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HomeMy WebLinkAboutNCG120023_MONITORING INFO_20160719 (FIX)ovg1c j PERMIT NO. DOC TYPE DOC DATE STORMWATER DIVISION CODING SHEET NCG PERMITS /v c-c ❑ HISTORICAL FILE MONITORING REPORTS n aol YYYYM M DD CDMi Smth 5400 Glenwood Avenue, Suite 400 Raleigh, North Carolina 27612 tel: 919-787-5620 fax: 919-781-5730 July 13, 2016 Attention: Central Files North Carolina Department of Environmental Quality Division of Water Resources 1617 Mail Service Center Raleigh, North Carolina 27699-1617 JUL 19 201s CENTRAL FILES DWR SECTION Subject: Semi -Annual Discharge Monitoring and Tier Two Sampling Report Monitoring Period: January 1 through June 30, 2016 Onslow County Landfill: Permit Number 67-09 Certificate of Coverage Number: NCG].20023 To the Division of Water Resources: CDM Smith Inc., on behalf of Onslow County (County), is submitting two copies of the Stormwater Discharge Monitoring Report for the Onslow County Landfill. Samples were collected from Outfalls 2 and 3 on May 31, 2016, after the facility received 1.38 inches of precipitation. Outfall 1 currently receives stormwater runoff from the closed portion of the Subtitle D landfill and was removed from the analytical monitoring requirements following a Division of Water Quality inspection on January 23, 2013. All samples were analyzed for fecal coliform, chernical oxygen demand (COD), and total suspended solids by Pace Analytical Services, Inc., located in Raleigh, North Carolina. Samples collected from Outfall 2 had detections of COD (147 milligrams per liter (mg/L)) and fecal coliform (6,000 colonies per 100 milliliters (mL)) above their respective benchmark value. The benchmark values for COD and fecal coliform are 120 mg/L and 1,000 colonies per 100 mL, respectively. Samples collected from Outfall 3 were below the benchmark values with the exception of COD (152 mg/L). Tier Two monitoring was implemented for Outfall 3 in January 2015 after consecutive detections of COD above the benchmark value. Stormwater from Outfall 3 is discharged to a former borrow pit and does not leave the property. The drainage area for Outfall 3 includes the partially closed and active operations area of the east slope of the Subtitle D landfill. Elevated COD at Outfall 3 is a result of washouts on the active slope. Per the County's Tier One responses and operations plan, all washouts are repaired and the slope is reseeded as necessary following precipitation events. Per the Tier 2 response requirements, samples will be collected monthly for all parameters from Outfall 3 until three consecutive sampling events show the parameters are below the benchmark A 1� WATER + ENVIRONMENT +TRANSPORTATION + ENERGY + FACILITIES 66M. Smtth Division of Water Resources July 13, 2016 Page 2 values. Monthly monitoring in accordance with the Tier 2 requirements will continue. The County will maintain a record of the Tier 1 and 2 responses and monitoring results at the landfill. If you have any questions or require further explanation, do not hesitate to call me at (919) 325-3566. Sincerely, Daniel H. Forbes CDM Smith Inc. cc: Scott Bost, Onslow County Mathew Colone, CDM Smith Inc. 10 Semi-annual Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG120000 Date submitted July 5, 2016 CERTIFICATE OF COVERAGE NO. NCG12 0 0 2 3 FACILITY NAME _O_nslow County Landfill COUNTY Onslow PERSON COLLECTING SAMPLES Mark Darwin LABORATORY Pace Analytical, _I_nC. Lab Cert. # 37712/37731 Comments on sample collection or analysis: Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR 2016 SAMPLE PERIOD X❑ Jan -June ❑ July -Dec or X❑ Monthly' May (month) DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA ❑Zero -flow ❑Water Supply ❑SA Mother Former Borrow Pit PLEASE REMEMBER TO SIGN ON THE REVERSE -) No discharge this period?' Outfall No. Date Sample Collected, (mo/dd/yr) 24-hour rainfall amount, Inches 3 Chemical Oxygen Demand Fecal Coliform Total Suspended Solids Benchmarks =__> - - 120 mg/L 1000 count per 100 ml. 100 mg/L or 50 mg/L 2 5/31 /16 1.38 147 6,000 18.9 3 5/31 /16 1.38 152 200 50.5 1 Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. Z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. 4 See General Permit text, Table 3, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Note: Results must be reported in numerical format. For example, do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non - numerical format. When results are below the applicable limits, they must be reported in the format, <XX me/L", where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Conversely, where fecal coliform results exceed the dilution upper limit, report the result as ">XX". Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. see General Permit text. Permit Date: 11/1/2012-10/31/2017 SWU-248, last revised 10/25/2012 Page 1 of 2 Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. ❑ No discharge this period?' Dutfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount; Inches3 Non -polar O&G/TPH by EPA 1664 (SGT-HEM) Total Suspended Solids pH Benchmarks ===> - 15 mg/L 100 mg/L or 50 mg/La 6.0 — 9.0 SU Footnotes from Part A also apply to this Part B Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. FOR PART AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART 11 SECTION B. s 2 EXCEEDANCES IN A ROW FOR THE SAME PARA veE-T ER AT THE SAME OUTFALLTRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. e TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ® NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ® NO ❑ REGIONAL OFFICE CONTACT NAME: Bethany Ge0rg0Ullas Mail an original and one copy of this DMR _including all "No Discharge" reports, within 30 dos of receipt of the lab results Lor at end of monitorinq period in the case of "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and a[[ attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." ature of Permit Date: 11/1/2012-10/31/2017 (Date) SWU-248, last revised 10/25/2012 Page 2 of 2 aceAnalytical® wwwpacelabs.com June 08, 2016 Mr. Dan Forbes CDM 5400 Glenwood Ave Suite 300 Raleigh, NC 27612 RE: Project: Outfall5/31 Pace Project No.: 92299556 Dear Mr. Forbes: Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Enclosed are the analytical results for sample(s) received by the laboratory on May 31, 2016. The results relate only to the samples included in this report. Results reported herein conform to the most current TN standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. If you have any questions concerning this report, please feel free to contact me. Sincerely, Chris Derouen Christopher.derouen@pacelabs.com Project Manager Enclosures KCR� TNI i ae�RA� REPORT OF LABORATORY ANALYSIS This report shall not be reproduces, except in full, without the written consent of Pace Analytical Services, Inc.. Page 1 of 11 aceAnalyircal www.pacelabsxam Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Project: Outfall 5131 Pace Project No.: 92299556 Raleigh Certification IDs 6701 Conference Drive, Raleigh, NC 27607 North Carolina Wastewater Certification #: 67 Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification M E87648 Massachusetts Certification M M-NC030 North Carolina Drinking Water Certification M 37712 CERTIFICATIONS North Carolina Bioassay Certification #: 16 North Carolina Drinking Water Certification #: 37731 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 VrginialVELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 2 of 11 lceAnalytical www.pacejabs.wn Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 2BB04 (828)254-7176 SAMPLE ANALYTE COUNT Project: Pace Project No.: Outfall 5131 92299556 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92299556001 OUTFALL 3 SM 9222D RC 1 PASI-R SM 2540D MJP 1 PASI-A SM 5220D WRC 1 PASI-A 92299556002 OUTFALL 2 SM 9222D RC 1 PASI-R SM 2540D MJP 1 PASI-A SM 5220D WRC 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 3 of 11 0 aceAnalytical www.pamiabs.com Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Project: Outfall 5/31 Pace Project No.: 92299556 Sample: OUTFALL 3 Lab ID: 92299556001 Collected: 05/31/16 10:45 Received: 05/31/16 14:00 Matrix: Water Parameters Results Units Report: Limit DF Prepared Analyzed CAS No. Oual MBIO 9222D Fecal Coliform PAL Analytical Method: SM 9222D Fecal Coliforms 200 CFU1100 mL 1.0 1 05/31/16 15:02 2540D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids 50.5 mg/L 12.5 1 06/02/16 09:51 5220D COD Analytical Method: SM 5220D Chemical Oxygen Demand 152 mg/L 25.0 1 06/08/16 15:00 Sample: OUTFALL2 Lab ID: 92299556002 Collected: 05/31/16 11:10 Received: 05131/1614;00 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Oual RABIO 9222D Fecal Coliform RAL Analytical Method: SM 9222D Fecal Coliforms 6000 CFU1100 mL 1.0 1 05/31/16 15:02 1g 2540D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids 18.9 mg/L 45 1 06/02/16 09:51 5220D COD Analytical Method: SM 5220D Chemical Oxygen Demand 147 mg1L 25.0 1 06/08/16 15:00 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/08/2016 05:29 PM without the written consent of Pace Analytical Services, Inc.. Page 4 of 11 ace Analytical ' tvtvw.pacalabs.crom Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Project: Outfall 5131 Pace Project No.: 92299556 QC Batch: RBIO16171 QC Batch Method: SM 9222D Associated Lab Samples: 92299556001, 92299556002 METHOD BLANK: 1745703 Associated Lab Samples: 92299556001, 92299556002 Parameter Units Fecal Col'Iforms CFU1100 mL SAMPLE DUPLICATE: 1745704 Parameter Units Fecal Coliforms CFU1100 mL QUALITY CONTROL DATA Analysis Method: SM 9222D Analysis Description: 9222D MBIO Fecal Coliform - RAL Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 1.0 05/31/1615:02 92299556001 Dup Result Result RPD Qualifiers 200 4300 182 D6 Results presented on this page are in the units indicated by the "Units" column except whore an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/08/2016 05:29 PM without the written consent of Pace Analytical Services, Inc.. Page 5 of 11 IceAnalytical www.pweiaabs.com Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Project: Outfall 5131 Pace Project No.: 92299556 QC Batch: WET145280 Analysis Method: SM 2540D QC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids Associated Lab Samples: 92299556001, 92299556002 METHOD BLANK: 1746698 Matrix: Water Associated Lab Samples: 92299556001, 92299556002 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mg/L ND 2.5 06/02/16 09:47 LABORATORY CONTROL SAMPLE: 1746699 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Suspended Solids mg/L 250 244 98 90-110 SAMPLE DUPLICATE: 1746700 92299501001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 15.8 23.4 39 D6 SAMPLE DUPLICATE: 1746701 92299752003 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg1L 260 260 0 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/08/2016 05:29 PM without the written consent of Pace Analytical Services, Inc.. Page 6 of 11 aceAnalytical www.pacelabsxom Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Project: Outfall 5131 Pace Project No.: 92299556 QC Batch: WETA127855 Analysis Method: SM 5220D QC Batch Method: SM 5220D Analysis Description: 5220D COD Associated Lab Samples: 92299556001, 92299556002 METHOD BLANK: 1749583 Matrix: Water Associated Lab Samples: 92299556001, 92299556002 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Chemical Oxygen Demand mg1L ND 25.0 06/08/16 15:00 LABORATORY CONTROL SAMPLE: 1749584 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Chemical Oxygen Demand mg/L 750 751 100 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1749585 1749586 MS MSD 92299556001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Chemical Oxygen Demand mg/L 152 750 750 865 865 95 95 90-110 0 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1749587 1749588 MS MSD 92299889002 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Chemical Oxygen Demand mg1L ND 750 750 711 711 93 93 90-110 0 Results presented on this page are In the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 0610812016 05:29 PM without the written consent of Pace Analytical Services, Inc.. Page 7 of 11 IeAnaiXical www.pacelabs.com Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 2BB04 (828)254-7176 QUALIFIERS Project: Outfali 5/31 Pace Project No.: 92299556 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL- Practical Quantitation Limit. RL- Reporting Limit. S -Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration, Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. LABORATORIES PASI-A Pace Analytical Services -Asheville PASI-R Pace Analytical Services - Raleigh 'ANALYTE QUALIFIERS 1g This is a greater than value D6 The precision between the sample and sample duplicate exceeded laboratory control limits. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/08/2016 05:29 PM without the written consent of Pace Analytical Services, Inc.. Page 8 of 11 lceAnalyfical WW pacefabs.c= Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Outfall 5131 Pace Project No.: 92299556 Lab ID Sample ID QC Batch Method QC Batch 92299556001 OUTFALL 3 SM 9222D RB1016171 92299556002 OUTFALL 2 SM 9222D R131016171 92299556001 OUTFALL 3 SM 2540D WET145280 92299556002 OUTFALL 2 SM 2540D WET145280 92299556001 OUTFALL 3 SM 5220D WETA127855 92299556002 OUTFALL 2 SM 5220D WETA127855 Date: 06/08/2016 05:29 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Analytical Method Analytical Batch Page 9 of 11 uocument Name: uocument nevisea: Lortncuia • Sample Condition U rh Receipt(SCUR) Page i of 2 aceAnaloieal Document No.: Wuing Authority: F-RAL-CS-001-rev.os Pace Ralelph Qualitv Office -- , _s, f— lmamal use ONi v I Client Name: Project # Wo# : 92299556 W Courier. LJFed Ex UP5 ❑U5PS ❑ Commercial Dace [--]Other: 92299556 ffl11111 Custody Seal Present? Oyes VND Seals Intact? ❑Yes ONo Date/Initials Person Examining Cantents:$1)�J_ 1 I 1 V;+ Packing Material: ❑Bubble Wrap ❑Bubble Bags None ❑Other: 'thermometer: III SN:122065387 ❑IRSN: 122065371 T eoV e:��Wet ❑Brue []None ❑Samples on Ice, cooling process ha begun Correction Factor:AT Cooler Temp Corrected ('C): �e n Biological Tissue frozen? Dyes ON, 64/A Temp should be above f eezing to 6'C ���fff USDA Regulated Soil ( V N/A, water sample) Did samp!T originate In a quarantine zone within the United States: CA, NY, or SC (Check maps)? old samples originate from a foreign source (inte ationally, Yes No includingHawail and Puerto Rico)? []Yes (4No r COMMENTS: Chain of Cult Present? es 0 No J3fI/A 1. Chain of C Filled Out? My., No t•I/A 2. Chain of Custody Relinquished? es Q No ONJA 1 3. Sampler Name and/or Si nature on COC? Yes No EINJA 4, Sam les Arrived within Hold Time? Yes CIN. QNA._ S. Short Hold Time Analysis (02 hr)7 es No QN,JA 6. Rush Turn Around Time Re nested? ❑Yes Na N,rA 7. Sufficient Volume? es 0No ❑NrA 8. Correct Containers Used? �« ❑No ❑N/A 9. -Pace Containers Used? IN N A Containers Intact? Yes QN. N A 10. Filtered Volume Received for Dissolved Tests? Yes ❑No A 11. Note It sediment Is visible in the dissolved container Sample Labels Match COC? es ❑No ❑N/A 12. -includes Date/fime/ID/Ana sis Matrbr: All containers needing acid/base preservation have been checked? 