NCS000295_MONITORING INFO_20190227

A", F'o
STORMWATER DIVISION CODING SHEET
NCS PERMITS
PERMIT NO.
DOC TYPE
O FINAL PERMIT
MONITORING REPORTS
APPLICATION
❑ COMPLIANCE
❑ OTHER
DOC DATE
YYYYMMDD

JACKSON PAPER
MANUFACTURING
FEB 2 7
February 17, 2020
NCDEQ, Division of Water Resources, Information Processing Unit
Attn: Central hilts/eDMR
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
RE: Discharge Monitoring; Report (1st Quarter 2020 DMR)
NPDES Permit No. NCS000295
Jackson Paper Nanufacturing Company
Dear Division of Water Resources:
Please find enclosed Discharge Monitoring Report for Jackson Paper Manufacturing Company
NPDES Permit No. NICS000295 for reporting period starting January 1, 2020 and ending March
31, 2020.
Results from samples taken on January 24, 2020 show benchmark exceedances at Outfaall 003 for
1"SS and COD. Outfall 003 drains the areas around the boiler and sawdust/fuel receiving and
storage, boiler ash pit and boiler ash ponds, the recycle pulp facility, paper bale receiving clock and
storage, several masonry storage buildings for spare equipment and the railroad tracks. We will
continue our housekeeping efforts in these areas, including thorough cleaning of drainage ditches.
Per our current Tier Two response for Outfall 003, we will continue to conduct monthly monitoring
and reporting for all parameters at Outfall 003. Monthly (analytical and qualitative) monitoring
Will continue until three consecutive sample results are below the benchmark values. We will also
continue to monitor for all parameters in the receiving water (Scott's Creek) directly upstream and
downstream of the monitoring point in accordance with the Tier Two response.
NORTH CAROLINA'S LARGEST RECYCLED PAPER PRODUCER
152 Wr;T MAIN S'i'RI A 6) PO Box 667e Svi,vA, NC 28779 TE(. [phone] FAX [phone]

Results. from samples for Outfall 001 show a benchmark cxceedancc foI- TSS. OutfAll 001 is
located at a catch basin in the middle of the facility's front parking lot. The basin collects runoff
from the employee and visitor parking areas, roof drains Ironl the office building, and dclive[y
truck loadirlglunloading clocks. Portions of West Main Street, located cast of the facility; slopes
towards the facility so that stornlwater from till-, section of roadway runs 10\4'ardS OUtfall 001.
Recent ]sigh -water levels and flooding in Scott's Creek have caused Several episodes of water
backing up and flooding the fi-ont parking lot, potentially contributing to TSS. We will continue
with regular sweeping of the parking lots in an effort to bring TSS below the benchmark.
I certify that based on information and belief formal front reasonable inquiry, the statements and
information ill file doctmlent are true, accurate, and complete.
Please contact Kicsha Bridges at [phone] 226 If you have ally clucstiouS or need ally
additional ]llforlllatlon.
Sine cly,
Carr Tynda 1
President / Chief Operating Officer
Jackson Paper Manufacturing Company
Enclosure: Stormwater Discharge Monitoring Report
cc: JPMC File

Stormwater Discharge Outfall (SDO)
Monitoring Report
Permit'Number NCS000295
Facility ,Name: Jackson Paper Manufacturing Company
Person Collecting Samples: Kiesha Bridges
Certified Laboratory: Pace Analytical Services, LLC Project # 92462190
Samples Collected During Calendar Year: 2020
(This monitoring report shall be received by the Division no later than 30 days from the date the
facility receives the sampling results from the laboratory.)
Count•: Jackson
Pho xt. 226
'ATURE OF PERJOITTFE OR DESIGNEE)
By this signature. 1 certify that this report is accurate
and complete to the nest of my knowledge.
Oil and Grease
Turbidity
TSS
pH
COD
Benchmark
15
50
(6-9)
120
Benchmark
No
Benchmark
Benchmark
Benchmark
Date
Result
Result
Result
Result
Result
Outfall
Exceedance
Benchmark
Exceedance
Exceedance
Exceedance
Sampled
ma/L
YIN
N'TU
m /L
YIN
YIN(mg/I,)
YIN
1/24/20
001
ND
No
17.9
64.0
Yes
6.6
No
25.3
\°o
8:45am
1/24/20
402
N D
No
5.2
4.5
No
6.8
No
ND
No
g:SOam
1/24/20
003
ND
No
474.0
216.0
Yes
7.1
No
200.0
Yes
9:00am
1/24/20
004
ND
No
16.0
33.7
No
6.4
No
25.3
No
9:1 Oam
Creek Pre
1/24/19
ND
N/A
1.7
1 L5
N/A
6.2
N/A
ND
NIA
,mill
9:25am
Creek Post
1124/ 99
*See
N/A
7.0
17.2
N/A
6.3
NIA
ND
NIA
Mill
9:45am
Note
ND: Not detected at or above adjusted reporting limit.
*Note: Pace sample 92462190006 (creek Past Mill Oil & Grease) broke as container mode contact with another laboratory sample during fog -in at Pace analytical Huntersville.
A letter from the Quality Assurance Manager at Pace is attached to this report.
Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? _Yes x No
iNleasurcable
Storm Event?
Yes
0.38

