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HomeMy WebLinkAboutNCG030323_MONITORING INFO_20190812j� STORMWATER DIVISION CODING SHEET NCG PERMITS PERMIT NO. �r C 3 b 3 3 DOC TYPE ❑ HISTORICAL FILE ❑MONITORING REPORTS DOC DATE ❑ b .-r V 0 YYYYM M D D STORMWATER DIVISION CODING SHEET NCG PERMITS PERMIT NO. /V c)-3 a DOC TYPE. ❑ HISTORICAL FILE MONITORING REPORTS DOC DATE ❑ a I C I a YYYYMMDD C - PC_j 1 j CONTAINER -PRODUCTS -CORPORATION CONTAINER PRODUCTS CORPORATION 112 North College Road P.O. Box 3767 Wibningmn, NC 28406 Tel. (910) 392-6100 Fax. (910) 392-6778 Web Page: hltp:/hest,m.c-p-ctnet E-mail: qualitv@c-p-c.cum R.FCF15\/FD 7/26/2019 AUG 12 2019 NC DENR, Division Water Quality DENR-LAND QUALITY STORMWATER PERMITTING 1617 Mail Service Center Raleigh, NC 27699-1617 ANNUAL Discharge Monitoring Reports Permit # NCG030323 This letter is for the annual reporting of Water Quality Records. Please find the Report for 2018. Sincerely, Tammy T. Thurston QA Manager CC: Storm Water Records Orlando, FL The results set forth herein are provided by SGS North Amcrica Inc. e-Hardcopy 2.0 Aulornaled Report Technical Report for Container Products Corp Stormwater Sampling; NC SGS Job Number: FA55085 Sampling Date: 06/14/18 Report to: Container Products Corp 112 N College Rd Wilmington, NC 28405 TTN: Tammy Thurston Total number of pages in report: 20 PW� 2 - O i ': 9eORAtO� ZA Test results contained within this data package meet the requirements Caitlin Brlce, M.S. of the National Environmental Laboratory Accreditation Program General Manager and/or state specific certification programs as applicable. Client Service contact: Ken Overstreet 407-425-6700 Ceriifrcatiow: FL(E83510), LA(03051), KS(E-10327), IL(200063), NC(573), NJ(FIM2), NY(12022), SC(96038001) Don ELAP(ANAB L2229), AZ(AZ0806), CA(2937), TX(r104704404), PA(68-03573), VA(460177), AK, AR, IA, KY, MA, MS, ND, NH, NV. OK, OR. UT, WA, WV This report shall not be reproduced, except in Its entirety, without the written approval of SGS. Test remits relate only to samples analyzed. SGS North America Inc. • 4405 Vineland Road • Suite C-15 • Orlando, FL 32811 • tel: 407A25-6700 • fax: 407-425-0707 SGS is the sole authority for authorizing edits or modifications to this document. Please share your ideas about Unauthorized modification of this report is strictly prohibited. how we can serve you better at: Review standard terms at: http://www.sgs.conVenItcr -md-conditions EHS.US.CmtomerC=@sgs.com 4 of 20 FA55085 Table of Contents -1- Section1: Sample Summary................................................................................................... Section2: Summary of Hits.................................................................................................... Section3: Sample Results........................................................................................................ 