NCS000115_DMR_20200221

Date: February 20,2020
Novozymes,NA Inc.
77 Perry's Chapel Church Rd. novozymese
Franklinton,N.C. 27525 Rethink Tomorrow
NCDEQ Division Of Water Quality RECEIVED
1617 Mail Service Center Raleigh,N.C.27699-1617
Attn:Division Of Water Quality MAR 0 5 2020
DENR-LAND QUALITY
STORMWATER PERMITTING
Storm Water Sampling, NPDES Permit No.NCS000115J
Dear Sir/Madam,
During review of storm water sampling results,it was observed that there was a slight exceeded
benchmark in Biochemical Oxygen Demand(BOD)from our Outfall 2 location.
Upon immediate investigation,per Tier One requirements,it was discovered that although during
sample event no signs of potential issues were present,in the area approximately 20 yards from
where samples are collected the combination of filtration systems not being properly
maintained/serviced and the off-loading of raw materials,specifically sugar,are considered causes of
the recent exceedance of BOD.Plans are in place to have personnel begin with cleaning filtration
systems and more caution taken place while material is being handled.
Also,due to storms during previous week,high winds were probable cause of material being blown
into grass areas near Outfall 2.
Continued monitoring by Environmental Services Department will take place in order to prevent
future exceeded benchmarks in Biological Oxygen Demand (BOD) from Outfall 2.
Kind Regard
e6A1
Joe Ladd
Environmental Compliance Coordinator
Environmental Services

r
STORMWATER DISCHARGE OUTFALL(SDO)
MONITORING REPORT
Permit Number NCS 000115 SAMPLES COLLECTED DURING CALENDAR YEAR: 2020
(This monitoring report shall be received by the Division no later than 30 days from
the date the facility receives the sampling results from the laboratory.)
FACILITY NAME Novozymes, NA Inc. COUNTY Franklin
PERSON COLLECTING SAMPLE(S) Joe Ladd PHONE NO.(919 )494-3000
CERTIFIED LABORATORY(S) Enco Labs Lab#
Lab#
SIGNATURE OF PERMITTEE OR DESIGNEE
REQUIRED ON PAGE 2.
Part A: Specific Monitoring Requirements
Outfall Date 50050
No. Sample Total Total pH HOD COD TSS
Collected Flow(if app.) Rainfall
mo/dd/yr MG inches
1 2/11/2020 .25" 7.0 3.3 22 83
Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month?Oyes @no
(if yes,complete Part B)
Part B:Vehicle Maintenance Activity Monitoring Requirements
Outfall Date 50050 00556 00530 00400
No. Sample Total Flow Total Oil&Grease Non-polar Total pH New Motor
Collected (if applicable) Rainfall (if appl.) O&G/TPH Suspended Oil Usage
(Method 1664 Solids
SGT-HEM),if
appl.
mo/dd/yr MG inches mg/I mg/1 unit gal/mo
Form SWU-247,last revised 6/12/2015
Page 1 of 2

f -.
STORM EVENT CHARACTERISTICS: Mail Original and one copy to:
Division of Energy Mineral and Land Resources
Date 2/11/20 Attn:Central Files
Total Event Precipitation(inches): .25" 1617 Mail Service Center
Event Duration(hours): (only if applicable—see permit.) Raleigh,North Carolina 27699-1617
(if more than one storm event was sampled)
Date
Total Event Precipitation(inches):
Event Duration(hours): (only if applicable—see permit.)
"I certify,under penalty of law,that this document and all attachments were prepared under my direction or supervision in accordance with a
system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person
or persons who manage the system,or those persons directly responsible for gathering the information,the information submitted is,to the
best of my knowledge and belief,true,accurate,and complete. I am aware that there are significant penalties for submitting false information,
including the possibi' of fine d imprisonment for knowing violations."
/ . ' / 2/20/2020
(Signature of Per ee)A
(Date)
•
Form SWU-247,last revised 6/12/2015
Page 2 of 2