11 Yes []No❑N/A 13. All containers needing preservation are found to be In compliance with EPA recommendation? (HNOs, Ha504, HClc2; N30H >9 Sulfide, NaOH>12 Cyanide) Yes []No ❑N/A Exceptions: VOA, Coliform, TOC, Oil and Grease, ORO/801S {water DOCLLHg es Drig 11NA Samples checked for dechlorinatfon Yes No N A. 14. }leads ace In VOA Vials >5-6mm 7 Yes OND A 15. Up Blank present? []Yes ❑No N/A 16. Trip Blank Custody Seals Present? ❑Yes ❑No N/A Pace Trip Blank Lot # (if purchased): CLIENT NOTIFICATION/RESOLUTION f ersorfContacted: Comments/Resolution: Project Manager.SCURF Ravlaw: Field Data Required? []Yes []no Date/lime: Date: G/r / i4 Project Manager SRF Review: _ _ Date: Note: whenever there is a discrepancy affecting North Carolina compliance samples, a copy �f this form will be sent tq the Norlh roilm Out of holo, Incorrect preservative, out of temp, Incorrect containers) DEHNR Certlflcatlan Office (i.e. Page 10 of 11 acmnalytical www.pacalabs.com 6701 Conference Drive. Raleigh, NC 27607 ph: (919) 834-4984, fax (919) 834-6497 NCWW Certd67, NCDW CerM7791 Chain of Custody Relinquished by (si nat[rrt�Y1 try a DL, 61 ate LQ tk� qOlC1 RelinquWled by (signature) Received by (signature) D e Tlma Relinquished by (slgneturs) Received by (signature) Date Tima Receipt Conaitions (L UOnly) ❑ 4tTC E Temp: or Res. Chlorine: ❑ Absent ❑ Present ❑ nla Acid preserv. t27 ❑ Yes ❑ No ❑ nla Base preserv. >127 ❑Yes ❑No ❑rJa Page 11 of 11 CDM Smith 5400 Glenwood Avenue, Suite 400 Raleigh, North Carolina 27612 tel: 919-325-3500 fax: 919-781-5730 May 13, 2016 Attention: Central Files North Carolina Department of Environmental Quality Division of Water Resources 1617 Mail Service Center Raleigh, North Carolina 27699-1617 RECEIVED MAY 16 �Ulb CENTRAL FILES DWR SECTf()lV Subject: Outfall 3 Discharge Monitoring Report - Tier 2 Response Monitoring Period - April 2016 Onslow County Landfill - Permit Number 67-09 Certificate of Coverage Number - NCG120023 To the Division of Water Resources: CDM Smith Inc., on behalf of Onslow County (County), is submitting two copies of the Stormwater Discharge Monitoring Report for Outfall 3. Samples collected from Outfall 3 during the 2014 semi-annual sampling events had detections of fecal coliform and chemical oxygen demand above the benchmark values. In response to the benchmark value exceedances, the County implemented Tier 1 and 2 responses. There was no discharge from Outfall 3 in April 2016. Per the Tier 11 response requirements, samples will be collected monthly from Outfall 3 for all parameters until three consecutive sampling events show the parameters are below the benchmark values. The County will maintain a record of the Tier 1 and 2 responses and monitoring results at the landfill. If you have any questions or require further explanation, do not hesitate to call me at (919) 325-3566. Sincerely, Daniel H. Forbes CDM Smith Inc. cc: Scott Bost, Onslow County Mark Gifford, Onslow County i,i WATER + ENVIRONMENT +TRANSPORTATION + ENERGY + FACILITIES Semi-annual Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG120000 Date submitted — May 13, 2016 CERTIFICATE OF COVERAGE NO. NCG12 0 0 2 3 FACILITY NAME Onslow Count dfil Lanl COUNTY Onslow PERSON COLLECTING SAMPLES No Samples Collected _ LABORATORY _ Lab Cert. # Comments on sample collection or analysis: Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR 2016 SAMPLE PERIOD ❑ Jan -June ❑ July -Dec or X❑ Monthly' April {month) DISCHARGING TO CLASS ❑ORW []HQW ❑Trout ❑PNA ❑Zero -flow ❑Water Supply ❑SA RECEIVED X❑Other Former Borrow Pit MAY 16 ZU1b PLEASE REMEMBER TO SIGN ON THE REVERSE CENTRAL FILES DWR SECTION ❑X No discharge this period?z Outfall No. Date Sample Collected (mo/dd/yr) 24-hour rainfall amount, Inches Chemical Oxygen Demand Fecal Coliform Total Suspended Solids Benchmarks =__> _ - 120 mg/L 1000 count per 100 mL 100 mg/L or 50 mg/L° 3 1 Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. 2 For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. 4 See General Permit text, Table 3, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Note: Results must be reported in numerical format. For example, do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non - numerical format. When results are below the applicable limits, they must be reported in the formate "<XX me/L", where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Conversely, where fecal coliform results exceed the dilution upper limit, report the result as ">XX". !Vote: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Permit Date: 11/1/2012-10/31/2017 SWU-248, last revised 10/25/2012 Page 1 of 2 Part 8: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. ❑ No discharge this period?2 Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, IncheS3 Non -polar O&G/TPH by EPA 2664 (SGT-HEM) Total Suspended Solids pH Benchmarks 15 mg/L 100 mg/L or 50 mg/L4 6.0 — 9.0 SU Footnotes from Part A also apply to this Part B Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART 11 SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES ®NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ® NO ❑ REGIONAL OFFICE CONTACT NAME: Bethany Georgoulias Mail an oriainal and one copv of this DMR, includina all "No Discharae" reports. within 30 days of receipt of the lab results .(or ot_end-oLmonitoring period in the case of "No Discharae" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am away that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violatioris." (Signature of Permittee) Zo /C, (Date) Permit Date:11/1/2012-10/31/2017 SWU-248, last revised 10/25/2012 Page 2 of 2 Semi-annual Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit-No.-NCG120000- Date submitted February 26, 2016 CERTIFICATE OF COVERAGE NO. NCG12 0 0 2 3 FACILITY NAME Onslow County Landfill COUNTY Onslow PERSON COLLECTING SAMPLES Janelle Bauer LABORATORY Pace Analytical, Inc. Lab Cert-. # 37712/37731- Comments on sample collection -or -analysis: Part A: Stormwater Benchmarks and MonitoringResults SAMPLE COLLECTION YEAR 2016 SAMPLE PERIOD ❑ Jan -June ❑ July -Dec or © Monthly( January (month) DISCHARGING TO CLASS ❑ORW ❑HQW. ❑Trout ❑PNA ❑zero -flow- ❑Water:Supply_ [:]SA - RECEIVED X❑Other _ Former- Borrow. Pit MAR 0 4 2016 PLEASE REMEMBER TO SIGN ON THE REVERSE CENTRAL FILES DNJR SECTION No discharge this period?z Outfall Na. Date Sample Collected( (mo/dded 24-hour rainfall amount, Inches Chemical Oxygen Demand Fecal Coliform Total Suspended Solids Benchmarks - - 120 mg/L 1000 count per 100.mL . 100.mg/L or 50 mg/L. 3 1/29116 0.17 205 3,200 0JY 1 Monthly sampling (instead of semi-annual) must begin with the second consecutive.benchmark exceedance for -the -same parameter at..the same outfall..- z For sampling periods with -no discharge,at.any single-outfall,.:you_must-still submit this-discharge_monitoring.report:with a:checkmark-here..- 3The total precipitation must be: recorded.using data ;from ,aman-site rain gauge:.- Unattended. sites -maybe eligiblefor a waiver. of.the-raingauge;requirement:- 4 See General. Permit text, Table 3, identifying the especially sensitive receiving water classifications -where the-more-protective-benchmark=applies: Note: Results must be reported in numerical format. For example, do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non - numerical format. When results are below the applicable limits, they must be reported in the format "<XX m L" where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Conversely, where fecal coliform results exceed the dilution upper limit, report the result as ">XX". Note: If you report a sample value in excess of the benchmark, -you= must implement -Tier--1, -Tier 2, or -Tier 3 responses. .:See- General -Permit text. - Permit Date: 11/1/2012-10/31/2017 SWU-248, last revised.10/25/2012 Page 1 of 2 Part B: Vehicle Maintenance • Area MonitoringAesults:-only for facilities -averaging >=55•gal•of-new-off per month. n No discharge this period?2 Outfall No. Date Sample Collected (mo/dd/yr) 24-hour rainfall amount, Inches; Non -polar O&G/TPH by EPA 1664 (SGT-HEM) Total Suspended Solids pH Benchmarks -===> _ - 15 mg/L 100 mg/L or 50 mg/L 6.0 - 9.0 SU Footnotes from Part A also apply to this Part B Note: if you report a sample valve in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General -Permit text FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER I REQUIREMENTS. SEE PERMIT PART 11 SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE'SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART 11 SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES [Y] Nn ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ®NO ❑ REGIONAL OFFICE CONTACT NAME: Bethany eor gouliaS Mail an on ina_I and one copy of this DMR.-includina all No Dsscharae"- reports;- within 30 days of receipt of the lab results for at end of monitoring period in the case of "No Discharaea reports) to: Division of Water Quality Attn: DWQ Central Fifes 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for. -gathering the information, the information submitted is, to the best of my:knowledge and belief, true, accurate, -and complete. I am aryaTthat there are significant penalties for submitting false information, -including the possibility of fines and imprisonment for knowing violations." ��5' (Signature of (Date) Permit Date: 11/1/2012-10/31/2017 SWU-248, last revised 10/25/2012 Page 2 of 2 �I CDM Smith 5400 Glenwood Avenue, Suite 400 Raleigh, North Carolina 27612 tel: 919-787-5620 fax: 919-781-5730 February 29, 2016 Attention: Central Files North Carolina Department of Environmental Quality Division of Water Resources 1617 Mail Service Center Raleigh, North Carolina 27699-1617 Subject: Outfall 3 Discharge Monitoring Report - Tier 2 Response Monitoring Period - January 2016 Onslow County Landfill - Permit Number 67-09 Certificate of Coverage Number - NCG120023 To the Division of Water Resources: CDM Smith Inc., on behalf of Onslow County (County), is submitting two copies of the Stormwater Discharge Monitoring Report for Outfall 3. Samples collected from Outfall 3 during the 2014 semi-annual sampling events had detections of fecal coliform and chemical oxygen demand (COD) above their respective benchmark value. Stormwater from the outfall is discharged to a former borrow pit and does not leave the property. In response to the benchmark value exceedances, the County implemented Tier 1 and 2 responses. Samples were collected from Outfall 3 on January 29, 2016, and analyzed for COD, fecal coliform, and total suspended solids (TSS) by Pace Analytical, Inc. COD was detected at 205 milligrams per liter (mg/L), fecal coliform was detected at 3,200 colonies per 100 milliliters, and TSS were detected at 234 mg/L. These concentrations exceeded their respective benchmark value. Note that accumulated soils in the sedimentation basin and drainage channel for Out -fall 3 will be removed during the upcoming Phase 4 Subtitle D Landfill expansion project. Per the Tier 2 response requirements, samples will be collected monthly for all parameters from Outfall 3 until three consecutive sampling events show the parameters are below the benchmark values. Monthly monitoring in accordance with the Tier 2 requirements will continue. The County will maintain a record of the Tier 1 and 2 responses and monitoring results at the landfill. elf WATER + ENVIRONMENT + TRANSPORTATION + ENERGY + FACILITIES CDM- Smith Division of Water Resources February 29, 2016 Page 2 If you have any questions or require further explanation, do not hesitate to call me at (919) 325-3566. Sincerely, Daniel H. Forbes CDM Smith Inc. cc: Scott Bost, Onslow County Mathew Colone, CDM Smith Inc. aceAnalytical. www.paoelabs.ton February 04, 2016 Mr. Dan Forbes CDM 5400 Glenwood Ave Suite 300 Raleigh, NC 27612 RE: Project: Onslow NPDES 1129 Pace Project No.: 92284690 Dear Mr. Forbes: Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Enclosed are the analytical results for sample(s) received by the laboratory on January 29, 2016, The results relate only to the samples included in this report. Results reported herein conform to the most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. If you have any questions concerning this report, please feel free to contact me. Sincerely, Chris Derouen christopher.derouen@pacelabs.com Project Manager Enclosures , INkCCR r REPORT OF LABORATORYANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 1 of 11 aceAnalytical wow.pacekb& nt Project: Onslow NPDES 1/29 Pace Project No.: 92284690 Raleigh Certification Ids 6701 Conference Drive, Raleigh, NC 27607 North Carolina Wastewater Certification M 67 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Asheville Certification Ids 2225 Riverside Drive, Asheville, NC 28804 Flodda/NELAP Certification M E87648 Massachusetts Certification #: M-NC030 North Carolina Drinking Water Certification #: 37712 CERTIFICATIONS North Carolina Bioassay Certification M 16 North Carolina Drinking Water Certification M 37731 North Carolina Wastewater Certification M 40 South Carolina Certification #: 99030001 West Virginia Certification M 356 VirginialVELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 2 of 11 aceAnalytical www.pacslabs.com SAMPLE ANALYrE COUNT Project: Onsiow NPDES 1129 Pace Project No.: 92254690 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92284690001 OUTFALL 3 SM 9222D RC 1 PASI-R SM 2540D MSH 1 PASI-A SM 5220D WRC 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 3 of 11 aceAnalyfir,a xnrwpscelab&= ANALYTICAL RESULTS Project: Onslow NPDES 1129 Pace Project No.: 92284690 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254.7176 Sample: OUTFALL 3 Parameters Lab ID: 92284690001 Collected: 0, /29116 09:30 Results Units Report Limit DF Received: 01/29/16 12:00 Matrix: Water Prepared Analyzed CAS No. Qual MBIO 9222D Fecal Conform RAIL Analytical Method: SM 9222❑ Fecal Coliforms 3200 CFU1100 mL 1.0 1 01/29/16 14:58 2540D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids 234 mglL 21.7 1 02/01/16 16:20 5220D COD Analytical Method: SM 5220D Chemical Oxygen Demand 205 mg1L 25.0 1 02/03/16 22:45 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/04/2016 05:40 PM without the written consent of Pace Analytical Services, Inc.. Page 4 of 11 a ce Analytical www.psaebtils mr Project: Onslow NPOES 1/29 Pace Project No.: 92284690 QC Batch: RBIO/5914 QC Batch Method: SM 9222D Associated Lab Samples: 92284690001 METHOD BLANK: 1657025 Associated Lab Samples: 92284690001 Parameter Units Fecal Coliforms CFU/100 mL SAMPLE DUPLICATE: 1657026 Parameter Fecal Coliforms QUALITY CONTROL DATA Analysis Method: Analysis Description Matrix: Water Blank Result NO 92284655003 Units Result CFU1100 mL 4.0 Reporting SM 9222D 9222D MBIO Fecal Coliform - RAIL Limit Analyzed Qualifiers 1.0 01/29/16 14:58 Oup Result RPD Qualifiers 4.0 0 1g Pace Analytical Services, Inc. 2225 Riverside Dr, Asheville, NC 28804 (828)254-7176 Results presented on this page are In the units indicated by the'Units' column except where an alternate unit is presented to the right of the result REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/04/2016 05:40 PM without the written consent of Pace Analytical Services, Inc.. Page 5 of 11 6 aceAnalytrcal wwwpeoatabs.com QUALITY CONTROL DATA Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Project: Onslow NPDES 1l29 Pace Project No.: 92284690 OC Batch: WET142790 Analysis Method: SM 2540D QC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids Associated Lab Samples: 92284690001 METHOD BLANK: 1657519 Matrix: Water Associated Lab Samples: 92284690001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mglL ND 2.5 02/01/16 16:16 LABORATORY CONTROL SAMPLE: 1657520 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Suspended Solids mglL 250 230 92 90-110 SAMPLE DUPLICATE: 1657521 92284705001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg1L 8.0 8.0 0 SAMPLE DUPLICATE: 1657522 92284603001 Dup Parameter Units Result Result: RPD Qualifiers Total Suspended Solids mglL 40.5 41.5 2 Results presented on this page are in the units indicated by the -Units" column except where an alternate unit Is presented to the right of the resutt. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02t04/2016 05:40 PM without the written consent of Pace Analytical Services, Inc.. Page 6 of 11 acmnalytical xwx pasawmeom QUALITY CONTROL DATA Project: Onslow NPDES 1129 Pace Project No.: 92284690 QC Batch: WETA126290 Analysis Method: SM 5220D QC Batch Method: SM 5220D Analysis Description: 5220D COD Associated Lab Samples: 92284590001 METHOD BLANK: 1658774 Associated Lab Samples: 92284690001 Parameter Units Chemical Oxygen Demand mg/L LABORATORY CONTROL SAMPLE: 1658775 Parameter Units Chemical Oxygen Demand mg/L Pace Analytical services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 25.0 02/03/16 22:45 Spike LCS LCS % Rec Cone. Result % Rec Limits Qualifiers 750 732 98 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1658776 1658777 MS MSD 92284708001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qua] Chemical Oxygen Demand mg1L 1190 3000 3000 3730 3730 84 84 90-110 0 M1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1658778 16:58779 MS MSD 92284690001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Quai Chemical Oxygen Demand mg1L 205 750 750 910 910 94 94 90-110 0 Results presented on this page are In the units Indicated by the "units" column excep: where an altemate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/04/2016 05:40 PM without the written consent of Pace Analytical Services, Inc.. Page 7 of 11 aceAnalytrcal o ~pacowacom QUALIFIf_RS Project: Onslow NPDES 1129 Pace Project No.: 92284690 DEFINITIONS Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL- Reporting Limit. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPID - Relafive Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260, N-Nitrosodiphenylamine decomposes and cannot be separated from Diphen}damine using Method 8270, The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited anatytes. TNI -The NELAC Institute. LABORATORIES PASI-A Pace Analytical Services - Asheville PASI-R Pace Analytical Services - Raleigh ANALYTE QUALIFIERS 1g This is a less than value Mi Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/04/2016 05:40 PM without the written consent of Pace Analytical Services, Inc.. Page 8 of 11 aceAnalytical" WWW pecefeba.com QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Onslow NP❑ES 1/29 Pace Project No.: 92284690 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Lab ID Sample ID QC Batch Method QC Batch Analytical Method 92284690001 OUTFALL 3 SM 92220 RBIO/5914 92284690001 OUTFALL 3 SM 2540D WET142790 92284690001 OUTFALL 3 SM 52200 WETA126290 Analytical Batch Date: 02/04/2016 05:40 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 9 of 11 r CEA!?8�j/flCt?i CHAIN -OF -CUSTODY ! Analytical Request Document ,he ChSw oMssbdy a a LEGAL DOC MEW. All mium tit fields must be oonOetmd aodnaWy- I r /NPDEs _ r GRouislo wATiER r DRiNKjNG wATF=R I_ .. • Waste Water ww SAMPLE ID on OL Ak AR i a MU • f • 1 .�. / ® ■■■■■■■■■■■©■■■son ■■©■■■■■■■■■■ a� 0 CD Q) CO fL 'r++o~. nw.: By spiny v= for+ vw an 3w4 0 V=n NS 30 Oy 02rnrw 4 twm and aVeWng to U" dw m of t.5% w mwoh Wang :*,ew.s not aaa.ow 30 *q. FALL-O-D ev.07. 15-May-20D7 Document Name.. Sample Condition U on Re+: Document No.: Client Name: Project #; Courier: ❑Fed Ex ❑UPS ❑USPS Client ❑Commercial ❑Pace ❑other: i]ocument Revised: 260Cfi015 page i of 2 Issuing Authority: Pace Huntersvllle Quality Office WO#:92284690_J 92284690 I I I I I I I I I I I I I I Custody Seal on Cooler/Box present? ❑Yes ONo Seals Intact? []Yes PtNo Packing Material: [--]BubbleWrap ❑Bubble Bags None ❑Other:_ Thermometer IR Gun SN:12MS387 Used; IR Gun SN; 222065371 Type of Ica; • V)Wet [:]Blue ❑None (]samples on Ice, cooling process has begun Cooler Temp Corrected {'Q: p Biological Tissue Froxen? Des ❑No nAlAtTemp should be above f eezfng to WC " Correction Factor; 0.0`C Date and Initials of Person Examining Contents:1 ZCi USDA Regulated Soil ( 2] N/A, water sample) Old samples originate in a quarantine sons within the United States; CA, NY, or SC (check maps)? Did samples originate from a foreign source (Internationaliti Yes o including Hawa)I and Puerto Rico)? E Yes No If Yes to either question, fill out a Regulated Soil Checklist and Include with SCUR/CCIC paperwork. COMMENTS: Chain of Custody Present? Yes ONo N/A 1. Chain of Custody Filled Out? Yes ONo. LIKA 2. Chain of Custody Relinquished? Yes On, N A 3. Simpler Name and/or Signature an COL? f Yas ON, (:INIA 4. Samples Arrived within Hold Time? Yas No UNLA 5. - Short Hold Time Ana lysIs L<72 hr 7 ihYes QNo N A 6. U 1 FIX Rush Turn Around Time Re nested? Yes No N A 7. Sufficient Volume? Pas ONO N A 8. Correct Containers Used? -Pace Containers Used? Yes es . Oft No ❑N/A QNtA 9. Containers Intact? Yes No N A 10. --Filtered Volume Received for Alssolved Tests? QYes No N A 11. Note If sediment Is visible in the dissolved container Sample Labels Match COO -Includes Date/Time/ID/Analysis Matrix: ZI mYes ©No ❑N/A 12. All containers needing acid/base preservatlon have been checked? All containers needing preservation are found to be In compllonce with EPA recommendation? (HNOs. H%504, HCI<2;NaOH >9Sulfide, NaOH>1201anlde) Exceptions; VOA, Coilform, TOC, Oil and Grease, ORO/8015 water DOC,LLH ,,....11�. es Yes es ❑No ©No No ❑N/A ❑N/A N A 13. Samples checked for dechtorization Yes CINo N A :14. Heads ace In VOAVIals >5-6mm ? Yes No N/A :15. Trip Blank Present? Trip Blank Custody Seals Present? Pace Trip Blank Lot # (Ifpurchased): Des ©Yes ©Na QNo /A VNIA 1:6. CLIENT NOTiFICATION/RESOLUTION Person Contacted: Comments/Resolutton: 1 Q,ti* Amu Date/Time: Field Data Required? []Ye3 ❑fdo Project Manager SCURPRevieW:. Dale: 11- //C_ Note: Whenever there Is a discrepancy affecting North Carolina compliance samples, a copy of this form wlllEe sent tot North Carolina oEHNR Certification Office (Le. out of hold, incorrect preservative, out of temp, Incorrect containers), Page 11 of 11 Semi-annual Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG120000 Date submitted April 21, 2016 _ CERTIFICATE OF COVERAGE NO. NCGjf-Q7Q_2_3F SAMPLE COLLECTION YEAR 2016 FACILITY NAME _Onslow County Landfill Y SAMPLE PERIOD ❑ Jan -June ❑ July -Dec COUNTY Onslow or X❑ Monthly'_ March (month) PERSON COLLECTING SAMPLES No Samples Collected DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA LABORATORY Lab Cert. # ❑Zero -flow [:]WaterSupply ❑SA Comments on sample collection or analysis: other Former Barrow Pit Part A: Stormwater Benchmarks and Monitoring Results PLEASE REMEMBER TO SIGN ON THE REVERSE 4 ❑X No discharge this period?' Outfall No. Date Sample Collected (mo/dd/yr) 24-hour rainfall amount, Inches Chemical Oxygen Demand Fecal Coliform Tota! Suspended Solids Benchmarks =__> _ - 120 mg/L 1000 count per 100 mL 100 mg/L or 50 mg/L4 3 p;=rr1,n/[=n /4Z!/%n [ U b //// /Lz::� DWR 3ECT14N ;!'�•'UnAIA l IUN 'ROMS?NG UNIT v /P 1 Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmar'k exceedance for the same parameter at the same outfall. 2 For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. 4 See General Permit text, Table 3, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Note: Results must be reported in numerical format. For example, do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non - numerical format. When results are below the applicable limits, they must be reported in the format, "<XX me/L", where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Conversely, where fecal coliform results exceed the dilution upper limit, report the result as ">XX". Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Permit Date: 11/1/2012-10/31/2017 SWU-248, last revised 10/25/2012 Page 1 of 2 Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. ❑ No discharge this period?z Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches3 Non -polar O&G/TPH by EPA 1664 (SGT-HEM) Total Suspended Solids pH Benchmarks ==_> - 15 mg/L 100 mg/L or 50 mg/0 6.0 — 9.0 SU Footnotes from Part A also apply to this Part B Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier Z, or Tier 3 responses. See General Permit text. FOR PART A AND PART B MONITORING RESULTS: + A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. + 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE cnnnE OLITFA r% C7GER TIER 2 REQUIREMENTS. SEE PERMIT PART p SECTION B. e TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ® NO IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ® NO REGIONAL OFFICE CONTACT NAME: BethanyGeorgoulias Mail an original and one copy of this DMR, including all "No Discharge" reports, within 30 days of receipt of the lab results (or at end of monitoring period in the case of "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1.61.7 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." 7 z691& (Date) Permit Date: 11/1/2012-10/31/2017 SWU-248, last revised 10/25/2012 Page 2 of 2 Semi-annual Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG120000 Date submitted April 5, 2016 CERTIFICATE OF COVERAGE NO. NCG12 0 0 2 3 FACILITY NAME _ Onslow County Landfill ^ COUNTY Onslow PERSON COLLECTING SAMPLES Janelle Bauer LABORATORY Pace Analytical, Inc. Lab Cert. # 37712/37731 Comments on sample collection or analysis: Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR 2016 r u SAMPLE PERIOD ❑ Jan -dune ❑ July -Dec or 21 Monthly'_ February_ (mon`th DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA ❑Zero -flow ❑Water Supply }) SA X❑Other V PLEASE REMEMBER TO SIGN ON THE RME5. 4 ❑ No discharge this period?' Outfall Na. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches3 Chemical Oxygen Demand Fecal Coliform Tota! Suspended Solids Benchmarks =__> - - 120 mg/L 1000 count per 100 mL 100 mg/L or 50 mg/L4 3 2/24/16 0.39 484 2,200 282 ' Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. Z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. 4 See General Permit text, Table 3, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Note: Results must be reported in numerical format. For example, do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non - numerical format. When results are below the applicable limits, they must be reported in the formats "<XX me/L", where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Conversely, where fecal coliform results exceed the dilution upper limit, report the result as ">XX". Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Permit Date: 11/1/2012-10/31/2017 SWU-248, last revised 10/25/2012 Page 1 of 2 Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. ❑ No discharge this period-?2 Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, lnche53 Nan -polar O&G/TPH by EPA 1664 (SGT-HEM) Total Suspended Solids pH Benchmarks 15 mg/L 100 mg/L or 50 mg/L4 6.0 — 9.0 SU Footnotes from Part A also apply to this Part B Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART Il SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ® NO IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ®NO REGIONAL OFFICE CONTACT NAME: Bethany GeOrCloulIaS Mail an original and one copy of this DMR, including a!! "No_Di_scharAe"reports, within 30 days of receipt o the lab results (or at end of monitoring period in the case of "No Discharge" ruorts) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware tha�,there are significant penalties For submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature` of Permittee) Permit Date:11/1/2012-10/31/2017 (Date) SWU-248, last revised 10/25/2012 Page 2 of 2 Fart B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. ❑ No discharge this period?' Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches; Non -polar 0&G/TPH by EPA 1664 (SGT-HEM) Total Suspended Solids pH Benchmarlrs =__> - 15 mg/L 100 mg/L or 50 mg/L4 6.0 — 9.0 SU Footnotes from Part A also apply to this Part B Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. FOR PART A AND PART B MONITORING RESULTS: o A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART 11 SECTION B. e 2 EXCEEDANCES IN A ROW FOR THE SAME PARA"dIETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ® NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ® NOFJ REGIONAL OFFICE CONTACT NAME: Bethany GeorgouliaS Mail an original and one copy of this DMR. including all "No Discharge" reports, within 30 days of receipt _of the lob results (or of end of monitorina period in the case of "No Discharae" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." '( ate) Permit Date: 11/1/2012-10/31/2017 SWU-248, last revised 10/25/2012 Page 2 of 2 Semi-annual Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG120000 Date submitted -January-13, 2016- CERTIFICATE OF COVERAGE NO. NCG12 0 0 2 3 FACILITY NAME Onslow County Landfill COUNTY Onslow PERSON COLLECTING SAMPLES Janelle Bauer LABORATORY Pace. Analytical, Inc. Lab-Cert.-#- 37712/37731 Comments on sample collection or analysis: Part A: Stormwater Benchmarks and Monitoring Results_ SAMPLE COLLECTION YEAR 2015 SAMPLE PERIOD ❑ Jan -June X❑ July -Dec or Q Monthly' December (month) DISCHARGING =TO.CLASS-❑ORW- ❑HQW- ❑Trout= ❑PNA- ❑Zero -flow: •❑Water Suppiy_ ❑SA-_ ®Other Former Borrow Pit PLEASE REMEMBER TO SIGN ON THE REVERSE 4 ❑ No discharge this-period?-2 Outfall No. Date Sample Collected (mo/dd/yr) 24-hour rainfall amount; Inches3 Chemical Oxygen Demand Fecal Colifarm _,_, „ ��.,.d� suspended Solids Benchmmrks - - 120 mg/L 1000 count per 100 mL 100 mg/L or 50 mg/L- 3 12/08/15 1.02 132 60,000 199 1 Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. Z For sampling periods with no discharge-at:any single-outfall; you -must still submit this discharge -monitoring report with;a-checkmark here.- 3 The total precipitation must be recorded using data from an on -site rain gauge. - Unattended sites -maybe eligible for a -waiver of the rain=gauge requirement. ° See General Permit text, Table 3, identifying the especially sensitive receiving water classifications wherethemore protective benchmark applies.. Note: Results must be reported in numerical format. For example, do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non - numerical format.. When results are below- the.applicable.limits,.they . must be reported in the.format; "<XX mz10 where°XX-is the;numericai.value of the. -- detection limit, reporting limit, etc. in mg/L. Conversely, where fecal coliform results exceed the dilution upper limit, report the result as ">XX". Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Permit Date: 11/1/2012-10/31/2017 SWU-248, last revised 10/25/2012 Page 1 of 2 �CDM Smith 5400 Glenwood Avenue, Suite 400 Raleigh, North Carolina 27612 tel: 919-787-5620 fax: 919-781-5730 January 21, 2016 Attention: DWQ Central Files North Carolina Department of Environmental Quality Division of Water Quality 1617 Mail Service Center Raleigh, North Carolina 27699-1617 Subject: Outfall 3 Discharge Monitoring Report -Tier 2 Response Monitoring Period - December 2015 0 m C— m Onslow County Landfill - Permit Number 67-09 Z z Certificate of Coverage Number - NCG12 0023 rn n r a+o I 'n N C To the Division of Water Quality: rn m rn CDM Smith Inc., on behalf of Onslow County (County), is submitting two copies of the Stormwater Discharge Monitoring Report for Outfall 3. Samples collected from Outfall 3 during the 2014 semi-annual sampling events had detections of fecal coliform and chemical oxygen demand (COD) above the benchmark values. Stormwater from the outfall is discharged to a former borrow pit and does not leave the property. In response to the benchmark value exceedances, the County implemented Tier 1 and 2 responses. Samples were collected from Outfall 3 on December 8, 2015, and analyzed for COD, fecal coliform, and total suspended solids (TSS) by Pace Analytical, Inc. COD was detected at 132 milligrams per liter (mg/L), fecal coliform was detected at 60,00() colonies per 100 milliliters, and TS5 were detected at 199 mg/L. These concentrations exceeded their respective benchmark value. Note that the concentrations of TSS and COD were below their respective benchmark value in samples collected from Outfall 3 in November 2015. Per the Tier 2 response requirements, samples will be collected monthly for all parameters from Outfall 3 until three consecutive sampling events show the parameters are below the benchmark values. Monthly monitoring in accordance with the Tier 2 requirements will continue. The County will maintain a record of the Tier 1 and 2 responses and monitoring results at the landfill. 