3.1: FA55085-1: FRONT DRAIN....................................................................................... 3.2: FA55085-2: BACK DRAIN......................................................................................... Section4: Misc. Forms............................................................................................................ 4.1: Chain of Custody........................................................................................................... Sections: a 3 4 5 12 18 19 2 of 20 —SGSr FA55055 SGS North America Inc. Sample Summary Container Products Corp Stormwater Sampling; NC Job No: FA55085 ample Collected Matrix Client lumber Date Time By Received Code Type Sample ID FA55085-1 06/14/18 00:00 TT 06/15/18 AQ Water FRONT DRAIN FA55085-2 06/14/18 00:00 TT O6/15/18 AQ Water BACK DRAIN 0 3 of 20 -O�� Y FA5W85 Summary of Hits Job Number: FA55085 Account: Container Products Corp Project: Stormwater Sampling: NC Collected: 06/14/18 Lab Sample ID Client Sample ID Result/ Analyte Qual RL MDL Units Method FA55095-1 FRONT DRAIN Page 1 of I Fluoranthene 0.60 J 4.8 0.53 ug/l EPA 625 Endosulfan-I a 0.081 0.0095 0.0015 ug/1 SW846 8081B Zinc 119 20 ugh SW846 6010D pH b 7.43 so SM4500H B-11/SW9040C FA55085-2 BACK DRAIN 4,4'-DDD a 0.0061 J 0.019 0.0048 ug/l SW846 8081B 4,4'-DDE c 0.0057 J 0.019 0.0048 ug/l SW846 8081B Endrin c 0.011 J 0.019 0.0020 ug/I SW846 8081B Endrin aldehyde 0.0060 J 0.019 0.0026 ug/1 SW846 8081E Lead 9.9 5.0 ug/1 SW846 6010D Zinc 392 20 ug/I SW846 6010D Solids, Total Suspended 104 25 mg/1 SM2540 D-I1 pH b 8.07 so SM4500H B-1 l/SW9040C (a) All hits confirmed by dual column analysis. (b) Field analysis required. Received out of hold time and analyzed by request. (c) All hits confirmed by dual column analysis. Primary and confirmation results differ by more than 40%. Lower value reported due to possible coelution. (�� 4 of 20 SG r FA55885 SGSf Orlando, FL Sample Results Report of Analysis Section 3 ' S of 20 SGSr FA55885 SGS North America Inc. Report of Analysis it Sample ID: FRONT DRAIN Sample ID: FA55085-1 ,ix: AQ - Water rod: EPA 625 EPA 625 ect: Stormwater Sampling: NC File ID DF Analyzed By #1 61701395.1) 1 06/21/18 22:05 WH #2 Initial Volume Final Volume Run #1 1050 ml 1.0 ml Run #2 ABN Special List Page 1 of 2 Date Sampled: 06/14/18 Date Received: 06/15/18 Percent Solids: n/a Prep Date Prep Batch Analytical Batch 06/21/18 12:10 OP70597 S6F52 CAS No. Compound Result RL MDL Units 59-50-7 4-Chloro-3-methyl Phenol ND 4.8 0.56 ug/l 95-57-8 2-Chlorophenol NO 4.8 0.60 ug/I 120-83-2 2,4-Dichlorophenol NO 4.8 0.80 ug/I 105-67-9 2,4-Dimethylphenol NO 4.8 0.70 ug/I 51-28-5 2,4-Dinitrophenol NO 24 4.8 ug/I 534-52-1 4,6-Dinitro-o-cresol NO 9.5 1.9 ug/I 88-75-5 2-Nitrophenol NO 4.8 0.81 ug/l 100-02-7 4-Nitrophenol NO 24 4.8 ug/I 87-86-5 Pentachlorophenol NO 24 4.8 ug/l 108-95-2 Phenol NO 4.8 0.48 ug/l 88-06-2 2,4,6-Trichlorophenol NO 4.8 0.72 ug/I 83-32-9 Acenaphthene NO 4.8 0.60 ug/I 208-96-8 