NCS000295_MONITORING INFO_20190624

�'o
STORMWATER DIVISION CODING SHEET
NCS PERMITS
PERMIT NO.
IV cS OOOQ � S
DOC TYPE
❑FINAL PERMIT
�4 MONITORING REPORTS
❑ APPLICATION
❑ COMPLIANCE
❑ OTHER
DOC DATE
❑ 3UI�
YYYYMMDD

JACKSON PAPER
MANUFACTURING
June 20, 2019
NCDEQ, Division of Water, Resources, Information Processing Unit
Attn: Central FllCs/cDM R
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
RECa
IVE-D
,IUN 2 4 ZW15
CL-f��1tF,L 1=1L`c:`"
RE: Discharge Monitoring Report Dy�lFZ SI- T10"'
NPDES Permit No. NCS000295
.1ackson Paper Manufacturing Company
Dear Division of Water Resources:
Please find enclosed Discharge Monitoring Report for Jackson Paper Manufacturing Conipaily
NPDES Permit No. NCS000295 for reporting period starting April I, 2019 and ending June 30,
2019.
Results from samples taken on .tune 7, 2019 from Outfall 001, 002, and 004 show no benchmark
execedances.
Results from Outfall 003 show an exceedance for TSS. In response to the exceedanec at Outfall
003, a Tlcr One response has been instituted.
Per our current Tier Two response for Outfall 001, we will continue to conduct monthly monitoring
and reporting for all parameters at Outfall 001. Monthly (analytical and qualitative) monitoring
will continue until three consecutive sample results are below the benchmark values. We will also
continue to monitor for al] parameters in the receiving water directly upstream and downstream of
the monitoring point in accordance with the Tice- Two response.
NORTH CAROLINA'S LARGEST RECYCLED PAPER PRODUCER
152 Wim MAIN SI It I rm I'Q Rc)x 0670 Svim,n, NC28771) f lil,(81$) 586-553,I FAX [phone]

I certify that based on information and belief formed from reasonable inquiry, the statements and
information in the document are true, accurate, and complete.
Please contact Kicsha Bridges at [phone] Ext. 226 if you have any questions or need any
additional information.
Sincerely,
Carr Tyndall
Vice -President Operations
Jackson Paper Manufacturing; Company
l.nclosurc: Stormwater Discharge Monitoring Report
cc: J PMC File

Stormwater Discharge Outfall (SDO)
Monitoring Report
Permit Number NCS000295
Facility Name: Jackson Paper Manufacturing Company
Person Collecting Samples: Kiesha Bridges
Certified Laboratory: Pace Analytical Services, LLC Project # 92432237
Samples Collected During Calendar Year: 2019
(This monitoring report shall be received by the Division no later than 30 days from the date the
facility receives the sampling results from the laboratory.)
County: Jackson
Phone NO. 828 586-5534 Ext. 226
(SIGNATURE OF PERNTITTEE OR DESIGNEE)
By this signature, I certify that this report is accurate
and complete to the best of my knowledge.
Oil and Grease
Turbidity
TSS
pll
COD
Benchmark
15
50
(6-9)
120
Benchmark
No
Benchmark
Benchmark
Benchmark
Date
Result
Result
Result
Result
Result
Outfall
Exceedance
Benchmark
Exceedance
F,xceedance
Exceedance
Sampled
mg/L)
(Y/N)
(NTU)
(m IL
YIN)
(Y/N)
(m /L
Y/N
617/19
001
ND
No
6.8
N/A
6.8
No
6.4
No
55.5
N,o
9: ] Oam
6/7/ 19
002
N D
No
3.1
NIA
3.3
No
6.5
No
ND
N o
8:50am
6/7119
003
ND
No
275.0
N/A
143.0
Yes
7.2
No
96.6
No
-9:25am
6/7/19
004
ND
No
4.4
N/A
8.0
No
6.2
No
ND
No
9:00am
Creek Pre
6/7119
ND
N/A
30.3
NIA
60.2
N/A
6.4
N/A
28.8
N/A
Mill
9:40am
Creek Post
6/1119
ND
NIA
47.3
N/A
72.0
NIA
6.4
N/A
31.3
N/A
Mill
9:50am
ND: Not detected at or above adjusted reporting limit.
Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? —Yes x No
Mc,nsureable
Storm Event?
Yes
0.7

Storm Event Characteristics:
Date: June 7, 2019
Totabevent-precipitation.(inches): 0'70 _
Duration of storm event: -12 hours
Drainage
Area Mail Original and one copy to:
III IV Division of Water Quality
26.45 1.77 Attn: Central [riles
890,802 77,101 1617 Mail Service Center
51,963 4,498 Raleigh, North Carolina 27699-1617
. 388,687:' , 33,64N
I
II
Area (acres)
Area (sf)
Volume {cf)
1.69
73,616
4,294
5.43
236,531
13,798
Estimated volume of -discharge sampled: Volume (gal) 32,121,
Time since last rain event: 19 days
_103,206-
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who
manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and
belief, true, accurate, and co plete. I am aware that there are significant penalties for submitting false information, including the possibility of fines
and imprisonment for knoWH6 viplations."
(Signature of Perm
Ca 2D
(Date)

