Loading...
HomeMy WebLinkAboutNCS000295_MONITORING INFO_20191231A. R STORMWATER DIVISION CODING SHEET NCS PERMITS PERMIT NO. nILSUU��(� DOC TYPE ❑FINAL PERMIT MONITORING REPORTS ❑ APPLICATION COMPLIANCE ❑ OTHER DOC DATE H YYYYMMDD JACKSON PAPER MANUFACTURING RECE �E December 27, 2019 DEC a 1201E NCDEQ, Division of Waler RCSOUCCCS Inlormation 1'rocessing Unit Attn: Central FileslcDMR 1617 Mail Service Center Raleigh, Nol-th Carolina 27699-1617 R1": Discharge Monitoring Report (4'r' Quarter 2019 DMR and November 2019 Tier Two DNIR) NPDLS Permit No. NCS000295 Jackson Paper Manufacturing Company Dcar Division of Watcr Resources: Ncasc find enclosed Discharge Monitoring Report for Jackson Paper Manufacturing Company NPDE�'S Per'niit No. NCS000295 for reporting period starting October 1, 2019 and ending December 31, 2019. Also included is the November "1 ict- Two monitoring results for Outfall 003. Results from sumples taken on [November 27, 2019 show benchmark exceedances at Outfall 003 for TSS and COD. 'there was a benchmark exceedance al Outfall 002 for 1411. E'er our current `1'ier Two responsc for Outfall 003, we will continue to conduct monthly monitoring arld reporting for all parameters at Outfall 003. Monthly (analytical and qualitative) monitoring will C011tilILlC until three consecutive sample results are below the benchmark values. We will also continue to monitor for all parameters in the receiving water directly upstream and downstream of the monitoring, point in accordance with the Tler Two response. I certify that based on lnlormallon and belief' lormed from reasonable inquiry, the Statements and anformallon an the document tyre tl-Lle, accurate, and complete. ]'lease contact Kiesha Bridges at (828)556-5534 Ext. 226 if you have ally questions or need any'additional information. Sine ly, Car:' Tyndall Vice -President Operations ,Jackson Paper Manufacturing Company fnclosurc: Stormwater Discharge Monitoring Report cc: JPMC file NORTH CAROLINA'S LARGEST RECYCLED PA!'['R PRODUCER 152 Wisr MAIN SIRIAr(D 1101ioe 6670 Svlv,v. NC28771) '1 E1.(828) 586-5534 FAX (828) 586-6755 Stormwater Discharge Outfall (SDO) INlonitoring Report Permit Number NCS000295 Facility Name: Jackson Paper Manufacturing Company Person Collecting Samples Kiesha Bridges Certified Laboratory: Pace Analytical Services LLC Project # 92455461 Samples Collected During Calendar Year: 2019 (This monitoring report shall be received by the Division no later than 30 days from the date the facility receives the sampling results from the laboratory.) County: Jackson Phone NO. (828)586-5534 Ext. 226 (SIGNATURE OF PERiNUTTEE OR DESIGNEE) By this signature. I certify that this report is accurate and complete to the best of my knowledge. Oil and Grease Turbidity TSS pH COD Benchmark i5 50 (6-9) 120 Benchmark Na Benchmark Benchmark Benchmark Date Result Result Result Result Result Outfall Exceedance Benchmark Exceedance Exceedance Exceedance Sampled mg/L Y/N N'I'U mall 1 /N YIN mall 1'/N 1125arn 001 ND No 5.8 14.0 No 6.2 No ND N'o 8:25am 11/27/19 002 ND No ND ND No 6.6 No ND N'o 8:45am 11/27/19 003 ND No 262.0 2080 Yes 6.9 No 144.0 Yes 8:5am 35am, 11/27/19 004 ND No 10.4 23.6 No 5.7 Yes ND No 8:15am Creek Pre 11/27/19 ND N/A 62.8 124.0 N°/A 6.4 N/A 27.0 N/A Mill 9:15am Creek Post 11/27/19 ND N/A 88.9 146.0 N/A 6A N/A 29.4 N/A Mill 9:30am ND. Not detected at or above adjusted reporting limit. Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? :Yes x No Nleasureable Storm Event? Yes 0.63 Storm Event Characteristics: Date: November 27, 2019 Total event,precipitaiion (inches):___ Duration of storm event: -15 hours Time since last rain event: -2 112 days (-63 hours) Drainage Area Mail Original and one copy to: Division of Water Quality Attn: Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 1 11 111 IV Area (acres) Area (sf) Volume (cf) 1.69 73,616 3,865 5.43 236,531 12,418 20.45 890,802 46,767 1.77 77,101 4,048 Volume.(gal) 28,909' . 92,8867 349,819 - 30,278- "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and com I am aware that there are significant penalties for submitting false information, including the possibility of fines and imDdsonment for known=p ations." (Signature of Permltee) (Da laceAnalj4icalo www.pacelehstom December 18, 2019 Kiesha Bridges Jackson Paper Mfg. Co. 152 West Main St. Sylva, NC 28779 RE: Project: STORMWATER 11/27/19 Pace Project No.: 92455461 Dear Kiesha Bridges: Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Enclosed are the analytical results for sample(s) received by the laboratory on November 27, 2019. The results relate only to the samples included in this report. Results reported herein conform to the most current, applicable TNIINELAC standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. Revised Report. The TPH O&G result has been corrected for sample 92455461-006. If you have any questions concerning this report, please feel free to contact me. Sincerely, Chris Derouen christopher.derouen@pacelabs.com (828)254-7176 Project Manager Enclosures cc: Keisha Bridges, Jackson Paper Mfg. Co. NCCQF�� qe0 A�Q� REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 20 laneAnalytcalo www.pacldabs.com Project: STORMWATER 11/27/19 Pace Project No.: 92455461 Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28604 (828)254-7176 Pace Analytical Services Charlotte 9800 KinceyAve. Ste 100, Huntersville, NC 28078 LouisianalNELAP Certification # LA170028 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 Pace Analytical Services Asheville 2225 Riverside Drive, Asheville, NC 28804 FloridalNELAP Certification #: E87648 Massachusetts Certification #: M-NC030 North Carolina Drinking Water Certification #: 37712 CERTIFICATIONS Snuth Carolina Certification #: 99006001 FloridalNELAP Certification #: E87627 Kentucky UST Certification #: 84 VirginiaNELAP Certification #: 460221 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 Virgin iaNELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 20 lacieAnalj4ical" iwww.Pacelabs.com SAMPLE ANALYTE COUNT Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Project: Pace Pro}ecl No.: STORMWATER 11/27/10 92455461 Analytes Lab ID Sample 1D Method Analysts Reported Laboratory 92455461001 OUTFALL#1 EPA1664D HH 1 PASI-C EPA 180.1 Rev 2.0 1093 EWS 1 PASI-A SM 254OD-2011 CJL 1 PASI-A EPA 9040C ECH 1 PASI-A SM 5220D-2011 GC 1 PASI-A 9245546i002 OUTFALL#2 EPA1664B HH 