Acenaphthylene NO 4.8 0.61 ug/I 120-12-7 Anthracene NO 4.8 0.76 ug/I 92-87-5 Benzidine a NO 24 4.8 ug/1 56-55-3 Benzo(a)anthracene ND 4.8 0.72 ug/I 50-32-8 Benzo(a)pyrene NO 4.8 0.75 ug/I 205-99-2 Benzo(b)fluoranthene ND 4.8 0.74 ug/I 191-24-2 Benzo(g,h,i)perylene ND 4.8 0.78 ug/I 207-08-9 Benzo(k)fluoranthene NO 4.8 0.82 ug/I 101-55-3 4-Bromophenyl Phenyl Ether ND 4.8 0.81 ug/l 85-68-7 Butyl Benzyl Phthalate NO 4.8 0.95 ug/l 111-91-1 bis(2-Chloroethoxy)methane ND 4.8 0.77 ug/I 111-44-4 bis(2-Chloroethyl)ether NO 4.8 0.70 ug/I 108-60-1 2,2'-Oxybis(1-chloropropane) NO 4.8 0.72 ug/I 91-58-7 2-Chloronaphthalene NO 4.8 0.48 ug/I 7005-72-3 4-Chlorophenyl Phenyl Ether NO 4.8 0.51 ug/l 218-01-9 Chrysene NO 4.8 0.81 ug/I 53-70-3 Dibenzo(a,h)anthracene NO 4.8 0.77 ug/I 95-50-1 1,2-Dichlorobenzene NO 4.8 0.48 ug/I 541-73-1 1,3-Dichlorobenzene NO 4.8 0.48 ugfl I06-46-7 1,4-Dichlorobenzene ND 4.8 0.48 ug/I Lea NO = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 6 of 20 FA55085 SGS North America Inc. Report of Analysis Page 2 of 2 Client Sample ID: FRONT DRAIN Lab Sample ID: FA55085-1 Date Sampled: 06/14/18 Matrix: AQ - Water Date Received: 06/15/18 Method: EPA 625 EPA 625 Percent Solids: n/a Project: Slormwater Sampling: NC ABN Special List CAS No. Compound Result RL MDL Units Q 91-94-1 3,3'-Dichlorobenzidine ND 4.8 0.61 ug/I 84-66-2 Diethyl Phthalate NO 4.8 0.95 ug/I 131-11-3 Dimelhyl Phthalate NO 4.8 0.95 ug/l 84-74-2 Di-n-butyl Phthalate NO 4.8 0.95 ug/l 117-84-0 Di-n-octyl Phthalate NO 4.8 0.95 ug/l 121-14-2 2,4-Dinitrotoluene NO 4.8 0.77 ug/I 606-20-2 2.6-Dinitrotoluene ND 4.8 0.68 ug/l 122-66-7 1,2-Diphenylhydrazine ND 4.8 0.72 ug/I 117-81-7 bis(2-Ethylhexyl)phthalate ND 4.8 0.95 ug/l 206-44-0 Fluoranthene 0.60 4.8 0.53 ug/I 86-73-7 Fluorene ND 4.8 0.67 ug/I 118-74-1 Hexachlorobenzene NO 4.8 0.66 ug/I 87-68-3 Hexachlorobutadiene ND 4.8 0.48 ug/I 77-47-4 Hexachlorocyclopentadiene NO 4.8 1.7 ug/l 67-72-1 Hexachloroethane NO 4.8 1.6 ug/I 193-39-5 Indeno(1,2,3-cd)pyrene ND 4.8 0.68 ug/l 78-59-1 Isophorone NO 4.8 0.74 ug/I 91-20-3 Naphthalene NO 4.8 0.48 ug/I 98-95-3 Nitrobenzene ND 4.8 0.89 ug/I 62-75-9 N-Nitrosodimethylamine ND 4.8 0.48 ug/I 621-64-7 N-Nitrosodi-n-propylamine ND 4.8 0.64 ug/I 86-30-6 N-Nitrosodiphenylamine b ND 4.8 0.77 ug/I 85-01-8 Phenanthrene NO 4.8 0.82 ug/I 129-00-0 Pyrene ND 4.8 0.65 ug/I 120-82-1 1,2,4-Trichlorobenzene ND 4.8 1.0 ug/l CAS No. Surrogate Recoveries Run# I. Run# 2 Limits 367-12-4 2-Fluorophenol 23% 14-67% 4165-62-2 Phenol-d5 13% 10-50% 118-79-6 2,4,6-Tribromophenol 82% 33-118% 4165-60-0 Nitrobenzene-d5 67% 42-108% 321-60-8 2-Fluorobiphenyl 70% 40-106% 1718-51-0 Terphenyl-d14 86% 39-121% (a) Associated ICV outside control limits high, however sample ND. (b) Associated CCV outside control limits high. Sample was ND. j ND = Not detected MDL = Method Detection Limit j = Indicates an estimated value RL = Reporting Limit B = Indicates analyle