(�IaneAnalyfical*
wwwpecelabs.00m
June 14, 2019
Kiesha Bridges
Jackson Paper Mfg. Co.
152 West Main St.
Sylva, NC 28779
RE: Project: Stormwater 617
Pace Project No.: 92432237
Dear Kiesha Bridges:
Pace Analytical Services, LLC
2225Riverside Dr.
Asheville, NC 28804
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on June 07, 2019. The
results relate only to the samples included in this report. Results reported herein conform to the most
current, applicable TNIINELAC standards and the laboratory's Quality Assurance Manual, where
applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Chris Derouen
[e-mail]
[phone]
Project Manager
Enclosures
cc: Kelsha Bridges, Jackson Paper Mfg. Co.
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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aceAnalytical
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Pace Analytical Services, LLC
2225 i2iversidc Di.
Asheville, NC 28804
[phone]
CERTIFICATIONS
Project: Stormwater 617
Pace Project No.: 92432237
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, INC 28078
South Carolina Certification #; 99006001
LOuisianaINELAP Certification # LA170028
FloddalNELAP Certification #: E87627
North Carolina Drinking Water Certification #: 37706
Kentucky UST Certification #: 84
North Carolina Field Services Certification #: 6342
VirginiaNELAP Certification #: 460221
North Carolina Wastewater Certification #: 12
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
FloridalNELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
VirginiaNELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
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(�IaneAnalyticalo
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�+�i�ll� w_� tl ����lr �Kf1��►�1
Project: Stormwater 617
Pace Project No.: 92432237
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Lab ID
Sample ID
Method
Analysts
Analytts
Reported
Laboratory
92432237001
OUTFALL # 1
EPA 1664E
JMS
1
PASI-C
EPA 180.1 Rev 2.0 1993
MFO
1
PASI-A
SM 254OD-2011
CEH
1
PASI-A
EPA 9040C
MDW
1
PASI-A
SM 5220D-2011
GC
1
PASI-A
92432237002
OUTFALL # 2
EPA 16648
JMS
1
PASI-C
EPA 1 80. 1 Rev 2.0 1993
MFO
1
PASI-A
SM 254OD-2011
CEH
1
PAS{ -A
EPA 9040C
MDW
1
PASI-A
SM 5220D-2011
GC
1
PASI-A
92432237003
OUTFALL # 3
EPA 1664B
JMS
1
PASI-C
EPA 180.1 Rev 2.0 1993
MFO
1
PASI-A
SM 254OD-2011
CEH
1
PASI-A
EPA 9040C
MDW
1
PASI-A
SM 5220D-2011
GC
1
PASI-A
92432237004
OUTFALL # 4
EPA 1664E
JMS
1
PASI-C
EPA 180.1 Rev 2.0 1993
MFO
1
PASI-A
SM 254OD-2011
CEH
1
PASI-A
EPA 9040C
MDW
1
PASI-A
SM 5220D-2011
GC
1
PASI-A
92432237005
CREEK PRE MILL
EPA 1664B
JMS
1
PASI-C
EPA 180.1 Rev 2.0 1993
MFO
1
PASI-A
SM 254OD-2011
CEH
1
PASI-A
EPA 9040C
MDW
1
PASI-A
SM 5220D-2011
GC
1
PASI-A
92432237006
CREEK POST MILL
EPA 1664B
JMS
1
PASI-C
EPA 1 80. 1 Rev 2,0 1993
MFO
1
PASI-A
SM 2540D.2011
CFH
1
PASI-A
EPA 9040C
MDW
1
PASI-A
SM 5220D-2011
GC
1
PASI-A
REPORT OF LABORATORY ANALYSIS
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Pace Analytical Services, LLC
2225 Riverside Dr.
(�IaneMalXical" Asheville, NC 28804
www.pacelabs.corrr [phone]
ANALYTICAL RESULTS
Project: Stormwater 617
Pace Project No.: 92432237
Sample: OUTFALL # 1 Lab ll): 92432237001 Collected: 06/07/19 09:10 Received: 06/07/19 11:32 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
1664 SGT-HEM, TPH
Analytical Method: EPA 1664B
Total Petroleum Hydrocarbons
ND mglL
5.0
1
06/13/19 06:13
180.1 Turbidity
Analytical Method: EPA 180.1 Rev 2.0 1993
Turbidity
6.8 NTU
1.0
1
06/08119 05:44
2540D Total Suspended Solids
Analytical Method: SM 254OD-2011
focal Suspended Solids
6.8 mglL
2.S
1
Ub/13119 13:06
9040 pH
Analytical Method: EPA 9040C
pH at 25 Degrees C
6.4 Sid, Units
0,10
1
06/09/19 05:26 ❑6,H3
5220D GOD
Analytical Method: SM 5220D-2011
Preparation Method:
SM 522OD-2011
Chemical Oxygen Demand
55.5 mglL
25.0
1
06/12/19 17:45 06/13/19 16:39
REPORT OF LABORATORY ANALYSIS
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Date: 06/1412019 04:56 PM without the written consent of Pace Analytical Services, LLC. Page 4 of 19

