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HomeMy WebLinkAboutNCS000295_MONITORING INFO_201911014v 0 STORMWATER DIVISION CODING SHEET NCS PERMITS PERMIT NO. /� J L S � L-) DOC TYPE ❑FINAL PERMIT [�( MONITORING REPORTS ❑ APPLICATION ❑ COMPLIANCE ❑ OTHER DOC ;)o I GI I I DATE ❑ YYYYMMDD JACKSON PAPER MANUFACTURING October 30, 2019 NCDEQ, Division of` Water RCSOLII-Ces, Infonnation Processing Unit Attu: Central files/e[)MIZ 1617 Mail Service Center Raleigh, North Carolina 27699-1617 RE-: Discharge Monitoring Report- October 2019 Monthly TiRELFEIt1 ED11 003 NI'DES Permit No. NCS000295 NIP 0 1 2019 Jackson Paper Manufacturing Company Dcar Division of Water lZesources: CENTRAL FFLE5 DWR SECTION Please find enclosed Discharge Monitoring Report for Jackson Paper Mamlfactul•ing Conlpally NPDE-S Permit No. NCS000295 for the month of October, 2019. We sampled OLItfill 1 003 and the receiving water directly upstream and downstream Of OL)tfal1 003 for all parameters listed 1n our permit on October16. 2019. Thcre were no benchmark excecdanccs at Outfall 003. Per our current "bier "hero response for Outfall 003, we will continue to conduct nlontIlly 111011itoritlg and reporting for all parameters at Outfall 003. Monthly (analytical and qualitative) monitoring Wili C011611LIC wltil three consecutive sample results are below the benchmark values. We will also C011611LIC to ]monitor for all parameters ill the receiving Water dit-Cfitly Upstl—Will and downstream off the monitoring point in accordance with the "I'ict- Two response. I certify that based on information and belief forlled from reasonable inquiry, the statements and information in the document arc true, accurate, and complete. ]'lease contact Kiesha Bridges at (828)586-5534 Ext additional in ormatlon. Sin � � •cly�_ v Carr yndtl11 Vice President Operations Jackson Paper Manufacturing Coinpany Enclosure: Stormwatcr Discharge Monitoring Rcpert CC: j?"4C HIC 226 if you have any questions or need any NORTH CAROLINA'S LARGEST RECYCLED PAPER PROOUC(:R 152 WFSF MAIN STRIETO PO Box 6670 Svl.vA. INIC 28779 TEL (828) 586-5534 FAX (828) 586-6755 Stormwater Discharge Outfall (SDO) Monitoring Report Permit Dumber NCS000295 Facilitp Name: Jackson Paper Manufacturing _Companv Person Collecting Samples: Kiesha Bridges Certified Laboratory: Pace Analvtical Services. LLC Project # 92449812 Samples Collected During Calendar Year: 2019 (This monitoring report shall be received by the Division no later than 30 days from the date the facility receives the sampling results from the laboratory.) Countv: Jackson Phony NO. 828 5 6-5534 xt. 226 4 NATURE OF PER, TTEE OR DESIGNEE) By this signature. I certify that this report is accurate and complete to the best of my knowledge. Oil and Crease furhidity 'l'SS pH COD Benchmark Is 50 (6-9) 120 Benchmark Benchmark Benchmark Benchmark Date Result Result \/A Result Result Result Outfall Exceedance Exceedance Exceedance Exceedance Sampled m /l. (YIN) U mg/L 1'/N YIN mg/L YIN 10/16/2019 003 N1D No 33.2 12.8 No 7.8 No ND No 8:45am Creek Pre 10/16/19 N,D 7.3 10.0 6.0 ND Mill 9:00am Creek Post 10/16/19 ND 8.4 9.8 6.8 ND Mill 9:10am ND: Not detected at or above adjusted reporting limit. Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? _Yes x No Nleasureable Storm Event? Yes 0.06 Storm Event Characteristics: Date: October 16, 2019 Totahevenhprecipitation (inches): Duration of storm event: 1 -1.5 hrs "Time since last rain event: -60 hrs Drainage Area 1 II HI IV Area {acres) Area (sf) Volume (cf) 1.69 73,616 368 5.43 236,531 1,183 20.45 890,802 4,454 1.77 77,101 386 Jolume (gal) _ 2,753 . 8;846 33,316 2,884. Mail Original and one copy to: Division of Water Quality Attn: Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment fqr )Mgrring violations." lo4 3(j ( `)L (Signature of Per r ittee) (Dat- (�5a'neAnalytical* www,peceiabs=m October 30, 2019 Kiesha Bridges Jackson Paper Mfg. Co. 152 West Main St. Sylva, NC 28779 RE: Project: STORMWATER OCTOBER 2019 Pace Project No.: 92449812 Dear Kiesha Bridges: Pace Analytical Services, LLC 2226 Riverside Dr. Ashevliie, NC 28804 (828}254-7176 Enclosed are the analytical results for sample(s) received by the laboratory on October 16, 2019. The results relate only to the samples included in this report. Results reported herein conform to the most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. If you have any questions concerning this report, please feel free to contact me. Sincerely, Chris Derouen Christopher.derouen@pacelabs.com (828)254-7176 Project Manager Enclosures cc: Keisha Bridges, Jackson Paper Mfg. Co. pc �0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 17 (�IaneAnalytical* wNw.pac84ftcam MA '"A I IaDUN H•�-1 Project: STORMWATER OCTOBER 2019 Pace Project No.: 92449812 Pace Analytical Services, LLC 2225 Riverside ❑r. Asheville, NC 28804 (828)254-71 M Charlotte Certification IDs 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 South Carolina Certification #: 99006001 Loulsfana/NELAP Certification # LA170028 FioridalNELAP Certification #: E87627 North Carolina Drinking Water Certification #: 377C6 Kentucky UST Certification M 84 North Carolina Field Services Certification #: 5342 VirginiaNELAP Certification #: 460221 North Carolina Wastewater Certification #: 12 Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87648 Massachusetts Certification #: M-NCO30 North Carolina Drinking Water Certification #: 37712 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 VirginiaNELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not he reproduced, except in full, without the written consent of Pace Analytical Services, LLC, Page 2 of 17 (�1aceAnalytical* *"..pacelabscom M-151»*L►-A AL�40:11] 11 Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Project: Pace Project No.: STORMWATER OCTOBER 2019 92449812 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92449812001 OUTFALL#3 EPA1664B HH 1 PASI-C EPA 180.1 Rev 2.0 1993 SMK 1 PASI-A SM 2540D-2011 MJP 1 PASI-A EPA 9040C ECH 1 PASI-A SM 5220D-2011 GC 1 PASI-A 92449812002 CREEK PRE MILL EPA 1664E HH 1 PASI-C EPA 180.1 Rev 2.0 1993 SMK 1 PASI-A SM 254OD-2011 MJP 1 PASI-A EPA 9040C ECH 1 PASI-A SM 5220D-2011 GC 1 PASI-A 92449812003 CREEK POST MILL EPA 1664B HH 1 PASI-C EPA 180.1 Rev 2.0 1993 SMK 1 PASI-A SM 2540D-2011 MJP 1 PASI-A EPA 9040C ECH 1 PASI-A SM 522OD-2011 GC 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not he reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 17 aceAnalj4ical o www.pwdds.com ANALYTICAL RESULTS Pace Analytical Services, LLC 2225 Riverside Dr, Asheville, NC 28804 (828)254-7176 Project: STORMWATER OCTOBER 2019 Pace