STORMWATER DISCHARGE OUTFALL(SDO)
MONITORING REPORT
Permit Number NCS 000115 SAMPLES COLLECTED DURING CALENDAR YEAR: 2020
(This monitoring report shall be received by the Division no later than 30 days from
the date the facility receives the sampling results from the laboratory.)
FACILITY NAME Novozymes, NA Inc. COUNTY Franklin
PERSON COLLECTING SAMPLE(S) Joe Ladd PHONE NO.(919 )494-3000
CERTIFIED LABORATORY(S) Enco Labs Lab#
Lab#
SIGNATURE OF PERMITTEE OR DESIGNEE
REQUIRED ON PAGE 2.
Part A:Specific Monitoring Requirements
Outfall Date 50050
No. Sample Total Total pH BOD COD TSS
Collected Flow(if app.) Rainfall
mo/dd/yr MG inches
2 2/11/2020 .25" 7.3 34 67 14
Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month?Oyes @no
(if yes,complete Part B)
Part B:Vehicle Maintenance Activity Monitoring Requirements
Outfall Date 50050 00556 00530 00400
No. Sample Total Flow Total Oil&Grease Non-polar Total pH New Motor
Collected (if applicable) Rainfall (if appl.) O&G/TPH Suspended Oil Usage
(Method 1664 Solids
SGT-HEM),if
appl.
mo/dd/yr MG inches mg/I mg/1 unit gal/mo
Form SWU-247,last revised 6/12/2015
Page 1 of 2

STORM EVENT CHARACTERISTICS: Mail Original and one copy to:
Division of Energy Mineral and Land Resources
Date 2/11/20 Attn:Central Files
Total Event Precipitation(inches): .25" 1617 Mail Service Center
Event Duration(hours): (only if applicable—see permit.) Raleigh,North Carolina 27699-1617
(if more than one storm event was sampled)
Date
Total Event Precipitation(inches):
Event Duration(hours): (only if applicable—see permit.)
"I certify,under penalty of law,that this document and all attachments were prepared under my direction or supervision in accordance with a
system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person
or persons who manage the system,or those persons directly responsible for gathering the information,the information submitted is,to the
best of my knowledge and belief,true,accurate,and complete. I am aware that there are significant penalties for submitting false information,
including the possib' ity of fines d imprisonment for knowing violations."
a:Ae f 2/20/2020
(Signature of Pei-puttee) (Date)
Form SWU-247,last revised 6/12/2015
Page 2 of 2

ENCO Laboratories
Accurate. Timely. Responsive. Innovative.
102-A Woodwinds Industrial Court
Cary NC,27511
Phone: [phone] FAX: [phone]
Tuesday, February 18, 2020
Novozymes North America (N0008)
Attn: Joe Ladd
77 Perry Chapel Church Road
Franklinton, NC 27525
RE: Laboratory Results for
Project Number: [none], Project Name/Desc: Stormwater Testing
ENCO Workorder(s):CD01285
Dear Joe Ladd,
Enclosed is a copy of your laboratory report for test samples received by our laboratory on
Tuesday, February 11, 2020.
Unless otherwise noted in an attached project narrative,all samples were received in
acceptable condition and processed in accordance with the referenced methods/procedures.
Results for these procedures apply only to the samples as submitted.
The analytical results contained in this report are in compliance with NELAC standards, except
as noted in the project narrative if applicable. This report shall not be reproduced except in
full,without the written approval of the Laboratory.
This report contains only those analyses performed by Environmental Conservation
Laboratories. Unless otherwise noted,all analyses were performed at ENCO Cary. Data from
outside organizations will be reported under separate cover.
If you have any questions or require further information, please do not hesitate to contact me.
Sincerely,
Aijb(
Chuck Smith
Project Manager
Enclosure(s)
FINAL This report relates only to the sample as received by the laboratory,and may only be reproduced in full. Page 1 of 8