found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 11` 7 of 20 FA55085 SGS North America Inc Report of Analysis Client Sample ID: FRONT DRAIN Lab Sample ID: FA55085-1 Date Sampled: 06/14/18 Matrix: AQ - Water Date Received: 06/15/18 Method: SW846 8081B SW846 3510C Percent Solids: n/a Project: Stormwaler Sampling; NC Page 1 of 1 File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 a KK89804.D 1 06/22/18 11:43 KL 06/21/18 12:25 OP70598 GKK2866 Run #2 Initial Volume Final Volume Run #1 1050 ml 5.0 ml Run #2 Pesticide PPL List CAS No. Compound Result RL MDL Units Q 309-00-2 Aldrin NO 0.0095 0.0026 ug/I 319-84-6 alpha-BHC NO 0.0095 0.0021 ug/I 319-85-7 beta-BHC b NO 0.0095 0.0024 ug/I 319-86-8 delta-BHC c NO 0.0095 0.0023 ug/I 58-89-9 gamma-BHC (Lindane) NO 0.0095 0.0021 ug/I 12789-03-6 Chlordane NO 0.095 0.036 ug/I 60-57-1 Dieldrin NO 0.0095 0.0023 ug/I 72-54-8 4,4'-DDD c NO 0.019 0.0048 ug/I 72-55-9 4,4'-DDE NO 0.019 0.0048 ug/I 50-29-3 4,4'-DDT NO 0.019 0.0048 ug/I 72-20-8 Endrin ND 0.019 0.0020 ug/I 1031-07-8 Endosulfan sulfate NO 0.019 0.0015 ug/I 7421-93-4 Endrin aldehyde ND 0.019 0.0026 ug/I 959-98-8 Endosulfan-I 0.081 0.0095 0.0015 ug/I 33213-65-9 Endosulfan-II ND 0.0095 0.0014 ug/I 76-44-8 Heptachlor ND 0.0095 0.0025 ug/I 1024-57-3 Heptachlor epoxide NO 0.0095 0.0019 ug/I 72-43-5 Methoxychlor NO 0.019 0.0048 ug/I 8001-35-2 Toxaphene ND 0.48 0.20 ug/I CAS No. Surrogate Recoveries Rua# 1 Run# 2 Limits 877-09-8 Tetrachloro-m-xylene 83% 42-127% 2051-24-3 Decachlorobiphenyl 34% 27-127% (a) All hits confirmed by dual column analysis. (b) Associated CCV outside control limits. (c) Associated CCV outside of control limits high, sample was ND. ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyle found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 8 of 20 FA55085 SGS North America Inc. Report of Analysis it Sample ID: FRONT DRAIN Sample ID: FA55085-1 Date Sampled: 06/14/18 rix: AQ - Water Date Received: 06/15/18 rod: SW846 8082A SW846 3510C Percent Solids: n/a ect: Stormwater Sampling; NC Page 1 of 1 File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #I XX070222.D 1 06/25/18 16:37 NJ 06/21/18 12:25 OP70599 GXX1246 Run #2 Initial Volume Final Volume :un #1 1050 ml 5.0 ml 'on #2 PCB List CAS No. Compound Result RL MDL Units Q 12674-11-2 Aroclor 1016 ND 0.095 0.038 ug/I 11104-28-2 Aroclor 1221 a ND 0.095 0.048 ug/1 11141-16-5 Aroclor 1232 NO 0.095 0.048 ug/I 53469-21-9 Aroclor 1242 ND 0.095 0.038 ug/I 12672-29-6 Aroclor1248 NO 0.095 0.038 ug/I 11097-69-1 Aroclor 1254 NO 0.095 0.038 ug/I 11096-82-5 Aroclor 1260 NO 0.095 0.038 ug/I CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 877-09-8 Tetrachloro-m-xylene 126% 38-127% 2051-24-3 Decachlorobiphenyl 48% 25-137% (a) Associated CCV outside of control limits high, sample was ND. ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyze found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound t 9 of 20 -SIGSr FA55085 SGS North America Inc. Report of Analysis Client Sample ID: FRONT DRAIN Lab Sample ID: FA55085-1 Date Sampled: 06/14/18 Matrix: AQ - Water Date Received: 06/15/18 Percent Solids: n/a Project: Stormwater Sampling; NC Page 1 of 1 Total Metals Analysis Analyte Result RL Units DF Prep Analyzed By Method Prep Method Copper <25 25 ug/I 1 06/21/18 06/21/18 LM SW8466010D1 SW8463010A2 Lead <5.0 5.0 ug/I 1 06/21/18 06/21/18 LM SW84660100 SW8463010A2 Zinc 119 20 ug/I 1 06/21/18 06/21/18 LM SW84660101)1 SW8463010A2 (1) Instrument QC Batch: MA14994 (2) Prep QC Batch: MP33912 RL = Reporting Limit 10 of 20 r FA55055 SGS North America Inc. Report of Analysis Client Sample ID: FRONT DRAIN Lab Sample ID: FA55085-1 Date Sampled: 06/14/18 Matrix: AQ - Water Date Received: 06/15/18 Percent Solids: n/a Project: Stormwater Sampling; NC Page 1 of 1 General Chemistry Analyte Result RL Units DF Analyzed By Method HEM Petroleum Hydrocarbo a <5.3 5.3 mg/1 l 06/29/18 14:48 BR EPA 1664A Solids, Total Suspended < 25 25 mg/1 1 06/20/18 17:45 BR SM2540 D-11 pH b 7.43 so 1 06/27/18 12:00 BW SM450011 13-11/SW9040C (a) Associated BS recovery outside control limits. (b) Field analysis required. Received out of hold time and analyzed by request. RL = Reporting Limit M ���� 11 of 20 FA55085 SGS North America Inc. Report of Analysis Page 1 of 2 Client Sample ID: BACK DRAIN Lab Sample ID: FA55085-2 Date Sampled: 06/14/18 Matrix: AQ - Water Date Received: 06/15/18 Method: EPA 625 EPA 625 Percent Solids: n/a Project: Stormwater Sampling; NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 61701396.1) 1 06/21/18 22:31 WH 06/21/18 12:10 OP70597 S61752 Run #2 Initial Volume Final Volume Run #1 1050 ml 1.0 ml Run #2 ABN Special List CAS No. Compound Result RL MDL Units Q 59-50-7 4-Chloro-3-methyl Phenol ND 4.8 0.56 ug/I 95-57-8 2-Chlorophenol ND 4.8 0.60 ug/1 120-83-2 2,4-Dichlorophenol ND 4.8 0.80 ug/I 105-67-9 2,4-Dimethylphenol ND 4.8 0.70 ug/I 51-28-5 2,4-Dinitrophenol ND 24 4.8 ug/I 534-52-1 4,6-Dinitro-o-cresol ND 9.5 1.9 ug/I 88-75-5 2-Nitrophenol ND 4.8 0.81 ug/I 100-02-7 4-Nitrophenol ND 24 4.8 ug/I 87-86-5 Pentachlorophenol ND 24 4.8 ug/I 108-95-2 Phenol ND 4.8 0.48 ug/I 88-06-2 2,4,6-Trichlorophenol ND 4.8 0.72 ug/I 83-32-9 Acenaphthene ND 4.8 0.60 ug/I 208-96-8 Acenaphthylene ND 4.8 0.61 ug/I 120-12-7 Anthracene ND 4.8 0.76 ug/1 92-87-5 Benzidine 0 ND 24 4.8 ug/I 56-55-3 Benzo(a)anthracene ND 4.8 0.72 ug/I 50-32-8 Benzo(a)pyrene ND 4.8 0.75 ug/I 205-99-2 Benzo(b)Buoranthene ND 4.8 0.74 ug/I 191-24-2 Benzo(g,h,i)perylene ND 4.8 0.78 ug/I 207-08-9 Benzo(k)Buoranthene ND 4.8 0.82 ug/I 101-55-3 4-Bromophenyl Phenyl Ether ND 4.8 0.81 ug/I 85-68-7 Butyl Benzyl Phthalate ND 4.8 0.95 ug/I 111-91-1 bis(2-Chloroetboxy)methane ND 4.8 0.77 ug/I 111-44-4 bis(2-Chloroethyl)ether ND 4.8 0.70 ug/I 108-60-1 2,2'-Oxybis(1-chloropropane) ND 4.8 0.72 ug/I 91-58-7 2-Chloronaphthalene ND 4.8 0.48 ug/I 7005-72-3 4-Chlorophenyl Phenyl Ether ND 4.8 0.51 ug/I 218-01-9 