Project No.: 92449812 Sample: OUTFALL #3 Lab ID: 92449812001 Collected: 10/16/10 08:45 Received: 10/16/19 11:35 Matrix: Water Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual 1664 SGT-HEM, TPH Analytical Method: EPA 1664B Total Petroleum Hydrocarbons NO mglL 5.0 1 10/29/19 16:44 180.1 Turbidity Analytical Method: EPA 180A Rev 2.0 1993 Turbidity 33.2 NTU 1.0 1 10/1611915:21 2540D Total Suspended Solids Analytical Method: SM 254OD-2011 Total Suspended Solids 12.8 mglL 2.5 1 10/19/19 09:47 9040 pH Analytical Method: EPA 9040C pH at 25 Degrees C 7.8 Std, Units 0.10 1 1 n/28119 15:33 H3 5220D COD Analytical Method; SM 5220D-2011 Preparation Method: SM 5220D-2011 Chemical Oxygen Demand ND mglL 25.0 1 10123M9 16:22 10/23/1920:34 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Dale: 10/30/2019 08:50 AM without the written consent of Pace Analytical Services, LLC. Page 4 of 17 ,�IaaeAnalyticalo WWW-Pft)W4b&0Wn ANALYTICAL RESULTS Pace Analytical Services, LLC 2225 Riverside or. Asheville, NC 26804 (828)254-7176 Project: STORMWATER OCTOBER 2019 Pace Project No.: 92449812 Sample: CREEK PRE MILL Lab ID: 92449812002 Collected: 10/16/19 09:00 Received: 10/16/19 11:35 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Oual 1664 SGT-HEM, TPH Analytical Method: EPA 1664B Total Petroleum Hydrocarbons ND mg1L 5.0 1 10/29/19 16:44 180.1 Turbidity Analytical Method: EPA 180.1 Rev 2.0 1993 Turbidity 7.3 NTU 1.0 1 10116/1915:21 2540D Total Suspended Solids Analytical Method: SM 254OD-2011 Total Suspended Solids 10.0 mg/L 2.5 1 10/19119 09:47 9040 pH Analytical Method: EPA 9040C pH at 25 Degrees C 6.0 Std. Units 0.10 1 10/28/19 15:50 H3 5220D COD Analytical Method: SM 5220D-2011 Preparation Method: SM 5220D-2011 Chemical Oxygen Demand ND mglL 25.0 1 10123/19 16:22 10/23/19 20:34 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10130/2019 08:50 AM without the written consent of Pace Anaiyticai Services, LLC. Page 5 of 17 (�IacleAnalyfical" mnvpacalab&c= ANALYTICAL RESULTS Pace Analytical Services, LLC 2225 Riverside ❑r. Asheville, NC 28804 (828)254-7176 Project: STORMWATER OCTOBER 2019 Pace Project No.: 92449812 Sample: CREEK POST MILL Lab ID: 92449812003 Collected: 10116/19 09:10 Received: 10116/19 11:35 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 1664 SGT-HEM, TPH Analytical Method: EPA 1664B Total Petroleum Hydrocarbons ND mg1L 5.0 1 10/29/19 16:45 180.1 Turbidity Analytical Method: EPA 180.1 Rev 2.0 1993 Turbidity 8.4 NTU 1.0 1 10/16/1915:22 2540D Total Suspended Solids Analytical Method: SM 2540D-2011 Total Suspended Solids 9.8 mg/L 2,5 1 10/19/10 09:47 9040 pH Analytical Method: EPA 9040C pH at 25 Degrees C 6.8 Std. Units 0.10 1 1012C119 16:25 H3 5220D COD Analytical Method: SM 5220D-2011 Preparation Method: SM 5220D-2011 Chemical Oxygen Demand ND mg1L 25.0 1 10/23/19 16:22 10/23/19 20:34 REPORT OF LABORATORY ANALYSIS T his report shall not be reproduced, except in full, Date: 10/30/2019 08:50 AM without the written consent of Pace Analytical Services, LLC. Page 6 of 17 aceAnalXical. wwwpacatO&oom QUALITY CONTROL DATA Project: STOfRMWATER OCTOBER 2019 Pace Project No.: 92449812 QC Batch: 506483 Analysis Method: EPA 1664E QC Batch Method: EPA 16648 Analysis Description: 1664 SGT-HEM, TPH Associated Lab Samples: 92449812001, 92449812002, 92449812003 Pace Analytical