1 PASI-C EPA 180,1 Rev 2.0 1993 EWS 1 PASI-A SM 2540D-2011 CJL 1 PASI-A EPA 0040C ECH 1 PASI-A SM 5220D-2011 GC 1 PASI-A 92455461003 OUTFALL#3 EPA 16648 HH 1 PASI-C EPA 180.1 Rev 2.0 1993 EWS 1 PASI-A SM 254OD-2011 CJL 1 PASI-A EPA 9040C ECH 1 PASI-A SM 522OD-2011 GC 1 PASI-A 92455461004 OUTFALL #4 EPA 16648 HH 1 PASI-C EPA 180.1 Rev 2.0 1993 EWS 1 PASI-A SM 254OD-2011 CJL 1 PASI-A EPA 9040C ECH 1 PASI-A SM 5220D-2011 GC 1 PASI-A 92455461005 CREEK PRE -MILL EPA 16648 HH 1 PASI-C EPA 180.1 Rev 2.0 1993 EWS 1 PASI-A SM 2540D-2011 CJL 1 PASI-A EPA 904nC ECH 1 PASI-A SM 5220D-2011 NAL 1 PAS! -A 92455461006 CREEK POST -MILL EPA 1664E HH 1 PASI-C EPA 180.1 Rev 2.0 1993 EWS 1 PASI-A SM 2540D-2011 CJL 1 PASI-A EPA 9040C ECH 1 PASI-A SM 5220D-2011 NAL 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not he reproduced, except in full, without the written consent of Pace Analyticai Services, LLC. Page 3 of 20 (�IaceAnalyficalo www.pacelabs.cara ANALYTICAL RESULTS Pace Analytical Services, LLC 2225 Riverside dr. Asheville, NC 28804 (828)254-7176 Project: STORMWATER 11/27/19 Pace Project No.: 92455461 Sample: OUTFALL #1 Lab ID: 92455461001 Collected: 11127/19 08:25 Received: 11127119 12:20 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. C1ual 1664 SGT-HEM, TPH Analytical Method: EPA 1664E Total Petroleum Hydrocarbons ND mglL 5.0 1 12M2/19 10:10 180.1 Turbidity Analytical Method: EPA 1130.1 Rev 2.0 1993 Turbidity 5.8 NTU 1.0 1 1112711915:50 2540D Total Suspended Solids Analytical Method: SM 25400-2011 Total Suspended Solids 14.0 mglL 2.5 1 12/02/19 18:54 9040 pH Analytical Method: EPA 9040C pH at 25 Degrees C 6.2 Std. Units 0.10 1 12/08/19 15:24 H3 5220D COD Analytical Method: SM 5220D-2011 Preparation Method: SM 5220D-2011 Chemical Oxygen Demand NO mg1L 25.0 1 12102/19 17:01 12/02/19 22:10 REPORT OF LABORATORY ANALYSIS This report shag not be reproduced, except in 1`0. Date: 12/1812019 01:29 PM without the w6lten consent of Pace Analytical Services, LLC. Page 4 of 20 aceAnalylcal www.par:elabsxam ANALYTICAL RESULTS Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 25804 (828)254-7176 Project: STORMWATER 11/27/19 Pace Project No.: 92455461 S Sample: OUTFALL #2 LabID: 92455461002 Collected: ll127119 08:45 Received: 11/27/19 12:20 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 1664 SGT-HEM, TPH Analytical Method: EPA 1664E Total Petroleum Hydrocarbons ND mg1L 5.0 1 12/12119 10:10 180.1 Turbidity Analytical Method: EPA 180.1 Rev 2.0 1993 Turbidity ND NTU 1.0 1 11/27/1915:52 2540D Total Suspended Solids Analytical Method: SM 2540D-2011 Total Suspended Solids ND rnglL 2.5 1 12102M9 18-55 9040 pH Analytical Method: EPA 9040C pH at 25 Degrees C 6.6 Sid. Units 0.10 1 121CB119 15:41 H3 52201) COD Analytical Method: SM 5220D-2011 Preparation Method: SM 5220D-2011 Chemical Oxygen Demand ND rnglL 25.0 1 12/02119 17:01 12/02/19 22:10 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/18/2019 01:29 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 20 6 ac,Mnalytical www.pacelahe.wm ANALYTICAL. RESULTS Pace Analytical Services, LLC 2225 Riverside ❑r. Asheville, NC 28804 (828)254-7176 Project: STORMWATER 11/27/19 Pace Project No.: 92455461 Sample: OUTFALL #3 Lab ID: 92455461003 Collected: 11/27/19 08:35 Received: 11/27/19 12:20 Matrix: Water Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual 1664 SGT-HEM, TPH Analytical Method: EPA 1664E Total Petroleum Hydrocarbons NO mg/L 5.0 1 12/12/19 10:10 180.1 Turbidity Analytical Method: FPA 180.1 Rev 2.0 1993 Turbidity 262 NTU 1.0 1 11/27/1015:50 2540D Total Suspended Solids Analytical Method: SM 2540D-2011 Total Suspended Solids 208 rnglL 50.0 1 12/02/19 18:55 9040 pH Analytical Method: EPA 9040C pH at 25 Degrees C 6.9 Std. Units 0.10 1 12/08119 15:30 H3 5220D COD Analytical Method: SM 5220D-2011 Preparation Method: SM 5220D-2011 Chemical Oxygen Demand 144 rng/L 25.0 1 12/02/19 17:01 12/02119 22:10 REPORT OF LABORATORY ANALYSIS This report shall nol be reproduced, except in full, Date: 12/1812019 01:29 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 20 ,�IaceAnalytical® www.pacelabs.com ANALYTICAL RESULTS Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Project: STORMWATER 11/27/19 Pace Project No.: 92455461 Sample: OUTFALL #4 Lab ID: 92455461004 Collected: 11/27119 08A5 Received: 11/27/19 12:20 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 1664 SGT-HEM, TPH Analytical Method: EPA 1664B Total Petroleum Hydrocarbons ND mglL 5.0 1 12/12119 10:11 180.1 Turbidity Analytical Method: EPA 180.1 Rev 2.0 1993 Turbidity 10.4 NTU 1.0 1 1112711915A9 2540D Total Suspended Solids Analytical Method: SM 254OD-2011 Total Suspended Solids 23.6 mglL 5.0 1 12/02/19 18:56 9040 pH Analytical Method: EPA 9040C pH at 25 Degrees C 5.7 Std. Units 0.10 1 12/08/19 15:09 H3 5220D COD Analytical Method: SM 5220D-2011 Preparation Method: SM 5220D-2011 Chemical Oxygen Demand ND tnglL 25.0 1 12/02/19 17:01 12/02/19 22:10 REPORT OF LABORATORY ANALYSIS Ws report shall not he reproduced, except in full. Dale: 12/18/2019 01:29 PM without the written consent of Pace Annlytiral Services, LLC, Page 7 of 20 lacieAnalXical" www.pacelabs.com ANALYTICAL RESULTS Pace Analytical Services, LLC 2225 Riverside ❑r. Asheville, NC 28804 (828)254-7176 Project: STORMWATER 11/27119 Pace Project No.: 92455461 Sample: CREEK PRE -MILL Lab ID: 92455401005 Collected: 11/27/19 09:15 Received: 11/27/19 12:20 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 1664 SGT-HEM, TPH Analytical Method: EPA 1664E lotal Petroleum Hydrocarbons ND mg1L 5.0 1 12/12/19 10:12 180.1 Turbidity Analytical Method: EPA 180.1 Rev 2.0 1993 Turbidity 62.8 NTU 1.0 1 11/2711915:52 2540D Total Suspended Solids Analytical Method: SM 2540D-2011 Total Suspended Solids 124 mg/L 12.5 1 12/02119 18:57 9040 pH Analytical Method: EPA 9040C pH at 25 Degrees C 6.4 Std. Units 0.10 1 12/08119 15:47 H3 5220D COD Analytical Method: SM 5220D-2011 Preparation Method: SM 5220D-2011 Chemical Oxygen Demand 27.0 mg/L 25.0 1 12/04119 14:03 12/05119 08:36 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/1812019 01:29 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 20 (�IweAnal(Xicalo www.pacelibs.com ANALYTICAL RESULTS Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Project: STORMWATER 11/27/19 Pace Project No.: 92455461 Sample: CREEK POST -MILL Lab ID: 92455461006 Collected: 11127/19 09:30 Received: 11127/19 12:20 