Storm Event Characteristics:
Date: January 24,2020
Total'event precipitation (inches):
Duration of storm event: —4 hours
Estimated volume of discharge sal
Time since last rain event: 4 days
Drainal
I
it
Area (acres)
Area (sf)
Volume (cf)
1.69
73,616
2,331
5.43
236,531
7,490
IOl[urie-ieall
17.437 �
56.026
Area
III IV
20.45 1.77
890,802 77,101
1.
Mail Original and one copy to:
Division of Water Quality
Attn: Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who
manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and
belief, true, accurate, and omplele. I am aware that there are significant penalties for submitting false information, including the possibility of fines
and im o Xkf lations."
(Signature of Per ittee) (Date)

(�55? ie A na lyfical
January 27, 2020
Jackson Paper Mfg. Co.
152 West Main St., Sylva NC 28779
Dear Keisha Bridges,
Pace Analytical. Services, LLC is committed to providing high quality
results and exemplary customer service to our clients. Pace received
samples for project `Stormwater 111 Quarter 2020' (Pace project
92.462190) on 1/25/2020 at our Huntersville laboratory.
Unfortunately, sample `Creek Postmill' (Pace sample 92462190006)
broke as the container made contact- with another laboratory sample
during log -in. We will strive to minimize occurrences such as these
in the future.
We apologize for any inconvenience or interruptions caused by this
and appreciate the opportunity to support your analytical needs.
Please do not hesitate to contact me or Taylor Ezell if you have any
questions or require additional information.
Sincerely,
ks,� IZZ9_1 __
Ross Simmons
Quality Assurance Manager
[c] 704.977,0959 [C] 704.875.9092
[e-mail]
9800 Kincey Avenue, Suite 100, Huntersville, NC 28078
PACELABS.COM

leAnaVical"
www.pacelabs.com .
February 04, 2020
Kiesha Bridges
Jackson Paper Mfg. Co.
152 West Main St.
Sylva, NC 28779
RE: Project: STORMWATER 1ST QUARTER 2020
Pace Project No.: 92462190
Pace Analytical Services, LLC
2225 Riverside dr.
Asheville, NC 28804
[phone]
Dear Kiesha Bridges:
Enclosed are the analytical results for sample(s) received by the laboratory on January 24, 2020.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNIINELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Chris Derouen
[e-mail]
[phone]
Project Manager
Enclosures
cc: Keisha Bridges, Jackson Paper Mfg. Co.
p4 pccj?
a `"o
qe0 Air
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 18

aceAnalytical
www.pacdabs.com
CERTIFICATIONS
Project: STORMWATER 1 ST QUARTER 2020
Pace Project No.: 92462190
Pace Analytical Services Charlotte
Pace Analytical Services, LLC
2225 Riverside Dr,
Asheville, NC 28804
[phone]
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
South Carolina Certifiication #: 99006001
LeuisianalNELAP Certification # LA170028
Florida/NELAP Certification #: E87627
North Carolina Drinking Water Certification #: 37706
Kentucky UST Certification #: 84
North Carolina Field Services Certification #: 5342
VirginiaNELAP Certification #: 460221
North Carolina Wastewater Certification #: 12
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
FlaridalNELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
VirginiaNELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not he reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 18