Services, LLC 2225 Riverside Or, Asheville, NC 28804 (828)254-7176 METHOD BLANK: 2719999 Matrix: Water Associated Lab Samples: 92449812001, 92449812002, 92449812003 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Petroleurn Hydrocarbons mg1L ND 5.0 10/29/19 16:44 LABORATORY CONTROL SAMPLE: 2720000 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Petroleum Hydrocarbons mglL 20 18.5 92 64-132 MATRIX SPIKE SAMPLE: 2720001 92449890001 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Total Petroleum Hydrocarbons mg1L ND 20 15.6 70 64-132 Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/3012019 08:50 AM without the written consent of Pace Analytical Services, LLC. Page 7 of 17 aceAnalytical wwlvpacWlab&c= QUALITY CONTROL DATA Project: STORMWATER OCTOBER 2019 Pace Project No.: 92449812 QC Batch: 503960 Analysis Method: EPA 180.1 Rev 2.0 1993 QC Balch Method: EPA 180.1 Rev 2.0 1993 Analysis Description: 180.1 Turbidity Associated Lab Samples: 92449812001, 92449812002, 92449812003 METHOD BLANK: 2708365 Matrix: Water Associated Lab Samples: 92449812001, 92449812002, 92449812003 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Turbidity NTU ND 1.0 10116I1915:20 Pace Analytical Services, LLC 2.225 Riverside Dr. Asheville, NC 28804 (828)254-7176 LABORATORY CONTROL SAMPLE: 2708366 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Turbidity NTU 10 10.5 105 90-110 SAMPLE DUPLICATE: 270B367 92449812001 Dup Parameter Units Result Result RPD Qualifiers Turbidity NTU 33.2 32.9 1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/30/2019 08:50 AM without the written consent of Pace Analytical Services, LLC. Page 8 of 17 (��7aceAnalyficale w mpacefabscorrt QUALITY CONTROL DATA Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Project: STORMWATER OCTOBER 2019 Pace Project No.: 92449812 QC Batch: 504599 Analysis Method: SM 2540D-2011 QC Batch Method: SM 254OD-2011 Analysis Description: 2540D Total Suspended Solids Associated Lab Samples: 92449812001, 92449812CO2, 92449812003 METHOD BLANK: 2711845 Matrix: Water Associated Lab Samples: 92449812001, 92449812002, 92449812003 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids ri ND 2.5 10/19/19 09:47 LABORATORY CONTROL SAMPLE: 2711846 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Suspended Solids mglL 250 250 100 90-110 SAMPLE DUPLICATE: 2711871 92450206001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 282 244 14 D6 SAMPLE DUPLICATE: 2711872 92449869002 Di Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 161 164 2 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not he reproduced, except in full, Date: 10/30/2019 08:50 AM without the written consent of Pace Analytical Services, L-C. Page 9 of 17 aceAPalyfrcal. wwwpacdabs.cam QUALITY CONTROL DATA Project: STORMWATER OCTOBER 2019 Pace Project No.: 92449812 QC Batch: 504653 Analysis Method: EPA 9040C QC Batch Method: EPA 9040C Analysis Description: 9040 pH Associated Lab Samples: 92449812003 SAMPLE DUPLICATE: 2711979 92450171003 Dup Parameter Units Result Result RPD Qualifiers pH at 25 Degrees C Std. Units 6.9 6.5 7 D6,H3 SAMPLE DUPLICATE: 2711980 Parameter Units pH at 25 Degrees C Std. Units 92449833003 Dup Result Result RPD Qualifiers 5.5 5.6 3 DB,H3 Pace Analytical Services, LLC 2225 Riverside Dr. Asheviiie, NC 28B04 (828)254-7176 