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 1664 SGT-HEM, TPH Analytical Method: EPA 16645 Total Petroleum Hydrocarbons ND rnglL 5.0 1 12/12/19 10:12 180.1 Turbidity Analytical Method: EPA 180.1 Rev 2.0 1993 Turbidity 88.9 NTU 1.0 1 11/27/1915:52 2540D Total Suspended Solids Analytical Method: SM 2540D-2011 Total Suspended Solids 146 mWL 12.5 1 12/02/19 18:57 9040 pH Analytical Method: EPA 9040C pH at 25 Degrees C 6.4 Std. Units 0.10 1 12/08/19 15:53 H3 5220D COD Analytical Method: SM 5220D-2011 Preparation Method: SM 5220D-2011 Chemical Oxygen Demand 29.4 mglL 25.0 1 12/04/19 14:03 12/05/19 08:36 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. Date: 12/18/2019 01:29 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 20 le Analytical www.pacala6s.carn QUALITY CONTROL DATA Project: STORMWATER 11/27/19 Pace Project No.: 9245,9461 QC Batch: 514414 Analysis Method: EPA 1664B QC Balch Method: EPA 1664E Analysis Description: 1664 SGT-HEM, TPH Associated Lab Samples: 92455461001, 92455461002, 92455461003, 92455461004, 92455461005, 92455461005 Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 METHOD BLANKS 2756854 Matrix: Water Associated Lab Samples: 92455461001, 92455461002, 92455461003, 92455461004, 92455461005, 92455461006 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Petroleum Hydrocarbons mg/L ND 5.0 12/12/19 09:43 LABORATORY CONTROL SAMPLE: 2756855 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Petroleum Hydrocarbons mg/L 20 16.0 Sa 64-132 MATRIX SPIKE SAMPLE: 2756856 92455892002 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Total Petroleum Hydrocarhons mg/L ND 20 16.8 78 64-132 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/18/2019 01:29 PM without the written consent of Pace Analytical Services, LLC. Page 10 of 20 (�IaceAnaVical" www.pacelabs.com QUALITY CONTROL DATA Pace Analytical Services, LI-C 2225 Riverside Dr, Asheville, NC 28804 (828)254-7176 Project: STORMWATER 11/27/19 Pace Project No.: 92455461 QC Batch: 512177 Analysis Method: EPA 180.1 Rev 2.0 1993 QC Batch Method: EPA 180.1 Rev 2.0 1993 Analysis Description: 180.1 Turbidity Associated Lab Samples: 92455461001, 92455461002, 92455461003, 92455461004, 92455461005, 92455461006 METHOD BLANK: 2746627 Matrix: Water Associated Lab Samples: 92455461001, 92455461002, 92455461003, 92455461004, 92455461005, 92455461006 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Turbidity NTU ND 1.0 11/27/1915:47 LABORATORY CONTROL SAMPLE: 2746628 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Turbidity NTU in 10.3 103 90-110 SAMPLE DUPLICATE: 2746629 92455461004 Dup Parameter Units Result Result RPD Qualifiers Turbidity NTU 10.4 10.1 3 Results presented on this page are in the units Ihdicated by the "Units" column except where an atternale unit is presented to the right or the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/18/2019 01;29 PM without the written consent of Pace Analytical Services, LLC. Page 11 of 20 (�IaceAnalyticale www.pacallbs.com QUALITY CONTROL DATA Pace Analytical Services, LLC 2.125 Riverside Dr. Asheville, NC 28804 (828)254-7176 Project: STORMWATER 11/27/19 Pace Project No.: 92455461 QC Batch: 512463 Analysis Method: SM 2540D-2011 QC Batch Method: SM 2540D-2011 Analysis Description: 2540D Total Suspended Solids Associated Lab Samples: 92455461001, 924554610 02, 92455461003, 92455461004, 92455461005, 92455461006 METHOD BLANK: 2747899 Matrix: Water Associated Lab Samples: 92455461001, 92455461002, 92455461003, 92455461004, 92455461005, 92455461006 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids rnglL ND 2.5 12/02/19 18:44 LABORATORY CONTROL SAMPLE: 2747900 Spike LCS LGS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Suspended Solids mg1L 250 236 94 90-110 SAMPLE DUPLICATE: 2747901 92455435001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mglL 15.2 9.0 52 D6 SAMPLE DUPLICATE: 2747902 92455461003 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg1L 208 182 13 Results presented on this page are In the unhs Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Data: 12/1812019 01:29 PM without the written consent of Pace Analytical Services, LLC. Page 12 of 20 laceAna,(Xical" www.pacelabs.com QUALITY CONTROL DATA Project: STORMWATER 11127/19 Pace Project No.: 92455461 QC Batch: 513579 Analysis Method: EPA 9040C QC Batch Method: EPA 9040C Analysis Description: 9040 pH Associated Lab Samples: 92455461001, 92455461002, 92455461003, 92455461004, 92455461005, 92455461006 SAMPLE DUPLICATE: 2753164 92454803001 Dup Parameter Units Result Result RPD Qualifiers pH at 25 Degrees C Std. Units 6.8 6.7 1 H3 SAMPLE DUPLICATE: 2753165 92455461003 Dup Parameter Units Result Result RPD qualifiers pH at 25 Degrees C Std. Units 6.9 6.9 0 H3 Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NO 29804 (828)254-7176 Results presented on this page, are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS 'This report shall not he reproduced, except in full, Date: 1211812019 01:29 PM without the written consent of Pace Analyticai Services, LLC. Page 13 of 20 aceAnalytical www.pacelabs.com QUALITY CONTROL DATA Project: STORMWATER 11/27119 Pace Project No.: 92455461 QC Batch: 512446 Analysis Method: SM 5220D-2011 QC Batch Method: SM 5220D-2011 Analysis Description: 5220D COD Associated Lab Samples: 92455461001, 92455461002, 92455461003, 92455461004 Pace Analytical Services, LLC 2225 Riverside ❑r. Asheville, NC 25804 (828)254-717B METHOD BLANK: 2747849 Matrix: Water Associated Lab Samples: 92455481001, 92455461002, 92455461003, 92455461004 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Chemical Oxygen Demand mg/L ND 25.0 12/02/19 22:05 LABORATORY CONTROL SAMPLE: 2747850 Spike LCS LCS e/ Rec Parameter Units Conc. Result % Rec Limits Qualifiers Chemical Oxygen Demand mg1L 750 745 99 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2747851 2747852 MS MSD 92455348004 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Chemical Oxygen Demand mg1L 2870 100 100 3250 3240 379 369 90-110 0 M1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2747853 2747854 MS MSD 92455292002 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RP❑ Qual Chemical Oxygen Demand mg1L 790 100 100 882 885 92 95 90-110 0 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/18/2019 01:29 PM without the written consent of Pace Analytical Services, LLC. Page 14 of 20 aceAnalj&al