ND uglL 0.50 1 10/15/18 11:37 10/16/18 12:55 11096-82-5 Surrogates Tetrachloro-m-xylene (S) 100 % 60-140 1 10/15/18 11.37 10/16/18 12:55 877-09-8 Decachlorobiphenyl (S) 86 % 60-140 1 10/15/18 11:37 10/16/18 12:55 2051-24-3 Total Nitrogen Calculation Analytical Method: TKN+NO3+NO2 Calculation Total Nitrogen 2.6 mg1L 0.52 1 10/18/18 14:54 351.2 Total Kjeldahl Nitrogen Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993 Nitrogen, Kjeldah), Total 2.2 mglL 0.50 1 10/14/18 14:41 10/16/18 01:07 7727-37-9 353.2 Nitrogen, N021NO3 pros. Analytical Method: EPA 353.2 Rev 2.0 1993 Nitrogen, NO2 plus NO3 0,43 mglL 0.020 1 10/17/18 10:49 REPORT OF LABORATORY ANALYSIS This report shalt not be reproduced, except in full, . Date: 10/23/2018 1112 AM without the written consent of Pace Analytical Services, LLC. Page 4 of 15 aceAnalytical. www.pmvlabs.com QUALITY CONTROL DATA Project: Stormwater Pace Project No.: 92403015 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QC Batch: 436173 Analysis Method: SM 2540D-2011 QC Batch Method: SM 2540D-2011 Analysis Description: 2540D Total Suspended Solids Associated Lab Samples: 92403015001 METHOD BLANK: 2399974 Matrix: Water Associated Lab Samples: 92403015001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mg/L ND 2.5 10/15/18 08:57 LABORATORY CONTROL SAMPLE: 2399975 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Suspended Solids mg/L 250 274 110 90-110 SAMPLE DUPLICATE: 2399976 92403122001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 6.4 5.9 8 D6 SAMPLE DUPLICATE: 2399977 92403125001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 6.6 7.1 7 D6 Results presented on this page are In the units Indicated by the "Units- column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/23/2018 11:12 AM without the written consent of Pace Analytical Services, LLC. Page 5 of 15 Iacl Analytical www.patelabs.corn (� QUALITY CONTROL DATA Pate Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntorsvi3e, NC 28078 (704)875-9092 Project: Stormwater Pace Project No.: 92403015 QC Batch: 437530 Analysis Method: EPA 1664E QC Batch Method: EPA 1664B Analysis Description: 1664 HEM, Oil and Grease Associated Lab Samples: 92403015001 METHOD BLANK: 2406070 Matrix: Water Associated Lab Samples: 92403015001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Oil and Grease mg1L ND 4.8 10/22/18 00:08 LABORATORY CONTROL SAMPLE: 2406071 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Oil and Grease mg1L 38.5 37.1 96 78-114 MATRIX SPIKE SAMPLE: 2406072 92402687001 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Oil and Grease mg1L ND 38.5 36.9 96 78-114 Results presented on this page are In the units Indicated by the -Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. Date: 1012312018 11:12 AM without the written consent of Pace Analytical Services, LLC. Page 6 of 15 • ac,Mnalytical www.paced &c= QUALITY CONTROL DATA Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: Stormwater Pace Project No.: 92403015 QC Batch: 436213 Analysis Method: EPA608.3 QC Batch Method: EPA 608.3 Analysis Description: 606 PCB Pest Red Vol Associated Lab Samples: 92403015001 METHOD BLANK: 2400290 Matrix: Water Associated Lab Samples: 92403015001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers PCB-1016 (Aroclor 1016) ug/L NO 0.50 10/16/18 14:11 PCB-1221 (Aroclor 1221) ug/L NO 0,50 1011611814:11 PCB-1232 (Aroclor 1232) ug/L NO 0.50 10/16/18 14:11 PCB-1242 (Aroclor 1242) ug1L NO 0.50 10/16/18 14:11 PCB-1248 (Aroclor 1248) ug/L NO 0.50 10/16/18 14:11 PCB-1254 (Aroclor 1254) ug/L NO 0.50 10/16118 14:11 PCB-1260 (Aroclor 1260) ug/L NO 0.50 10/16/18 14:11 Decachlorobiphenyl (S) % 