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the resutt. REPORT OF LABORATORY ANALYSIS Tlifs report shall not be reproduced, except in hull, Date: 10/30/2019 08:50 AM without the written consent of Pace Analytical Services, LLC. Page 10 of 17 (�Iace*ialytical" wwwpaWab&oarn QUALITY CONTROL DATA Project: STORMWATER OCTOBER 2019 Pace Project No.: 92449812 QC Batch: 506001 Analysis Method: EPA 9040C QC Batch Method: EPA 90400 Analysis Description: 9040 pH Associated Lah Samples: 924498'2001, 92449812002 SAMPLE DUPLICATE: 2718169 92449718001 Dup Parameter Units Result Result RPD Qualifiers pH at 25 Degrees C Std. Units 6.9 6.7 3 D6,H3 SAMPLE DUPLICATE: 2718170 92450780002 Dup Parameter Units Result Result RPD Qualifiers pH at 25 Degrees C Std. Units 5.8 5.3 10 D6,H3 Pace Analytical services, LLC 2225 Riverside Dr. Asheville, NO 28804 (828)254-7176 Results presented on this page arc in the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS -This report shall not be reproduced, except in full, Date: 10/30/2019 08:50 AM without the written consent of Pace Analytical Services, LLC. Page 11 of 17 • aceAnalytical * w.pacelabscam QUALITY CONTROL DATA Project: STORMWATER OCTOBER 2019 Pace Project No.: 92449812 QC Batch: 505349 Analysis Method: SM 5220D-2011 QC Batch Method: SM 5220D-2011 Analysis Description: 5220D COD Associated Lab Samples: 92449812001, 92449812002, 92449812003 METHOD BLANK: 2715093 Matrix: Water Associated Lab Samples: 92449812001, 92449812002, 92449812003 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Chemical Oxygen Demand mg1L ND 25.0 10/23/19 20:30 Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 LABORATORY CONTROL SAMPLE: 2715094 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Chemical Oxygen Demand mg1L 750 751 100 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2715095 2715096 MS MSD 92450104007 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Chemical Oxygen Demand mg1 349 100 100 452 450 103 101 90-110 1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2715097 2715098 MS MSD 92449730001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Chemical Oxygen Demand mg/L 240 100 100 296 298 55 57 90-110 1 M1 Results presented on this page are In the units indicated by the "n nits" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not he reproduced, except in full, Date: 10/30/2019 08:50 AM without the written consent of Pace Analytical Services, LLC, Page 12 of 17 aceMalytical. rvww.pacafaWom QUALIFIERS Project: STORMWATER OCTOBER 2019 Pace Project No.: 92449812 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL- Adjusted Method Detection Limit. Pace Analytical Services, LLC 2225 Riverside or. Asheville, NC 28804 (828)254-7176 PQL - Practical Quantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Diphenyihydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. LABORATORIES PASI-A Pace Analytical Services - Asheville PASI-C Pace Analytical Services - Charlotte ANALYTE QUALIFIERS D6 The precision between the sample and sample duplicate exceeded laboratory control limits. H3 Sample was received or analysis requested beyond the recognized method holding time. M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. REPORT OF LABORATORY ANALYSIS This report shall not bo reproduced, except in full, Date: 10130/2019 