laneAnallyticalo
www,paWa4com
►F-11" 1AI[OUR0N*3910P
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project: Slormwater 617
Pace Project No.: 92432237
Sample: OUTFALL # 2 Lab ID; 92432237002 Collected: 06/07/19 08:50 Received: 06/07/19 11:32 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
1664 SGT-HEM, TPH
Analytical Method: EPA 16648
Total Petroleum Hydrocarbons
ND mglL
5.0 1
06113/19 06:14
180.1 Turbidity
Analytical Method: EPA 180.1 Rev 2.0 1993
Turbidity
3.1 NTU
1.0 1
06/08/19 05:41
2540D Total Suspended Solids
Analytical Method: SM 2540D-2011
Total Suspended Solids
3.3 mglL
2.5 1
06113/19 13:06
9040 pH
Analytical Method: EPA 9040C
pH a1 25 Degrees C
6.5 Std. Units
0.10 1
06109/19 05:37 H3
5220D COD
Analytical Method: SM 5220D-2011
Preparation Method: SM 5220D-2011
Chemical Oxygen Demand
ND mg1L
25.0 1
06/12/19 17:45 06/13/19 16:40
REPORT OF LABORATORY ANALYSIS
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ANALYTICAL RESULTS
Pace Analytical Services, LLC
2225'!Riverside Dr,
Asheville, NC 28804
[phone]
Project: Stormwater 617
Pace Project No.: 92432237
Sample: OUTFALL # 3 Lab lD: 92432237003 Collected: 06/07119 09:25 Received: 06/07/19 11:32 Matrix: Water
Parameters Results Units Report Limit ❑F Prepared Analyzed CAS No. Quaff
1664 SGT-HEM, TPH
Analytical Method; EPA 1664E
Total Petroleum Hydrocarbons
ND mg1L
5.0 1
06/13119 06:14
180.1 Turbidity
Analytical Method: EPA 180.1 Rev 2.0 1993
Turbidity
275 NTU
1.0 1
06/08/19 05:46
2540D Total Suspended Solids
Analytical Method: SM 254OD-2011
Total Suspended Solids
143 mg1L
35.7 1
06/13119 13:06
9040 pH
Analytical Method: EPA 9040C
pH at 25 Degrees C
7.2 Std. Units
0.10 1
06/09/19 05:47 H3
5220D COD
Analytical Method: SM 5220D-2011
Preparation Method:
SM 5220D-2011
Chemical Oxygen Demand
96.6 mg1L
25.0 1
06/12/19 17:45 06/13/19 16:40
REPORT OF LABORATORY ANALYSIS
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Pace Analytical Services, LLC
2225 Riverside Dr.
lacieAnalyfical"" Asheville, NC 28804
wwwpacefabs.com {828 }254-7176
ANALYTICAL RESULTS
Project: Stormwater 617
Pace Project No.: 92432237
Sample: OUTFALL # 4
Lab ID: 92432237004 Collected: 06107/19 09:00
Received: 06/07/19 11:32 Matrix: Water
Parameters
Results Units Report Limit
DF
Prepared Analyzed CAS No. Qual
1664 SGT-HEM, TPH
Analytical Method: EPA 1664E
Total Petroleum Hydrocarbons
ND mglL 5.0
1
06/13/19 06:14
180.1 Turbidity
Analytical Method: EPA 180.1 Rev 2.0 1993
Turbidity
4.4 NTU 1.0
1
06/08119 05:43
2540D Total Suspended Solids
Analytical Method: SM 2540D-2011
Total Suspended Solids
8.0 mg1L 2.5
1
06/13119 13:07
9040 pH
Analytical Method: EPA 9040C
pH at 25 Degrees C
6.2 Std. Units 0.10
1
06/09119 05:53 H3
5220D COD
Analytical Method: SM 5220D-2011 Preparation Method: SM 5220D-2011
Chemical Oxygen Demand
ND mg1L 25.0
1
06/12/19 17:45 06/13119 16:40
REPORT OF LABORATORY ANALYSIS
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aceftlytical
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ANALYTICAL RESULTS
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
(8281254-7176
Project: Stormwater 617
Pace Project No.: 92432237
Sample: CREEK PRE MILL Lab ID: 92432237005 Collected: 06/07/19 09:40 Received: 06/07/19 11:32 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. I Qual
1664 SGT-HEM, TPH
Analyfcal Method: EPA 1664E
Total Petroleum Hydrocarbons
ND mglL 5.0 1
06113/19 06:15
180.1 Turbidity
Arialytical Method: EPA 180.1 Rev 2.0 1993
Turbidity
30.3 NTU 1.0 1
06/08/19 05:55
2540D Total Suspended Solids
Analytical Method: SM 2540D-2011
Total Suspended Solids
60.2 mg1L 5.0 1
06/13/19 13:07
9040 pH
Analytical Method: EPA9040C
pH at 25 Degrees C
6.4 Std. Units 0.10 1
06/09/19 05:58 H3
5220D COD
Analytical Method: SM 5220D-2011 Preparation Method: SM 5220D-2011
Chemical Oxygen Demand
28.8 mgll- 25.0 1
06/12/19 17:45 06/13/19 16:40
REPORT OF LABORATORY ANALYSIS
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ANALYTICAL RESULTS
Pace Analytical Services, LLC
2225 Riverside Or.
Asheville, NC 28804
[phone]
Project: Stormwater 617
Pace Project No.: 92432237
Sample: CREEK POST MILL Lab ID: 92432237006 Collected: 06/07/19 09:50 Received: 06/07/19 11:32 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No, Qual
1664 SGT-HEM, TPH
Analytical Method: EPA 165413
Total Petroleum Hydrocarbons
ND mg1L
5.0
1
06/13/19 06:15
180.1 Turbidity
Analytical Method: EPA 180.1 Rev 2.0 1993
Turbidity
47.3 NTU
1.0
1
06/08119 05:57
2540D Total Suspended Solids
Analytical Method: SM 2540D-2011
Total Suspended Solids
72.0 mg1L
6.2
1
06/13119 13:07
9040 pH
Analytical Method: EPA 9040C
pH at 25 Degrees C
6.4 Std. Units
0.10
1
06/09/19 06:04 H3
5220D COD
Analytical Method: SM 5220D-2011
Preparation Method:
SM 522OD-2011
Chemical Oxygen Demand
31.3 mg1L
25.0
1
06/12/19 17:45 06/13/19 16:41
REPORT OF LABORATORY ANALYSIS
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(�IacleAnalytical"
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QUALITY CONTROL DATA
Project: Stormwater 617
Pace Project No.: 92432237
QC Batch: 480855 Analysis Method: EPA 1664E
QC Batch Method: EPA 1664B Analysis Description: 1664 SGT-HEM, TPH
Associated Lab Samples: 92432237001, 92432237002, 92432237003, 92432237004, 92432237005, 92432237006
METHOD BLANK: 2601096 Matrix: Water
Associated Lab Samples: 92432237001, 92432237002, 92432237003, 92432237004, 92432237005, 92432237006
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Total Petroleum Hydrocarbons mg1L ND 4.8 06113/19 06:05
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
LABORATORY CONTROL SAMPLE: 2601097
Spike LOS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Total Petroleum Hydrocarbons mg1L 19.2 21.3 111 64-132
MATRIX SPIKE SAMPLE: 2601098
35473817002 Spike MS MS % Rec
Parameter Units Result Conc. Result % Rec Limits Qualifiers
Total Petroleum Hydrocarbons mg1L 4.8U 19.2 20.7 107 64-132
Results presented an this page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right or the result.
REPORT OF LABORATORY ANALYSIS
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Date: 06/14/2019 04:56 PM without the written consent at Pace Analytical Services, LLC'.
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QUALITY CONTROL DATA
Project: Stormwater 617
Pace Project No.: 92432237
QC Batch: 479916 Analysis Method: EPA 180.1 Rev 2.0 1993
QC Batch Method: EPA 180.1 Rev 2.0 1993 Analysis Description: 180.1 Turbidity
Associated Lab Samples: 92432237001, 92432237002, 92432237003, 92432237004, 92432237005, 92432237006
Pace Analytical Services, Li
2225 Riverside i
Asheville, NC 28804
(82B)254-7176
METHOD BLANK: 2597236
Matrix: Water
Associated Lab Samples: 92432237001,
92432237002, 92432237003, 92432237004, 92432237005,
92432237006
Blank Reporting
Parameter
Units
Result Limit
Analyzed Qualifiers
Turbidity
NTU
ND 1.0
06/08/19 05:33
LABORATORY CONTROL SAMPLE:
2597237
Spike LCS
LCS % Rec
Parameter
Units
Conc. Result
% Rec Limits Qualifiers
Turbidity
NTU
10 10.3
103 90.110
SAMPLE DUPLICATE: 2597238
92432124001 Dup
Parameter Units Result Result RPD Qualifiers
Turbidity NTU 1.4 1.5 8 H1
SAMPLE DUPLICATE: 2597239
92432193005 Di
Parameter Units Result Result RPD Qualifiers
Turbidity NTU 12.1 11.7 3
Results presented on this page are In the units Indicated by the "Units" Column except where an alternate unit Is presented to the light of the result.
REPORT OF LABORATORY ANALYSIS
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QUALITY CONTROL DATA
Project: Stormwater 617
Pace Project No.: 92432237
QC Batch: 480808 Analysis Method: SM 25400-2011
QC Batch Method: SM 254OD-2011 Analysis Description: 2540D Total Suspended Solids
Associated Lab Samples: 92432237001, 92432237002, 92432237003, 92432237004, 92432237005, 92432237006
METHOD BLANK: 2600982 Matrix: Water
Associated Lab Samples: 92432237001, 92432237002, 92432237003, 92432237004, 92432237005, 92432237006
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Total Suspended Solids mg/L. ND 2.5 06113/19 13:05
Pace Analytical Services, LLC
2225 Riverside Or,
Asheville, NC 28804
[phone]
LABORATORY CONTROL SAMPLE: 2600983
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Total Suspended Solids mg/L 250 242 97 90-110
SAMPLE DUPLICATE: 2601073
92432237003 Dup
Parameter Units Result Result RPD Qualifiers
Total Suspended Sollds mg/L 143 140 2
SAMPLE DUPLICATE: 2601074
92432249003 Dup
Parameter Units Result Result RPD Qualifiers
Total Suspended Solids mg/L 267 302 12 D6
Results presented an this page are in the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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(�IacleAnalyfical"
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QUALITY CONTROL DATA
Project: Stormwater 617
Pace Project No.: 92432237
QC Balch: 479987 Analysis Method: EPA 9040C
QC Batch Method: EPA 9040C Analysis Description: 9040 pH
Associated Lab Samples: 92432237001, 92432237002, 92432237003, 92432237004, 92432237005, 92432237006
SAMPLE DUPLICATE: 2597452
92432237001 Dup
Parameter Units Result Result RPD Qualifiers
pH at 25 Degrees C Std. Units 13A 6.0 7 D6,H3
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28BQ4
[phone]
Results presented on this page are In the units Indicated by the `Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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(�IaneAnalXical*
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QUALITY CONTROL DATA
Project: Stormwater 6/7
Pace Project No.: 92432237
QC Batch: 480787 Analysis Method: SM 5220D-2011
QC Batch Method: SM 5220D-2011 Analysis Description: 5220D COD
Associated Lab Samples: 92432237001, 92432237002, 92432237003, 92432237004, 92432237005, 92432237006
METHOD BLANK: 2600860 Matrix: Water
Associated Lab Samples: 92432237001, 92432237002, 92432237003, 92432237004, 92432237005, 92432237006
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Chemical Oxygen Demand mg1L ND 25.0 0611309 16:37
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
{828}254-7176
LABORATORY CONTROL SAMPLE: 2600861
Spike LCS LCS % Rec
Parameter Units Cone. Result % Rec Limits Qualifiers
Chemical Oxygen Demand mg1L 750 757 101 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2600862 2600863
MS MSD
92431794002 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Chemical Oxygen Demand mg/L 31,3 100 100 131 133 99 102 90-110 2
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2600864 2600865
MS MSD
92432237006 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Copc. Conc. Result Result % Rec % Rec Limits RPD Qual
Chemical Oxygen Demand mg/L 31.3 100 100 138 135 107 104 90-110 2
Results presented on this page are In the units Indicated by the "tin Its" columh except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06114/2019 04:56 PM without the written consent of Pace Analytical Services, LLC. Page 14 of 19