www.pactiabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28604 (828)254-7176 QUALITY CONTROL DATA Project: STORMWATER 11127/19 Pace Project No.: 92455461 QC Batch: 512813 Analysis Method: SM 5220D-2011 QC Batch Method: SM 5220D-2011 Analysis Description: 5220D COD Associated Lab Samples: 92455461005, 92455461006 METHOD BLANK: 2749258 Associated Lab Samples: 92455461005,92455461006 Parameter Units Chemical Oxygen Demand mg/L LABORATORY CONTROL SAMPLE: 2749259 Parameter Units Chemical Oxygen Demand mg/L Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 25.0 12/05/19 08:31 Spike LCS LCS e/ Rec Cone. Result % Rec Limits Qualifiers 750 744 99 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2749260 2749261 MS MSD 92455404001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc, Conc. Result Result % Rec % Rec Limits RPO Qual Chemical Oxygen Demand mg/L 102 100 100 181 181 79 79 90-110 0 M1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2749262 2749263 MS MSD 92455644001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RP❑ Qual Chemical Oxygen Demand mg/L ND 100 100 116 106 109 100 90-110 8 R1 Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not he reproduced, except in full, Date: 12/18/2019 01:29 PM without the written consent of Pace Analytical Services, LLC. Page 15 of 20 aceAnalytical tvww.FacelaCa.com QUALIFIERS Project: STORMWATER 11/27/19 Pace Project No.: 92455461 DEFINITIONS Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. POL - Practical Quantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate °10 recovery and RPD values. LGS(D) - Laboratory Control Sample (Duplicate) Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NO - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenytamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI -The NELAC Institute. LABORATORIES PAST -A Pace Analytical Services - Asheville PAS}-C Pace Analytical Services - Charlotte ANALYTE QUALIFIERS D6 The precision between the sample and sample duplicate exceeded laboratory control limits. H3 Sample was received or analysis requested beyond the recognized method holding time, M1 Matrix spike recovery exceeded OC limits. Batch accepted based on laboratory control sample (i recovery. Rl RPD value was outside control limits. REPORT OF LABORATORY ANALYSIS This report shall not he reproduced, except in full, Date: 12/1812019 01:29 PM without the written consent of Pace Analytical Services, LLC. Page 16 of 20 aceAnalytica!® www.pacellbs.cam QUALITY CONTROL DATA CROSS REFERENCE TABLE Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 2BB04 {828}254-7176 Project: Pace Project No.: STORMWATER 11/27/19 /32455461 Analytical Lab lD Sample ID QC Batch Method QC Batch Analytical Method Batch 92455461001 OUTFALL #1 EPA 1664B 514414 92455461002 OUTFALL 42 EPA 1664E 514414 92455461003 OUTFALL #3 EPA 1664B 514414 92455461004 OUTFALL #4 EPA 1664B 514414 92455461005 CREEK PRE -MILL EPA 1664B 514414 92455461006 CREEK POST -MILL EPA 1664E 514414 92455461001 OUTFALL #1 EPA 180.1 Rev 2.0 1993 512177 92455461002 OUTFALL #2 EPA 180.1 Rev 2.0 1993 512177 92455461003 OUTFALL #3 EPA 180.1 Rev 2.0 1993 512177 92455461004 OUTFALL #4 FPA 180.1 Rev 2.0 1993 512177 92455461005 CREEK PRE -MILL EPA 180.1 Rev 2.0 1993 512177 92455461006 CREEK POST -MILL EPA 180.1 Rev 2.0 1993 512177 92455461001 OUTFACE #1 SM 254OD-2011 512463 92455461002 OUTFALL #2 SM 254OD-2011 512463 92455461003 OUTFALL #3 SM 254OD-2011 512463 92455461004 OUTFACE #4 SM 254OD-2011 512463 92455461005 CREEK PRE -MILL SM 254OD-2011 512463 92455461006 CREEK POST -MILL SM 2540D-2011 512463 92455461001 OUTFALL 41 EPA 9040C 513579 92455461002 OUTFALL #2 EPA 9040C 513579 92455461003 OUTFALL #3 EPA 9040C 513579 92455461004 OUTFALL #4 EPA 904CC 513579 92455461005 CREEK PRE -MILL EPA 9040C 513579 92455461006 CREEK POST -MILL EPA 9040C 513579 92455461001 OUTFALL 41 SM 5220D-2011 512446 SM 5220D-2011 512470 92455461002 OUTFALL #2 SM 5220D-2011 512446 SM 5220D-2011 512470 92455461003 OUTFALL #3 SM 5220D-2011 512446 SM 5220D-2011 512470 92455461004 OUTFALL #4 SM 5220D-2011 512446 SM 5220D-2011 512470 92455461005 CREEK PRE -MILL SM 5220D-2011 512813 SM 5220D-2011 513022 92455461006 CREEK POST -MILL SM 5220D-2011 512813 SM 5220D-2011 513022 REPORT OF LABORATORY ANALYSIS This report shall not he reproduced, except in full, Date: 12/1812019 01:29 PM without the written consent of Pace Analytical Services, LLC. Page 17 of 20 aceAnalytical Document Name: Sample Condition Upon Recelpt(SCUR) Document Revised: February 7, 2018 Page 1 of 2 Document No.: F-CAR-CS-033-Rev,06 Issuing Authority: Pace Carolinas Quality Office Laboratory receiving samples - Asheville ® Eden[] Greenwood [] Huntersville ❑ Raleigh❑ Mechanicsville[] Client Name: W®# : 92455461 illillillipil ' pp Project h Courier: ❑Fed Ex QU S ❑_,._._ U5P5 Client !j 11 11 I 1 I ❑ Commercial ❑Pace ❑Other: 92455461 Custody Seal Present? ❑Yes E)No Seals Intact? Des EINo p /I �7 l? Date/Initials Person Examining Contents: !t Packing Material: []Bubble Wrap QBubble Bags ❑None ❑ Other Biological Tissue Frozen? Thermometer: (� / ®IRGuntD: --lQ rf' Type otke: ]Wet []Yes ❑No 20N/A ❑Blue []None Cooler Temp ('C): Correction Factor: Add/Subtract ('C) '— LO Cooler Temp (*C). 6, 1 l P Corrected ( ) Temp should be above freezing to VC []Samples out of temp criteria. Samples on ice, cabling process r has begun USDA Regulated Soil (® N/A, water sample) Did sample5 griginate in a quarantine zone within the United States: CA, NY, or 5C (check maps)? Did samples originate from a foreign source (int�nationally, ❑ Yes No inrlu6miz Hawali and Puerto Rico)? FlYes No Comments/Discrepancy: Chain of Custody Present? oYes No ❑N/A 1. Samples Arrived within Hold Time? MYes o N A 2. Short Hold Time Analysis (02 hr.)? ITY.