1100 WATER + ENVIRONMENT +TRANSPORTATION + ENERGY + FACILITIES CDM Division of Water Quality January 21, 2016 Page 2 if you have any questions or require further explanation, do not hesitate to call me at (919) 325-3566. Sincerely, Daniel H. Forbes CDM Smith Inc. cc: Scott Bost, Onslow County Mathew Colone, CDM Smith Inc. aceAnalytical WWW.Pacawbs.cnrn December 18, 2015 Mr. Dan Forbes CDM 5400 Glenwood Ave Suite 300 Raleigh, NC 27612 RE: Project: Onslow Co. LF NPDES 12/8 Pace Project No.: 92279041 Dear Mr. Forbes: Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Enclosed are the analytical results for sample(s) received by the laboratory on December 08, 2015: The results relate only to the samples included in this report. Results reported herein conform to the most current TN standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. If you have any questions concerning this report, please feel free to contact me. Sincerely, �z— — Chris Derouen christopher.derouen@pacelabs.com Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, exi;ept in full, without the written consent of Pecs Analytical Services, Inc.. Page 1 of 11 acmnalytical e www.pacgws.com Project: Onslow Co. LF NPDES 1218 Pace Project No.: 92279041 Raleigh Certification IDs 6701 Conference Drive, Raleigh, NC 27607 North Carolina Wastewater Certification M 67 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Asheville Certification Ibs 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87648 Massachusetts Certification #: M-NCO30 North Carolina Drinking Water Certification #: 37712 CERTIFICATIONS North Carolina Bioassay Certification #: 16 North Carolina Drinking Water Certification M 37731 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 West 1firginia Certification #: 356 UrginiaNELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, exczpt in full, without the written consent of Pace Analytical Services, inc.. Page 2 of 11 s aceAnalytical www.pacefabs.cam SAMPLE ANALYTE COUNT Project: Onslow Co. LF NPDES 12/8 Pace Project No.: 92279041 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Analyses Lab Io Sample 10 Method Analysts Reported Laboratory 92279041001 OUTFALL 3 SM 9222❑ RC 1 PASI-R SM 2540D SAM 1 PASI-A SM 5220D WRC 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, exr:ept in full, vAthoul the written consent of Pace Analyticai Services, Inc.. Page 3 of 11 (�IaceAnalyticale wnvwpecalabs com ANALYTICAL RESULTS Project: Onslow Co. LF NPDES 1218 Pace Project No.: 92279041 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Sample: OUTFALL 3 Lab ID: 92279041001 Collected: 12/08115 12:30 Received: 12/08/15 14A0 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual MBIO 9222D Fecal Coliform RAIL Analytical Method: SM 9222D Fecal Coliforms 60000 CFU1100 mL 1.0 1 12/08/15 17:01 19 2540D Total Suspended Solids Analytical Method: $M 25400 Total Suspended Solids 199 mg1L 31.2 1 12/11/15 13:09 5220D COD Analytical Method: SM 5220D Chemical Oxygen Demand 132 mg1L ,25.0 1 12/17/15 18:48 Date: 12/18/2015 03:21 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 4 of 11 • acmnalytical wwwpatxfabs.com Project: Onslow Co. LF NPDES 1218 Pace Project No.: 92279041 QC Batch: RBIO/5757 QC Batch Method: SM 9222D Associated Lab Samples: 92279041001 METHOD BLANK: 1623380 Associated Lab Samples: 92279041001 Parameter Units Fecal Coliforms CFU1100 mL SAMPLE DUPLICATE: 1623381 Parameter Fecal Coliforms QUALITY CONTROL DATA Analysis Method: SM 9222D Analysis Description: 9222D MBIO Fecal Coliform - RAL Matrix: Water Blank Repotting Result Limit Analyzed Qualifiers ND 1.0 12/08/15 17:01 92278897002 Dup Units Result Result RPD Qualifiers CFU1100 mL 2.0 2.0 0 29 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ResuRs presented an this page are in the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 1211812015 03:21 PM without the written consent of Pace Analytical Services, Inc.. Page 5 of i 1 aceAnalytrcal' www.pacelebs.txtm QUALITY CONTROL DATA Project: Onslow Co. LF NPDES 1218 Pace Project No.: 92279041 QC Batch: WETI41919 Analysis Method: SM 2540D QC Batch Method: SM 2WD Analysis Description: 2540D Total Suspended Solids Associated Lab Samples: 92279D41001 METHOD BLANK: 1626894 Associated Lab Samples: 92279041001 Parameter Units Total Suspended Solids mg1L LABORATORY CONTROL SAMPLE: 1626895 Parameter Units Total Suspended Solids mg/L Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 2.5 12/11/15 13:08 Spike LCS LCS % Rae Cone. Result % Rae Limits Qualifiers 250 236 94 90-110 SAMPLE DUPLICATE: 1626896 92279306005 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mgtL 19.6 18.3 7 D6 SAMPLE DUPLICATE: 1626897 92279191001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L ND ND rtesuits presented on this page are In the units Indicated by the "Units' column accept where an alternate unit Is presented to the right of the resuh. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/18/2015 03:21 PM without the written consent of Pace Analytical Services, Inc.. Page 6 of 11 s acmnalytical www.pac fftcorn Project: Onslow Co. LF NPOES 1218 Pace Project No.: 92279041 QC Batch: WETA125838 QC Batch Method: SM 52201) Associated Lab Samples: 92279041001 METHOD BLANK: 1631607 Associated Lab Samples: 92279041001 Parameter Units Chemical Oxygen Demand mg/L LABORATORY CONTROL SAMPLE: 1631608 Parameter Units Chemical Oxygen Demand mgfL QUALITY CONTROL DATA Analysis Method: Analysis Description Matrix: Water SM 5220D 5220D COD Pace Analytical Services, Inc. 2225 Riverside Dr, Asheville, NC 28804 (828)254-7176 Blank Reporting Result Limit Analyzed Qualifiers ND 25.0 12/17/15 18:48 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 750 772 103 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1631609 1631610 MS MSD 92280174004 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Chemical Oxygen Demand mg/L 89.0 750 750 810 810 96 96 90-110 0 H3 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1631611 1631612 MS MSD 92278896002 Spike Spike MS MSD MS MSD %Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Chemical Oxygen Demand mg1L 62.0 750 750 790 790 97 97 90-110 0 Aesurts presented on this page aft In the units Indicated by the "Units" column except wfiere an alternate unit Is presented to the right of the resulL REPORT OF LABORATORY. ANALYSIS This report shall not be reproduced, except in full, Date: 12/18/2015 03:21 PM without the written consent of Pace Analyticcd Services, Inc.. Page 7 of 11 ace Analytical o www.pKelabaaom QUALIFIERS Project: Onslow Co. LF NPDES 1218 Pace Project No.: 92279041 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL-Adjusted Method Detection Limit. POL - Practical Quandtation Limit. RL - Reporting Limit. Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 288134 (828)254-7176 S - Surrogate 1,2-Diphanyihydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(b) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylanitrile by EPA Method 8260. N-Nitrbsodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI -The NELAC Institute. LABORATORIES PASI-A Pace Analytical Services - Asheville PASI-R Pace Analytical Services - Raleigh ANALYTE QUALIFIERS 1g This is a greater than value 2g This is a less than value D6 The relative percent difference (RPD) between the sample and sample duplicate exceeded laboratory control limits. H3 Sample was received or analysis requested beyond the recognized method holding time. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/18/2015 03:21 PM without the written consent of Pace Analytical Services, Inc.. Page 8 of 11 aceAnalytical. www.pticeiabl C= QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Onslow Co. LF NPDES 1218 Pace Project No.: 92279041 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Lab 10 Sample ID QC Batch Method QC Batch Analytical Method 92279041001 OUTFALL 3 SM 9222D R131015757 92279041001 OUTFALL 3 SM 2540D WET141919 92279D41001 OUTFALL 3 SM 5220D WETA125838 Date: 12/18/2015 03:21 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytcal Services, Inc.. Analytical Batch Page 9 of 11 aceAnalytical' www.pacalabs.com 6701 Contererxe Drive, Raleigh, NC 27607 ph: (919) 834-4984, fax: (919) 83443497 NCWW CedW. NCDW Cert#37731 Chain of C;ustndy w.o.# Report Results To: Company: COA Address t, Ul -z_ Attn: � i �br be Phone: 014 G, - - Fax: Bill To: Project Reference: Project Number: Purchase Order #: 0 Standard Report Delivery ❑ Rush Report Delivery (w/surcharge) '*Rush wofects are subject to prior approval by Re4"4d by (etgr*M=) j cat ,�i.� L (, ( n 1 V/� Date j 7 'V Time Relinquished by (signature) Received by (signature) pate Time Relinquished by (signature) Received by (signature) Date Time Receipt Corrditbrrs (Lab lJse Only) ❑ 4t2°C ❑ Temp: _i °C Res. Chlodna: ❑ Absent ❑ Present ❑ Wa Add presem c2? ❑ Yes ❑ No ❑ nla Base prawn+ >12? ❑ Yes ❑ No ❑ rda Page 10 of 11 Document Name: Sample Condition Upon Document Revised: May 15, 2015 11)!CBAfta/ ar Recel t SCUR' Pa e 1 of 2" Document No.: issuing Authorities, F-RAL-CS-001-rev.03 Pace Raleigh Qualit Office Client Name: CiDM SM\AA(\ "Page 2 of 2 is for Internal Use Only Courier (Circle): Fed Ex UPS USPS Client Commercial Pace Other Custody Seal on CoolerlBox Present: yes Q' no Seals intact: /yes no Packing Material: Bubble Wrap "a, It-811198 Q No Other Circle Thermometer Used: IR Gun 2g8532a of Ice: le ;Blue None Samples on Ice, tooting process has begun IR Gun Bar A_9 91 Temp Correction Factor: Add 1 btrac_t ' C Corrected Cooler Temp.: 2 R � C Biological Tissue Is Frozen: Yes N WA Temp should be above freezing to VC Comments: Date and Initials o person examining chop n f Prey a i Chain of Custodx Present: Yes ONo ONIA '- Chain of Cust2q Filled Out: Yaa ONo OwA 2. Chain of Custody Relinquished: as ONo OwA 3. 'Sampler Name & Signature on COC: yea ONo OWA 4. Samples Arrived within Hold Time: Cdy., ON. ❑WA 5. Short Hold Time Ansi ie <72hr : Yee ONO OWA 6. Rush Turn Around Time Re nested: Dyes ON. OwA i. Suffident Volume: es ❑No 13WA 8. Correct Containers Used: -mace Contalners Used: as Olio tes pro OWA OWA 9. Containers Intact: AY95 Eb4b OWA 10, - Flltered volume received for Dissolved tests Oyes ONo 0 WA 11. Sample Labels match COC: -Includes date/tlmeliD/Anal is Matrba Yes ONo OwA 12. An containers needing preservatlon have been checked. All containers needing preservation are found to be in compliance vA[h EPA recommendation, amptien= VOA collfonn, TOC, oaa. W I-DRO wa ....aaaa �pYes I:TNo es ONo es ONO ❑r+rIIA ❑wA 1$. . Samples checked for dechlorination: ea ONO OWA 14. Headspace in VOA Vials >6mm : Oves ❑No OOA 15. Trip Blank Present: Trip Blank Custody Seals Present Pace Pace Trip Blank Lot # Of purchased): Oyes ONO OYes ONo N/A 16. Client Notification! Resolution: Field Data Required? Y I N Person Contacted: Data/Time: Comments/ !%"v ,...Ion SCURF ISRF RBVIOW : Date: Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Caroltna DEHNR CertlNuation Office (t.e out of hold, Incorrect preservable, out of temp, Incorrect containers) W08:92279041 IIB,IIllulllllllllll Page 11 of 11 r CDM Smith 5400 Glenwood Avenue, Suite 400 Raleigh, North Carolina 27612 tel: 919-787-5620 fax: 919-791-5730 April 5, 2016 Attention: Central Files North Carolina Department of Environmental Quality Division of Water Resources 1617 Mail Service Center Raleigh, North Carolina 27699-1617 RECEIVED APR 0 5 2016 CENTRAL FILES DWR SECTION Subject: Outfall 3 Stormwater Discharge Monitoring Report - Tier 2 Response Monitoring Period - February 2 66 Onslow County Landfill - Per, irri t Number 67-09 Certificate of Coverage Number - NCG120023 To the Division of Water Resources: I CDM Smith Inc., on behalf of Onslow County (County), is submitting two copies of the Stormwater Discharge Monitoring Report for Outfall 3. Samples collected from Outfall 3 during the 2014 semi-annual sampling events had detections of fecal coliform and chemical oxygen demand (COD) above their respective benchmark value. Stormwater from the outfall is discharged to a former borrow pit and does not leave the property. In response to the benchmark value exceedances, the County implemented Tier 1 and 2 responses. Samples were collected from Outfall 3 on February 24, 2016, and analyzed for COD, fecal coliform, and total suspended solids (TSS) by Pace Analytical, Inc. COD was detected at 484 milligrams per liter (mg/L), fecal coliform was detected at 2,200 colonies per 100 milliliters, and TSS were detected at 282 mg/L. These concentrations exceeded their respective benchmark value. Note that accumulated soils in the sedimentation basin and drainage channel for Outfall 3 will be removed during the upcoming Phase 4 Subtitle D Landfill expansion project. Construction activities are scheduled to start in May 2016. Per the Tier 2 response requirements, samples will be collected monthly for all parameters from Outfall 3 until three consecutive sampling events show the parameters are below the benchmark values. Monthly monitoring in accordance with the Tier 2 requirements will continue. The County will maintain a record of the Tier 1 and 2 responses and monitoring results at the landfill. io WATER + ENVIRONMENT +TRANSPORTATION + ENERGY + FACILITIES Smith Division of Water Resources April 5, 2016 Page 2 If you have any questions or require further explanation, do not hesitate to call me at (919) 325-3566. Sincerely, Daniel H. Forbes CDM Smith Inc. cc: Scott Bost, Onslow County Mark Gifford, Onslow County Mathew Colone, CDM Smith Inc. r aceAnalytical www.peoelffbicam Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 288D4 (828)254.7176 March 01, 2016 Mr. Dan Forbes CDM 5400 Glenwood Ave Suite 300 Raleigh, NC 27612 RE: Project: Onsiow Co. 2124 Pace Project No.: 92287696 Dear Mr. Forbes: Enclosed are the analytical results for sample(s) received by the laboratory on February 24, 2016. The results relate only to the samples included in this report. Results reported herein conform to the most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. If you have any questions concerning this report, please feel free to contact me. Sincerely, Chris Derouen Christopher.derouen@pacelabs.com Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 1 of 11 aceAnalytical www.pacelahs.ciom Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Project: Onslow Co. 2124 Pace Project No.: 92287696 Raleigh Certification IDs 6701 Conference Drive, Raleigh, NC 27607 North Carolina Wastewater Certification #: 67 Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 FloridalNELAP Certification #: E87648 Massachusetts Certification #: M-NC030 North Carolina Drinking Water Certification #: 37712 CERTIFICATIONS North Carolina Bioassay Certification #: 16 North Carolina Drinking Water Certification #: 37731 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 Virginia/VELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 2 of 11 aceAnalytrcal wwwpaceJobs'Mm Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254.7176 Project: Onslow Co. 2124 Pace Project No.: 92287696 Lab ID Sample ID 92287696001 OUTFALL 003 SAMPLE ANAL YTE COUNT Analytes Method Analysts Reported Laboratory SM 9222D RC 1 PASI-R SM 2540D MJP 1 PASI-A SM 52200 WRC 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Ana lytical Services, Inc.. Page 3 of 11 Pace Analytical Services, Inc. • 2225 Riverside Dr. acemalytrcal Asheville, NC 28804 www.pketabs.com (828)254-7176 ANALYTICAL_ RESULTS Project: Onslow Co. 2124 Pace Project No.: 92287696 Sample: OUTFALL 003 Parameters Lab ID: 92287696001 Collected: 02/24/16 10:30 Results Units Report Limit DF Received: 02124/16 13:05 Matrix: Water Prepared Analyzed CAS No. Qual MBIO 9222D Fecal Coliform RAL Analytical Method: SM 9222D Fecal Coliforms 2200 CFU1100 mL 1.0 1 02/24/16 15:21 2540D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids 282 mg/L 50.0 1 02/26/16 09:41 D6 5220D COD Analytical Method: SM 5220D Chemical Oxygen Demand 484 mg/L 25.0 1 03/01/16 14:30 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 03/01 /2016 05:35 PM without the written consent of Pace Analytical Services, Inc.. Page 4 of 11 • aceAnalytical www.pecelabs.crom Pace Analytical Services. Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Project: Onslow Co. 2124 Pace Project No.: 92287696 QC Batch: RB1015987 QC Batch Method: SM 9222D Associated Lab Samples: 92287696001 METHOD BLANK: 1673266 Associated Lab Samples: 92287696001 Parameter Units Fecal Coliforms CFU1100 mL SAMPLE DUPLICATE: 1673267 Parameter Fecal Coliforms QUALITY CONTROL DATA Analysis Method: SM 9222D Analysis Description: 9222D MBIO Fecal Coliform - RAL Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 1.0 02/24/1615'.21 92287589001 Dup Units Result Result RPD Qualifiers CFU1100 mL 2.0 2.0 0 1 g Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 03/01/2016 05:35 PM without the written consent of Pace Analytical Services, Inc.. Page 5 of 11 aceAnalytical WWWIPemiabs.com Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Project: Onslow Co. 2124 Pace Project No.: 92287696 QC Batch: WET143274 QC Batch Method: SM 2540D Associated Lab Samples: 92287696001 METHOD BLANK: 1674004 Associated Lab Samples: 92287696001 Parameter Units Total Suspended Solids mg1L LABORATORY CONTROL SAMPLE: 1674005 Parameter Units Total Suspended Solids mg/L SAMPLE DUPLICATE: 1674006 Parameter Units Total Suspended Solids mg/L QUALITY CONTROL DATA Analysis Method: SM 2540D Analysis Description: 2540D Total Suspended Solids Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 2.5 02/26/16 09:39 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 250 242 97 90-110 92287696001 Dup Result Result 282 232 SAMPLE DUPLICATE: 1674007 92287796001 Dup Parameter Units Result Result Total Suspended Solids mglL ND ND RPD Qualifiers 19 D6 RPD Qualifiers Results presented on this page are In the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 03/01/2016 05:35 PM without the written consent of Pace Analytical services, Inc.. Page 6 of 11 aceAnalyfical www.pacelabs.com Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Project: Onslow Co. 2124 Pace Project No.: 92287696 QC Batch: WETA/26605 Analysis Method: SM 5220D QC Batch Method: SM 5220D Analysis Description: 5220D COD Associated Lab Samples: 92287696001 METHOD BLANK: 1675396 Matrix: Water Associated Lab Samples: 92287696001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Chemical Oxygen Demand mg/L ND 25.0 03/01/16 14:30 LABORATORY CONTROL SAMPLE: 1675397 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Chemical Oxygen Demand mg/L 750 798 106 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1675398 1675399 MS MSD 92287840003 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Chemical Oxygen Demand mg/L 7170 15000 15000 17500 17500 69 69 90-110 0 M6 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1675400 1675401 MS MSD 92287793001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Chemical Oxygen Demand mg/L 705 750 750 1400 1400 93 93 90-110 0 Results presented on this page are in the units Indicated by the "Units" column except where an atternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. Date: 03/01/2016 05:35 PM without the written consent of Pace Analytical Services, Inc.. Page 7 of 11 aceAnalytical . www.pwelabs.com Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALIFIERS Project: Onslow Co. 2124 Pace Project No.: 92287696 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit. S -Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azcbenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. LABORATORIES PASI-A Pace Analytical Services -Asheville PASI-R Pace Analytical Services - Raleigh ANALYTE QUALIFIERS 1 g This is a less than value D6 The relative percent difference (RPD) between the sample and sample duplicate exceeded laboratory control limits. M6 Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution. REPORT OF LABORATORY ANALYSIS This report shalt not be reproduced, except in full, Date: 03/01/2016 05:35 PM without the written consent of Pace Analytical Services, Inc.. Page 8 of 11 aceAnalytical www.Pacelabs.com Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Onslow Co. 2124 Pace Project No,; 92287696 Analytical Lab ID Sample ID �QC Batch Method QC Batch Analytical Method Batch 92287696001 OUTFALL 003 SM 9222D RBI015987 92287696001 OUTFALL 003 SM 2540D WET/43274 92287696001 OUTFALL 003 SM 5220D WETA126605 Date: 03/01/2016 05:35 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 9 of 11 aceArralyt�ca! trrtww.pacalabe,cam 6701 Cortferenoe Drive, Ralolgh, NO 276D7 ph: (919) 8344984, fair: (919) 8346497 NCWW CertM7, NCDW CeW7731 Chain of Custody W.O.