aceAnalytical®
wwwpacelab&=
QUALIFIERS
Project: Stormwater 617
Pace Project No.. 92432237
DEFINITIONS
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
Ti - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit,
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D} - Laboratory Control Sample (Duplicate)
MS(D) Matrix Spike (Dup{icate)
❑UP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Ciean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis ofAcrolein and Actylonitrile by EPA
Method 8260,
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is Ti accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute,
LABORATORIES
PAST -A Pace Analytical Services -Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
D6 The precision between the sample and sample duplicate exceeded laboratory control limits.
H1 Analysis conducted outside the EPA method holding time.
H3 Sample was received or analysis requested beyond the recognized method holding time.
REPORT OF LABORATORY ANALYSIS
This report shall net be reproduced, except in full,
Date: 06/14/2019 04:56 PM without the written consent of Pace Analytical Services, t.LC, Page 15 of 19

aceAnalytical
www.pa&sbs.com
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project:
Pace Project No.:
Stormwater 617
92432237
Analytical
Lab ID
Sample ID
OC Batch Method
CIC Batch
Analytical Method
Batch
92432237001
OUTFALL # 1
EPA 1664B
480855
92432237002
OUTFALL # 2
EPA 1664B
480855
92432237003
OUTFALL # 3
EPA 1664B
480855
92432237004
OUTFALL 4 4
EPA 1664B
480855
92432237005
CREEK PRE MILL
EPA 1664B
480855
92432237006
CREEK POST MILL
EPA 1664B
480855
92432237001
OUTFALL 4 1
EPA 180.1 Rev 2.0 1993
479916
92432237002
OUTFALL # 2
EPA 180.1 Rev 2.0 1993
479916
92432237003
OUTFALL 4 3
EPA 180.1 Rev 2.0 1993
479916
92432237004
OUTFALL # 4
EPA 180.1 Rev 2.0 1993
479916
92432237005
CREEK PRE MILL
EPA 180.1 Rev 2.0 1993
479916
92432237006
CREEK POST MILL
EPA 180.1 Rev 2.0 1993
479916
92432237001
OUTFALL 4 1
SM 254OD-2011
480808
92432237002
OUTFALL 4 2
SM 254OD-2011
480808
92432237003
OUTFALL # 3
SM 254OD-2011
480808
92432237004
OUTFALL # 4
SM 254OD-2011
480808
92432237005
CREEK PRE MILL
SM 2540D-2011
480808
92432237006
CREEK POST MILL
SM 2540D-2011
480808
92432237001
OUTFALL # 1
EPA9040C
479987
92432237002
OUTFALL # 2
EPA 9040C
479987
92432237003
OUTFALL # 3
EPA 9040C
479987
92432237004
OUTFALL # 4
EPA 9040C
479987
92432237005
CREEK PRE MILL
EPA 9040C
479987
92432237006
CREEK POST MILL
EPA 9040C
479987
92432237001
OUTFALL # 1
SM 5220D-2011
480787
SM 5220D-2011
480835
92432237002
OUTFALL # 2
SM 5220D-2011
480787
SM 5220D-2011
480835
92432237003
OUTFALL # 3
SM 5220D-2011
480787
SM 5220D-2011
480835
92432237004
OUTFALL # 4
SM 5220D-2011
480787
SM 5220D-2011
480835
92432237005
CREEK PRE MILL
SM 5220D-2011
480787
SM 5220D-2011
480835
92432237006
CREEK POST MILL
SM 5220D-2011
480787
SM 5220D-2011
480835
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/14/2010 04:56 PM without the written consent of Pace Analytical Services, LLC.
Page 16 of 19

it dLeAnalybcal
!
Document Name:
Sample Condition Upon Receipt(SCUR)
Document Revised: February 7, 2018
Page 1 of 2
Document No.:
F-CAR-CS-033-Rev.06
Issuing Authority:
Pace Carolinas Quality Office
Laboratory receiving samples:
Asheville K Eden[] Greenwood ❑ Htlntersville❑ Raleigh❑ Mechanicsville❑
Client Name: W0# : 92432237
MEN=J C C �� 5 n "1 0 e. r- Project a:
Courier: ❑Fed Ex ❑UPS OUSPS ❑Client
❑ Commercial OPace ❑other: 5 '432237
Custody Seal Present? ❑Yes ®No Seals Intact? ❑Yes No I
Date/Initials Person Examining Contents:
Packing Material: ❑Bubble Wrap [Bubble Bags ❑None ❑ Other Biological Tissue Frozen?
Thermometer: / Wet ❑blue ❑None[]Yes ❑No MN/A
WIRGun
Type f iCooler Temp ('C): 3- d-j V Correction Factor: Add/Subtract ('C)
3' �' r Temp should be above freezing to 6'C
Cooler Temp Corrected ('C):
❑samples out of temp criteria. Samples on Ice, cooling process
has begun
USDA Regulated Boll (PS N/A, seater sample)
Did samples originate in a quarantine tone within the United 5tates: CA, NY, or SC {check maps)? Did samptes originate Tram a foreign source (internationally,
❑Yes ONO inrLiline Hawali and Puerto Ricol? F­lYes KINo
Comments/Discrepancy:
Chain of Custody Present?
Yes
❑No
❑N/A
1.
Samples Arrived within Hold Time?
Yes
❑No
N/A
2.
Short }told Time Analysis (02 hr.)?
.tJYes
XNo0
NIA
3. V d
Rush Turn Around Time Requested?
OYes
WN0
❑N/A
4.
Sufficient Volume?
taffes
ElNo
N/A
5.
Correct Containers Used?
-Pace Containers Used?
'MYes
Yes
❑No
EI.No
[]N/A
❑N/A
6.
Containers Intact?
hYes
ON.
❑N/A
7.
Dissolved analysis: Samples Field Filtered?
❑Yes
❑No
/A
8.
Sample Labels Match COC?
-Includes Date/Time/ID/Analysis Matrix:
oYes
LJ T
[]No
❑N/A
9.
Headspace in VOA Vials (>5.6mm)?
❑Yes
No
N/A
10.
Trip Blank Present?
Trip Blank Custody Seals Present?
❑Yes
❑Yes
[]NO
No
fqN/A
N/A
11.
COMMENTS/SAMPLE DISCREPANCY Field Data Required? []Yes [:]No
Lot ID of split containers:
CLIENT NOTIFICATION/RESotu riON
Person contacted:
Project Manager SCURF Review:
Project Manager 5RF Review:
Date/Time:
Date:
� � r
Date: /° "Z1�
Page 17 of 19