104 60-140 10/16/18 14:11 Tetrachloro-m-xylene (S) % 77 60-140 10/16/18 14:11 LABORATORY CONTROL SAMPLE: 2400291 Spike LCS LCS % Rec Parameter Units Cone. Result % Rec Limits Qualifiers Decachlorobiphenyl (S) % 112 60-140 Tetrachloro-m-xylene (S) % 102 60-140 MATRIX SPIKE SAMPLE: 2400292 92403281001 Spike MS MS % Rec Parameter Units Result Cone. Result % Rec Limits Qualifiers Decachlorobiphenyl (S) % 104 60-140 Tetrachloro-m-xylene (S) % 125 60-140 SAMPLE DUPLICATE: 2400293 92403281002 Dup Parameter Units Result Result RPD Qualifiers PCB-1016 (Aroclor 1016) ug/L NO ND PCBA221 (Aroclor 1221) ug1L NO ND PCB-1232 (Aroclor 1232) ug1L NO NO PCB-1242 (Aroclor 1242) ug1L NO NO PCB-1248 (Aroclor 1248) ug1L NO NO PCB-1254 (Aroclor 1254) ug/L NO NO PCB-1260 (Aroclor 1260) ug1L NO NO Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10123/2018 11:12 AM without the written consent of Pace Analytical Services, LLC. Page 7 of 15 (�Iacmnalyfical" w m..pecelabs.=n QUALITY CONTROL DATA Project: Stormwater Pace Project No.: 92403015 QC Batch: 436148 Analysis Method: EPA 351.2 Rev 2.0 1993 QC Batch Method: EPA 351.2 Rev 2.0 1993 Analysis Description: 351.2 TKN Associated Lab Samples: 92403015001 METHOD BLANK: 2399875 Associated Lab Samples: 92403015001 Parameter Units Nitrogen, Kjeldahl, Total mg1L LABORATORY CONTROL SAMPLE: 2399876 Parameter Units Nitrogen, Kjeldahl, Total mg1L Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 0.50 10/16/18 00:56 Spike LCS LCS % Rec Conc, Result % Rec Limits Qualifiers 10 9.4 94 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2399877 2399878 MS MSD 92402844001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Kjeldahl, Total mg/L 1.1 10 10 9.7 10.9 86 98 90-110 11 M1,R1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2399879 2399880 MS MSD 92403137001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Kjeldahl, Total mg/L 4.8 10 10 15.5 15.6 107 109 90-110 1 Results presented on this page are In the units indicated by the "Units" column except where an altemale unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/23/2018 11:12 AM without the written consent of Pace Analytical Services, L.L.C. Page 8 of 15 aceAnalytical" www.pacelabs.cvm QUALITY CONTROL DATA Project: Stormwater Pace Project No.: 92403015 QC Batch: 436373 Analysis Method: EPA 353.2 Rev 2.0 1993 QC Batch Method: EPA 353.2 Rev 2.0 1993 Analysis Description: 353.2 Nitrate + Nitrite, preserved Associated Lab Samples: 92403015001 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875.9092 METHOD BLANK: 2400847 Matrix: Water Associated Lab Samples: 92403015001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Nitrogen, NO2 plus NO3 mg/L ND 0.020 10/17/18 10:15 LABORATORY CONTROL SAMPLE: 2400848 Spike LCS LCS % Rec Parameter Units Cone. Result % Rec Limits Qualifiers Nitrogen, NO2 plus NO3 mg/L 2.5 2.5 100 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2400849 2400850 MS MSD 92402332002 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual Nitrogen, NO2 plus NO3 mg/L 4.0 2.5 2.5 6.0 6.0 82 81 75-125 0 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2400851 2400852 MS MSD 92402419001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual Nitrogen, NO2 plus NO3 mg/L 0.24 2.5 2.5 1.6 1.6 55 55 75-125 1 M1 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/23/2018 11:12 AM without the written consent of Pace Analytical Services, LLC. Page 9 of 15 ac6Analyfical www.pacelabs.