# Report Results To: Bill To: Company: . G DM 6mI+Vl CO K S'mii�i Address: 5400 E *I WCUd Ag d �� i fe WD 1-U ►) Attn: _ bah VOIr17 S Phone: iR (CI ) 3 2'5 3O 00 Fax: Sampled by (signature): �r Project Reference: Q Project Number: Purchase Order#: ld Standard Report Delivery ❑ Rush Report Delivery (w/surcharge) -Rush pl*cta are subject to prior approval by the laboratory Requested Due Date: Outbil3 C-t 1103o oU++01 s 3 WD out fGtl9 C7 -2�--I WW f �ccs (o 1030 Rel4iqulshad by (signature) ��� R by (al ature) Date 1 •z4-la T1mo 1305 Re[ uished by (signature) Raodrved by (signature) Date 'fame Rellnqutstted by (slgnetuna) Reoelved by (signature) Date Time Reoelpt Conditions (Lab Use tfily) ❑ 4*2°C ❑ Temp:SIC Res. Chiorine: ❑ Absent ❑ Present ❑ n/a Add preserv. t27 ❑ Yes ❑ No ❑ nla Base presaN. >127 ❑ Yes ❑ No ❑ Na Page 10 of 11 'DucUAIept Revise!: u"O^ j2015 aseAnalytlCal a Sample Condition U ¢i 1*01 t $129 Pa e 1 ofi2 Document No.; = Issuing Authority, F-RAL-CS-001-rev.03 Pace Huntersville Quali Office Client Name: Project M. W0' , 92287696 err ❑Fed Ex []ups ❑USPS VCtlen[ mmerclal ❑Pace ❑Other: 82287596 1/ :ody Seal on Cooler/Box Present? . ❑Yes JgNo Seals Intact? . C]Yes 140 i dng Material: ❑Bubble Wrap ❑Bubble Rags ]None ❑Other: _ mometer r- IR Gun SN:122065387 Used: ❑ I Gun SN! 122065371 Type of ice: • [ Wet D11te ❑None ❑Samptes on Ice, cooling process has begun Cooler Temp Corrected ('C): , 7- 9101ogled lissua Frozen? []Yes []No A�INVA + should be above freezing to VC Correction Facton 0.0 T • Date and Inittals of Person Examintng Contents; �{ L Rogtilated Soil ( N/A, water sample) imples oVnate I a quarantine zone vAthin the United Statds: CA, NY, or SC (check maps)? Did 4amples ortglna a from a forel•Bn source (Internationally, • . s VWO ' IndudingHawall apd Puerto Alco)? Dyes No I f Yes to either question, III 1,6ut a Reguldted Sall Checklist and Includu with SCUR/COC paperwork. COMMENTS: in of Custody Present? TALOS Na N A 1• In of Custody Filled Out? Yes No N A' 2. In of Custody Relin wished? Yes .. No N A S. + ler Name an or Si attire on COC? QNO , N/A 4. tes Arrived within Hold Time? Yes No 0,JN LA 5. rt Hold Time Anat sis 4Z hr ? viy.$ No LLN A 6. Al h Turn Around Tim a Requested? Yes No NA 7, Ilslent Votume7 t1yo '13 ' A' 8 • rect Contal ners Used? Pace Containers Used? Yes. • []No es No ON/A N A 9. . +talners intact? Yes ON. E3ffA S0 ered Volume Received for DlssbWd Tdsts? Yes No OVA 11.. Nale.f sediment Is visible in the dlssohred container npie Labels Match CDC? ;Includes.Date m � ID Anal 1s -Matrix: l�4yes TTT 'ONO ©N/A 12, Y containers needing add/bass preservation have been mkod? containers needing preservation are found to be in npllance with EPA recommendaoon? 403, H,50a, 9CI<2; NaOH >9 Sulfide, NaOH>12 Cyanide) xpflons: VOA, Collform, TOC, Oil and Grease, 0/9015 water D0PL1l4g es Yes s ONO J]No Na ❑N/A ©N/A EINIA •13. m les checked for dechlodzation Yes - No N A 14. ads ace In VOA Vials >S•6mm ? 13NO 15. p Blank Present? - p Blank Custody Seals Present? •, .. ce Tri Blank Lot q if urchased : 'Oyes; ; Ores:. ONo ONO rN/A 16. ; +, CLIENT NQTIFICATION_ Ji t> d. UT16N Fleld Data Required? 13Ye3 119 rson Contacted: DatefNye. mments/Resolution: :• rrolect Manager SCtJIT` ievrdve Date!': 2• S // Whenever there is a discrepancy affecting North CaYollna corrpllaMe ttmples, a copy of this form Abe sentto the North rollna HNR�on Offlte (l.e. out of Incorrect preservative, out of tamp ln6nritt contalneis)• Page 11 of 11 Semi-annual Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No: NCG120000 Date submitted November 23, 2015 CERTIFICATE OF COVERAGE NO. NCG12 0 0 2 3 FACILITY NAME Onslow. County Landfill COUNTY Onslow PERSON COLLECTING SAMPLES Daniel Forbes LABORATORY Pace Analytical, Inc. Lab Cert. # 37712/37731 Comments on sample collection or analysis: Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR 2015 SAMPLE PERIOD .❑.Jan -June ©,July -Dec or X❑ Monthly'_ November (month) DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA ❑Zero -flow ❑water.Supply .❑SA ®Other Former Borrow Pit PLEASE REMEMBER TO SIGN ON THE REVERSE 4 ❑ No discharge this-period?2 Qutfall No. Date Sample Collected) (mo/ d/yrCollected' 24-hour rainfall amount, Inches3 chemical.Oxygen Demand_ -Fecal Coliform. Total Suspended.Solids- Sim.011„, urns ===s - - 120 mg/L 1000 count per 100 mL 100 mg/L or 50 mg/0 3 11 /03/15 0.57 118 20,000 32.2 'Monthly sampling (instead of semi-annuaI):must- begin with the secondconsecutive benchmark-exceedance for,the-same parameter -at the -same outfalL. Z For sampling periods with -no -discharge -at anysingle outfall; you -must -still -submit this -discharge -monitoring -report with-a-checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver -of the rain gauge requirement. 4 See General Permit text, Table 3, identifying the especially sensitive -receiving -water classifications where the more protective benchmark applies. - Note: Results must be reported in numerical format. For example, do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non - numerical format.. Whenresults are below the applicable limits, they must .be - reported .in.the-format ."<XX m L" where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Conversely, where fecal coliform results exceed the dilution upper limit, report the result as ">XX". Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tiers, or Tier 3.responses._ See General Permit text.- Permit Date: 11/1/2012-10/31/2017 SWU-248, last revised 10/25/2012 Page 1 of 2 Part 8: Vehicle Maintenance Area Monitoring Results: only for facilities -averaging-> 55 gal of new oil per month. No discharge this period:2 Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches? Non -polar O&G/TPH by EPA 1664 (5GT-HEM) Total Suspended Solids pH Benchmarks 15 mg/L 100 mg/L or 5o mg/L 6.0 — 9.0 SU Footnotes from Part A also apply to this Part B Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCETRIGGERS TIER TREQUIREMENTS.-SEE-PERMIT PART 11 SECTION B: • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER ATTHE SMAE Oil T FALL TRIGGER TIER 2 REQUIREMENTS: SEE-PERMIT-PARTAI SECTION B. • T itR 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR -THE SAME PARAMETERATANY-ONE OUTFALL? -YES -®-NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ® NO 0 REGIONAL OFFICE CONTACT NAME: Bethany Geor oUllas Mall an original and one copy of this DMR, including all "No _D_ ischarae'=reports, within 30 days of receipt of the lob results (or at end of monitoring period in the case of "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN .THIS:CERTIFICATION .FOR NY -INFORMATION REPORTED: - "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. am aware th tthere are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." L (Signature of Permittee) (Date) Permit Date:11/1/2012--10/31/2017 SWU-248; last revised 10/25/2012 Page 2 of 2 (�Iacmnalyfical* WMpacelabs.com November 10, 2015 Mr. Dan Forbes CDM 5400 Glenwood Ave Suite 300 Raleigh, NC 27612 RE: Project: Onslow NPDES 1113 Pace Project No.: 92274445 Dear Mr. Forbes: Pace Analytical Services, Inc. 2225 Riverside Dr. Ashoville, NC 28804 (828)254-7576 Enclosed are the analytical results for sample(s) received by the laboratory on November 03, 2015. The results relate only to the samples included in this report. Results reported herein conform to the most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. If you have any questions concerning this report, please feel free to contact me. Sincerely, Chris Derouen christopher.derouen@pacelabs.com Project Manager Enclosures �e p,CUi��f TN14 t4eORA�� REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 1 of 11 (�IaceAnalyticala w ww.Pecelabs.c= Project: Onslow NPDES 1113 Pace Project No.: 92274445 Raleigh Certification IDs 6701 Conference Drive, Raleigh, NC 27607 North Carolina Wastewater Certification #: 67 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87648 Massachusetts Certification #: M-NCO30 North Carolina Drinking Water Certification #: 37712 CERTIFICATIONS North Carolina Bioassay Certification #: 16 North Carolina Drinking Water Certification #: 37731 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 West Virginia Certification #: 356 Virginia/VELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc„ Page 2 of 11 lacmnalyfical* wwwpaoalabs =n SAMPLE ANALYTE COUNT Project: Onslow NPDES 1113 Pace Project No.: 92274445 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Analyses Lab ID Sample ID Method Analysts Reported Laboratory 92274445001 OUTFALL 3 SM 9222D RC 1 PASI-R SM 2WD SAM 1 PASI-A M 5220D WRC 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 3 of 11 0 IacleAnalj4ical (�www.p&*Abs.=n ANALYTICAL RESULTS Project: Onslow NPDES 1113 Pace Project No.: 92274445 Pace Analytical Services, Inc. 2225 Riverside dr. Asheville, NC 28804 (828)254-7176 Sample: OUTFALL 3 Lab ID: 92274"5001 Collected: 111103115 10:30 Received: 11/03/15 13:50 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual MBIO 9222D Fecal Coliform RAIL Analytical Method: SM 9222D Fecal Coliforms 20000 CFU1100 mL 1.0 1 11/03/15 15:24 2540D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids 32.2 mg1L 6.2 1 11/05/15 10:11 5220D COD Analytical Method: SM 5220D Chemical Oxygen Demand 118 mg1L 25.0 1 11/09/15 13:40 Date: 11/10/2016 03:00 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 4 of 11 (�Iacmnalyfical* www.pacefabs.com QUALITY CONTROL DATA Project: Onslow NPDES 1113 Pace Project No.: 92274446 QC Batch: RB1015670 Analysis Method: SM 9222D QC Batch Method: SM 9222D Analysis Description: 92220 MBIO Fecal Coliform - RAL Associated Lab Samples: 92274445001 METHOD BLANK: 1598247 Matrix: Water Associated Lab Samples: 92274445001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Fecal Coliforms CFU/100 mL ND 1.0 11/03/15 15:24 SAMPLE DUPLICATE: 1598248 92274424001 Dup Parameter Units Result Result RPD Qualifiers Fecal Coliforms CFU1100 mL 172 91.0 62 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 288104 (828)254-7176 Results presented on this page are In the units Indicated by the "Units" column arc*pt where an alternate unit is presented to the right of the result REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. Date: 11/10/2015 03:00 PM without the written consent of Pace Analytical Services, Inc.. Page 5 of 11 laneAnalyticale wrvw.paceWmcom QUALITY CONTROL DATA Project: Onslow NPDES 1113 Pace Project No.: 92274445 QC Batch: WET141221 Analysis Method: SM 2540D QC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids Associated Lab Samples: 92274445001 METHOD BLANK: 1599363 Matrix: Water Associated Lab Samples: 92274445001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mg1L ND 2.5 11/05/15 10:06 LABORATORY CONTROL SAMPLE: 1599364 Spike Parameter Units Cone, Total Suspended Solids mg1L 250 SAMPLE DUPLICATE: 1599365 92274774001 Parameter Units Result Total Suspended Solids mg/L 97.3 LCS LCS Result % Rec 252 101 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 % Rec Limits Qualifiers 90-110 Dup Result RPD Qualifiers 131 30 D6 SAMPLE DUPLICATE: 1599366 92274544001 Dup Parameter Units Result Result Total Suspended Solids mg1L 10.2 14.2 RPD Qualifiers 33 D6 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. Date: 11/10/2015 03:00 PM without the wntten consent of Pace Analytical Services, Inc.. Page 6 of 11 (�IacieAnalytical" ~..psceiabs.00rn Project: Onslow, NPDES 11/3 Pace Project No.: 92274445 QC Batch: WETA/25312 QC Balch Method: SM 5220D Associated Lab Samples: 92274445001 METHOD BLANK: 1602017 Associated Lab Samples: 92274445001 Parameter Units Chemical Oxygen Demand mg1L LABORATORY CONTROL SAMPLE: 1602018 Parameter Units Chemical Oxygen Demand mg/L Pace Analytical Services, Inc'. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Analysis Method: SM 5220D Analysis Description: 5220D COD Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 25.0 11/09115 13:40 Spike LCS LCS % Rec Cone. Result % Rec Limits Qualifiers 750 742 99 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1602019 1602020 MS MSD 92274934001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cone. 'Cone. Result Result % Rec % Rec Limits RPD Qual Chemical Oxygen Demand mg1L 1740 3000 3000 4350 4350 87 87 90-110 0 M1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1602021 1602022 MS MSD 92274962001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual Chemical Oxygen Demand mg/L 40.0 750 750 729 729 92 92 90-110 0 Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11 /1012015 03:00 PM without the written consent of Pace Analytical Services, Inc.. Page 7 of 11 (�Iac,M.nalXimftpacelabs.cam QUALIFIERS Project: Onslow NPDES 1113 Pace Project No.: 92274445 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit. Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosod iphenyla mine decomposes and cannot be separated from Diphen, amine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TIN accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. LABORATORIES PAST -A Pace Analytical Services -Asheville PASI-R Pace Analytical Services - Raleigh ANALYTE QUALIFIERS D6 The relative percent difference (RPD) between the sample and sample duplicate exceeded laboratory control limits. M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 1111 G12015 03:00 PM without the written consent of Pace Analytical Services, Inc.. Page 8 of 11 aceAnalytical wmpacelabs.wm QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Onslow NPDES 1113 Pace Project No.: 92274445 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Lab 1D Sample ID QC Batch Method QC Batch Analytical Method 92274445001 OUTFALL 3 SM 9222D RB10I5670 92274445001 OUTFALL 3 SM 2540D WET141221 92274445001 OUTFALL 3 SM 5220D WETA125312 Date: 11 /10/2015 03:00 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Analytical Batch Page 9 of 11 CHAINOF-CUSTODY/Analytical Request Document AWa The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be Completed a=vately. � eetbn A SeCOon 6 Seedon C pul»d CileM Irdortoriiori: Required Project Irdomntion? kwolve adbrmatim page 1 t3f 1 olgPW CDM R&PW TO: Forbes. Dan Artwibm. (r� F- 111'ross1 6400 Gim vwaad Am Suns 400 copy To: Campony Name; „r. . awCA NC 2M12 Addruee: Oft 1.. . -h.. ��e '7:.':• '•�I:. 7'• maik 7oae Pw4Ora- e: Pecs Ouch Dane: A t1- s- Fax PM)= Name: Ormscrw NPDes POLO PrO,OM M&WOr. Oquealed Doe Data: k Prayett M; pow prods ti. -Q COLLECTED Presar"tIVeS ;ib oMu�g w.w Ow ,� w w ww. ur,+r � z SAMPLE ID ;Y5'° 0. b STARr END y o One Characor per boa. we. wP w 11f o ri # [Ads must •} on.r of $ample Ids must be unique 7- is V � w W c0 U /►j �} '] �f 1 i 2 d DATE TIME DATETIME NO �.�� 3 b ii�3�,s tom -3 �h3}a Y y5• 'r:#�;S�,sli►+F �M�`.�DdaD1E1iF7'7!� '�,_y..'.y�,_� :9`'. _ ®. ,�-! �w,.,,r,�-��r�{•! �y'ri��4 '?!m1E.7iz �!F-a SC tet 's •ii'' "•i FQ;,ar. +1 R..;..,Se..«. • �- .Ez•a .s. �."ir'_'1' ib...I. _ •. .., y •rt 4':1 s: o> ' P. - 1 - 1113,,r 13So f i �t aar�eaet7���• ti, _;.