aceAnalytiol
WWW.pacelrtbs.rom
Project: STORMWATER 1ST QUARTER 2020
Pace Project No.: 92462190
Lab ID Sample 10
92462190001 OUTFALL #1
92462190002 OUTFALL #2
92462190003 OUTFALL #3
92462190004 OUTFALL #4
92462190005 CREEK PREMILL
92462190006 CREEK POSTMILL
SAMPLE ANALYTE COUNT
Method
EPA 1664E
EPA 180.1 Rcv 2.0 1993
SM 254OD-2011
EPA 9040C
SM 5220D-2011
EPA 1664B
EPA 180.1 Rev 2.0 1993
SM 2540D-2011
EPA 9040C
SM 5220D-2011
EPA 1664B
EPA 180.1 Rev 2.0 1993
SM 254OD-2011
EPA 9040C
SM 5220D-2011
EPA 1664B
EPA 180.1 Rev 2.0 1993
SM 254OD-2011
EPA 9040C
SM 5220D-2011
EPA 1664E
EPA 180.1 Rev 2.0 1993
SM 2540D-2011
EPA 9040C
SM 5220D-2011
EPA 180.1 Rev 2.0 1903
SM 254OD-2011
EPA 9040C
SM 5220D-2011
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
2225 Riverside dr.
Asheville, NC 28804
[phone]
Analysts
Analytes
Reported
Laboratory
WAM
1
PASI-C
JPi.
1
PASI-A
CJL
1
PASI-A
SMK
1
PASI-A
NAL
1
PASI-A
WAM
1
PASI-C
JP1
1
PASI-A
CJL
1
PASI-A
SMK
1
PASI-A
NAL
1
PASI-A
WAM
1
PASI-C
JP1
1
PASI-A
CJL
1
PASI-A
SMK
1
PASI-A
NAL
1
PASI-A
WAM
1
PASI-C
J131
1
PASI-A
CJL
1
PASI-A
SMK
1
PASI-A
NAL
1
PASI-A
WAM
1
PASI-C
JP1
1
PASI-A
CJL
1
PASI-A
SMK
1
PASI-A
NAL
1
PASI-A
JPi
1
PASI-A
CJL
1
PASI-A
SMK
1
PASI-A
NAL
1
PAS4-A
Page 3 of 18

Pace Analytical Services, LLC
of
laceAnalXical 2225 Riverside for.
Asheville, NC 28804
www.pactlabs.com [phone]
ANALYTICAL RESULTS
Project: STORMWATER 1ST QUARTER 2020
Pace Project No.: 92462190
Sample: OUTFALL #1 Lab ID: 92462190001 Collected: 01/24/20 08:45 Received: 01/24/20 12:57 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
1664 SGT-HEM, TPH
Analytical Method: EPA 1664E
Total Petroleum Hydrocarbons
ND mg/L
5.0 1
02/04/20 10:21
180.1 Turbidity
Analytical Method: EPA 180.1 Rev 2.0
1993
Turbidity
17.9 NTU
1.0 1
01125/20 04:35
25400 Total Suspended Solids
Analytical Method: SM 254OD-2011
Total Suspended Solids
64.0 mglL
8.3 1
01/29/20 17:28
9040 pH
Analytical Method: EPA 9040C
pH at 25 Degrees C
6.6 Std. Units
0.10 1
02/02/20 15:05 H3
52200 COD
Analytical Method: SM 5220D-2011
Preparation Method:
SM 5220D-2011
Chemical Oxygen Demand
25.3 mg1L
25.0 1
02/02120 13:31 02/04/20 09:19
REPORT OF LABORATORY ANALYSIS
This report shall not he reproduced, except in full,
Date: 0210412020 04:10 PM without the written consent of Pace Analytical Services, LLC. Page 4 of 18

IeAnalytrcal
www.pacelabs.tom
ANALYTICAL RESULTS
Pace Analytical Services, LLC
2225 Riverside Or.
Asheville, NC 28804
[phone]
Project: STORMWATER 1ST QUARTER 2020
Pace Project No.: 92462190
Sample: OUTPALL #2 Lab ID: 92462190002 Collected: 01/24/20 08:50 Received: 01/24/20 12:57 Matrix: Water
Parameters Results Units Report Limit OF Prepared Anaiyzed CAS No. Qual
1664 SGT-HEM, TPH
Analytical Method: EPA 1664B
Total Petroleum Hydrocarbons
ND mg1L 5.0 1
02/04/20 10:21
180.1 Turbidity
Analytical Method: EPA 180.1 Rev 2.0 1993
Turbidity
5.2 NTU 1.0 1
01/25/20 04:38
2540D Total Suspended Solids
Analytical Method: SM 254OD-2011
Total Suspended Solids
4.5 mgI 4.2 1
01/29120 17:28
9040 pH
Analytical Method: EPA 9040C
pH at 25 Degrees C
6.8 Std. Units 0A0 1
02/02/20 15:17 H3
5220D COD
Analytical Method: SM 5220D-2011 Preparation Method:
SM 5220D-2011
Chemical Oxygen Demand
ND rng1L 25.0 1
02/02/20 13:31 02/04120 09:20
REPORT OF LABORATORY ANALYSIS
This report Shall not he reproduced, except in full,
Date: 02/04/2020 04:10 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 18