= QUALIFIERS Project: Stormwater Pace Project No.: 92403015 DEFINITIONS Pate Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 DF - Diludon Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. M D L -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration, Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate i RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. LABORATORIES PASI-A Pace Analytical Services -Asheville PASI-C Pace Analytical Services - Charlotte PASI-E Pace Analytical Services - Eden ANALYTE QUALIFIERS D6 The precision between the sample and sample duplicate exceeded laboratory control limits. M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. R1 RPD value was outside control limits. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. Date: 10/23/2018 11:12 AM without the written consent of Pace Analytical Services, LLC. Page 10 of 15 acmnalX cal o www.pecelabs com QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Stormwater Pace Project No.: 92403015 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huniersville, NC 28078 (704)875-9092 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92403015001 SDP-001 SM 254OD-2011 436173 92403015001 SDP-001 EPA 1664E 437530 92403015001 SDP-001 EPA608.3 436213 EPA608.3 436433 92403015001 SDP-001 TKN+NO3+NO2 437006 Calculation 92403015001 SDP-001 EPA 351.2 Rev 2.0 1993 436148 EPA 351.2 Rev 2.0 1993 436330 92403015001 SDP-001 EPA 353.2 Rev 2.0 1993 436373 Date: 10/23/2018 11:12 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 11 of 15 Document Name: Document Revised: February 7, 2018 Sample Condition Upon Receipt(SCUR) Page 1 of 2 Document.No.:,_ -- — issufrrgAutlrbJr4 ,,eAnaojcal' F-CAR-CS-033-Rev.06 Pace Carolinas Quality Office Laboratory receiving samples-. Asheville ❑ Eden[] Greenwood Fluntersvilie ❑ Raleigh(] Mechanicsville[] Nam- - Client Name: Project #: 1 WO# : 924030V5 - Courier: []Fed Ex' CUPS ❑USPS Client 1 i NNII ❑ Commercial []PacePace ❑Other: 92403015 III Custody Seal Present? ❑Yes . o Seals Intact? ❑YesYo j Date/InI ialsPersonExaminingContents: �r7 Packing Material: ❑Bubble Wrap Alubble Bags ❑None ❑ Other Biological Tissue Frozen? Thermom _ % �( ❑Yes ❑No 14N/A AIIR Gun ID: do ] Type of Ice: y_Z w ❑81ue []None Cooler Temp ('C): ('C): —1 .S O Correction Factof. Ad Subtract ('C)� \G' . f Temp should he above freezing to 6'C Cooler Temp Corrected ('C): Qsamples out of temp criteria. Sampleson ice, cooling process hasbegun USDA Regulated Soil {(,V/A, water sample) Did samples originate in a q aran tine zone within the United States: CA, NY, or SC {check maps)? Did samples originate from a foreign source (internationally, Myes svo including Hawaii and Puerto Rico)? nYes .40 Comments/Discrepancy: Chain of Custody Present? es ©No QN/A 1. Samples Arrivedwithin Hold Time? Yes ❑N ON/A 2. Short Hold Time Analysis (<77 hr.)? ❑Yes N ❑N/A 3. Rush Turn Around Time Requested? QYes No ONJA 4. Sufficient Volume? es ❑No ❑N/A S. Correct Containers Used? -Pace Containers Used? Y?- as ONO (]No ON/A QN/A 6. Containers Intact? 25 ONO N/A 7. Dissolved analysis: Samples Field Filtered? QYes ❑No N/A 8. } Sample tabels Match COC? -Includes Date/Time/ID/Analysis Matrix: 2<es �✓ ❑No ❑N/A 9. Headspace in VOA Vials (�,S-6mm)? ❑Yes ONO N/A 10. - Trip Blank Present? Trip Blank Custody Seals Present? ❑Yes Yes ©No ❑No N/A N/A 11. COMMENTS/SAMPLE DISCREPANCY Field Data Required? ❑Yes [:]No c--a PaN, -5 cz c6 at v3 0(- - - ID-of,split-LOntainers:.___..__._.