„ky-��'if,. ,.,�Ai_ ix-.` � ';�>*'�.��:�:�r � �K:. ::k� ?F; �t,.:.: ._,e,:-..-�k��rPi' r .e • r,'t'��.i•'..�{3r1>d"�,':4j"at.x'�1P't+y"e• - .•.' . D �d PRINT Name ar 3MWLML s p g r z hH b SIGNATURE or SAMPLER DATE Slyned: f - - Document Name: Sample Condition UPpn Docume it Revised: May 15, 2015 a69An!Vlcal+ ww.4.pneerc.+nr t Recel t (SCUR) Pa e 1 of 2` Document No.: ._. Issuing Authorities: F-RAt--CS-001-rev.03 Pace Raleigh Quality Office 'Page of 2 Is for Internal Use Only Client Name:_ Courier (Circle): Fed Ex UPS USPS Client Commercial Pace Other Custody Seal on Cooler/Box Present: yes no Seals intact: Oyes no Packing Material: bubble Wrap B agstf None n Other ^- -Circle Thermometer Used: IR Gun 5 :12208538 of Ice: et lue None Samples o Ice, cooling process has begun— IR Gun B 065371 Temp Correotion Factor: Add i[ btract . Corrected Cooler Temp.: t`l r C C Date a atTissue Is Frozen: Yes d Initials of p rson examining Temp should be above freezing to 6'C Comments: Chain of Cuslod Present: oy.. ON. ONIA 1. Chain of Custody Filled Out: es ON. OwA 2. Chain of Custody Relinquished: es ON* ❑wA 3. Sampler Name & Signature on COC: 6y. ON. ❑NIA 4. Samples Arrived vrfthln Hold Time: os [IN. ❑NIA 5. Short Hold Time Analysis a72hr : j6Yes ❑No ONIA 6. Rush Turn Around Time Requested: ❑Yes Na ONIA 7. Sufficient Volume: Yes (IN. ❑wA 8. Correct Containers Used: ee ONO ❑NIA 9. -Pace Containers Used: 11 )r . ON. ❑NIA Containers Intact: 93YOS ONO ❑NIA 10. Filtered volume received for Dissolved tests ❑vas ONO NIA 11, Sample Labels match COC: 16YOLS ONO ❑NIA 12, ry, w„,wllwa l,apyula vpww lYa4Vll ,I... _11 W,aa.np,i. You ONO OruA 13_ All containers needing preservatlon are found to be In Yes 11 No ONIA oornpllawe with EPA recommendation. l excepGorm VOA. cdlform. TOC. OdG, WI-DRO (weler) Yee ❑No Sam les checked for dechlorination: Yes ONO ONIA 14. Heads ace In VOA Vials ?6mm : ❑Yos ONO NIA 15. Trip Blank Present: ❑Yes ONO ANIA 16, Trip Blank Custody Seals Present ❑Yea ❑No NIA Pace Trip Blank Lot # if purchased): Client Notification/ Resolution: Fleld Data IF equfred7 Y / N Person Contacted: Datefflmu: C-�mmentsl Resc•'utlu: . SCURF ISRF Date: t� f , y WO : 92274445 Review:: Note: Whenever Ihere Is a discrepancy affecting North Carlo compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certllicallon Office ( 1.9 out of hold, Incorrect preservative, out of temp, 92274445 Incorrect containers) • I Page 11 of 11 I CDM Smith 5400 Glenwood Avenue, Suite 400 Raleigh, North Carolina 27612 tel: 919-787-5620 fax: 919-791-5730 November 23, 2015 REcEI ED Attention: DWQ Central Files CENTRAL North Carolina Department of SECTION Environmental Quality Division of Water Quality 1617 Mail Service Center Raleigh, North Carolina 27699-1617 Subject: Outfall 3 Discharge Monitoring Report - Tier 2 Response Monitoring Period - November 2015 Onslow County Landfill - Permit Number 67-09 Certificate of Coverage Number - NCG120023 To the Division of Water Quality: CDM Smith Inc., on behalf of Onslow County (County), is submitting two copies of the Stormwater Discharge Monitoring Report for Outfall 3. Samples collected from Outfall 3 during the 2014 semi-annual sampling events had detections of fecal coliform and chemical oxygen demand (COD) above the benchmark values. Stormwater from the outfall is discharged to a former borrow pit and does not leave the property. In response to the benchmark value exceedances, the County implemented Tier 1 and 2 responses. Samples were collected from Outfall 3 on November 3, 2015, and were analyzed for COD, fecal coliform, and total suspended solids (TSS). COD was detected at 118 milligrams per liter (mg/L), fecal coliform was detected at 20,000 colonies per 100 milliliters, and TSS were detected at 32.2 mg/L. The fecal coliform detection was above the benchmark value. Per the Tier 2 response requirements, samples will be collected monthly for all parameters from Outfall 3 until three consecutive sampling events show the parameters are below the benchmark values. Monthly monitoring in accordance with the Tier 2 requirements will continue. The County will maintain a record of the Tier 1 and 2 responses and monitoring results at the landfill. 0 WATER + E14VIRONMENT +TRANSPORTATION + ENERGY + FACILITIES CDM Division of Water Quality November 23, 2015 Page 2 If you have any questions or require further explanation, do not hesitate to call me at (919) 325-3566. Sincerely, Daniel H. Forbes CDM Smith Inc. cc: Scott Bost, Onslow County Mathew Colone, CDM Smith Inc. Semi-annual Stormwater Disc_haree Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG120000 Date submitted November 23, 201.5 CERTIFICATE OF COVERAGE NO. NCG12 0 0 2 3 FACILITY NAME Onslow County Landfill COUNTY Onslow PERSON COLLECTING.SAMPLES No Samples Collected LABORATORY Lab Cert. # - Comments on sample collection or analysis: - Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR 2015 SAMPLE PERIOD ❑ Jan -June ❑ July -Dec or © Monthly' _ October (month) DISCHARGING TO CLASS ❑ORW- ❑HQW- ❑Trout- ❑P-NA ❑Zero -flow ❑Water supply- ❑SA- ®Other- - Forme , Borrow. Pit. PLEASE REMEMBER TO SIGN ON THE REVERSE c� 0 No discharge this period?' G Outfall No. Date Sample Collected' imp/ Collected' 24-hour rainfall amoun, t Inches"Chemical oxygen Demand Fecal Coliform Total Suspended Solids Benchmarks 120 mg/L 1000 count per 100 mL 100 mg/L or 50 mg/L4 3 W _M 1 Monthly sampling (instead of semi-annual) must begin with the second consecutive, benchmark.exceedance.for.the same: parameter at the same:outfall. 2 For sampling periods with no discharge at any single outfall, you must -still submit.this discharge -monitoring -report with a-checkmark here.- 3 The total precipitationmust be recorded using data from -an on -site rain gauge. Unattended -sites may -be eligible fora waiver -of -the rain gauge requirement. ° See GeneralPermittext, Table 3; identifyingtheespecially sensitive receiving water"classifications,where the -more protective benchmark applies: - Note: Results must be reported in numerical format. For example, do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non - numerical format. When results are below the applicable limits, they must be reported in the format, "<XX mg/L", where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Conversely, where fecal coliform results exceed the dilution upper limit, report the result as ">XX". Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2,-or Tier-3-responses. See -General Permit text. Permit Date: 11/1/2012-10/31/2017 SWU-248, last revised 10/25/2012 Page 1 of 2 Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month.. ❑ No discharge this period?z Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount; Inches3 ,Non -polar O&G/TPH by EPA 1664 (SGT-HEM) Total Suspended Solids pH Benchmarks—> - - 15 mg/L 100 mg/L or50 mg/L 6:0 — 9.0 SU Footnotes from Part A also apply to this-Part-B- Note: If you report a sample value in excess of the benchmark; you must implement firer I,- Tier 2,-or Tier 3 responses.- See General °Permit text. FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS_ -SEE-PERMIT PART Ii-SECTION-B. • 2 EXCEFDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2'REQUIREMENTS: SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ® NO ❑ IF YES; HAVE YOU CONTACTED THE DWQ'REGIONAL OFFICE? YES JX_1 NO°❑ REGIONAL OFFICE CONTACT NAME: Bethany G4%Of�OUIIaS Mail an original and one copy of this DMR, includina all `No Discharae" reports, within 30 days of receipt of the lab results for at end of monitarina period in the case of "No Discharae" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the:best.of my knowledge and belief,.true, accurate, and complete. I am aware that there are significant penalties for submitting fafse information, including the possibility of fines and imprisonment for.:knowing violations ° of Permitteej Permit Date:11/1/2012-10/31/2017 (Date) SWU-248, last revised 10/2S/2012 Page 2 of 2 I CDM Smith 5400 Glenwood Avenue, Suite 400 Raleigh, North Carolina 27612 tel: 919-325-3500 fax: 919-781-5730 November 23, 2015 Attention: DWQ Central Files North Carolina Department of Environmental Quality Division of Water Quality 1617 Mail Service Center Raleigh, North Carolina 27699-1617 RECEIVE® NOV 3 A 2015 09NTRAL FILES DWR SECTION Subject: Outfall 3 Discharge Monitoring Report - Tier 2 Response Monitoring Period - October 2015 Onsl.ow County Landfill Certificate of Coverage Number - NCG120023 To the Division of Water Quality: CDM Smith Inc., on behalf of Onslow County (County), is submitting two copies of the Stormwater Discharge Monitoring Report for Outfall 3. Samples collected from Outfall 3 during the 2014 semi-annual sampling events had detections of fecal coliform and chemical oxygen demand above the benchmark values. In response to the benchmark value exceedances, the County implemented Tier 1 and 2 responses. There was no discharge from Outfall 3 in October 2015. Per the Tier II response requirements, samples will be collected monthly for all parameters from Outfall 3 until three consecutive sampling events show the parameters are below the benchmark values. The County will maintain a record of the Tier 1 and 2 responses and monitoring results at the landfill. If you have any questions or require further explanation, do not hesitate to call me at (919) 325-3566. Sincerely, Daniel H. Forbes CDM Smith Inc. cc: Scott Bost, Onslow County Mathew Colone, CDM Smith Inc. is WATER + ENVIRONMENT + TRANSPORTATION + ENERGY + FACILITIES Semi-annual Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG120000 Date submitted November 11, 2015 CERTIFICATE OF COVERAGE NO. NCG12 0 0 2 3 FACILITY NAME Onslow County La ill COUNTY Onslow PERSON COLLECTING SAMPLES Daniel Forbes LABORATORY Pace Analytical, Inc. Lab Cert. # 3771:2/37731 Comments on sample collection or analysis: Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR 2015 SAMPLE PERIOD ❑ Jan -June. X❑ July -Dec or © Monthly' September (month) DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA ❑Zero -flow ❑WaterSupply ❑SA QOther Former Borrow Pit PLEASE REMEMBER TO SIGN ON THE REVERSE 4 No discharge this period?2 Outfall No. Date Sample Collected jmo/dd/yr) 24-hour rainfall amount, Inches" Chemical Oxygen Demand Fecal Coliform Total Suspended Solids Benchmarks ===> - - 120 mg/L 1000 count per 100 ml. 100 mg/L or 50 mg/L4 2 9/28/15 0.62 3 +.0 1,000 3.7 3 9/28/15 0.62 130 6,000 30.7 lm s Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same-parameterat the'same-outfall. Z For sampling periods with no -discharge -at -any single outfall, you must -still submit this discharge monitoring report with:a checkmark:here: - 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible fora waiver of the. rain.gauge requirement.. 4 See General Permit text, Table 3, identifying the especially sensitive receiving water rclassifications where the more protective benchmark°applies. Note: Results must be reported in numerical format. For example, do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non - numerical format. When results are below the-applicable°limits; they -must -be reported in the format "<XX-me/t -where-XX-is the -numerical value -of the detection limit, reporting limit, etc. in mg/L. Conversely, where fecal coliform results exceed the dilution upper limit, report the result as ">XX". Note: If you report a sample value in excess of the benchmark, you must implement Tier1, Tier 2, or Tier 3 responses. See General Permit text. Permit Date: 11/1/2012-10/31/2017 SWU-248, last revised 10/25/2012 Page 1 of 2 Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. ❑ No discharge this period?z Outfall No. Date Sample Collected} (mo/dd/yr) 24-hour rainfall amount, Inches3 Non -polar O&G/TPH by EPA 1664 (SGT-HEM) Total Suspended Solids pN Benchmarks 15 mg/L 100 mg/L or 50 mg/0 6.0 — 9.0 SU Footnotes from Part A also apply to this Part B Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier Z, or Tier 3 responses. See General Permit text. FOR PART A AND PART B MONITORING RESULTS: . • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT -PART It SECTION B_ • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART 11 SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ® NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ® NO ❑ REGIONAL OFFICE COnITACT NAME. Qethiai; �y Geor ljouilas Mail.an original.and-one-copy of this-DMR,.includina-all "No Discharge" reports, within 30 days of receipt of the lob results for at end of monitoring period in the case of "No Discharae" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all.attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly -responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of 06rmittee) Permit Date:11/1/2012-10/31/2017 �/ram` rs (Date) SWU-248, last revised 10/25/2012 Page 2 of 2 ace Analytical www.pecelahs.mrrr October 26, 2015 Mr. Dan Forbes CDM 5400 Glenwood Ave Suite 300 Raleigh, NC 27612 RE: Project: Onslow County 9/28 Pace Project No.: 92269504 Dear Mr. Forbes: Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Enclosed are the analytical results for sample(s) received by the laboratory on September 28, 2015. The results relate only to the samples included in this report. Results reported herein conform to the most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. If you have any questions concerning this report, please Feel free to contact me. Sincerely, Chris Derouen Christopher.derouen@pacelabs.com Project Manager Enclosures pcc r `98aRAS�� REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 1 of 11 v ace Analytical ww.pacelabs.com Project: Onslow County 9128 Pace Project No.: 92269504 Raleigh Certification IDs 6701 Conference Drive, Raleigh, NC 27607 North Carolina Wastewater Certification #: 67 Pace Analytical Services, Inc. 2225 Riverside Dr, Asheville, NC 28804 (828)254-7176 Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 FloridalNELAP Certification #: E87648 Massachusetts Certification #: M-NCO30 North Carolina Drinking Water Certification #: 37712 CERTIFICATIONS North Carolina Bioassay Certification #: 16 North Carolina Drinking Water Certification #: 37731 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 West Virginia Certification #: 356 VirginiafdELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 2 of 11 aceAnalytical wwwpecalabs.rom SAMPLE ANALYTE COUNT Project: Onslow County 9128 Pace Project No.: 92269504 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Lab ID Sample ID Method Analysts Analytes Reported Laboratory 92269504001 OUTFALL 2 SM 9222D RC 1 PASI-R SM 2540D RC 1 PASI-R SM 5220D WRC 1 PASI-A 92269504002 OUTFALL 3 SM 9222D RC 1 PASI-R SM 2540D RC 1 PASI-R SM 5220D WRC 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 3 of 11 4 o lac e Analytical www.pacefahs.corrr ANALYTICAL RESULTS Project: Onslow County 9128 Pace Project No.: 92269504 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Sample: OUTFALL 2 Lab ID: 92269504001 Collected: 09/28/15 12:20 Received: 09/28/15 14:50 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual MBIO 9222D Fecal Coliform RAL Analytical Method: SM 9222D Fecal Coliforms 1800 CFU/100 mL 1.0 1 09/28/15 16:14 2540D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids 3.7 mg/L 2.5 1 09/29/15 12:40 5220D COD Analytical Method: SM 52200 Chemical Oxygen Demand 34.0 mg/L 25.0 1 10/01/15 16:00 Sample: OUTFALL 3 Lab ID: 92269504002 Collected: 09128115 12:10 Received: 09/28/15 14:50 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual MBIO 9222D Fecal Coliform RAL Analytical Method: SM 9222D Fecal Coliforms 6000 CFU1100 mL 1.0 1 09/28/15 16:14 10 2546D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids 30.7 mg1L :5,6 1 09/29/15 12:40 5220D COD Analytical Method: SM 5220D Chemical Oxygen Demand 130 mg/L 25.0 1 10/01/15 16:00 Date: 10/26/2015 05:42 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 4 of 11 aceAnalytrcal www.paralabs.com Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (628)254-7176 QUALITY CONTROL DATA Project: Onslow County 9128 Pace Project No.: 92269504 QC Batch: RBIO/5544 Analysis Method: SM 9222D QC Batch Method: SM 9222D Analysis Description: 9222D MBIO Fecal Coliform - RAIL Associated Lab Samples: 92269504001, 92269504002 METHOD BLANK: 1570917 Matrix: Water Associated Lab Samples: 92269504001, 92269504002 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Fecal Coliforms CFU1100 mL ND 1.0 09/28/15 16:14 SAMPLE DUPLICATE: 1570918 92269504001 Dup Parameter Units Result Result RPD Qualifiers Fecal Coliforms CFU1100 mL 1800 2000 11 Results presented on this page are In the units Indicated by the "Units' column