(�55'cieAnalXical"
www.pacdahs.com
ANALYTICAL RESULTS
Pace Analytical Services, LLC
2225 Riverside Dr,
Asheville, NC 28804
[phone]
Project: STORMWATER 1ST QUARTER 2020
Pace Project No,: 92462190
Sample: OUTFALL #3 Lab ID: 92462190003 Collected: 01/24/20 09:00 Received: 01124/20 12:57 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
1664 SGT-HEM, TPH
Analytical Method: EPA 16643
Total Petroleum Hydrocarbons
ND rng1L
5.0 1
02/04/20 10:21
180.1 Turbidity
Analytical Method: EPA 180.1 Rev 2.0
1993
Turbidity
474 NTU
1.0 1
01125/20 04:39
254013 Total Suspended Solids
Analytical Method: SM 254OD-2011
Total Suspended Solids
216 m91L
50.0 1
01/29/20 17:28
9040 pH
Analytical Method: EPA 9040C
pH at 25 Degrees C
7.1 Std, Units
0.10 1
02/02/20 15:22 H3
522GD COD
Analytical Method: SM 5220D-2011
Preparation Method:
SM 5220D-2011
Chemical Oxygen Demand
200 mg1L
25.0 1
02/02/20 13:31 02/04/20 09:20
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02104/2020 04:10 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 18

5ceAna1j&a1"
www.pacdahs.com
ANALYTICAL RESULTS
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project: STORMWATER 1ST QUARTER 2020
Pace Project No.: 92462190
Sample: OUTFALL #4 Lab lD: 92462190004 Collected: 01/24120 09:10 Received: 01/24120 12:57 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
1664 SGT-HEM, TPH
Analytical Method: EPA 1664B
Total Petroleum Hydrocarbons
ND mglL 5.0 1
02/04/20 10:21
180.1 Turbidity
Analytical Method: EPA 180.1 Ruv 2.0 1993
Turbidity
16.0 NTU 1.0 1
01/25/20 04:40
25401) Total Suspended Solids
Analytical Method: SM 254OD-2011
Total Suspended Solids
33.7 mglL 83 1
01/29/20 17:28
9040 pH
Analytical Method: EPA 9040C
pH at 25 Degrees C
6.4 Std. Units 0.10 1
02/02120 15:28 H3
5220D COD
Analytical Method: SM 5220D-2011 Preparation Method: SM 5220D-2011
Chemical Oxygen Demand
25.3 mglL 25.0 1
02/02/20 13:31 02/04/20 09:21
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/04/2020 04:10 PM without the written consent of Pace Analytical Services, LLC. Pago 7 of 18

(�IacieAnalytical
www.pacelabs.com
ANALYTICAL RESULTS
Pace Analytical Services, LLC
2225 Riverside Dr,
Asheville, NC 28804
[phone]
Project: STORMWATER 1 ST QUARTER 2020
Pace Project No.: 92462190
Sample: CREEK PREMILL Lab ID: 92462190005 Collected: 01/24/20 09:25 Received: 01/24/20 12:57 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
1664 SGT-HEM, TPH
Analytical Method: EPA 1664B
Total Petroleum Hydrocarbons
ND mg/L
5.0
1
02/04/20 10:21
180.1 Turbidity
Analytical Method: EPA 180.1 Rev 2.0 1993
Turbidity
1.7 NTU
1.0
1
01125/20 04:43
2540D Total Suspended Solids
Analytical Method: SM 2540D-2011
Total Suspended Solids
11.5 mg1L
2.5
1
01129/20 17:29
9040 pH
Analytical Method: EPA 9040C
pH at 25 Degrees C
6.2 Std. Units
0.10
1
02102/20 15:34 H3
5220D COD
Analytical Method: SM 5220D-2011
Preparation Method: SM 5220D-2011
Chemical Oxygen Demand
ND mglL
25.0
1
02/02/20 13:31 02/04/20 09:21
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/04/2020 04:10 PM without the written consent of Pare Analytical Services, LLC. Page, 8 of 18

Pace Analytical Services, LLC
2225 Riverside Dr.
(�IacieAnalytical Asheville, NC 28804
www.pacolibi.com [phone]
ANALYTICAL RESULTS
Project: STORMWATER 1ST QUARTER 2020
Pace Project No.: 92462190
Sample: CREEK POSTMILL Lab ID; 92462190006 Collected: 01/24/20 09:45 Received: 01/24/20 12:57 Matrix: Water
Parameters Results Units Report limit DF Prepared Analyzed CAS No. Qual
180.1 Turbidity
Analytical Method: EPA 180.1 Rev 2.O 1993
Turbidity
7.0 NTU
1.0 1 01125/20 04:47
2540D Total Suspended Solids
Analytical Method: SM 2540D-2011
Total Suspended Solids
17.2 mglL
2.5 1 01/29/20 17:29
9040 pH
Analytical Method: EPA 9040C
pH at 25 Degrees C
6.3 Std. Units
0.10 1 02/02/20 15:39 H3
5220D COO
Analytical Method: SM 5220D-2011
Preparation Method: SM 5220D-2011
Chemical Oxygen Demand
ND mglL
25.0 1 02/02/20 13:31 02104/20 (19:21
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/04/2020 04:10 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 18