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SAMPLE SUMMARY/LABORATORY CHRONICLE
Client ID: Outfall 1 Lab ID: CD01285-01 Sampled: 02/11/20 09:45 Received: 02/11/20 16:07
Parameter Preparation Hold Date/Time(s1 Preo Date/Time(sl Analysis Date/Time(s1
SM 2540D-2011 NO PREP 02/18/20 02/13/20 09:29 02/13/20 09:29
SM 5210 B-2011 NO PREP 02/13/20 09:45 02/12/20 10:40 02/12/20 10:40
SM 52200-2011 Same 03/10/20 02/17/20 12:06 02/17/20 15:45
Client ID: Outfall 2 Lab ID: CD01285-02 Sampled: 02/11/20 10:15 Received: 02/11/20 16:07
Parameter Preparation Hold Date/Time(s1 prep Date/Time(s1 Analysis Date/Time(s1
SM 25400-2011 NO PREP 02/18/20 02/13/20 09:29 02/13/20 09:29
SM 5210 B-2011 NO PREP 02/13/20 10:15 02/12/20 10:40 02/12/20 10:40
SM 52200-2011 Same 03/10/20 02/17/20 12:06 02/17/20 15:45
FINAL This report relates only to the sample as received by the laboratory,and may only be reproduced in full. Page 2 of 8

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SAMPLE DETECTION SUMMARY
Client ID: Outfall 1 Lab ID: CD01285-01
AlielAs Resuly4 Flaq MIX P L ruAta Method Notes
Biochemical Oxygen Demand 3.3 2.0 2.0 mg/L SM 5210 B-2011
Chemical Oxygen Demand 22 10 10 mg/L SM 5220D-2011
Total Suspended Solids 83 25 25 mg/L SM 2540D-2011
Client ID: Outfall 2 Lab ID: CD01285-02
Analvte Results Flaq MU PS& Units Method Notes
Biochemical Oxygen Demand 34 2.0 2.0 mg/L SM 5210 B-2011
Chemical Oxygen Demand 67 10 10 mg/L SM 5220D-2011
Total Suspended Solids 14 4.2 4.2 mg/L SM 2540D-2011
FINAL This report relates only to the sample as received by the laboratory,and may only be reproduced in full. Page 3 of 8

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ANALYTICAL RESULTS
1
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Description: Outfall 1 Lab Sample ID:CD01285-01 Received: 02/11/20 16:07
Matrix: Surface Water Sampled:02/11/20 09:45 Work Order:CD01285
Project: Stormwater Testing Sampled By:Joe Ladd
Classical Chemistry ParametersIl
^-ENCO Cary certified analyte[NC 591]
Analvte FCAS Numberl Results flan Units QE E12L EQl Batch Method Analyzed By Notes
Biochemical Oxygen Demand^ 3.3 mg/L 1 2.0 2.0 0612005 SM 5210 8-2011 02/12/20 10:40 JOC
Chemical Oxygen Demand^ 22 mg/L 1 10 10 0B17025 SM 5220D-2011 02/17/20 15:45 JOC
Total Suspended Solids^ 83 mg/L 10 25 25 0B13004 SM 2540D-2011 02/13/20 09:29 BDC
Description: Outfall 2 Lab Sample ID:CD01285-02 Received: 02/11/20 16:07
Matrix: Surface Water Sampled:02/11/20 10:15 Work Order:CD01285
Project: Stormwater Testing Sampled By:Joe Ladd
Classical Chemistry Parameters
1
^-ENCO Cary certified analyte[NC 591]
Analvte ICAS Numberl Results flag Units DE MPS PQ.L latch Melba! Analyzed By Notes
Biochemical Oxygen Demand^ 34 mg/L 1 2.0 2.0 0B12005 SM 5210 B-2011 02/12/20 10:40 JOC
Chemical Oxygen Demand^ 67 mg/L 1 10 10 0B17025 SM 5220D-2011 02/17/20 15:45 JOC
Total Suspended Solids^ 14 mg/L 1.67 4.2 4.2 0B13004 SM 2540D-2011 02/13/20 09:29 BDC
FINAL This report relates only to the sample as received by the laboratory,and may only be reproduced in full. Page 4 of 8