except where an alternate unit is presented to the right of the result. REPORT OF LABORATOiRY ANALYSIS This report shall not be reproduced, except in full. Date: 10/26/2015 05:42 PM without the written consent of Pace Analytical Services, Inc.. Page 5 of 11 aceAnalytical wwwpecelabs com Project: Onslow County 9128 Pace Project No.: 92269504 QC Batch: RWET18693 QC Balch Method: SM 2540D Associated Lab Samples: 92269504001, 92269504002 METHOD BLANK: 1569194 Associated Lab Samples: 92269504001, 92269504002 Parameter Units Total Suspended Solids mglL LABORATORY CONTROL SAMPLE: 1569195 Parameter Units Total Suspended Solids mglL Pace Analytical Services, Inc. 2225 Riverside dr. Asheville, NC 28804 (828)254a176 QUALITY CONTROL DATA Analysis Method: SM 2540D Analysis Description: 2540D Total Suspended Solids Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 2.5 09129/1512:37 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 250 260 104 90-110 SAMPLE DUPLICATE: 1569519 92269368001 Dup Parameter Units Result Result Total Suspended Solids mglL 11.8 10.2 RPD Qualifiers 14 D6 Results presented on this page are in the units indicated by the "Units' column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/26/2015 05:42 PM without the written consent of Pace Analytical Services, Inc.. Page 6 of 11 aceAnalytical ..pacalahs.com QUALITY CONTROL DATA Project: Onslow County 9128 Pace Project No.: 92269504 QC Batch: WETA124750 Analysis Method: SM 5220D QC Batch Method: SM 5220D Analysis Description: 5220D COD Associated Lab Samples: 92269504001, 92269504002 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 METHOD BLANK: 1570935 Matrix: Water Associated Lab Samples: 92269504001, 92269504002 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Chemical Oxygen Demand mg1L NO 25.0 10/01/15 16:00 LABORATORY CONTROL SAMPLE: 1570936 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Chemical Oxygen Demand mg1L 750 731 97 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1570937 1570938 MS MSD 92269580001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Chemical Oxygen Demand mg/L 89.0 750 750 764 764 90 90 90-110 0 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1570939 1570940 MS MSD 92269653004 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Chemical Oxygen Demand mg1L ND 750 750 711 711 94 94 90-110 0 Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/26/2015 05:42 PM without the written consent of Pace Analytical Services, Inc.. Page 7 of 11 lacie'Analytical www.pecelsbs.com QUALIFIERS Project: Onslow County 9128 Pace Project No.: 92269504 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL - Adjusted Method Detection Limit. PQL - Practical Quantitation Limit, RL- Reporting Limit. Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculabie. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenyla mine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI -The NELAC Institute. LABORATORIES PASI-A Pace Analytical Services -Asheville PASI-R Pace Analytical Services - Raleigh ANALYTE QUALIFIERS 1 g This is a greater than value. D6 The relative percent difference (RPD) between the sample and sample duplicate exceeded laboratory control limits. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/26/2015 05A2 PM without the written consent of Pace Analytical Services, Inc.. Page 8 of 11 aceAnalytieal xnvw.pacsfab&=n QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Onslow County 9/28 Pace Project No.: 92269504 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Lab ID Sample ID QC Batch Method QC Batch Analytical Method 92269504001 OUTFALL 2 SM 9222D RB1015544 92269504002 OUTFALL 3 SM 9222D RB1015544 92269504001 OUTFALL 2 SM 2540D RWET/8693 92269504002 OUTFALL 3 SM 25400 RWET18693 92269504001 OUTFALL 2 SM 52200 WETA/24750 92269504002 OUTFALL 3 SM 5220D WETA/24750 Date: 10/26/2015 05:42 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Analytical Batch Page 9 of 11 ZeAnqgytical CHAIN -OF -CUSTODY 1 Analytical Request Document TAe Chain-W-Custody Is a LEGAL DOCUMENT. Ail relavaM flalds must be completed aocruatey. - •-------- Section A Section B 8e0on C Page: � of Required Cfierrt hrfomot m - Required ProJed Were Aon: IM40;w ln[ormulion: co'"0B' Caw. s; Report To: croon: y r�{I]�S 2003841 t JS1 `im Copy To' 'ma' REGULATORY AGENCY PQES I— Gmum ! UST s RCRA WATER F DRINKING WATER OTFiFR Errretl 70:y/� Purwm Order No.: Paw 0rv10 y� L CM Fe>r 32s- 3s+.c. ���, • fit- 5730 Name: ORsttd ./ Cw.,4 eLe Rid Nw�per bite Location NL ectNrasrher: PeaPreGbN: STATE - aquas tlonD CGrnt edavnrren mgbi:cods Al YRIX 1 CAOE s a. COLLECTED Preservatives 5: . Odrar}ny water DW c, Water ater wT Y PH s tj corTART re tY Q z Product 5oulsaa 51. p O y SAMPLE ID Ape �? � 7 Au „a AR d ur a z a F- Sample 0s; MUST eE UNIOUE Tissue TS O e_ r1,5181 Other OT0 W w ID O c Z` O O to C 0 J"I s I . C SD IL y DATE TIME (NOTE TIME _ _ = Z Z y M Pace Project NoJ tab I.D. j lzza 3 im 21 DytFLIA�s-,s ! zlo 3 z 3 4 S 8 T 8 9 f0 !f f2 ADDtt7ORAL GONMIENTS REtINQUISNED BYrAFFiLtA770N DATE 7 ME Y ON Tw'E SAMPLE COND111ONS r ORIGINAL SAMPLERKAMEAMSWPUTURE e PRYIT Name of SAftPtER , Q.'1; Gt "�U t• o sruRt: of s�wPLER: wae p }/ f ~ a w wn y+n; Oti Z.i' 1 ZUF v O a %Tfor{am New By sprig tills rme you we soeept6o PaWs NET 30 day wow^ t e. erW e0redrq to late ct+ar9a d lA% Aertnerrtl WTf( k- o rot Paid +Nlhin 30 ftL F-ALL-Q-Mev.07. 15-May-2007 Document Name: Sample Condition Upon Document wised: May 15, 2015 . c?C8Analgical° Receipt SCUR e 1 of 2* in Document No.: Issg Authorities: F-RAi-CS-001-rev.03 Pace Rl h Quality Office Client Name:LMVOMAA�n _ Courier (Circle): Fed Ex UPS USPS Client Commercial Pace Custody Seal on CoolerBox Present: El yes no Seals Intact: Vyes Packing Material: ❑ Bubble Wrap ags None rj Other Circle Thermometer Used: IR G20 Ty of Ice Wlue None IR Gun71 'Page 2 o 2 Is for Internal Use Only Other no Samples on i , cooling process has begun Temp Correction Factor: Ad Subtract C Date and nitials o! po on a mining Corrected Cooler Temp.: C Biological Tlssuo Is Frozen: Yes No NIA choking e P e Tamp should be above freezing to B'C Comments: Chain of Custody Present: 11YOS ONO ❑wA 1: Chain of Custody Filled Out: 04,01. ❑No ❑wA 2, Chain of Cust2gj Relinquished: ee ❑No ❑wA 3: Sampler Name R Si nature on COC: es ON., ❑wA 4. Samples Arrived within Hold Time: Yea ONO ❑wA 5. Short Hold Time Analysis <72hr : f 0yes ❑No ON/A Rush Turn Around Time Requested: ❑res No ❑NIA 7. Sufficlenl Volume: IdYes ❑No ONIA 8: Correct Containers Used: Yes ONO ❑N1A 9. -Pace Containers Used: Yes ❑No 0N1A Containers Intact: as ONO ❑NIA 10. Filtered volume received for Dissolved tests ❑Yes ONO rA 11. Sample Labels match COG: o ONO ❑N/A 12.- -Includes dateltimeAD/Anal is Matrix: All oontalners needing preservation have been chucked. n,/� ❑Na ❑N1A 13. All containers needing preservation are found to be in �W.. ❑No ❑N/A -compliance with EPA reoommendatlon. exceptions: VOA, coliform, TOC. 050. WI-DRo (water) Yea ONO Sam las checked for dechlorination: IxesONO ❑N/A 14. Heads ace in VOA Vials >6mm : Oyes ONO ❑ 15. Trip Blank Present: ©Yes ❑No 16. Trip Blank Custody Seals Present rv'A ❑Yea ONO "rr1A Pace Trip Blank Lot /1 if purchased): Client Notification/ Resolution: Person Contacted: Comments/ Resolution: SCURF/SRF Review:: Date, DateMme: Field Data 4quired? Y f N W # : 922695®4 Note! Whenever there Is a discrepancy affecting North Ca4ffni compliance sampigs, a copy of this form will be sent to the North Carolina DEHNR 1! I I I 1iI CertIffcallon Office (l.e out of hold, Incorrect preservative, out of temp, 92268504 Incorrect containers) Page 11 of 11 CDM Smith 5400 Glenwood Avenue, Suite 400 Raleigh, North Carolina 27612 tel: 919-787-5620 fax: 919-781-5730 November 11, 2015 RECEIVED Attention: Central Files NOV 16 2015 North Carolina Department of Environmental Quality CENTRAL FILES Division of Water Quality MIR SECTION 1617 Mail Service Center Raleigh, North Carolina 27699-1617 Subject: Semi -Annual Discharge Monitoring and Tier Two Sampling Report Monitoring Period: July 1 through December 31, 2015 Onslow County Landfill: Permit Number 67-09 Certificate of Coverage Number: NCG120023 To the Division of Water Quality: CDM Smith Inc., on behalf of Onslow County (County), is submitting two copies of the Stormwater Discharge Monitoring Report for the Onslow County Landfill. Samples were collected from Outfalls 2 and 3 on September 28, 2015, after the facility received 0.62 inches of precipitation. Outfall 1 currently receives stormwater runoff from the closed portion of the Subtitle D landfill and was removed from the analytical monitoring requirements following a Division of Water Quality inspection on January 23, 2013. All samples were analyzed for fecal coliform, chemical oxygen demand (COD), and total suspended solids by Pace Analytical Services, Inc. located in Raleigh, North Carolina. Samples collected from Outfall 2 were below the benchmark values with the exception of fecal coliform. Fecal coliform was detected at 1,800 colonies, per 100 milliliters (mL). The benchmark value for fecal coliform is 1,000 colonies per 100 mL. Samples collected from Outfall 3 had detections of COD (130 milligrams per liter (mg/L)) and fecal coliform (6,000 colonies per 100 mL) above their respective benchmark value. The benchmark value for COD is 120 mg/L. Tier Two monitoring was implemented for Outfall 3 in January 2015 after consecutive detections of COD above the benchmark value. Stormwater from Outfall 3 is discharged to a former borrow pit and does not leave the property. The drainage area for Outfall 3 includes the partially closed and active operations area of the east slope of the Subtitle D landfill. Elevated COD at Outfall 3 is a result of washouts on the active slope. Per the County's Tier One responses and operations plan, all washouts are repaired and the slope is reseeded as necessary following precipitation events. Per the Tier 2 response requirements, samples will be collected monthly for all parameters from Outfall 3 until three consecutive sampling events show the parameters are below the benchmark A i,t WATER + ENVIRONMENT + TRANSPORTATION + ENERGY + FACILITIES Smith Division of Water Quality November 11, 2015 Page 2 values. Monthly monitoring in accordance with the Tier, 2 requirements will continue. The County will maintain a record of the Tier 1 and 2 responses and monitoring results at the landfill. If you have any questions or require further explanation, do not hesitate to call me at (919) 325-3566. Sincerely, Daniel H. Forbes CDM Smith Inc. cc: Scott Bost, Onslow County Mathew Colone, CDM Smith Inc. Semi-annual Stormwater Discharge Monitorina Report for North Carolina Division of Water Quality General Permit No. NCG120000 Date submitted September 8, 2015 CERTIFICATE OF COVERAGE NO. NCG12 0 0 2 3 FACILITY NAME Onslow County Landfill COUNTY Onslow PERSON COLLECTING SAMPLES No Samples Collected LABORATORY Lab Cert. # Comments on sample collection or analysis: Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR 2015 SAMPLE PERIOD ❑ Jan -June ❑ July -Dec or X❑ Monthly' JUIy (month) DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA ❑Zero -flow ❑Water Supply ❑SA X❑Other Former Borrow Pit, PLEASE REMEMBER TO SIGN ON THE REVERSE F7B [_ No discharge this period?' Outfall No. -Date Sample Collected (mo/dd/yr) 24-hour rainfall amount, Inches-' Chemical Oxygen Demand Fecal Coliform Total Suspended Solids Benchmarks 120 mg/L 1000 count per100 mL 100 mg/L or 50 mg/L° 3 a. Monthly sampling -(instead of semi-annual) must begin with -the second consecutive benchmark exceedance for the same parameter at the same outfall. For.sarnpling periods with: no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The ,total .precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. " See General Permit text, Table 3, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Note: Results must be reported in numerical format. For example, do not re ort Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non - numerical format. When results are below the applicable limits, they must be reported in the format. "<XX me/L", where XX is the numerical value of the detection .limit, reporting limit, etc. in. mg/L. Conversely, where fecal coliform results exceed the dilution upper limit, report the result as ">XX". Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Permit Date: 11/1/2012-10/31/2017 SWU-248, last revised 10/25/2012 Page 1 of 2 Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. El-No-dischargethis period?z Outfall No. Date Sample Collected' (mo/dd/yr) 24-Dour rainfall amount, Inches; Non -polar O&G/TPH by EPA 1664 (SGT-HEM) Total Suspended Spuds pH Benchmarks --> _ - 15 mg/L 100 mg/L or 50 mg/L 6.0 — 9.0 SU Footnotes from Part A also apply to this Part B Note: -lf you report a -sample value in excess of the benchmark, -you must -implement rer I, Tier 2, or Tier 3 responses. See General Permit text FOR PARTA AND PARTS MONITORING RESULTS: • - A BENCHMARK EXCEE DANCE TRIGGERS TIER-1 REQUIREMENTS. SEE PERMIT PART 11 SECTION B. • 21XCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART 11 SECTION B. • TIER 3:. HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK,EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES ®NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YFs IXI NO FI REGIONAL OFFICE CONTACT NAME: Beth any Georgoulias Mail an oriainal and one copy of this DMR.-including.all 'No Discharaep reports.. -within 30 days of receipt .of -the .lab results tar at end of monitorin-a-per'a in the case of "No Discharae" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 -YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the Information submitted. Based on my inquiry of the person or persons who manage the system, or those persons -directly responsible forgathering the information, -the information submitted -is; to the°best of my knowledge and -belief; true; accurate, and complete. 1 - am aware that there are significant penalties for submitting -false information; including the possibilityofAnes and:imprisonment:for knowing violations." (Signature of Permittee) Permit Date:11/1/2012-10/31/2017 (Date) SW U-248, last revised 10/25/2012 Page 2 of 2 Crnith 5400 Glenwood Avenue, Suite 400 Raleigh, North Carolina 27612 tel: 919-325-3500 fax; 919-781-5730 September 8, 2015 Attention: DWQ Central Files North Carolina Department of Environment and Natural Resources Division of Water Quality 1617 Mail Service Center Raleigh, North Carolina 27699-1617 Subject: Outfall 3 Discharge Monitoring Report - Tier 2 Response Monitoring Period - July 2015 Onslow County Landfill Certificate of Coverage Number - NC13120023 To the Division of Water Quality: RECIE11 0- VED SEP 15 Z015 CENTRAL FILE DWR SECTION CDM Smith Inc., on behalf of Onslow County (County), is submitting two copies of the Stormwater Discharge Monitoring Report for Outfall 3. Samples collected from Outfall 3 during the 2014 semi-annual sampling events had detections of fecal c:oliform and chemical oxygen demand above the benchmark values. In response to the benchmark value exceedances, the County. implemented Tier 1 and 2 responses. There was no discharge from Outfall 3 in July 2015. Per the Tier II response requirements, samples will be collected monthly for all parameters from Outfall 3 until three consecutive sampling events show the parameters are below the benchmark values. The County will maintain a record of the Tier 1 and 2 responses and monitoring results at the landfill. If you have any questions or require further explanation, do not hesitate to call me at (919) 325-3566. Sincerely, Daniel H. Forbes CDM Smith Inc. cc: Scott Bost, Onslow County Mathew Colone, CDM Smith Inc. 04 WATER + ENVIRONMENT + TRANSPORTATION + ENERGY + FACILITIES -Semi-annual Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG120000 Date submitted September 8, 2015 CERTIFICATE OF COVERAGE NO. NCG12 0 0 2 3 -FACILITY NAME Onslow County Landfill COUNTY Onslow PERSON COLLECTING SAMPLES Janelle Bauer LABORATORY Pace Analytical, InC. Lab Cert. # 37712/37731 -Comments-on.sample ,collection or analysis: PartA:-Stormwater,Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR 2015 SAMPLE PERIOD ❑ Jan -June ❑ July -Dec or 0 Monthly" August (month) DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA ❑Zero -flow ❑Water Supply ❑SA X❑Other Former Borrow Pit PLEASE REMEMBER TO SIGN ON THE REVERSE 4 ❑ No discharge this perrod?2 Outfall No. Date Sample Collected (mo/dd/yr) 24-hour rainfall amount, Inches3 Chemical Oxygen Demand Fecal Coliform Total Suspended Solids -Benchmarks ===: - - -120 mg/L 1000 count per 100'mL 100 mg/L or 50 mg/L" 3 8/27/15 1.03 173 21,000 555 C7 N 1.Monthly. sampling (instead .of.semi-annual).must.begin.with . thesecond consecutive.benchmark exceedance for the same parameter at the same outfall. Z-For_sampling:periods-with 7no discharge -at any single-outfall; you must -still submit this discharge monitoring report with a checkmark here. 3The total. precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. " See General Permit text, Table 3, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Note: Results must be reported in numerical format. For example, do.not.report Below Detection .Limit, BDL, <PQL,.Non-detect, ND, or other similar non - numerical format. When results are below the applicable limits, they must be reported in the format. "<XX mg/L", where XX is the numerical value of the detection limit, reporting limit, -etc: in-mg/L.