lacieAnalyfil
ulm.pariflaha.com
QUALITY CONTROL DATA
Project: STORMWATER 1ST QUARTER 2020
Pace Project No.: 92462190
QC Batch: 522995 Analysis Method: EPA 1664E
QC Batch Method: EPA 1664E Analysis Description: 1664 SGT-HEM, TPH
Associated Lab Samples: 92462190001, 92462190002, 92462190003, 92462190004, 92462190005
METHOD BLANK: 2796837 Matrix: Water
Associated Lab Samples: 92462190001, 92462190002. 92462190003, 92452190004, 92462190005
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Total Petroleum Hydrocarbons mg/L ND 5.0 02/04/20 10:01
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
LABORATORY CONTROL SAMPLE:
2796838
Spike LCS
LCS
% Rec
Parameter
Units
Conc. Result
% Rec
Limits
Qualifiers
Total Petroleum Hydrocarbons
mg/L
20 18.9
94
64-132
MATRIX SPIKE SAMPLE:
2796839
70119974001 Spike
MS
MS
% Rec
Parameter
Units
Result Conc.
Result
% Rec
Limits Qualifiers
Total Petroleum Hydrocarbons
i
<5.0 20
19.9
80
64-132
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
phis reporl shall not he reproduced, except in full,
Date: 02/04/2020 04A 0 PM without the written censent of Pace Analytical Services, LLC. Page 10 of 18

acmnalyfical
www.pardabi.com
Pace Analytical Services, L,LC
2225 Riverside Dr.
Asheville, i 2BB04
[phone]
QUALITY CONTROL DATA
Project: STORMWATER 1ST QUARTER 2020
Pace Project No.: 9246219D
QC Batch: 521382
Analysis Method: EPA 180.1 Rev 2.0 1993
QC Batch Method: EPA 180.1 Rev 2.0 1993
Analysis Description: 180.1 Turbidity
Associated Lab Samples: 92462190001, 92462190002,
92462190003, 92462190004, 92462190005, 92462190006
METHOD BLANK: 2789479
Matrix: Water
Associated Lab Samples: 92462190001, 92462190002,
92462190003, 92462190004, 92462190005, 92462190006
Blank Reporting
Parameter Units
Result Limit Analyzed Qualifiers
Turbidity NTU
ND 1.0 01/25/20 04:31
LABORATORY CONTROL SAMPLE: 2789480
Spike LCS LCS % Rec
Parameter Units
Conc. Result % Rec Limits Qualifiers
Turbidity NTU
10 10.0 100 90-110
SAMPLE DUPLICATE: 2789481
92462173001 Dup
Parameter Units
Result Result RPD Qualifiers
Turbidity NTU
ND .74J
SAMPLE DUPLICATE: 2789482
92462231002 Dup
Parameter Units
Result Result RPD Qualifiers
Turbidity NTU
82.3 82.8 1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/04/2020 04:10 PM without the written consent of Pace Analytical Services, i Page 11 of 18

lacmnalyfical'
WW.pacelabs.com
QUALITY CONTROL DATA
Project: STORMWATER 1ST QUARTER 2020
Pace Project No.: 92462190
QC Batch: 522169 Analysis Method: SM 2540D-2011
QC Batch Method: SM 254OD-2011 Analysis Description: 2540D Total Suspended Solids
Associated Lab Samples: 92462190001, 92462190002, 02462190003, 92462190004, 92462190005, 92462190006
METHOD BLANK: 2792923 Matrix: Water
Associated Lab Samples: 924fi2190001, 92462190002, 92462190003, 92462190004, 92462190005, 92462190006
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Total Suspended Solids mglL ND 2.5 01/29120 17:24
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28844
[phone]
LABORATORY CONTROL SAMPLE: 2792924
Spike LCS LCS % Rec
Parameter Units Conc, Result % Rec Limits Qualifiers
Total Suspended Solids mglL 250 242 97 90-110
SAMPLE DUPLICATE: 2792925
92462700001 Dup
Parameter Units Result Result RPD Qualifiers
Total Suspended Solids mglL 1500 2520 51 D6
SAMPLE DUPLICATE: 2792926
92452206001 Dup
Parameter Units Result Result RPD Qualifiers
Total Suspended Solids mg1L 26.5 28.5 7
Results presented on this page are In the units Indlcated by the "units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report Shall not he reproduced, except in full.
Date: 02/04/2020 04:10 PM without the written consent of Pace Analytical Services, LLC.
Page 12 of 18