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BP21.1-500 mL Plastic Unpreserved (N/A)
BP1U-1 liter Plastic Unpreserved (N/A)
BP45-125 mL Plastic H2SO4 (pH < 2) (Cl.)
MN-250 mL plastic HNO3 (pH < 2)
BP42-125 m1 Plastic ZN Acetate & NaOH (>9)
BP4C-125 mL Plastic NaOH (pH > 12) (CI-)
WGFU-Wide-mouthed Glass jar Unpreserved
AG1U-1 liter Amber Unpreserved (N/A) (CI-)
AG1H-1 liter Amber HCI (pH < 2)
AG3U-250 mL Amber Unpreserved (N/A) (CI-)
EZ
AGSS-1 liter Amber H2SO4 (pfi < 2)
gIzzz
AG3S-250 mL Amber H2SO4 (pH < 2)
AG3A(DG3A)-250 mL Amber NH4CI (N/A)(CI-)
DG9H-40 mL VOA HCI. (N/A)
VG9T-40 mL VOA Na2S203 (N/A)
VGOU-40 mL VOA U.p (N/A)
DG9P-40 mL VOA H3PD4 (N/A)
VOAK (6 vials per kit)-5035 kit (N/A)
V/GK (3 vials per kit)-VPH/Gas kit (N/A)
SP5T-125 mL Sterile Plastic (N/A - lab)
SP2T-250 mL Sterile Plastic (N/A— lab)
BP3A-250 mL Plastic (NH2)2504 (9.3-9.7)
AGOU-100 mL Amber Unpreserved vials (N/A)
VSGU-20 mL Scintillation vials (N/A)
069U-40 mL Amber Unpreserved vials (N/A)

i
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CHAIN -OF -CUSTODY I Analytical Request Document
The Chain -of -Custody is a LEGAL DOCUMENT, AN relevant fields must be completed accurately. o
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Section A Section B Section C
a
7387
RagUirad Client Information: Required Project Inlormation: Invoice Informalion:
C r Report To: \es hcL i� C A°�:
206
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Company Name:
REGULATORY AGENCY
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F- NPDES r GROUND WATER r DRINKING WATER
F- UST i— RCRA r OTHER
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DATE
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DATE
TIME
SAMPLE CONDITIONS
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SAMPLER NAME AND SIGNATURE
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JACKSON PAPER
MANUFACTURING
May 16, 2019
NCDI Q, Division of Water RCS011l'CCS, lllforrnation Processing Unit
Attn: Central Flles/cDMIZ
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
RE: Discharge Monitoring Report- April 2019 Monthly "Pier 2 Report
NPDES Permit No. NCS000295
Jackson Paper Mani=factui-ing Company
Dear Division of Water Resources:
Enclosed is the discharge monitoring report for April 2019.
We sampled Outfall 001 and the receiving water' directly upstrearll and downstream of Outfall 001
for all parameters listed in our permit on April 26, 2019. Results show benchmark exceedances for
TSS and COD. We are working to determine the cause for the exceedances and develop feasible
controls. Upstream and downstream water quality was not affected.
I certify that based on infon7ration and belief formed from reasonable inquiry, the statements and
lllforlllatloll III the doCLtnlent are true, aCCUratc, and complete.
I'lease contact Kiesha Bridges at [phone] Ext. 226 if you have any questions or need any
additional information.
Sincerely,
Carr "Tyndall MPS
Vice -President Operations �`��1
Jackson Paper Manufacturing Company �,`` a4 G
lHnclosurc: Stormwater Discharge Monitoring Report
cc: JPMC File
NORTH CAROLINA'S LARGEST RECYCLED PAPER PRODUCER
t52 %VIS1 10AIIJ STRI1.1 G)P0 hox 66? OSvixw NC28779 TFL(828) 586-5534 FAX[phone],5

Stormwater Discharge Outfall (SDO)
ilfonitoring Report
Permit Number NCS000295
Facility Name: Jackson Paper Manufacturing Company
Person Collecting Samples Kiesha Bridges
Certified Laboratory: Pace Analytical Services, LLC Project # 92426954
Samples Collected During Calendar Year: 2019
(This monitoring report shall be received by the Division no later than 30 days from the date the
facility receives the sampling results from the laboratory)
County: Jackson
Ph nc NO. 828 5 i-5534 Ext. 226
(SJG:NATURE OF PE .91TTEE OR DESIGNEE)
By this signature. 1 certify that this report is accurate
and complete to the best of my knowledge.
Oil and Grease
Turbidity
FSS
pH
COD
Benchmark
15
50
(6-9)
120
Benchmark
Benchmark
Benchmark
Benchmark
Date
Result
Result
N/A
Result
Result
Result
Outfall
Exceedance
Esceedance
Fsceedance
Esceedance
Sampled
m61L
YIN
N"1'U
mUIL
YIN
Y/N
nw/L
YIN
001
4/26/2019
ND
No
45.4
351.0
Yes
6.9
Yes
357.0
Yes
8:55am
Creek Pre
4/26/19
ND
No
2.8
25.2
6.3
ND
Mill
9:loam
Creek Post
4/26/0
ND
No
4.4
23.9
6.4
ND
Mill
9:20am
NO.* Not detected at or above adjusted reporting limit.
Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? _Yes x No
i•ieasureable
Storm Event?
Yes
0.15

Storm Event Characteristics:
Date: April 26, 2019
Total eventiprecipitation (inches): 0.15
Duration of storm event: 45 minutes
Drainage
Area
Mail Original and one copy to:
IV Division of Water Quality
1.77 Attn: Central Files
77,101 1617 Mail Service Center
964 Raleigh, North Carolina 27699-1617
7,209;
u
In
Area (acres)
Area (sf)
volume (co
1.69
73,616
920
5,43
236,531
2,957
20.45
890,802
11,135
Estimated volume of- discharge sampled: lValurne (gat)
Time since last rain event: 3 days
6,883.
22,ii6.
83,290.
" I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who
manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and
belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines
a prisonment fo kno ' violations."
SI Ci
(Signature of Per T
ittee) (Da )