Chrysene ND 4.8 0.81 ug/I 53-70-3 Dibenzo(a,h)anthracene ND 4.8 0.77 ug/I 95-50-1 1,2-Dichloro0enzene ND 4.8 0.48 ug/I 541-73-1 1,3-Dichlorobenzene ND 4.8 0.48 ug/I 106-46-7 IA-Dichlorobenzene ND 4.8 0.48 ug/I ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound _SG8� 12 of 20 FA55085 SGS North America Inc. Report of Analysis Page 2 of 2 Client Sample ID: BACK DRAIN Lab Sample ID: FA55085-2 Date Sampled: 06/14/18 Matrix: AQ - Water Date Received: 06/15/18 Method: EPA 625 EPA 625 Percent Solids: n/a Project: Stormwater Sampling; NC ABN Special List CAS No. Compound Result RL MDL Units Q 91-94-1 3,3'-Dichlorobenzidine ND 4.8 0.61 ug/I 84-66-2 Diethyl Phthalate ND 4.8 0.95 ug/I 131-11-3 Dimethyl Phthalate ND 4.8 0.95 ug/I 84-74-2 Di-n-butyl Phthalate ND 4.8 0.95 ug/I 117-84-0 Di-n-oclyl Phthalate ND 4.8 0.95 ug/I 121-14-2 2,4-Dinilrotoluene ND 4.8 0.77 ug/I 606-20-2 2,6-Dinitrotoluene ND 4.8 0.68 ug/I 122-66-7 1,2-Diphenylhydrazine ND 4.8 0.72 ug/I 117-81-7 bis(2-E(hylhexyl)phthalate ND 4.8 0.95 ug/I 206-44-0 Fluoranthene ND 4.8 0.53 ug/I 86-73-7 Fluorene ND 4.8 0.67 ug/I 118-74-1 Hexachlorobenzene ND 4.8 0.66 ug/I 87-68-3 Hexachlorobutadiene ND 4.8 0.48 ug/I 77-47-4 Hexachlorocyclopentadiene ND 4.8 1.7 ug/I 67-72-1 Hexachloroethane ND 4.8 1.6 ug/l 193-39-5 Indeno(1,2,3-cd)pyrene ND 4.8 0.68 ug/I 78-59-1 Isophorone ND 4.8 0.74 ug/I 91-20-3 Naphthalene ND 4.8 0.48 ug/I 98-95-3 Nitrobenzene ND 4.8 0.89 ug/I 62-75-9 N-Nitrosodimethylamine ND 4.8 0.48 ug/I 621-64-7 N-Nitrosodi-n-propylamine ND 4.8 0.64 ug/I 86-30-6 N-Nitrosodiphenylamine b ND 4.8 0.77 ug/I 85-01-8 Phenanthrene ND 4.8 0.82 ug/I 129-00-0 Pyrene ND 4.8 0.65 ug/I 120-82-1 1,2,4-Trichlorobenzene ND 4.8 1.0 ug/I CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 367-12-4 2-Fluorophenol 21% 14-67% 4165-62-2 Phenol-d5 13% 10-50% 118-79-6 2,4,6-Tribromophenol 83% 33-118% 4165-60-0 Nitrobenzene-d5 62% 42-108% 321-60-8 2-Fluorobiphenyl 66% 40-106% 1718-51-0 Terphenyl-dl4 83% 39-121% (a) Associated ICV outside control limits high, however sample ND. (b) Associated CCV outside control limits high. Sample was ND. ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 13 of 20 SG8� FA55085 SGS North America Inc. Report of Analysis Page 1 of 1 Client Sample ID: BACK DRAIN Lab Sample ID: FA55085-2 Date Sampled: 06/14/18 Matrix: AQ - Water Date Received: 06/15/18 Method: SW8468081B SW8463510C Percent Solids: n/a Project: Stormwater Sampling; NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 x KK89805.D 1 06/22/18 12:00 KL 06/21/18 12:25 OP70598 GKK2866 Run #2 Initial Volume Final Volume Run #1 1050 ml 5.0 ml Run #2 Pesticide PPL List CAS No. Compound Result RL MDL Units 309-00-2 Aldrin ND 0.0095 0.0026 ug/I 319-84-6 alpha-BHC ND 0.0095 0.0021 ug/I 319-85-7 beta-BHC ND 0.0095 0.0024 ug/I 319-86-8 delta-BHC ND 0.0095 0.0023 ug/I 58-89-9 gamma-BHC (Lindane) ND 0.0095 0.0021 ug/I 12789-03-6 Chlordane ND 0.095 0.036 ug/I 60-57-1 Dieldrin