(�IaneAnalXical"`
WW.pacallbsrotn
QUALITY CONTROL DATA
Project: STORMWATER 1ST QUARTER 2020
Pace Project No.: 92462190
QC Batch: 522696 Analysis Method: EPA 9040C
QC Batch Method: EPA 9040C Analysis Description: 9040 pH
Associated Lab Samples: 92462190001, 92462190002, 92462190003, 92462190004, 92462190005, 92462190006
SAMPLE DUPLICATE: 2795606
92461323004 Dup
Parameter Units Result Result RP❑ Qualifiers
pH at 25 Degrees C Std. Units 7.7 7.6 1 H3
SAMPLE DUPLICATE: 2795607
92462190001 Dup
Parameter Units Result Result RPD Qualifiers
pH at 25 Degrees C Std. Units 6.6 6.1 7 H3
Pace Analytical Services, LLC
2225 Riverside dr.
Asheville, NC 28804
[phone]
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the tight of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/0412020 04:10 PM without the written consent of Pace Analytical Services, LLC.
Page 13 of 18

aceAnalytical
www.pacelabs.com
QUALITY CONTROL DATA
Project: STORMWATER 1ST QUARTER 2020
Pace Project No.: 92462190
QC Batch: 522721 Analysis Method: SM 52200-2011
QC Batch Method: SM 52200-2011 Analysis Description: 5220D COD
Associated Lab Samples: 92462190001, 92462190002, 92462190003, 92462190004, 92462190005, 92462190006
METHOD BLANK: 2795706 Matrix: Water
Associated Lab Samples: 92462190001, 92462190002, 92462190003, 92462190004, 92462190005, 92462190006
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Chemical Oxygen Demand mg/L ND 25.0 02/04/20 09:13
LABORATORY CONTROL SAMPLE: 2795707
Spike
Parameter Units Conc.
Chemical Oxygen Demand mg/L 750
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
LCS LCS % Rec
Result % Rec Limits Qualifiers
764 102 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2795708 2795709
MS MSD
2628234001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc, Conc. Result Result % Rec % Rec Limits RPD Qua]
Chemical Oxygen Demand 1 1380 100 100 1430 1590 46 207 90-110 11 1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2795710 2795711
MS MSD
92462615001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Chemical Oxygen Demand 1 3010 100 100 2890 2830 -127 -184 90-110 2 M1
Resulls presented on this page are In the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full.
Date: 02/04/2020 04:10 PM without the written consent of Pace Analytical Services, LLC.
Page 14 of 18

(�IaceAnalyticalo
www,puetabs=
QUALIFIERS
Project: STORMWATER 1 ST QUARTER 2020
Pace Project No.: 92462190
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due 10 dilution of the sample aliquot,
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL- Adjusted Method Detection Limit,
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The luwest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services -Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
D6 The precision between the sample and sample duplicate exceeded laboratory control limits.
H3 Sample was received or analysis requested beyond the recognized method holding time.
M1 Matrix spike recovery exceeded QG limits. Batch accepted based on laboratory control sample (LCS) recovery.
R1 RPD value was outside control limits.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/04/2020 04:10 PM without the written consent of Pace Analytical Services, LLG. Page 15 of 18