(�IaceAnalyfical
www.pacelabs.com
May 03, 2019
Kiesha Bridges
Jackson Paper Mfg. Co.
152 West Main St.
Sylva, NC 28779
RE: Project: Stormwater 412019
Pace Project No.: 92426954
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Dear Kiesha Bridges:
Enclosed are the analytical results for sample(s) received by the laboratory on April 26, 2019. The
results relate only to the samples included in this report. Results reported herein conform to the most
current, applicable TNIINELAC standards and the laboratory's Quality Assurance Manual, where
applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Chris Derouen
[e-mail]
[phone]
Project Manager
Enclosures
cc: Keisha Bridges, Jackson Paper Mfg. Co.
REPORT OF LABORATORY ANALYSIS
This report shall not he reproduced, except in full,
without the written consent of Pace Analytical Services, L-C.
Page 1 of 16

acmnalytical
wwwpacdabs.c=
Pace Analytical Services, LLG
2225 Riverside Dr.
Asheville, l 28804
[phone]
CERTIFICATIONS
Project: Stormwater 4/2019
Pace Project No.: 92426954
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
South Carolina Certification M 99006001
Louisiana/NELAP Certification # LA170028
Florida/NELAP Certification #: E87fi27
North Carolina Drinking Water Certification #: 37706
Kentucky UST Certificaflon #: 84
North Carolina Field Services Certification #: 5342
VirginiaNELAP Certification M 460221
North Carolina Wastewater Certification #: 12
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
FloridalNELAP Certification #: E87648
Massachusetts Certification #: M-NCO30
North Carolina [drinking Water Certification #: 37712
North Carolina Wastewater Certification M 40
South Carolina Certification #: 99030001
VirginiaNELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall nol he reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 16

(�IacieAnalytical*
W".pacelabscam
Project: Stormwaler 412019
Pace Project No.: 92426954
Lab ID Sample ID
92426954001 Outfall i
92426954002 Creek Pre Mill
92426954003 Creek Post Mill
Pace Analytical Services, Ll-C
2225 Riverside Dr.
Asheville, NC 28804
[phone]
SAMPLE ANALYTE COUNT
Method
Analysts
Analytes
Reported
Laboratory
EPA 1664E
JMS
1
PASI-C
EPA 180.1 Rev 2.0 1993
GC
1
PASI-A
SM 254OD-2011
MJP
1
PASI-A
EPA9040C
SMK
1
PASI-A
SM 5220D-2011
GC
1
PASI-A
EPA 1664E
JMS
1
PASI-C
EPA 180.1 Rev 2.0 1993
GC
1
PASI-A
SM 254OD-2011
MJP
1
PASI-A
EPA9040C
SMK
1
PASI-A
SM 5220D-2011
GC
1
PASI-A
EPA 1664B
JMS
1
PASI-C
EPA 180.1 Rev 2.0 1993
GC
1
PASi-A
SM 254OD-2011
MJP
1
PASI-A
EPA9040C
SMK
1
PASI-A
SM 5220D-2011
GC
1
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shell not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 3 of 16

(�IacleAnalyfical
wwwpacelabs com
ANALYTICAL RESULTS
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NO 28804
[phone]
Project: Storrnwater 412019
Pace Project No.: 92426954
Sample: Outtall 1 Lab 1D: 92426954001 Collected: 04/26/19 08:55 Received: 04/26/19 11:58 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
1664 SGT-HEM, TPH
Analytical Method: EPA 16648
Total Petroleum Hydrocarbons
ND mg1L
5.0 1
05/01/19 06:09
180.1 Turbidity
Analytical Method: EPA 180.1 Rev 2.0 1993
Turbidity
45.4 NTU
1.0 1
04/2611919:20
2540D Total Suspended Solids
Analytical Method: SM 2540D-2011
Total Suspended Solids
351 mglL
16.7 1
05/01/19 11:09
9040 pH
Analytical Method: EPA 9040C
pH at 25 Degrees C
6.9 Std. Units
C.10 1
04/28119 12:47 H3
5220D COD
Analytical Method: SM 5220D-2011
Preparation Method:
SM 5220D-2011
Chemical Oxygen Demand
357 mg1L
25.0 1
05/02/19 16:30 05/02/19 21:26
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 0510312019 04:35 PM without the written consent of Pace Analytical Services, LLC, Page 4 of 16

Pace Analytical Services, LLC
Iacl
Analytleal 2225 Rive25 04
Asheville, NC 28804
(�www,Pacelabaoom {828 }254-7176
ANALYTICAL RESULTS
Project: Stormwater 412019
Pace Project No.: 92426954
Sample: Creek Pre Mitt Lab ID: 92426954002 Collected: 04/26/19 09:10 Received: 04/26/19 11:58 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
1664 SGT-HEM, TPH
Analytical Method: EPA 1664B
Total Petroleum Hydrocarbons
ND mglL
5.0 1
05/01/19 06:09
180.1 Turbidity
Analytical Method: EPA 1 B0.1 Rev 2.0 1993
Turbidity
2.8 NTU
1.0 1
04/26/1919:21
2540D Total Suspended Solids
Analytical Method: SM 254OD-2011
Total Suspended Solids
25.2 rng1L
2.5 1
05/01/10 11:09
9040 pH
Analytical Method: EPA 9040C
pH at 25 Degrees C
6.3 Sid, Lln4s
0.10 1
04/28/19 12:47 H3
5220D COD
Analytical Method: SM 5220D-2011
Preparation Method: SM 5220D-2011
Chemical Oxygen Demand
NO rnglL
25.0 1
05/02/19 16:30 051021l9 21:26
REPORT OF LABORATORY ANALYSIS
'this report shall not be reproduced, except in full,
Date: 05/03/2019 04:35 PM without the written consent of Pace Analylical Services, LLC, Page 5 of 16

(�IaneAnalyticale
www,pa W0bs.corn
ANALYTICAL RESULTS
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project: Stormwater 412019
Pace Project No.: 92426954
Sample: Creek Post Mill Lab ID: 92426954003 Collected: 04/26/19 09:20 Received: 04/26119 11:58 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
1664 SGT-HEM, TPH
Analytical Method: EPA 1664B
Total Petroleum Hydrocarbons
ND mg1L
5.0 1
05/01/19 06:10
180.1 Turbidity
Analytical Method: EPA 180.1 Rev 2.0 1993
Turbidity
4.4 NTU
1.0 1
04/26/11319:23
2540D Total Suspended Solids
Analytical Method: SM 254OD-2011
Total Suspended Solids
23.9 mg1L
2.5 1
05/01/19 11:09
9040 pH
Analytical Method: EPA 9040C
pH at 25 Degrees C
6.4 Sid, Units
0.10 1
04/28119 12A7 H3
5220D COD
Analytical Method: SM 5220D-2011
Preparation Method: SM 5220D-2011
Chemical Oxygen Demand
ND mg/L
25.0 1
05/02/19 16:30 05/021l9 21:26
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Dale: 05/03/2019 04:35 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 16