ND 0.0095 0.0023 ug/I 72-54-8 4,4'-DDD 0.0061 0.019 0.0048 ug/I 72-55-9 4,4'-DDE b 0.0057 0.019 0.0048 ug/I 50-29-3 4,4'-DDT ND 0.019 0.0048 ug/I 72-20-8 Endrin b 0.011 0.019 0.0020 ug/I 1031-07-8 Endosulfan sulfate ND 0.019 0.0015 ug/I 7421-93-4 Endrin aldehyde b 0.0060 0.019 0.0026 ug/I 959-98-8 Endosuifan-I ND 0.0095 0.0015 ug/I 33213-65-9 Endosulfan-I1 ND 0.0095 0.0014 ug/I 76-44-8 Heptachlor ND 0.0095 0.0025 ug/I 1024-57-3 Heptachlor epoxide ND 0.0095 0.0019 ug/I 72-43-5 Methoxychlor ND 0.019 0.0048 ug/I 8001-35-2 Toxaphene ND 0.48 0.20 ug/I CAS No. Surrogate Recoveries Run# I Run# 2 Limits 877-09-8 Teirachloro-m-xylene 80% 42-127% 2051-24-3 Decachlorobiphenyl 38% 27-127% C7 J J J J (a) All hits confirmed by dual column analysis. (b) Primary and confirmation results differ by more than 40%. Lower value reported due to possible coelution. ND = Not detected MDL = Method Detection Limit RL = Reporting Limit E = Indicates value exceeds calibration range J = Indicates an estimated value B = Indicates analyte found in associated method blank N = Indicates presumptive evidence of a compound _ay.Ga�r 14 of 20 FA55085 SGS North America Inc. Report of Analysis it Sample ID: BACK DRAIN Sample ID: FA55085-2 rix: AQ - Water iod: SW846 8082A SW846 3510C ect: Stormwater Sampling; NC File ID DF Analyzed By #1 XX070223.D 1 06/25/18 16:51 NJ #2 Initial Volume Final Volume Run #1 1050 ml 5.0 nil Run #2 Page 1 of 1 iWo Date Sampled: 06/14/18 Date Received: 06/15/18 Percent Solids: n/a Prep Date Prep Batch Analytical Batch 06/21/1812:25 OP70599 GXX1246 PCB List CAS No. Compound Result RL MDL Units Q 12674-I1-2 Aroclor 1016 ND 0.095 0.038 ug/I 11104-28-2 Aroclor 1221 a ND 0.095 0.048 ug/I 11141-16-5 Aroclor 1232 ND 0.095 0.048 ug/I 53469-21-9 Aroclor 1242 ND 0.095 0.038 ug/I 12672-29-6 Aroclor 1248 ND 0.095 0.038 ug/I 11097-69-1 Aroclor 1254 ND 0.095 0.038 ug/I 11096-82-5 Aroclor 1260 ND 0.095 0.038 ug/I CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 877-09-8 Tetrachloro-m-xylene 123% 38-127% 2051-24-3 Decachlcrobiphenyl 51% 25-137% (a) Associated CCV outside of control limits high, sample was ND ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 15 of 20 _oy-lL9a Fg55085 SCS North America Inc. Report of Analysis tt Sample ID: BACK DRAIN Sample ID: FA55085-2 Date Sampled: 06/14/18 rix: AQ - Water Date Received: 06/15/18 Percent Solids: n/a ect: Stormwater Sampling; NC Total Metals Analysis Analyte Result RL Copper < 25 25 Lead 9.9 5.0 Zinc 392 20 (1) Instrument QC Batch: MA14994 (2) Prep QC Batch: MP33912 RL = Reporting Limit Page I of 1 N Units DF Prep Analyad By Method Prep Method ug/I 1 06/21/18 06/21/18 I.M SW8466010D1 SW8463010A2 ug/I 1 06/21/18 06/21/18 LM SW8466010D1 SW8463010A2 ❑g/1 1 06/21/18 06/21/18 LM SW8466010D1 SW8463010A2 16 of 20 FA5508S SGS North America Inc. Report of Analysis Client Sample ID: BACK DRAIN Lab Sample ID: FA55085-2 Date Sampled: 06/14/18 Matrix: AQ - Water Date