-94�❑N/A 3. Dar I ! f Rush Turn Around Time Requested? ❑Yes WNo ❑N/A 4. Sufficient Volume? MYes EjNo ❑N/A 5. Correct Containers Used? -Pace Containers Used? {�,E{Yes QoYes ❑No No C] N/A []N/A 6. Containers Intact? Yes No ❑N/A 7. Dissolved analysis: Samples Field Filtered? ❑Yes No ®N/A 8. Sample Labels Match COC? Includes Date/Time/ID/Analysis Matrix: (29Yes []No ❑N/A 9. Headspace in VOA Vials (>5-6mm)? ❑Yes Na N A 10. Trip Blank Present? Trip Blank Custody Seals Present? ❑Yes []No ayes N. [9N/A ftl�4/A 11. COMMENTS/SAMPLE DISCREPANCY CLIENT NOTIFICATION/RESOLUTION Person contacted: Project Manager SCURF Review: Project Manager SRF Review: Date/Time: Lot ID of spit containers: Date: Date: Field Data Required? []Yes ❑No Page 18 of 20 Document Name: Document Revised: February 7, 2018 �12ceAnalyfkal' Sample Condition Upon Receipt(SCUR) Pagel of 2 Document No.: Issuing Authority: F-CAR-CS-033-Rev.06 Pace Carolinas Quality Office *Check mark top half of box if pH and/or dechlorination is Project verified and within the acceptance range for preservation samples. Exceptions: VOA, Coliform, TOC, oil and Grease, SRO/8015 (water) DOC, tLHg "Bottom half of box is to list number of bottle W®#:92455461 PM: CD1 Due Dale: 12/13/19 CLIENT: 93-Jackson P E d — a a c a u d E V 0. m S7 Z a u c a u d E M 0. m 'O Z a a c O V J E N a m a u d c N d rl a co V N Y a O vi J 7 0. m N V L z ^ J o ffl 4 m O Z a N ¢ N V CY Q a m v �"� n p Z a a E 7 0. m a 7 d o E 3 ? n c 7 `a � i'S a y c> 2 Q a ri l7 ¢ : a i= c > E J E t7 a N V O ry 2 Q u = l7 a N V S 0 �n z E E a L7 a v U 2 n a N N M t7 a Z V ¢ > E Q Ct uNi rNo Z a Q E t7 > y n 4 0 E C 01 t7 > a a M a > E Gl L7 c a Z 0 o m N ° .S a Q 7 _ Q Y a .. w C 'y l.7 > G " 9 ¢ a N E v, rN-1 ur I Z .,na a d N E o w n 61 V 0 x z u J E o ,800 to z v > ar c ? q`, E Q E 8 a 2 = c g �v = c N 7 z N } d d n ? d E a E 1 fI 'iK j V z I \\NN 3 I \\\N 4 5 6 7 8 9 10 11 12 \\N I pH Adjustment Log for Preserved Samples Sample ID Type of Preservative pH upon receipt Date preservation adjusted Time preservation adjusted Amount of Preservative added lot 0 Note: Whenever there is a discreparcy affecting North Caroiina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification office fi.e. Out of hold, Incorrect preservative, out of temp, incorrect containers. Page 19 of 20 f� PaceAnalytical' CHAIN -OF -CUSTODY I Analytical Request Document The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately. wxw.ysceram.wm m Section A Section B Section C page: of D_ Required Client lnformatiom Requlmd Project lnfdrmabon: Imroice Inform Ilion: C,nmpany: p Report To: !! JJ Attant;on: - �'r",[{c:�� 2067385 lrrrff.u�nl/t �� ITS .�;�. fit ,Sr1G_ Address: J Copy To: Company Name: REGULATORY AGENCY Address' I r NPDES i GROUND WATER r DRINKING WATER UST F RCRA OTHER Email To:. Purchase IC�C.i-SCE C.CKye, .'r�.fl�f Order No.: '-2 �� �5'T PaQuote ce nnlorcnco: Pltdne: J Fax: Project Name:.; J"-t'Ir)LJe4t'�— jj �) 7 ) Pam ect Prot site Location STATE: ReqI Iu ted Duct Dat*!TAT: Project Number: P:Ka ProfJ, N. Requested Analysis Filtered (YIN) Section D Matrix Codes — z Regvlred0w:wormation MATRIX r CODe o COLLECTED Preservatives > rauP¢'sir; CONPOS,TL Iti DrirTking Wafer Ow water wT u ZO Priam Walvr Product P SoiVSolid SL _ m 5-1 LMxAW1 j w Z SAMPLE ID oil °L �' (A-Z.0-91.-) Aires AR Sample IDs MUST BE UNIQUE Tissue TS p O w n- a w z ti m 1= N !t '- , c U �'`�' �1.z y(v z z _ yi Other OT X j W O Q a a LLi d d [/J n C7 0 = ru ts.. m L C N DATE TIME DATE TIME in a = Y z z O Q Pace Project NciJ Lab I.D. 3 fit) 4 ltsr -4: it -q* �t ✓, �.. ft�1l Iis'. ✓ s/ i- I 5 r. reer prz-mr I Ld� �, tl 7 Cf� 157 �" '✓ v ^ Jso r- e 2 c iL t�t.Sf' - I ir%, (.-� i �7:.� � ✓ v :� '� ;��' 7 8 9 10 11 12 A13DMONAL COMMENTS RE.LINQUiSHED BY I AFFILIATION DATE TIME ACCEPTED BY / A/FFFIILIA-1/1 N TIME SAMPLE SAMPLE CONDITIONS rtir 4.i.i sG/rL y��� %/' h?'20 L/� i � r"" '..l- � F` % JDATE r 1 ZW P O O'-5 `� I I SAMPLER NAME AND SIGNATURE ORIGINAL m L o = J/ PRINT Ndme Of SAMPLER: K C.SI) G���._ � n ? } z _ J ATE SE natl D SIGNATURE of SAMPLER: V.t m m— � U E E -rL- Tr (AT.'2: 'tmportani Note: By sirywtp th. torn you are —cep" Porn'. NET 30 day paymcr4lcmn and xyv-mu to late Gwges d 1.5%Per rr N mry iir c mot Paid 'a- A d r.. - F-ALL-4.02orev.07, 15-May-2007 JACKSON PAPER MANUFACTURING R E C F i December 27, 2019E 3 j z�l NCDEQ, Division of Water Resources, Information Processing Unit Attn: Central Files/cl)MR 1�t'`�' `i-tom f lt�; 1 1617 Mail Service Center Raleigh, North Carolina 27699-1617 FZE: Discharge Monitoring Report- December 2019, Tic1• T,,vo Report, Outfall 003 NPI)P's Permit No. NCS000295 .Jackson Paper Manufacturing Company, Dear Division of Water Resources: Please find enclosed Discharge Monitoring Report for Jackson Paper Manufacturing Company NIMES Permit No. NCS000295 for the month of December, 2019. We sampled Outfall 003 and receiving water directly upstream and downstream of' Outfall 003 For all parameters listed in our permit on December 9, 2019. There were no benchmark execedances at Outfall 003. Per our current Tier Two response for Outfall 003, we will continue to conduct monthly monitoring and reporting for all parameters at Outf"111 003. Monthly (analytical and qualitative) monitoring will contirnrc until three consecutive sample results are below the benchmark values. We will also continue to monitor for all parameters in the receiving water directly upstream and downstream of the monitoring point in accordance with the Tier'] wo response. I certify that rased oil information and belief formed from reasonable inquiry, the statements and information in the document are true, accurate, and complete. Please contact Kicsha Bridges at (828)586-5534 Fxt. 226 i f you have any questions or need any additional I lllorlllatlon. S i llev -el m Alec; PCGsid'e It Operations Jackson Paper Manufacturing Company ]?nclosurc: Stormwatcr Discharge Monitoring Report cc: JPMC bile NORTH CAROLINA'S LARGEST RECYCLED PAPER PRODUCER 152 Wisr MAIN S'11,r_F10 PC Box 6070 SY[VA, NC28779 TFL(828) 580-5534 FAX (828)586-6755 Stormwater Discharge Outfall (SDO) Monitoring Report Permit Number NCS000295 Facility Name: Jackson Paper,Manufacturing Company Person Collecting Samples: Kiesha Bridges Certified Laboratory: Pace Analytical Services, LLG Project # 92456505 Samples Collected During Calendar Year: 2019 (This monitoring report shall be received by the Division no later than 30 days from the date the facility receives the sampling results from the laboratory.) County: Jackson Ph ne NO. 828 586-5-34 Ext. 226 (SIG-NA-FURE OF PER4 ITTEE OR DESIGNEE) By this signature. I certify that this report is accurate and complete to the best of my knowledge. Oil and Grease rurbidity TSS pH COD Benchmark 15 5o (6-9) 120 Date Result Benchmark Result No Result Benchmark Result Benchmark Result Benchmark Outfall Exceedance Benchmark Exceedance Exceedance Exceedance Sampled m IL Y/,ti 1Tli m /L Y/N Y/N mg/L YIN 12/9/19 003 ND No 26.7 12.8 No 7.2 No 60.9 No 9:45amarn Creek Pre 1219119 ND N/A 5.5 14.9 N/A 6.3 N/A N D N/A Mill 10:00am Creek Post 12/9/19 ND N/A 7.2 16.5 N/A 6.4 N/A ND N/A Mill 10;1 Oam NO., Not detected at or above adjusted reporting limit. Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? _Yes x No llcasureahle Storm Event? Yes 0.28 Storm Event Characteristics: Date: December 9, 2019 Totalievent precipitation (inches)_ 0:28 Duration of storm event: -3 Hours F cfimaFari vnlnma nf. riicrfiarna camnlorl Time since last rain event: 7 Days Drainage Area 1 11 III IV Area (acres) Area (sO Volume (cf) 1.69 73,616 1,718 5.43 236,531 5,519 20.45 890,802 20,785 1.77 77,101 1,799 /olume,tgal) . 12;849. 41,283 155;475 _ 13,457. Mail Original and one copy to: Division of Water Quality Attn: Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate and omplete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment fo� kr�{ing violations." (Dat D aaeAnalytrcal www,pacolahl.com December 23, 2019 Kiesha Bridges Jackson Paper Mfg. Co. 152 West Main St. Sylva, NC 28779 RE: Project: STORMWATER 1219119 Pace Project No.: 92456505 Pace Analytical Services, LLC 2225 Riverside Dr, Asheville, NC 28864 (B28)254-7176 Dear Kiesha Bridges: Enclosed are the analytical results for sample(s) received by the laboratory on December 09, 2019. The results relate only to the samples included in this report. Results reported herein conform to the most current, applicable TNIINELAC standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. If you have any questions concerning this report, please feel free to contact me. Sincerely, Chris Derouen christopher.derouen@pacelabs.com (828)254-7176 Project Manager Enclosures cc: Keisha Bridges, Jackson Paper Mfg. Co. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical services, LLC. Page 1 of 16 (�IacieAnalytical" www.pacetabsnm Project: STORMWATER 1219119 Pace Project No.: 92456505 Pace Analytical Services, LLC 2225 Riverside dr. Asheville, NC 28804 (828)254-7178 Pace Analytical Services Charlotte 9800 Kincey Ave. Ste 100, Nuntersville, NC 28078 LouisianaINELAP Certification # LA170028 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 Pace Analytical Services Asheville 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87648 Massachusetts Certification #: M-NC030 North Carolina Drinking Water Certification #: 37712 CERTIFICATIONS South Carolina Certification #: 99006001 FloridalNELAP Certification #: E87627 Kentucky UST Certification #: 84 VirginiaA/ELAP Certification #: 460221 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 VirginiaNELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall net he reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 16 aceAnalylyical. www.pacelibs.com �91\T177I=V-.1\rl Will It:9+11111111LIll I Pace Analytical Services, LLC 2225 Riverside Dr, Asheville, NC 28804 (828)254-7176 Project: Pace Project No.: STORMWATER 12/9/19 92456505 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92456505001 OUTFALL #3 EPA 1664B HH 1 PASI-C EPA 180.1 Rev 2.0 1993 SMK 1 PASI-A SM 254OD-2011 CJL 1 PASI-A EPA 9040C ECH 1 PASI-A SM 5220D-2011 JP1 1 PASI-A 92456505002 CREEK PREMILL EPA 1664B HH 1 PASI-C EPA 180A Rev 2.0 1993 SMK 1 PASI-A SM 254OD-2011 CJL 1 PASI-A EPA 9040C ECH 1 PASI-A SM 52200-2011 JP1 1 PASI-A 92456505003 CREEK POSTMILL EPA 1664B HH 1 PASI-C EPA 180.1 Rev 2.0 1993 SMK 1 PASI-A SM 2540D-2011 CJL 1 PASI-A EPA 9040C ECH 1 PASI-A SM 5220D-2011 JP1 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 16 (�IaceAnalytical* www.pacelmbs.com ANALYTICAL RESULTS Pace Analytical Services, LLC 2225 Riverside Dr, Asheville, NC 28804 (828 )254-7176 Project: STORMWATER 1219119 Pace Project No.: 92456505 Sample: OUTFALL #3 Lab ID: 92456505001 Collected: 12/09/19 09:45 Received: 12/09/19 12:30 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No, Qual 1664 SGT-HEM, TPH Analytical Method: EPA 1664E Total Petroleum Hydrocarbons ND mg1L 4.8 1 12/20119 09:14 180.1 Turbidity Analytical Method: EPA 180.1 Rev 2.0 1993 Turbidity 26.7 NTU 1.0 1 12/10/1916:31 2540D Total Suspended Solids Analytical Method: SM 2540D-2011 Total Suspended Solids 12.8 mg[L 6.2 1 12/12/19 12:58 9040 pH Analytical Method: EPA 9040C pH at 25 Degrees C 7.2 Std. Units 0,10 1 12/22/19 16:11 H3 52200 COD Analytical Method: SM 5220D-2011 Preparation Method: SM 5220D-2011 Chemical Oxygen Demand 60.9 mg/L 25.0 1 12/16/19 23:16 12/18/19 02:45 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12123/2019 12:46 PM without the written consent of Pace Analytical Services, LLC, Page 4 of 16 laceAnapical' arww.pacdabssom ANALYTICAL RESULTS Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Project: STORMWATER 1219119 Pace Project No.: 92456505 Sample: CREEK PREMILL Lab ID: 92456505002 Collected: 12/09/19 10:00 Received: 12/09/19 12:30 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 1664 SGT-HEM, TPH Analytical Method: EPA 1664E Total Petroleum Hydrocarbons ND mg/L 4.8 1 12/20/19 09:14 180.1 Turbidity Analytical Method: EPA 180.1 Rev 2.0 1993 Turbidity 5.5 NTU 1.0 1 12/1011916:31 2540D Total Suspended Solids Analytical Method: SM 2540D-2011 Total Suspended Solids 14.9 mg1L 3.3 1 12/12119 12:58 9040 pH Analytical Method: EPA9040C pH at 25 Degrees C 6.3 Std. Units 0.10 1 12/22119 16:17 H3 5220D COD Analytical Method: SM 5220D-2011 Preparation Method: SM 5220D-2011 Chemical Oxygen Demand ND rng/L 25.0 1 12/16/19 23:16 12/18/19 02:45 REPORT OF LABORATORY ANALYSIS This report shall not he reproduced, except in full, Dale: 12/23/2019 12:46 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 16 ac,Mnalytical. www.pacelabs.com ANALYTICAL RESULTS Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Project: STORMWATER 1219119 Pace Project No,: 92456505 Sample: CREEK POSTMILL Lab ID: 92456505003 Collected: 12/09/19 10:10 Received: 12/09/19 12:30 Matrix: Water Parameters Results Units Report Limit DE Prepared Analyzed CAS No. Qual 1664 SGT-HEM, TPH Analytical Method: EPA 1664B Total Petroleum Hydrocarbons ND mg/L 4.8 1 12/20/19 09:14 180.1 Turbidity Analytical Method: EPA 180.1 Rev 2.0 1993 Turbidity 7.2 NTU 1.0 1 12/10/1916:31 2540D Total Suspended Solids Analytical Method: SM 25400-2011 Total Suspended Solids 16.5 mg1L 3.3 1 12/12/19 12:59 9040 pH Analytical Method: EPA 9040C pH at 25 Degrees C 6.4 Std, Units 0.10 1 12/22/19 16:23 H3 5220D COD Analytical Method: SM 5220D-2011 Preparation Method: SM 5220D-2011 Chemical Oxygen Demand ND mg/L 25.0 1 12/16/19 23:16 12/18/19 02:47 