(�I'acmnalyfical*
*WW..pat:elabS =
QUALITY CONTROL DATA
Project: Stormwater 412019
Pace Project No.- 92426954
QC Batch: 472486 Analysis Method: EPA 1664E
QC Batch Method: EPA 1664B Analysis Description: 1664 SGT-HEM, TPH
Associated Lab Samples: 92426954001, 92426954002, 92426954003
METHOD BLANK: 2563179 Matrix: Water
Associated Lab Samples: 92426954001, 92426054002, 92426954003
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Total Petroleum Hydrocarbons mg/L ND 4.8 05101/19 C6:06
Pace Analytical Services, LLC
2.225 Riverside Dr.
Asheville, NC 26804
[phone]
LABORATORY CONTROL SAMPLE:
2563180
Spike LCS
LCS
% Rec
Parameter
Units
Conc. Result
% Rec
Limits
Qualifiers
Total Petroleum Hydrocarbons
mg1L
19.2 21.7
113
64-132
MATRIX SPIKE SAMPLE:
2563181
92427268001 Spike
MS
MS
% Rec
Parameter
Units
Result Conc.
Result
% Rec
Limits Qualifiers
Total Petroleum Hydrocarbons
mglL
NO 19.2
21.4
110
64-132
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/03/2019 04:35 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 16

aceAnalytical
WWW..P&C0/AbSL= n
QUALITY CONTROL DATA
Project: Stormwa ter 412019
Pace Project No.: 92426954
QC Batch: 471859 Analysis Method: EPA 180.1 Rev 2.0 1993
QC Balch Method: EPA 180.1 Rev 2.0 1993 Analysis Description: 180.1 Turbidity
Associated Lab Samples: 92426954001, 92426954002, 92426954003
METHOD BLANK: 2560704 Matrix: Water
Associated Lab Samples: 92426954001, 92426954002, 92426954003
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Turbidity NTU ND 1.0 04/2611919:03
LABORATORY CONTROL SAMPLE: 2560705
Pace Analytical Services, I-LG
2225 Riverside dr.
Ashevilie, NC 28804
[phone]
Spike LCS LCS
% Rec
Parameter
Units
Conc. Result "/o R e c
Limits Qualifiers
Turbidity
NTU
10 10.5 105
90-110
SAMPLE DUPLICATE: 2560706
92425966001 Dup
Parameter
Units
Result Result RPD
Qualifiers
Turbidity
NTU
ND .92J
Results presented oh this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result,
REPORT OF LABORATORY ANALYSIS
This report shall not he reproduced, except in full,
Date: 05/03/2019 04:35 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 16

aceAnalytical
www.pacelabs.com
QUALITY CONTROL DATA
Project: Stormwater 412019
Pace Project No.: 92426954
QC Batch: 472545 Analysis Method: SM 2540D-2011
QC Batch Method: SM 2540D-2011 Analysis Description: 2540D Total Suspended Solids
Associated Lab Samples: 92426954001, 92426954002, 92426954003
METHOD BLANK: 2563355 Matrix: Water
Associated Lab Samples: 92426954001, 92426954002, 92426954003
Biank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Total Suspended Solids mglL ND 2.5 05/01/10 11:06
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
LABORATORY CONTROL SAMPLE: 2563356
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Total Suspended Solids mg1L 251 250 100 90-110
SAMPLE DUPLICATE: 2563357
92427007001 Dip
Parameter Units Result Result RPD Qualifiers
Total Suspended Solids mglL 1780 1820 2
SAMPLE DUPLICATE: 2563358
92426986001 Dup
Parameter Units Result Result RPD Qualifiers
Total Suspended Solids mg/L 1820 1860 2
Resuhs presented on this page are in the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not he reproduced, except in full,
Date: 05/03/2019 04:35 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 16

(�lacieAnalytical"
' wwn!pacdahsc=
QUALITY CONTROL DATA
Project: Stormwater 412019
Pace Project No.: 92426954
QC Batch: 471097 Analysis Method: EPA 9040C
QC Batch Method: EPA 9040C Analysis Description: 9040 pH
Associated Lab Samples: 92426954001, 92426954002, 92426954003
SAMPLE DUPLICATE'. 2561058
92426639001 Dup
Pararneter Units Result Result RPD Qualifiers
pH at 25 Degrees C Sid. Units 6.9 6.8 2 H3
SAMPLE DUPLICATE: 2561059
92426161001 Dup
Parameter Units Result Result RPD Qualifiers
pH at 25 Degrees C Std. Units 5.3 5.0 7 H3
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, 128804
[phone]
Results presented on 1H. page are in the units indicated by the "units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/03/2019 04:35 PM without the written consent of Pace Analytical Services, LLC.
Page 10 of 16

(�lacieAnallytical"
' wwwpacelahsoom
QUALITY CONTROL DATA
Project: Stonnwater 4I2019
Pace Project No.: 92426954
QC Batch: 472950 Analysis Method: SM 5220D-2011
QC Batch Method: SM 5220D-2011 Analysis Description: 5220D COD
Associated Lab Samples: 92426954001, 92426954002, 92426954003
METHOD BLANK: 2565471 Matrix: Water
Associated Lab Samples: 92426954001, 92426954002, 92426954003
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Chemical Oxygen Demand mglL ND 25.0 05/02119 21:22
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
LABORATORY CONTROL SAMPLE: 2565472
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Chemical Oxygen Demand mg/L 750 755 101 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2565473 2565474
MS MSD
92426758001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Chemical Oxygen Demand mglL 7560 100 100 7560 7370 0 -190 90-110 3 M1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2565475 2565476
MS MSD
92427246003 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Chemical Oxygen Demand mglL 31.6 100 100 136 139 105 107 90-110 2
Results presented on this page are In the units indicated by the "Units" column except where an alternate unit Is presented to lho right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/03/2019 04:35 PM without the written consent of Pace Analytical Services, LLC.
Page 11 of 16

aceAnalytical
"wpacerabawn
QUALIFIERS
Project: Stormwater 4l2019
Pace Project 1 92426954
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot,
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL- Adjusted Method Detection Limit.
Pace Analytical Services, Li
2225 Riverside Dr.
Asheville,1 28804
[phone]
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot he separated from Azobenzene using Method 8270, The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have heen used to calculate % recovery and RPD values.
LCS(0) - Laboratory Control Sample (Duplicate)
Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not CaicUlable.
SS - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TN -The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services - Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUAUFIERS
H3 Sample was received or analysis requested beyond the recognized method holding time.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS} recovery.
DEPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/03/2019 04:35 PM without the written consent of Pace Analytical Services, LLC. Page 12 of 16

(�IaceAnalyfical'
www.pacefaeaoam
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project:
Pace Project No.:
Stormwater 412019
92426954
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92426954001
Outfall 1
EPA 1664B
472486
92426954002
Creek Pre Mill
EPA 16646
472486
92426954003
Creek Post Mill
EPA 16643
472486
92426954001
Outfall 1
EPA 180.1 Rev 2.0 1993
471859
92426954002
Creek Pre Mill
EPA 1801 Rev 2.0 1993
471859
92426954003
Creek Post Mill
EPA 180.1 Rev 2.0 1993
471859
92426954001
Outfall 1
SM 2540D-2011
472545
92426954002
Creek Pre Mill
SM 254OD-2011
472545
92426954003
Creek Post Mill
SM 2540D-2011
472545
92426954001
Outfall 1
EPA 9040C
471997
92426954002
Creek Pre Mill
EPA 9040C
471997
92426954003
Creek Post Mill
EPA 9040C
471997
92426954001
Outfall 1
SM 5220D-2011
472950
SM 5220D-2011
472993
92426954002
Creek Pre Mill
SM 5220D-2011
472950
SM 5220D-2011
472993
92426954003
Creek Post Mill
SM 5220D-2011
472950
SM 5220D-2011
472993
Date: 05/03/2019 04:35 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 13 of 16