aceAnalXical
www.pectlabs.com
QUALITY CONTROL
Project: STCRMWATER 1ST QUARTER 2020
Pace Project No.: 92452190
DATA CROSS REFERENCE
Pace Analytical Services, LLC
2225 Riverside 04
Asheville, NC 26604
[phone]
TABLE
Analytical
Lap ID
Sample ID
QC Batch Method
QC Batch Analytical Method
Batch
92462190001
OUTFALL #1
EPA 1664E
522995
92462190002
OUTFALL #2
EPA 1664E
522995
92462190003
OUTFALL #3
EPA 1664E
522995
92462190004
OUTFALL #4
EPA 1664E
522995
92462190005
CREEK PREMILL
EPA 1664E
522995
92462190001
OUTFALL #1
EPA 180.1 Rev 2.0 1993
521382
92462190002
OUTFALL #2
EPA 180.1 Rev 2.0 1993
521382
92462190003
OUTFALL #3
EPA 180.1 Rev 2.0 1993
521382
92462190004
OUTFALL #4
EPA 18D.1 Rev 2.0 1993
521382
92462190005
CREEK PREMILL
EPA 180.1 Rev 2.0 1993
521382
92462190006
CREEK POSTMILL
EPA 180.1 Rev 2.0 1993
521382
92462190001
OUTFALL #1
SM 254OD-2011
522169
92462190002
OUTFALL #2
SM 254OD-2011
522169
92462190003
OUTFALL #3
SM 254OD-2011
522169
92462190004
OUTFALL #4
SM 254OD-2011
522169
92462190005
CREEK PREMILL
SM 254OD-2011
522169
92462190006
CREEK POSTMILL
SM 2540D-2011
522169
92462190001
OUTFALL #1
EPA 9040C
522696
92462190002
OUTFALL #2
EPA 9040C
522696
92462190003
OUTFALL #3
EPA 9040C
522696
92462100004
OUTFALL #4
EPA 9040C
522696
92462190005
CREEK PREMILL
EPA 9040C
522696
92462190006
CREEK POSTMILL
EPA 9040C
522696
92462190001
OUTFALL #1
SM 522OD-2011
522721
SM 5220D-2011
523000
92462190002
OUTFALL #2
SM 5220D-2011
522721
SM 5220D-2011
523000
92462190003
OUTFALL #3
SM 5220D-2011
522721
SM 5220D-2011
523000
92462190004
OUTFALL #4
SM 5220D-2011
522721
SM 5220D-2011
523000
92462190005
CREEK PREMILL
SM 522OD-2011
522721
SM 5220D-2011
523000
92462190006
CREEK POSTMILL
SM 5220D-2011
522721
SM 5220D-2011
523000
REPORT OF LABORATORY ANALYSIS
This report shall not he reproduced, except in full,
Date: 02/64/2020 04:10 PM without the written consent of Pace Analytical Services, LLC. Page 16 of 18

wo# : 9246219®
CHAIN -OF -CUSTODY Analytical Request Document LAB USE ONLY-/
-P ceAnalytrcal' I
r
Chain-oi•Custody is a LEGAL DOCUMENT - Complete at] relevent fields
Company: Billing Information: ALL 924621SO
J gm
Ad IVG,1p 7 rI Container PreservativeT e " Lab Project Manager:
13 w j� Czjti Sit _.•F l3^Jl�'s�7�
�Of[ TOt";,,, / 'J
t r . r t\ f 1Cl�j� •�
n'J it To: _
r t (.�GC' C'-� I�!C �� Y7 �:V:�• • t t
•' Preservative Types: (1) nitric acid, (2)
(6) melhanol, (7) sodium bisulfate, (3) sodium
(t) ammonium hydroxide, (D) TSP, (Ul UnWeserved.
sulfuric acid, (3) hydrochloric acid, (4) sodium hydroxide, I5) zinc acetate,
thiasulfate• (9) hexane, (A) ascorbic acid, (B) ammonium sulfate,
40) Other
Copy To:
Site Collecti6n Info/AttSress:
5
Analyses
Lab Profile/line:
5:,(��(i c(t C.v. C.C(0r-4
Customer Project Name/Number:
State: County/City: • Time Zone Collected:
'ET
Lab Sample Receipt Checklist:
PT [ 1 MT ( 1 CT (.-I
`j
Custody Seals Present/Intact Y ry NA
Custody Sign9tures Present Y N lit NA
Collector_ Si nature Present NA
Phone: 5. 3�1
Site/Facility ID q:
Corppliance Monitoring?
I • Yes ( ) NO
Email:
Bottles Intact N Mk
Correct sorties N tJA
Collected By (print):
Purchase Order p: C' s
DW PWS l0 !!;
`� i t �'} k t. + iir�
t
�-
Quote k:
DW Location Code:
4!�
r
L-
Sufficient volunva N ttA
Samples Received on Ice N taA
voA - Headspace Acceptable Y N iA
UR SDA Y N•
Collected By [Signature):
Turnaround Date Required; f
Immediately Pace on Ice:
'
%1_�,�(,y •�sc.s.
/�G
['y} Ves ( } No
✓}
1
egulated Soils
samples in Holding Time �N NA
Residual ChlorineArea • t Y OS NA
Sample Disposal: r'
Rush:
Field Filtered (if applicable):
[.I Dispose as appropriate [ I Return
[ ] Same Day [ ) Next Day
I I Yes [' ] No
Cl Strips:
Sample Acceptable (_I)N NA
[ ]Archive'
[ ] 2 Day [ [ 3 pay [ ] 4 Day [ ] 5 Day
Analysis:
y
s,
pH
p8 strips: ^
e�
I E Hold:
[Expedite Charees Apply)
4
`
Sulfide Present Y NA
Lead Acetate Strips:
' Matrix Codes (Insert in Matrix box below): Drinking Water (DW), Ground Water (GW), Wastewater (WW),
Product (P), Soil/Solid (SL), Oil (OL), Wipe (WP), Air (AR), Tissue (TS), Bioassay (B), Vapor (V), Other (OT)
rJ
4+(
l/)
r
-s`
LA 9 115E ONLY:
Lab Sample M I Comments:
Comp /
Collected (or
Composite End
Res
# of
Customer Sample [D
P
Matrix'
Grab
Composite Start)
Cl
Ctns,
Date
time
Date
Time
.f•cii -fi< i
:r-i i cc'f1
G
ll:1`{r:��
��'� -
✓
✓
l/
✓
.-.
Q.: a5z
V
-
fta
*YNCustomer
Remarks / Special Conditions Possible Hazards:
Type of Ice Used: Wet Blue Dry None
SHORT HOLDS PRESENT (<72 hours
N/A
Lab Sample Temperature Info:
Temp Blank Received: Y 0 NA
Therm IM03- 7-0 0/
Packing Material Used:
Lab Tracking 9):
2410276
Cooler 1 Temp Upon Receipt•». i /,Ic
•p�-�
Radchem sample(s) screened (<500 cpm): Y N NtJ
Samples received via:
FEDEX UPS c, t Courier Pace Courier
Cooler 1 Therm Corr. Fact T: 14—'oC
Cooler 1 Corrected Tempr-j�• ' `r oC
Comments:
Relinquished
12 f 677
Received byf/�Companyy::: (Signaturre[[,
Datc/Time: J: 1 7
MT{L LA13 USE ONLY
fable#:
Mpp'41'Date/Time:
�(,ffi!(iif �f
fl/ ' I��
�- i��
Acctnu m:
Relinquished by/Company: (Signature)
Date/Time:
Received by/Company: (Signature)
Date/Time:
Template:
P Tri Blank Received: Y NA
Prelogin:
HCL McOH TSP ther
Relinquished by/Company: (Signature)
Date/Time:
Received by/Company: (Signature►
DaterCime:
PM:
Non Conform Page:
pg:
,(`-ce(s):
YES / "D of:
i