__. CLIENT NOTIFICATION/RESOLUTION IVLre.r Fos Person contacted: it I Date/Time: 7 Project Manager SCURF Review: Date; 4 Project Manager SRF Review: Date; 1(}L1 C� Page 12 of 15 r dL'e� lCal Document fame: Sample Condition Upon Receipt(SCUR) Document Revised: February 7, 2018 Page 1 of 2 Document No.; F=CAR=C5-'033=Rev.06- Issuing AutftorityL- T Pace Carolinas Quality Office *Check mark top half of box if pH and/or dechlorination is Project # J verified and within the acceptance range for preservation jl samples. I Exceptions: VOA, Coliform, TOC, oil and Grease, DRO/8015 (water) DOC, LLHg ! **Bottom half of box is to list number of bottle L WO#:924®3®i5 PM: NMG Due Date: 10/22/18 CLIENT: 92-SPX Golds E E 1v Z CIA a a a. E 04 ry Z) a a m z 2 0 v y 7 m i E N 7D m a m 2 V v v m a E O N D N a m ` v > d 4 a v _ D r1 a m iz N V a v n _ A E in N VI V a m N V n 1n Z = m E O N z m q m o m Z y a w Z N E �n N N C a M M A a z E vi H U V a m v a C = M U o E LL [� 3 a v MP M Q _ .y t7 a = a U S E ¢ _ r� C7 a a p N E a p N M.-1 t7 a V V P a E _ VI t7 a V n v O ry 2 E a E 4 N V1 M 0 a = z v E ¢ N T try O a en 0 a d Z a a > E V i M U o Z m H a O > E Q ti C1 47 > Q = b ¢ 0 > E O C M Q 7 Q Z p 0 a O > E Q d M 0 a Q Y in m 10n i n ° i� X a O > a Y 17 a } y n �° ,a Y tJ � > I z a G `a E r+ r v1 a wt A ? u t9 d m v h E LM N r N a ^ 01 Oi 0 ry = z u m a E N 4 a Co W �U aZi Q 3 v E a .� E M 7 C 0w Cc a Z n m a o _ro c u E 17 > z v1 } v v c E a E C O t7 n 1 f t z 3\N\\ \ 1 a N1 11 N\ 5 ` \N N\N I NN 7 \R \N N\ a I 9 N\\\ \\L N- LO I \\N\ \\\N 12 N- pH Adjustment Log for Preserved Samples Sample ID Type of Preservative pH upon receipt Date preservation adjusted Time preservation adjusted Amount of Preservative added Lot N Mote: Whenever :here is a discrepancy affecting North Carolina compliance samples, a copy of this form w4l be Sent to the North Carolina DEHNR Certification Office (i.e, Out of hold, incorrect preservative, out of temp, incorrect containers, Page 13 of 15 CHAIN -OF -CUSTODY / Analytical Request Document r The Chairs -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed ac irately. F� Section A Section a Section C _ 7 Required Client Information: Required Project Information: Invoice Information: PagO . t Of Company: SPX Goldsboro Reportro: Craiq Fulcher Attention: Address: 2701 Nighv.ay 117 Soutn Copy To: Company Name: Golosboro, NC 27530 Addim: — a. Rd ulat A enc Email- I Puncnase Order a: Pace Quote: Phone: JFax Project Name: Starmwater Pace Project Manager. nicole.pasiorrn ki@ acetabs,com, - - --State 1 Location ,' _. ' - Requested Due Date: Project 0: Pace Profile 73: EW30-1 NC ! R iiestnd AiriMyi4s Filtered IY _ A- - - - - - _ AAATRIK CODE $ �] COLLECTED z Preservatives- a� u V Wsla VR VAv ,L, A Prea+at P SAMPLE ID a a START END ti `.. T One Character perbox. w�P. wP w w .a .m m o tA•7,' 0-91 . -) .a b5 O >- m a U # o �Sample Ids must be umiquo Wier x ,µ., w o 'D �O �� ill PATE TIME DATE TIME a m : 7 T = S z 2 4 ,a' - O a 2 t ^' Sr�O ' oo iJi fi I��fo li' C 1C >[ K u K I W 1 2.. 3' 44 JI I 6' I :7 i R 9s I 2- I _ R71r-.7- •''" AOOITIONALCOYNENTS RELWOUISHED BY 71LFFILWTION - DATE. t� .TIME �^• - CEPTED BY I AFFWATION -DATE' • ME i SAMPLE CONDITIONS. - - I ` SAMPLER NAME AND SIGNATURE'• _ _ - —"-'..t'_` •ga •=�., _ _ �2-�,. - c PRINT Name of SAMPLER: ^ c a m a u Z o w m o z 8 S z SIGNATURE of SAMPLER: DATE Signed: w F1± a m m d 0 UI) Section A Rcty.i.od CA. ni kjo—� lion: CHAIN -OF -CUSTODY I Analytical Request Document The Chain-of-Cuzlodyir a LEGAL DOCUMENT. All rel4vant Geld; MUSt be CompizEed S"Mon a Secdon C Rcruimd Project 1,1`an.aziow. lnlo..niflon! CC-P—Y, I SYX Wi3 taro i".-Par.Ta G!Y;JFLja.n . T.--.-- Ajd-u I VO I 1 117 S-M Zopy To: C 0n. P,-j I Y N;-, re: N- 2753a PMF.,* Mn3q�. ,3 i-t" f L 6 Duo rklw ',P; •• Pmr.lo r. &Lfij NC .. .. ...... COLLECTED I SAMPLE ID ad a0 START Q.* Ch�-t- Per b-c W- -N (A4- C-9 1. -) — ASimple Id. r;-= be Urique or 73 DATE TiVZ DATE Tl:,iz Z, z x z Z L x� Y ai tR N, to- 1-1 CIe, A/ PRINT 1,14ll*e at SAIAPLER: SIGNATURE of SP..MPLER: DATE Signed;