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/23/20113 12:46 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 16 laneAnalytical" www.pacelahs.com QUALITY CONTROL DATA Project: STORMWATER 12/9119 Pace Project No.: 92456505 Pace Analytical Services, LLC 2225 Riverside Dr, Asheville, NC 2BB04 (828)254-7176 QC Batch: 515960 Analysis Method: EPA 1664B QC Batch Method: EPA 1664E Analysis Description: 1564 SGT-HEM, TPH Associated Lab Samples: 92456505001, 92456505002, 92456505003 METHOD BLANK: 2764713 Matrix: Water Associated Lab Samples: 92456505001, 92456505002, 92456505003 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Petroleum Hydrocarbons mg/L ND 5.0 12/20/19 07:37 LABORATORY CONTROL SAMPLE: 2764714 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Petroleum Hydrocarbons mg1L 19.2 18.3 95 64-132 MATRIX SPIKE SAMPLE: 2764715 92457428001 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Total Petroleum Hydrocarbons mg/L ND 19.2 7.8 34 64-132 Results presented an this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right at the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/23/2019 12:46 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 16 leAnalyfical wwtw.paetlabt.etmt QUALITY CONTROL DATA Project: STORMWATER 1219/19 Pace Project No.: 92456505 QC Batch: 513876 Analysis Method: EPA 180.1 Rev 2.0 1993 QC Batch Method: EPA 180.1 Rev 2.0 1993 Analysis Description: 180.1 Turbidity Associated Lab Samples: 924565C5001, 92456505002, 92456505003 METHOD BLANK: 2754441 Matrix: Water Associated Lab Samples: 92456505001, 92456505002, 92456505003 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Turbidity NTU ND 1.0 12110/1916:31 LABORATORY CONTROL SAMPLE: 2754442 Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, 128804 (828)254-7176 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Turbidity NTU 10 9.8 98 90-110 SAMPLE DUPLICATE: 2754443 92456518001 Dup Parameter Units Result Result RPD Qualifiers Turbidity NTU 30.0 29.4 2 Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/23/2019 12:46 PM without the written consent of face Analytical Services, LLC. Page 8 of 16 laceAnalytical"' www.pactdahs.com QUALITY CONTROL DATA Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Project: STORMWATER 12/9119 Pare Project No.: 92456505 QC Batch: 514472 Analysis Method: SM 254OD-2011 QC Batch Method: SM 2540D-2011 Analysis Description: 2540D Total Suspended Solids Associated Lab Samples: 92456505001, 92456505002, 92456505003 METHOD BLANK: 2757442 Matrix: Water Associated Lab Samples: 92456505001, 92456505002, 92456505003 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids n1g1L ND 2.5 12/12/19 12:55 LABORATORY CONTROL SAMPLE: 2757443 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Suspended Solids mg/L 250 252 101 90-110 SAMPLE DUPLICATE: 2757444 92456864001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 210 218 4 SAMPLE DUPLICATE: 2757445 92456572001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 1740 1780 2 Results presented an this page are in the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 1212312019 12:46 PM without the Written consent of Pace Analytical Services, LLC. Page 9 of 16 (�IacieAnalyfical* www.pacela4stern QUALITY CONTROL DATA Project: STORMWATER 1219119 Pace Project No.: 92456505 QC Batch: 516217 Analysis Method: EPA 9040C QC Batch Method: EPA 9040C Analysis Description: 9040 pH Associated Lab Samples: 92456505001, 92456505002, 92456505003 SAMPLE DUPLICATE: 2765961 92456487001 Dup Parameter Units Result Result RPD Qualifiers pH at 25 Degrees C Std. Units 7.2 7.1 1 H3 SAMPLE DUPLICATE: 2765962 92456515001 Dup Parameter Units Result Result RPD Qualifiers pH at 25 Degrees C Std. Units 6.1 5.8 5 D6,1-13 Pace Analytical Services, LLC 2225 Riverside Dr, Asheville, NC 28804 (828)254-7176 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit Is presented to the right at the result. REPORT OF LABORATORY ANALYSIS This report shalE not be reproduced, except in full, Date: 12/2312019 12:46 PM without the written consent of Pace Analytical Services, LLC. Page 10 of 16 laceAnaii` www.pacelali3x0 n QUALITY CONTROL DATA Project: STORMWATER 1219119 Pace Project No.: 92456505 OC Batch: 515145 Analysis Method: SM 5220D-2011 QC Batch Method: SM 5220D-2011 Analysis Description: 5220D COD Associated Lab Samples: 92456505001, 92456505002, 92456505003 METHOD BLANK: 2760688 Matrix: Water Associated Lab Samples: 92456505001, 92456505002, 92456505003 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Chemical Oxygen Demand mg/L NO 25.0 12/18119 02:43 Pace Analytical Services, LLC 2225 [Riverside Dr. Asheville, NC 28804 (828)254-7176 LABORATORY CONTROL SAMPLE: 2760689 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Chemical Oxygen Demand mglL 750 753 100 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2760700 2760701 MS MSD 92456505002 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Chemical Oxygen Demand mg1L NO 100 100 109 107 106 103 90-110 2 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2760702 2760703 MS MSD 92456505003 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Chemical Oxygen Demand mg/L ND 100 100 111 111 108 106 90-110 0 Results presented an this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right at the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/2312019 12:46 PM without the written ccrosent of Pace Ana iytical Services, LLC. Page 11 of 16 aceAnalj&al www.pacilabs.com QUALIFIERS Project: STORMWATER 1219119 Pace Project No.: 92456505 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit, TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL- Adjusted Method Detection Limit. Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NO 28804 (828)254-7176 PQL - Practical Quantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Diphonylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each enalyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis ofAcrolein and Acrylonitrile by EPA Method 8260. N-Nilrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI -The NELAC Institute. LABORATORIES PASI-A Pace Analytical Services - Asheville PASI-C Pace Analytical Services - Charlotte ANALYTE QUALIFIERS D6 The precision between the sample and sample duplicate exceeded laboratory control limits. H3 Sample was received or analysis requested beyond the recognized method holding time. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/23/2019 12:46 PM without the written consent of Pace Analytical Services, LLC. Page 12 of 16 aceAnalytical www.pacetabs.cam QUALITY CONTROL DATA CROSS REFERENCE TABLE Pace Analytical Services, LLC 2225 Riverside Dr, Asheville, INC 28804 (828)254-7176 Project: Pace Project No.: STORMWATER 1219119 92456505 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92456505001 OUTFALL #3 EPA 1664B 515960 92456505002 CREEK PREMILL EPA1664B 515960 92456505003 CREEK POSTMILL EPA 1664E 515960 92456505001 OUTFALL #3 EPA 180.1 Rev 2.0 1993 513876 92456505002 CREEK PREMILL EPA 180.1 Rev 2.0 1993 513876 92456505003 CREEK POSTMILL EPA 180.1 Rev 2.0 1993 513876 92456505001 OUTFALL #3 SM 254OD-2011 514472 92456505002 CREEK PREMILL SM 254OD-2011 514472 92456505003 CREEK POSTMILL SM 254OD-2011 514472 92456505001 OUTFALL #3 EPA 9040C 516217 92456505002 CREEK PREMILL EPA 9040C 516217 92456505003 CREEK POSTMILL EPA9040C 516217 92456505001 OUTFALL #3 SM 5220D-2011 515145 SM 5220D-2011 515394 92456505002 CREEK PREMILL SM 5220D-2011 515145 SM 5220D-2011 515394 92456505003 CREEK POSTMILL SM 5220D-2011 515145 SM 5220D-2011 515394 Date: 12/23/2019 12:46 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLG. Page 13 of 16 Document Name: Document Revised: February 7, 2018 F CeAnalytical Sample Condition Upon Recelpt(SCUR) Page 1 of 2 Document No.: Issuing Authority: F-CAR-CS-033-Rev.06 Pace Carolinas quality Office Laboratory receiving sa ples: Asheville Eden❑ Greenwood ❑ HuntersviIIe ❑ Raleigh❑ Mechanicsville[] Client Name: Project # 1ro 7T .i Wad (�24565®5 Courier: ❑Fed Ex []UPS ❑USPS ❑ Commercial ❑Pace ❑Other: 92456505 Custody Seal Present? ❑Yes Alt-4'- Seals Intact? ❑Yes ,,Deo Date/Initials Person ExaminingCantents:f✓J�"—Y Packing Material: ❑Bubble Wrap Bubble Bags []None ❑ Other Biological Tissue Fr n? Thermometer; ❑Yes [:]No /A ,BTR Gun ID: j / Type of Ice: �t ❑Blue ❑None Cooler Temp ('C): �j Correction Factor; Add/Subtract ('C) 0 " ' Temp should be above freezing to 6'C Cooler Temp Corrected ('C): (]Samples out of temp criteria. Samples on ice, cooling process hashegun USDA Regulated Soil NIA, water sample) Did samples originate in a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source (internationally, ❑Yes MNo includlrz Hawaii and Puerto Rico)? MYes ❑No Comments/Discrepancy: Chain of Custody Present? Yes ❑No Q N/A 1. Samples Arrived within Hold Time? Yes ❑No NIA 2. Short Hold Time Analysis (<72 hr.)? qafes No N/A 3. Rush Turn Around Time Requested? ❑Yes o N/A 4. Sufficient Volume? Elfes ❑No Q N/A 5. Correct Containers Used? -Pace Containers Used? 'j,�es fyYes []No ❑No [:]NIA N/A 6. Containers intact? E3<s ❑No ❑N//�A 7. Dissolved analysis; Samples Field Filtered? ❑Yes ONO, 'BN/A 8. Sample Labels Match COC? -Includes Date/Time/ID/Analysis Matrix; 71'E� Q6 ❑N/A r 9. } 7uri) C� j Mgr r f:f �� pn C6( l�r� Headspace in VOA Vials (>5-6mm)? ❑Yes No ,❑Il/'A 10. Trip Blank Present? Trip Blank Custody Seals Present? Oyes ❑Ym o []NO ❑N/A ---51�,A 11, COMMENTS/SAMPLE DISCREPANCY Field Data Required? ❑Yes ❑No Lot ID of split containers: CLIENT NOTIFICATION/RESOLUTION Person contacted: Project Manager SCURF Review: Project Manager SRF Review: Date/Time: Date: Date: Page 14 of 16 ` Document Name: Document Revised: February7, 2018 CeAnalytical' Sam le Condition Upon Receipt(SCUR) Page 1 of 2 Document No.: Issuing Authority. g Y: ' r F•CAR•CS-033•Rev.06 Pace Carolinas Quality Office *Check mark top half of box if pH and/or dechlorination is verified and within the acceptance range for preservation samples. Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/8015 (v,aterl DOC, LLHg **Bottom half of box is to list number of bottle Project Wo# : 9Z4565o5 PM: CD1 Due Date: 12/23/19 CLIENT: 93-Jackson P 2 z 77 n W J L h C C C > > > U u V a a a E E E a E ,f a a m m m Q z Z 0! a m a 0. m u N V v 4 N U m E J a m N y rs Q z V u Nttf z M m O m Z m ¢ z V _ m E H N v m rN+.> A n P ro E � c! a m y 1tl (i t7 « p _ LL ID 4 i! rn�! N ; 4 y p A u ri T .� 4 z fl j N E E N 3 m 4 a Q a "m .-I .+ d ri 0 n G E E N N v! m Q z z fl E o a Q a' m R z r V Q Q v x c+ V m N Q -+ E Q r- ti 7 Z C < 1 aV f 7 n 7 2 v a r < o V d to�yy 6 x f�.l o w `u m 4 7 4 a Y M y C7 Z Z a QI m E 11 N & Z 2x a E C N N - h O Z V E 0 ran m @ c 7 E E o Q o n c , o > z. •n ? I O 6 a m G 1 2 3 EL A 5 LL N\\F7 8 N\N- 10 \N\� N\ J12 pH Adjustment Log for Preserved Samples Sample to Type of Preservative pH upon recelpt Date preservation adjusted Tlme preservation adivited Amount of Preservative added Lot # —Icnever there is a discrepancy ntiecting North Carolina compliance samples, a copy of this form rrihbe sent to the North Carolina DEHNR Certification Office (i.e. Out of hold, incorrect preservative, out of temp, Incorrect containers. Page 15 of 16 2neAnalj6cal' r...0a" tq.cem CHAIN -OF -CUSTODY / Analytical Request Document The Chalnof-Custody is a LEGAL DOCUMENT. AR relevant fields must be completed accurately. Section A Section B Section C Page: of Required Client Information: Requlmd Project Inf`orrnation: Invoice Information: Report To Attention: 2193140 SO r ( .� i ddress, 5 • �. Copy To: Company Namc: REGULATORY AGENCY Address. r NPOES r— GROUND WATER F DRINKING WATER � UST j RCRq r OTHER E o: Purchase ksa<, I rt m cc rr Order No.: j S 7 PawU-tn Rcicr : �y PM:o�. Site Location Roqu d Due ITT: Project Number: Pace prefxe if:STATE. Requested Analysis Filtered (YIN) Section D Matrix Codes ~ z Requlratl[tirms kliarrrsilion MATRIX 7 CODE c COLLECTED Preservatives >18 Drinking Water DW = au z 2 Water WT WW tj C31TE 1 �oWalef Prodc _ m START EN=RR�e z ilrsoka SL Oil s p� } O SAMPLE ID W m m Wlpe WP {A-Z. 0.91 ) Air AR to p 2 a Z b v F c o Sample Os MUST BE UNICIUE Tissue TS O a w m m _ other OT U X W F J Z OU y O c a. o a tL O z0 to kv 10 O w 121 '= DATE nMe DATE TIME H i z = z z O J t Pace Project No./ Lap I.D. 2 j I� rf ) fti.tk -2-,✓ •�QCf a s s T a 9 10 i1 12 ADDITIONAL COMMENTS RELINQUISHED BY 1 AFFILIATION DATE TIME ACCEPTED BY 1 AFFiL1AT1ON DATE TIME SAMPLE CON13MONS /2- 30 d Mn.tiJ j614cP� U- , 2- 3 � 1 -P-A 17cl y SAMPLER NAME AND SIGNATURE `o ORIGINAL N PRINT Name of SAMPLER: c _ a 2 a o U z e z DATE Si 0 SIGNATURE of SAMPLER: ' ? ! E C u 0 q y E .-. in (MM1DDgrYY)'. •knponael Nola: By skj-9 this lorry you .r a septng Pace's NET 30 ary poyn rm tenor and aryc V M tale rhxges of 1-5% per —nutfG any — mr (.-fit .0— 36 drys_ F-ALL•0-020rev.07. 15-May-2007