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QUALITY CONTROL DATA
h
Classical Chemistry Parameters-Quality ControlII
Batch 0812005-NO PREP
Blank(0812005-BLK1) Prepared&Analyzed:02/12/2020 10:40
Spike Source %REC RPD
Analvte Result Ela9 POl. Units Level Result %REC Linda RPD Limit Notes
Biochemical Oxygen Demand 2.0 U 2.0 mg/L B-03
LCS(01312005-BS1) Prepared&Analyzed:02/12/2020 10:40
Spike Source %REC RPD
Analvte Result Ilan P0k Units Level Result %REC Limits RPD Limit Notes
Biochemical Oxygen Demand 200 2.0 mg/L 198 102 85-115
Duplicate(0B12005-DUP1) Prepared&Analyzed:02/12/2020 10:40
Source:CC20544-01
Spike Source %REC RPD
Analvte Result Elan QUnitsLevel Result %REC Limits RPD Limit Notes
Biochemical Oxygen Demand 6.7 2.0 mg/L 6.6 2 30
Batch 0813004-NO PREP
Blank(0B13004-BLK1) Prepared&Analyzed:02/13/2020 09:29
Spike Source %REC RPD
Analvte Result flan P0k Units Level Result %REC Limits RPD Limit Notes
Total Suspended Solids 2.5 U 2.5 mg/L
LCS(0B13004-B51) Prepared&Analyzed:02/13/2020 09:29
Spike Source %REC RPD
Analvte Result Elan P0k Units Level Result %REC Limits RPD Limit Notes
Total Suspended Solids 92 2.5 mg/L 100 92 80-120
Duplicate(0B13004-DUP1) Prepared&Analyzed:02/13/2020 09:29
Source:CD01285-01
Spike Source %REC RPD
Analvte Result flea £01. Units Level Result %REC Limits RPD Limit Notes
Total Suspended Solids 91 25 mg/L 83 9 20
Duplicate(0B13004-DUP2) Prepared&Analyzed:02/13/2020 09:29
Source:CD01495-02
Spike Source %REC RPD
-Anal ite Result Ilan EQL Units Level Result %REC Limits RPD Limit Notes
Total Suspended Solids 110 12 mg/L 110 3 20
Batch OB17025-Same
Blank(0B17025-BLK1) Prepared:02/17/2020 12:02 Analyzed:02/17/2020 15:45
Spike Source %REC RPD
Analvte Result flan POI. Units Level Result %REC jam& RPD Limit Notes
Chemical Oxygen Demand 10 U 10 mg/L
LCS(0B17025-BS1) Prepared:02/17/2020 12:02 Analyzed:02/17/2020 15:45
Spike Source %REC RPD
_Malian Result Elan EQL Units Level Result %REC Limits RPD Limit Notes
Chemical Oxygen Demand 500 10 mg/L 500 101 90-110
FINAL This report relates only to the sample as received by the laboratory,and may only be reproduced in full. Page 5 of 8

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QUALITY CONTROL DATA
1
Classical Chemistry Parameters-Quality Control
Batch OB17025-Same-Continued L
_Matrix
Spike(0B17025-MS1) Prepared:02/17/2020 12:02 Analyzed:02/17/2020 15:45
Source:CC11394-01
Spike Source %REC RPD
Analvte Result Flag POL Units Level Result %REC Unfits RPD Limit Notes
Chemical Oxygen Demand 2600 40 mg/L 2000 620 100 90-110
Matrix Spike Dup(0B17025-MSD1) Prepared:02/17/2020 12:02 Analyzed:02/17/2020 15:45
Source:CC11394-01
Spike Source %REC RPD
Analvte Result Flag POL Units Level Result %REC kraal RPD lima Notes
Chemical Oxygen Demand 2600 40 mg/L 2000 620 100 90-110 0.3 5
FINAL This report relates only to the sample as received by the laboratory,and may only be reproduced in full. Page 6 of 8

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FLAGS/NOTES AND DEFINITIONS
B The analyte was detected in the associated method blank.
D The sample was analyzed at dilution.
The reported value is between the laboratory method detection limit(MDL)and the laboratory method
reporting limit(MRL),adjusted for actual sample preparation data and moisture content,where applicable.
U The analyte was analyzed for but not detected to the level shown,adjusted for actual sample preparation
data and moisture content,where applicable.
E The concentration indicated for this analyte is an estimated value above the calibration range of the
instrument.This value is considered an estimate.
MRL Method Reporting Limit.The MRL is roughly equivalent to the practical quantitation limit(PQL)and is
based on the low point of the calibration curve,when applicable,sample preparation factor,dilution
factor,and, in the case of soil samples,moisture content.
PQL PQL: Practical Quantitation Limit. The PQL presented is the laboratory MRL.
N The analysis indicates the presence of an analyte for which there is presumptive evidence(85%or greater
confidence)to make a"tentative identification".
P Greater than 25%concentration difference was observed between the primary and secondary GC column.
The lower concentration is reported.
[CALC] Calculated analyte-MDL/MRL reported to the highest reporting limit of the component analyses.
B-03 Blank exceeds the method required oxygen depletion of<0.20 mg/L.
FINAL This report relates only to the sample as received by the laboratory,and may only be reproduced in full. Page 7 of 8