08:50 AM without the written consent of Pace Analytical Services, LLC. Page 13 of 17 aceMalXical wnrwpacelaftcam QUALITY CONTROL DATA CROSS REFERENCE TABLE Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28604 (828)254-7176 Project: Pace Project No.: STORMWATER OCTOBER 2019 92449812 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92449812001 OUTFALL #3 EPA 1664B 506483 92449812002 CREEK PRE MILL EPA 1664E 506483 92449812003 CREEK POST MILL EPA 1664E 506493 92449812001 OUTFALL 43 EPA 180.1 Rev 2.0 1993 503960 92449812002 CREEK PRE MILL EPA 180.1 Rev 2.0 1993 503960 92449812003 CREEK POST MILL EPA 180.1 Rev 2.0 1993 503960 92449812001 OUTFALL #3 SM 2540D-2011 504599 92449812002 CREEK PRE MILL SM 254OD-2011 504599 92449812003 CREEK POST MILL SM 254OD-2011 504599 92449812001 OUTFALL #3 EPA 9040C 506001 92449812002 CREEK PRE MILL EPA 9040C 506001 92449812003 CREEK POST MILL EPA 9040C 504653 92449812001 OUTFALL #3 SM 5220D-2011 505349 SM 5220D-2011 505410 92449812002 CREEK PRE MILL SM 5220D-2011 505349 SM 5220D-2011 505410 92449812003 CREEK POST MILL SM 5220D-2011 505349 SM 5220D-2011 505410 Date: 10/30/2019 08:50 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 14 of 17 Document Name: Document Revised: February 7, 2018 r �C2An8IytlC�1 Sample Condition Upon Receipt(SCUR) Page 1 of 2 DocumentNo.: Issuing Authority: F-CAR-CS-033-Rev.06 Pace Carolinas quality Office Laboratory receiving samples: Asheville, Eden❑ Greenwood ❑ Huntersville❑ Raleigh[] Mechanicsville❑ Client Name: WV# : 92449812 n Projec t,otCcr 021 n) C0 t 4f: Courier: []Fed Ex ❑UPS ❑LISPS ,Erclient ❑ Cam mercial ❑Pace ❑Other: 92449812 Custody Seal Present? []Yes o Seals intact? ❑Yes ZNo J Date/Initials Person Examining Contents: ioi6lr Packing Material: []Bubble Wrap ❑Bubble Bags one ❑ Other Biological Tissue Frozen? //// Thermometer; �IR Gun 10: 43Tt! 1 Type of Ice: ) et ❑Blue Oyes ❑No Env/A ❑!lone Cooler Temp ('C): r% O Correction Factor: Add/Subtract ('C) 12,0 0 Temp should be above freezing to VC Cooler Temp Corrected ('C): []Samples out of temp criteria. Samples on ice, cooling process has begun �� USDA Regulated Soil N/A, water sample) J�-' Did samples originate in a quarantine zone within the United States; CA, NY, or SC (check maps)? Dld samples originate from a foreign source (internationally, Dyes nNo Incicdine Hawaii and PuertoRicol? ❑Yes ❑No Comments/Discrepancy: Chain of Custody present? Yes ❑No ©N/A 1. Samples Arrived within Hold Tme? Yes ❑No EINJA 2. Short Hold Time Analysis (<72 hr.)? es []NO NIA 3. Rush Turn Around Time Requested? []Yes No NJA 4. Sufficient Volume? es No ❑N/A 5. Correct Containers Used? -Pace Containers Used? Yes Yes []No []No ❑N/A ❑N/A 6. Containers Intact? Yes ❑No ❑N/A 7. Dissolved analysis: Samples Field Filtered? []Yes E5No []N/A S. Sample Labels Match COC? Toes -Includes Date/Time/ID/Analysis Matrix: ft/ []NO ❑NIA 9. Headspace in VOA Vials (>5-6mm)? Dyes otio N/A 10. Trip Blank Present? ❑Yes Trfp Blank Custody Seals Present? Yes [:]No No NIA N/A 11. COMMENTS/SAMPLE DISCREPANCY Lot ID of split containers: CLIENT NOTIFICATION/RESOLUTION Person contacted: Project Manager SCURF Review: Project Manager SRF Review: Date/Time: Date: Date: Field Data Required? []Yes Page 15 of 17 /� Document Name: Document Revised: February 7, 2018 J /C8/�f1a1`�►1Cc�1 Sample Condition Upon Recelpt(SCUR) Page 1 of 2 Document No.: Issuing Authority: �� � F-CAR-CS-033-Rev.Ob Pace Carolinas Quality Office *Check mark top half of box if pH and/or dechlorination is verified and within the acceptance range for preservation samples. Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/8015 (water) DOC, LLHg **Bottom half of box is to list number of bottle Project# WO# : 92449812 PM: C01 Due Date: 10/30/19 CLIENT: 93-Jackson P E c N C a E > a a m C > `a E > M a m m C 7 a E 7 N a m O. `m mt!N 7 rt a m n V a E in Jf v d Co v n z a J O Z M a in Z ca m ra a J E N N a a to Nz ^ n a E N U V a in o ° E vy } w 0 M E Q `u '+ l7 4 N a E Q u S .ti 0 4 g[! m E Q J E N �7 M 0 Q v Q V 0 �= n E G m wl 1il W Uf C M a O Q Ln N 1%1 M W .9 Y Z a N m O 4 M 0 Q ¢ 0 J E a = G W O 4 Z 0 vi Z Q 0 > E O h p1 0 > 5 C 0 J E Q 7 n l7 > < O 6 0 J E 0. 01 t7 C d a N -5 to bd 4 0 > Q -" n e `. Y t7 > 4 z .. N F ul a Z v E to F.. N 0. M 7 n N M Z> io J o N Q M a T °� d p c E E r-i Z > c .Q c J E ry a Q; �^ m vM J E Q a 1 I 2 � A\N\ 3 4 5 6 7 B 9 10 it 12 INN pH Adjustment Log for Preserved Samples Sample ID Type of Preservative pH upon receipt Date preservation adjusted Time preservatlon adjusted Amount of Preservative added Lot ft Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will to sent to the North Carolina DEHNR Certification Office [i.e. Out of hold, Incorrect preservative, out of temp, incorrect containers. Page 16 of 17 J PaceAnalytical' CHAIN -OF -CUSTODY I Analytical Request Document r The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately. l r r .paeelatra.eem Page: of Cq Section A Section S Section C Required Client Information: Required Project Information: imroice Information: Campan RCpOrl To: ' Attention: 13 514 9 3 •i���cl�t f"' ,a 1�1 z.51�r� S Adtl Copy Company Name: REGULATORY AGENCY SL 11l-Ci �tG . � �'� Address' F NPDES r GROUNDWATER j— DRINKING WATER . r UST r- RCRA i OTHER Emaif7or � �� r���� Purchaso Kh' " _'c's`C�ielcj U� "!►Pt r' Order No.: f --7 Q i T Pace O,ae Rol one; _ F Project `�1�' 1 SS 3` X' 'z Name: ttia ' L7c ft`r'r` �� Pa00 P'Ot� Site Location STATE: f I 4{ Requeso oyO l�J/yrr [j Project Number. Pam P"rdoX: Requested Analysis Filtered (Y/N) I4 section O Manix Codes — °' Preservatives x Required Client Inla ban MATRIX (COO£ COLLECTED D-king Wow DW 5 u water 1rr'f m as,.rw 'L ' w:,.tnwarn, ww Producl P i W Z } saiusolid SL p m �► - SAMPLE ID oil Ot. u, N :' ` m (A-Z. 0-9l;) Aires AR p Lu a z v F y - a Sample IDs MUST BE UNIQUE Tissue TS D w z aA � in m r �' U Other OT X o N o t ,/�jRg,<Z w a a O r= rL Z U m w m 0 m 9 7- ~ sn DATE TIME GATE TIME w S S z Z Z O p Pace Project Na.! L3t1 I.D. (IJ!-r4ri, 3� � ) �lr � �C "�15c rt l J _Y< AV, I— a u I z ;-zC,le-- ire. 1Y) r I idIV, Cf:een. m ✓ ✓ ' / / I I I I- Uc72 3 rr C,1 eC n�;i `�i1 1� C' ,kII.. C'—) 0 cn in A VI v A I I�uo3 a s 6 7 8 9 10 ,1 tZ ADDITIONAL COMMENTS RELINQUISHED BY I AFFILIATION DATE TIME ACCEPTED BY I AFFILIATION DATE TIME SAMPLE CONDITIONS ORIGINAL SAMPLER NAME AND SIGNATURE Z T q C '� >_ ' } _ PRINT Name of SAMPLER: %rii �: hc, 6511r ;�S rm = E V SIGNATURE of SAMPLER-—' DpTE signed MM1DDlYY -ln p=w Note: By %gmnU thr loon you are azap" PaoWs NET 30 day r ayw t cur and myeecki w late ckvlles of 1.5% Par roorf, rlw any inwicw.t wl p;td'.-Wnn 30 dad F-ALL-0.020rcv.07. 15-May-2007