i Oocumenti!zme: gocumentRevised: 5ebruar,,7,20_9
f Sample Condition Upon Receipt{SCUR) Page 1 of 3
r'?C>✓mal.-.-tt-al , Document�!o.: IsscaiigAutho6ur
F-CAR-CS-033-Rev-06 pace Carolinas GORY Office
Laboratory receiving samples: Mecharsicsville❑
Asheville ❑ Eden[:] Greenwood ❑ Hunrersville ❑ RaWgh❑
Client Name: W® :92426954
sy ✓ Project l#:
Courier: ❑cac Ex ou—r-s -1 ❑USPS Client N III 111111111111111111
J Commercial []Pace []Other: 92426954
Custody Seal Present? ❑1'es J Seals Intact? ❑•de, [I�o y j of}rl�
p eIIrlti31SPerscn Examining Contents:
Packing 1AatariaF. Bubble Wrap []Bubble Bats []'!one ❑ Other biological Tissue Frozen?
Thermometer: !y (_ Type of Des ❑t10 ?i!A
❑ IR Gun ID: 3�bE4� l:e: J!'!c[ ❑clue ❑ilcn�
Cooler Temp l°Ct: 11 - J Correction Factur; Addi Subtract ('%:) G .
Tom s`c,lu 1;a aha'JE fre-2aing to 6'C
Cooler Temp Corrected ('C): `f • S �_, i 71�; rr.af t','D cr!ter!a, Samples o.. ice, ccolin$ process
USDA Regulated Soil ( .:/A, ::,atersamplei
D d samples a.7,�ai•rara in a qc=rand^,E ZJn? t:'IEilln the UniCed 5tatea: CA, i ly, Or ] (clleCl{ ITiapS)? Did sr 71?a Cri3:rate:r.m fareign sour_e (intes❑na�tlJnally,
IrI'(es I`fiin ita':'ir:�a:':aa?rd?uertaRco}a❑Yes o
)
I
Comr^,entsf urstrepanc• : a
1
2. 77
3.
4.
Chain&Cu,tody?resent? s ❑rla ❑rl1
S_rples.orrissd: ithinHold Time? Yes ❑;la N/A
Short Hold TirneAnalysi5 (472 hr.)? :a; h10 rlla
Rush Turn Around Time Requested?
5uf Icient Vclume?
Correct Containers Used?
Pace Cantainers Used?
f
Yes
©.JC
ONO
�m/A
I
Containers Intact?
Yes
?Ia
❑1,4 A
7.
2.
Dissolved analysis: 5amples Field Filtered? Yes ONO raiA
Sample Labels Match COO?
-iP.CludesDataMrne(IDJaralysis NlatrEY:
. :s
w�
❑Mo
©,I;A
4.
Heads ace in VOA Vials (-�5-6mm)?
❑y._s
_ ©
iA"A
10.
11.
Trio Blank Present? [4'?_x 11Xo []hllA
Trip Blank Custody Seals ?resent? ❑Yes ❑h:o hJ1A
COMN'LENT5/SA141PLE DISCREPANCY
CtiEhJT hiOTIFICATIONIRESOLUTIOhI
Person contacted:
Proiect Manager SCURF Revievi:
Project Manager SRF Review:
G
Cate/Time:
Field Data Rcqulred? QYas ❑.Nlo
Lot IDt salit cantziners:
r
Date J ,r
Page 14 or 16

:_�� �� - Dr, ;:rnent,??rae: 1c;t..nt�tie:i,ad:� eesu� f •, _.
�'nip#a C�n�iSion U;un 4eczi F(SCU0.} aav
IiiUlzg autharirl:
F-Cr?�•CS-Q'1}.Rev.06 C!c {arciins Q'.aii:y 3iiite
'[hecic mark'IDP half Of boy if 0 and/or decilloi inacion is N _ � �� f��`+��%�
Project WV 4 U 4
+terifFetf ani7,rystkin the acce,��azca rarge ror pre,er+rai�rl
salnpies' Oue Date: 05/10/19
cceptiani: ir4.,, CoEitarn Fiji : CD
aC,11Hg
`*$o�tom half of box : is to list nm"5e, o; bottle CLIENT: 93—Jackson P
71
y
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1
7
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I/ w ]. •'^,' } '"i C .+i C 1
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Pi-1 AdjI siment LOB `,oi PCeserVefd'c? 1���
Sarnpla ip ! 7ypP of 9r=seriati'ie off s:porl receipt { fiate preservation sdius;ed Tr{ne; e ; si ca a no nt �f Pr2szPvaFiv? lot 1
if If a:st:d add=_a
r'lerg If 3 di Ft?�J;.C7 a�?C[:P�!hfi; Ca;a!!n? SRzii]RCa iafnalef3 Co�'7 J� tilii frlr;»-lil Fe iBpC t] LPC tlQah ia; ol'na �E�F?iF Ce::i;ic]'.iar IIffice Ei.a
:Tli qt n41d, rn Carr9CC Br?Pei'+a Ci'1?, Jut pi :°n: B, inGirr: EURtaiflSri,
Page 15 of 16

CHAIN-OF-CUSTODY 1 Analytical Request Document
The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately.
'r-C'- c;/-u ialyLtuai
Page: of
m
Section A Section B
Section C
0 9 6 5 8 3 5 a
Required Client Information: Required Project Information:
Invoice Information:
Company— Report To:
�� �shc_ Ur�d[i
AUention:
e�
• '
.Cz .
❑ NPDES Cl GROUND
WATER Q DRINKING WATER
Address. `' Copy To:
t50 We-stfocIr1 St.
Company Name:
El UST ❑RCRA
ClOther
SYf JC ,Jc, 7 i
Address:
❑GA ❑IL 0IN ❑MI ❑MN QNC
• •
Email To: Purchase Order No.:
Pace Quote Reference:
❑OH [_I SC CIWI ❑ OTHER
Phone Fax Project Name:
�:1u5• Ss3Lr u v �G31 1 S. Tl1t iGTC."
Pace Project Manager:
i�rr •�f
Filtered(YFN)
Requested Due DatefTAT: Project Number:
Pace Profile #:
Requested
Section D Required Client fnformalion rdATRnf Vand MatnF Codes CODE
Analysis:
Preservatives
OR ICING WATC.17 DW
WT
a
SAMPLE I ❑ WwsTE WATf'ROCPJCT[R 'AM
o
K w9
COLLECTED
501 OLfD SL
One Character per box. OIL OL
WIPE WP
(A-Z, U-9 t .-) AIR
g
a1
0
COMPOSITE START COMPOSITE ENTNGRA9
71
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N q �
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AR
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~ TISSUE TS
u
DATE
TIME DATE TIME
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r = _ = Z ` O
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Lab I.D
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Additional Comments:
•777
' • ' '
SAMPLE CONDITION
Y
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1.zGin�✓" �f?I T /�'%�L � 1 ZIr�✓ �� 7e` l i��T%�
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Pr Name of SAMPLE i/ • t
(� n
SIG of AMPLE /%
DATE Sia ed (MM f DO I YY)
o
v
H
ALL0020r9v.3.31
Mar05
�/
SEE REVERSE 510E FOR INSTRUCTIONS ORiGIIVAL .�+",+J'y - _ _