( 1 — - ENVIRONMENTAL CONSERVATION LABORATORIES CHAIN-OF-CUSTODY RECORD ma al
www.encolabs.can
to775 Centre]port Dr. 48�0 F-xecubve Perk Cart.sole 11, ttrt-A Waodwnnds Industrial CL
_ Orlando.FL 32824 Jacksonville,FL 3221660e9 Cary,NC 27511
1407)82&531a Jacksonville,(904)�s aoo� Fax(904)288 s2,o (919)467-30e0 Fax(919)as735 fs Page of
Client Name Project NuMer
Analyses Requested Turnaround
Navozymes North America(N0008) [none] Times
Address Project NnadDsse
Note:Rush requests subpG to
77 Perry Chapel Church Road Stomnwater Testing acceptance by the taclty
Cily/ST/Zp Poe/Oiling trio
Franklinton,NC 27525 3800487045 o CI 0 _Standard
Tel Fax Reporting Contact 0 W -
484-3370 Jae Ladd in i 6/''..
Expedited
Sanple,s)Name.Affiliation(Print) Biling Contact . N
+S� 1 n !Jourz.rwt4 S Accounts Payable V) Cl) Due /_/
Sampler(s) . site Location/Terte zone 'Y O O tab Worko der
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- l/�_�^�^/1 R
��(See Codes)(Combine as necessary) y V�/ ■��+5
Collection Matrix Total a of
rem• Sample ID(Field identification) le line Comp I Grab see codes) Containers Sample Comments
_
Outfal 1 0 t t?!J-43 04345. 6 & SW 3 X X X See(2cnutex 'S
Outfal 2 C2/)J 1b2,c 14I S Gib SW 3 X X X — �elbW
<-Total#of Containers
Sample Kit Prepared By Date/Time Relinquished By cone Received DalarTme
0-� L // I(f a 2-(( .)k.CmilmantreaoecWI Reporting Requirements rivitnOilihed By
2
'/S/.lpme
�f coal� �7` P' " • �• Relinquished By Date/Tine •� Daia,Tme
•
•
Cooler I s&Temps on Receipt 'Condeon Upon RScellif
5. (0 Acceptable Unacceptable
Matrix:Gw-Groundwater SO-Soil OW-Drinking Water SE-Sediment SW-Surface Water WV-Wastewater A-Air 0-Other Metal in comments) Preservation:41ce H-HCI N-HNO3 SH2SO4 NO-NaOH 0-Other(detail in comments)
Noe:Al samples submitted to ENCO Labs are in accordance with the terms and conditions listed on the reverse of this form,unless prior written agreements exist

Sample Preservation Verification
ENCO Cary (Epjcc )`
Work Order: CD01285 Project: Stormwater Testing
Client: Novozymes North America (N0008) Project#: [none]
Logged In: 11-Feb-20 16:16 Logged By: Rachel Ann Yonis
2.1 1 1 7
Preservation Check Performed By: N Date/Time: 7-0 1
CD01285-01
Cont T Pres(pH) pH Checked/ j Date/Time Used/Comments
Type Requirement In Control pH Adjusted Adjusted Reagent
C 250mLP+H2SO4 <2 L%/ N / NA Y / // NA
CD01285-02
Cont Type
Pros(pH) pH Checked/ Datefiime
Requirement In Control pH Adjusted Adjusted Reagent Used/Comments
C 250mLP+H2SO4 <2 A,_()1 N / NA Y (N)NA
Reagent Name ID Reagent Name ID Reagent Name ID
1 3 5
.2 4 6
pH Strip ID: PH Strips COA0898
C:1elmnt\Prir,.,..,...... ,..,,.a.,..,,.,„m..,,,,tat Page 1 of 1