7J Document Name; Document Revised: February7, 2018
+ Sample Condition Upon Receipt(SCUR) Page 1 of 2
acemalj*al Document No.: Issuing Authority:
F-CAR-CS-033-Rev.06 Pace Carolinas Quality Office
*Check mark top half of box if pH and/or dechlorination is
verified and within the acceptance range for preservation
samples.
Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/8015 (water) DOC, LLHg
**Bottom half of box Is to list number of bottle
Projei WO# • 92462190
PM: COI Due Dale: 02/07/20
CLIENT: 93-Jaokson P
R
U
W
WW1
L
U
^''
V
=
4
V
O
z
b
n
A
d
`
10
?
a
2
_
N
z
�
Cr
V
S
N
G
_
V
C
Z
�
a
Z
z
rt1
Z
1p
r:1
N
n
A
W
a
C
u
vWi
O.
C
7
y
vai
a
C
'
y
d
7
u
D
_�
a
p
Z
S
=
Q
H
n
y
d
a
V
Y
a
'
ti
v
0
N
a
E
Z
m0
N
.j
Z
0
VI
mo
M
Lry
7G
0.
V
2
U
H
N
N
y
Z.
:20
a
y
NO
a
F
w
E
m
a
E
o
9L
pEE
H
E
E
E
5
o
M
a
v
a
r;
E
E
d
J
En
o
¢
>
E
0
a
O
E
p
0
E
0
>
E
a
y
m
E
E
a
E
¢
pp�
E
aE
E
1;
w
H
a
a
m
N
m
a
coca
r0.t
A
to
v
a
m
M
n
ro
V
a
Co
v
a
�
3
_
•-�
U'
a
M
0
¢
M
U
a
.y
�
Q
a
N
m
4D
a
0
m
go
a
Y
m
0
o
m
0
>
VO
I
o
t7
>
0
�
x
O
7
>
N
N
a
c
t'J
Q
V
v�i
}
l7
O
2
1
!
l
3
}
✓
\
\
f
XV
-
6
I
7
8
17
\
12
pH Adjustment Log for Preserved Samples
Sample ID Type of Preservative pH upon receipt Date preservation adjusted Time presrriatlon Amount of Preservative Lat A
adlui I added
Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this farm v II be lent to the North Carolina DEIINR Certification Office (i.e.
Out of hold, incorrect preservative, out of temp, Incorrect containers.
Page 18 of 18