Received: 06/15/18 Percent Solids: n/a Project: Stormwaler Sampling; NC Page 1 of 1 N General Chemistry Analyte Result RL Units DF Analyzed By Method HEM Petroleum Hydrocarbo 0 <5.3 5.3 mg/l 1 06/29/18 14:48 BR EPA 1664A Solids, Total Suspended 104 25 mg/l 1 06/20/18 17:45 BR SMZ540 D-11 pH n 8.07 su 1 06/27/18 12:00 Bw SM4500D B-1IISW9040C (a) Associated BS recovery outside control limits. (b) Field analysis required. Received out of hold time and analyzed by request. RL = Reporting Limit 17 of 20 6i!.W1A71r FA55095 SGSI Orlando, FL Misc. Forms Custody Documents and Other Forms Includes the following where applicable: • Chain of Custody Section 4 0 18 of 20 _SGS f FA55085 SGS Accutest Southeast ACCUTEST Chain Custody kMk SGS ACCUTEST JOKE: VAGE_OF_ _ ... .... I i•t�i : �••.'- '�^.I�^�•••"�'�I® iFtf�{�.fm', 1 —IC,1,A r;1•`Y'i�A��•_ i MINN MEN MINE IMMEMOMMOMMIMMII�■■■■■■■■■■�■■■■■■I■■■I� MEN ■■ ■■I• ONE I>s NOMMEMI�I>•II>•■■■■■■■■■■■■■■■■■■■■� I.MEN III>•I��III■■■■■■■■■■■■■■■■■■■■■� tN:t'.Stiki�.:7mrrt■r+'IiHIIiEliHtii�i^iTi^?7.-�.^^^,�itli�iili�;ti#:flt�fti�i[ . . Ide'1 ■■.,•:.. ■ ■ 7l1 Mal. 114'..113USSAGR{a��`LTIT�.^�zri�r—:r�r*-�^'•—'• .:.,.,^-��.�I^T-rT���yiff C11lLI/i9��^ ��rav`� ii111itlltttt'1ltllil TIM,,.t %: 1• SGS COC Ftr ..5217. .NAU51 FA55085: Chain of Custody Page 1 of 2 a.96 1 19 of 20 _S-Gs t— FA5W55 Job Number. FA55085 Date / Time Received: 6/157118 9:0000 AM SGS Sample Receipt Summary Client: CPC Project: STORMWATER Delivery Method: FED EX Airhill Its: 439402210538 Therm ID:Temps IR 1; ; hemCool r 2: 0.4; p of Coolers: 2 Cooler Temps (Raw Measured) °C: Coder 1: (2.2); Cooler 2: (0.8); Coder Temps (Corrected)'C: Cooler 1: (2.6); Cooler 2: (1.2); Cooler Information 1. Custody Seats Present 2. Custody Seals Intact 3. Temp criteria achieved 4. Cooler temp verification 5. Cooler media Trio Blank information 1. Trip Blank present / cooler 2. TIP Blank fisted on COC 3. Type Of TB Received Y or N Sample Information Y or N N/A l7 ❑ 1. Sarnpie tabds waseat an bottles R ❑ W ❑ 2. Samples preserved properly R ❑ v(7j ❑ 3. SuBkient volume./containers recwl for analysis: Ij ❑ IRGun 4. Condition of sample it= Ice (Baal S. Sarrrple recta w drki HT YJ ❑ 6. Dates/T"MDs an COC mahh Sample Label ,[7i ❑ _ Y or N NIA 7. VOCs have headspace ❑ �pj ❑ rN] ❑ ❑ 8. Bottles received for unspecified tests ❑ B �7 ❑ ❑ 9. Compositi g instructions; dear ❑ ❑ t�i W or S N/A 10. Voa Sod tuslJars received past 48Mz? ❑ ❑ R 11.% Solids Jar received? ❑ ❑ ❑ ❑ 'R 12. Residual Chlorine Present? ❑ ❑ R Misc. Information Number of Encores: 25-Gram 5-Gram Number of 5035 Field Kits: _ Test Ship Lot is: PH 0-3 230315 PH 1U-12 219813A Residual Chlorine Test Strip Lot A: Comments NO ANALYSIS MARKED ON COC. NO DATE OR TIME FOR SAMPLES s+raot AM Technician: HEATHERW Date: 6115120189.00:00Reviewer. flee., aS2V1] Number of Lab Filtered Metals: Other. (Specify) Date: FA55085: Chain of Custody Page 2 of 2 0 I 20 of 20 0 _,USr- FASSOBS