- Conversely, where:fecal-coliform results -exceed. -the dilution -upper limit, report the result as ">XX". --Note if you report a sample value -in -excess -of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Permit Date: 11/1/2012-10/31/2017 SWU-248, last revised 10/25/2012 Page 1 of 2 Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. No discharge this period?' Outfall No. Date Sample Collected (mo/dd/yr) 24-hour rainfall amount, Inches3 Non -polar O&G/TPH by EPA 1664 (SGT-HEM} Total Suspended Solids pH Benchmarks => _ - 15 mg/L 100 mg/L or 50 mg/0 6.0 -- 9.0 SU Footnotes from Part A also apply to this Part B Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. FOR PART A AND PARTS MONITORIN-G RESULTS: _A BENCHMARK-EXCEEDANCE TRIGGERS-TIER-1 REQUIREMENTS. -SEE PERMIT PART II SECTION B. • 2-EXCEEDANCES IN A -ROW -FOR THE-SAM. E-PARAMETER AT THE SAME OUTFALL-TRIGGER TIER 2-REQUIREMENTS. SEE PERMIT PART II SECTION B. • 7IER3:_ HAS. YOUR FACILITY.HAD-4.0R MORE-BENCHMARK.EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL7 YES M—NO n IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ®NO REGIONAL.OFFICE,CONTACT NAME: Bethany GeorgOUfas Malf an-oriainafand one copy of this,-DMR, includina_all "No Discharae" reports within 30 days of receipt of the lob results for at end ofmonitorina period in the case of Discharae" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION_ FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware tl" there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Date) Permit:Date: 11/1/2012-10/31/2017 SWU-248, last revised 10/25/2012 Page 2 of 2 I CDM Smith 5400 Glenwood Avenue, Suite 400 Raleigh, North Carolina 27612 tel: 919-787-5620 fax: 919-781-5730 September 8, 2015 Attention: DWQ Central Files North Carolina Department of Environment and Natural Resources Division of Water Quality 1617 Mail Service Center Raleigh, North Carolina 27699-1617 RECEIVED SEP 15 2015 CENTRAL FILES OWR SECTION Subject: Outfall 3 Discharge Monitoring Report - Tier 2 Response Monitoring Period - August 2015 Onslow County Landfill - Permit Number 67-09 Certificate of Coverage Number - NCG120023 To the Division of Water Quality: CDM Smith Inc., on behalf of Onslow County (County), is submitting two copies of the Stormwater Discharge Monitoring Report for Outfall 3. Samples collected from Outfall 3 during the 2014 semi-annual sampling events had detections of fecal coliform and chemical oxygen demand (COD) above the benchmark values. Stormwater from the outfall is discharged to a former borrow pit and does not leave the property. In response to the benchmark value exceedances, the County implemented Tier 1 and 2 responses. Samples were collected from Outfall 3 on August 27, 2015, and were analyzed for COD, fecal coliform, and total suspended solids (TSS). COD was detected at 173 milligrams per liter (mg/L), fecal coliform was detected at 21,006 colonies per 100 milliliters, and TSS were detected at 556 mg/L. These detections were above the benchmark values. Per the Tier 2 response requirements, samples will be collected monthly for all parameters from Outfall 3 until three consecutive sampling events show the parameters are below the benchmark values. Monthly monitoring in accordance with the Tier 2 requirements will continue. The County will maintain a record of the Tier 1 and 2 responses and monitoring results at the landfill. Ot WATER + ENVIRONMENT +TRANSPORTATION + ENERGY + FACILITIES Division of Water Quality September 8, 2015 Page 2 If you have any questions or require further explanation, do not hesitate to call me at (919) 325-3566. Sincerely, Daniel H. Forbes CDM Smith Inc. cc: Scott Bost, Onslow County Mathew Colone, CDM Smith Inc. acMnalytical' l�rwwpacefabs.com Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 September 03, 2015 Mr. Dan Forbes CDM 5400 Glenwood Ave Suite 300 Raleigh, NC 27612 RE: Project: 4nslow County LF 8127 Pace Project No.: 92265296 Dear Mr. Forbes: Enclosed are the analytical results for sample(s) received by the laboratory on August 27, 2015. The results relate only to the samples included in this report. Results reported herein conform to the most current TNI standards and the laboratory's Qualify Assurance Manual, where applicable, unless otherwise noted in the body of the report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. If you have any questions concerning this report, please feel free to contact me. Sincerely, Chris Derouen christopher.derouen@pacelabs.com Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 1 of 11 acmnalyficalo ~..pecelabs.cam Project: Onslow County LF 8127 Pace Project No.: 92265296 Raleigh Certification IDs 6701 Conference Drive, Raleigh, NC 27607 North Carolina Wastewater Certification M 67 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification M E87648 Massachusetts Certification M M-NC030 North Carolina Drinking Water Certification #: 37712 CERTIFICATIONS North Carolina Bioassay Certification M 16 North Carolina Drinking Water Certification M 37731 North Carolina Wastewater Certification M 40 South Carolina Certification #: 99030004 West Virginia Certification M 356 VirginiaNELAP Certification M 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 2 of 11 aceARaly�ical� ivww.pecalabs.corrr SAMPLE ANALWE COUNT Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Project: Pace Project No.: Onslow County LF 8/27 92265296 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92265296001 OUTFALL 3 SM 9222D JW1 1 PASI-R SM 2540D RC 1 PASI-R SM 5220D EWS 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Without the written consent of Pace Analytical Services, Inc.. Page 3 of 11 aceAnalytical .ww'Pecelabs.com Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 26804 (828)254-7176 ANALYTICAL RESULTS Project: Onslow County LF 8127 Pace Project No.: 92265296 Sample: OUTFALL 3 Lab ID: 92265296001 Collected: 013/27/15 12:15 Received: 08/27/15 14:15 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual MBIO 9222D Fecal Coliform RAL Analytical Method: SM 9222D Fecal Coliforms 21000 CFU1100 mL 1.0 1 08/27/15 15:40 2540D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids 556 mg/L 50.0 1 08/28/15 09:00 5220D COD Analytical Method: SM 5220D Chemical Oxygen Demand 173 mg/L 25.0 1 09/02/16 09:00 Date: 09/03/2015 02:03 PM REPORT OF UtBORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 4 of 11 acmnalytical 'WWW.pncelaftcom Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NG 28804 (828)254-7176 Project: Onslow County LF 8127 Pace Project No.: 92265296 QC Batch: RBIO/5429 QC Batch Method: SM 9222D Associated Lab Samples: 92265296001 METHOD BLANK: 1544272 Associated Lab Samples: 92265296001 Parameter Units Fecal Coliforms CFU1100 mL SAMPLE DUPLICATE: 1544273 Parameter Fecal Coliforms QUALITY CONTROL DATA Analysis Method: Analysis Description: Matrix: Water SM 9222D 9222D MBIO Fecal Coliform - RAL Blank Reporting Result Limit Analyzed ND 1.0 08127/1515:40 92265172001 Dup Units Result Result RPD CFU/100 mL ND ND Qualifiers Qualifiers Results presented on this page are In the units Indicated by the "Unitr' column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not, be reproduced, except in full, Date: 09/03/2015 02:03 PM without the written consent of Pace Analytical Services, Inc.. Page 5 of 11 IeAnalytical Www.peoekbs.00m Project: Onslow County LF 8127 Pace Project No.: 92265296 QC Batch: RWET/8618 QC Batch Method: SM 2540D Associated Lab Samples: 92265296001 METHOD BLANK: 1543679 Associated Lab Samples: 92265296001 Parameter Units Total Suspended Solids mg/L LABORATORY CONTROL SAMPLE: 1543680 Parameter Units Total Suspended Solids mg/L SAMPLE DUPLICATE: 1543681 Parameter Units Total Suspended Solids mg/L SAMPLE DUPLICATE: 1543682 Parameter Units Total Suspended Solids mg/L QUALITY CONTROL DATA Analysis Method: SM 2540D Analysis Description: 2540D Total Suspended Solids Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 2.5 08/28/15 08:53 Spike I_CS Conc. Result 250 248 92265097003 Dup Result Result 356 352 92265307003 Dup Result Result 336 304 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 LCS % Rec % Rec Limits Qualifiers 99 90-110 RPD Qualifiers 1 RPD Qualifiers 10 D6 Results presented on this page are in the units indicated by the 'Units' column except where an alternate unit is presented to the right of the result REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 09/03/2015 02:03 PM without the written consent of Pace Analytical Services, Inc.. Page 6 of 11 • aceAnalytical WW..pacel8bxcom QUALITY CONTROL DATA Project: Onslow County LF 8127 Pace Project No.: 92265296 QC Batch: WETA124335 Analysis Method: SM 5220D QC Batch Method: SM 52200 Analysis Description: 5220D COD Associated Lab Samples: 92265296001 METHOD BLANK: 1545691 Associated Lab Samples: 92265296001 Parameter Units Chemical Oxygen Demand mglL Matrix: Water Blank Reporting Result Limit Analyzer! Qualifiers ND 25.0 09/02/15 09:00 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 LABORATORY CONTROL SAMPLE: 1545692 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Chemical Oxygen Demand mglL 750 742 99 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1545693 1545694 MS MSD 92265296001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RP❑ Qual Chemical Oxygen Demand mg1L 173 750 750 885 874 95 93 90-110 1 Results presented on this page are In the units Indlcated by the "ttnits" column except where an alternate unit Is presented to the right or the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in Full, Date: 09/03/2015 02:03 PM without the written consent of Pace Analytical Services, Inc.. Page 7 of 11 0 aceAnalyircal ~.paceW&corn QUALIFIERS Project: Onslow County LF 8127 Pace Project No.: 92265296 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL- Reporting Limit. Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azt,benzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calcuiable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI -The NELAC Institute. LABORATORIES PASI-A Pace Analytical Services - Asheville PASI-R Pace Analytical Services - Raleigh ANALYTE QUALIFIERS D6 The relative percent difference (RPD) between the sample and sample duplicate exceeded laboratory control limits. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 09/03/2015 02:03 PM without the written consent of Pace Analytical Services, Inc.. Page 8 of 11 aceAnalytical. .www.pacehftcom QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Onslow County LF 8127 Pace Project No.: 92265296 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 288G4 (828)254-7176 Lab ID Sample ID QC Batch Method QC Batch Analytical Method 92265296001 OUTFALL 3 SM 9222D R131015429 92265296001 OUTFALL 3 SM 2540D RWET18618 92265296001 OUTFALL 3 SM 5220D WETA124335 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Analytical Batch Date: 09/03/2015 02:03 PM Page 9 of 11 ..-Paceft"i al' . �Y, u CHAIN -OF -CUSTODY 1 Analytical Request Document The Chein•ar-� is a LEGAL DOCUMENT. AS relevant f kJ3 Must be compWW acaft)Ny. C) Seetlan A Socuon B Section C Page t of RogWmd Client Inbmwjom s Required Projefl IMomlason: C0 Pw- RapersTa r' Invoice lnform�oon: 1821031 C D M bfn%T, �}`. ocM wEe rJ J Adl—SII 1Pli d �. sq.4,4% Copy T � eoo�pany rvame: REGULATORY AGENCY r' ter gh , N L J.-+(l fjy Addrew ! NPDES f- GROUNDWATER F DRINKING WATER f` UST f' RCRA F- OTHER Emell To: y., Purchase cl �� V�S G(M};��ti Ordor No.: Pace ouae R.twwsa: PNa-- t n loA Cad n LF ' 31to Lora n J SiArL: N Requested Due DaWFAT_ project Nwrocr: Vrartrr. Requested Arm"Is Fdtargd (YIN) ' SecliOn D MsMbc Codes R.gwnaCaani eybmo7ae tienTstnt 7 ease COLLECTED 4 PfessrvaLlves 4 OrG" Wmw taw vVator WT a p x o WaLu ww m exra Posirs START ooaraosrE MOM" � J LUsaroa •: d SL SAMPLE ID _ w� °�, 40 u Sample IDS MUST BE UNIQUE Tkssuo TS O a Omw Q'f V H Q m ^ o T v �oQ oyes s f��CSZ�G DATE TIME oATE nME _ 01 x x x z j~ z 2, o 1"a y 10 12 Pate Project NoJ Lab I.D. ,CQ0 u 1 I c, 2 s s e 7 a 9 10 „ 't2 RJIME APMT"COMMEWMRELINQUISHED$YIAFFIL4ITION DATE ! DATE. TOMSAMPL6CONDTT10N3 I ORIGINAL SIWPLERNAMEAMSIGAATURE PRIM' Name of SAMPLErt x -a E DTE stGNATUREofSAMPLER. (Mm orm,, 'W00AW N" ay spry V Me loom you era 1 ro=W. p Pace,$ NET 30 6ay Payroare %= am apwing 10 Lyle charges ar t-S% par arorm 1ao arty u J, no$ pate ehMn 30 says. Fti4LL•0-020rev. , t M2v- Document Name: Sample Conditlon Upon Document Revised: May 15, 2015 / !2c6AwricaI" Recef f SCUR Page 1 of 2• Document No.: Issuing Authorities: '"`�'� F-RAl_-CS-001-rev.03 Pace Raleigh Quality Office Client Name: Af1 Courier (Circle): Fed Ex UPS USPS Client Commercial Pace Custody Seal on Cooler/Box Present: yes no Seals Intact: Wyes Packing Material, ❑ Bubble Wrap Bubble Sags None Other r Circle Thermometer Used., IR Gun :122065387 ;e of Ice' W� Blue None IR Gun BrA-Up-5f-1220607t 'Page 2 of 2 Is for Internal Use Only Other_ no Samples on Ice, cooling process has begun Temp Correctlon'Factor, Add I �WtraicLcznA IC .Corrected Cooler Temp.: 3 C Biological Tissue Is Frozen: Yes u N41 Temp shourd be above freezing to 61C Comments,. Date and Initials of perso examining check. c t I ese A Chain of Custody present: J6y14 ON. ❑WA 1. Chain ofCiJsIody Filled Out: 1116Yuu ❑No ❑NIA 2_ Chain of Custody Relinquished: VYoa ❑No ❑NIA 3. Sam�ler Name & Si nature on COO: j6Y. [IN. ❑NIA 4. Samples Arrived within Hold Time: Yes ❑No ❑NIA 15. Short Hold Time Analysis a72hr : Yes ❑No ❑NIA 8. . Rush Turn Around Time Requested: ❑Yea Na OWA 7. Sufficlenl Volume: 19yos ❑No ❑NlA 8. Correct Containers Used: -Pace Containers Used: Yes ❑No Yes ❑No ❑NIA ❑NIA 9.` Containers Intact: Yes ❑No ❑NIA 10. Filtered volume received for Dissolved tests [:]Yes ❑No NIA 11. Sample labels match COC: -Includes clateltime/lDlAnalyals Matrix: Yas ❑No ❑NIA 12. Ali containers needing preservation have been checked. Ali containers need<ng preservation are found to t>e In compliance with EPA recommendation, anceptions: VOA. coliform, TOC, O&ti. Wl- RO (water) QYe9 ❑No You ❑No . Yes ❑No ❑N/A ❑NIA 13. Samples checked fcr dechlorinalion: Yes ❑No ❑N1A 14, Reads ace in VOA Vials >6mm : ❑Yes ❑No Trip Blank Present: Trip Blank Custody Seals Present Pace Trip Blank Lot # if purchased : OYes ONo DYes ❑No 115. MI16. NIA Client NOtificationl Resolution: Field -Data Required? Y 1 N Person Contacted: Datemme: Comments/ Resolution: - SCURF /SRF !L Rate:Kj W®# : _ 92265296 Review:; r pp pp ++ I Note: Whenever there is a discrepancy affecting North Carolina compliance) samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office ( Le out of hold, incorrect proservative, out of temp, 92265296 Incorrect containers) -, Page II of11 -Semi-annual=Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG120000 Date submitted July 20, 2015 CERTIFICATE OF COVERAGE NO: NCG12 0 0 2. 3 FACILITY NAME Onslow County Landfill COUNTY Onslow PERSON;COLLECTING SAMPLES Daniel Forbes LABORATORY Pace Analytical, InC. Lab Cert. # 37712/37731 Comments on sample collection or analysis: Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR 2015 SAMPLE PERIOD ❑ Jan -June ❑ July -Dec or X❑ Monthly' June (month) DISCHARGING TO CLASS ❑X ORW ❑HQW ❑Trout ❑PNA ❑Zero -flow ❑Water Supply [_]SA Mother Former Borrow Pit PLEASE REMEMBER TO SIGN ON THE REVERSE -) No discharge this period? Outfall No. Date Sample Collected (mo/dd/yr) 24hour rainfall amount, Inches3 Chemical Oxygen Demand Fecal Coliform Total Suspended Solids .Benchmarks ===> _ - 120.mg/L 1000 count per 100 mL 100 mg/L or SO mg/L 3 6/30/15 2.42 142 1,800 49.5 I Month ly.sampling.(instead-of semi-annual),must begin -with -the second. consecutive- bench mark exceedance for-thesame-parameter at the same outfall. z.For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring. report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. 4 See General Permit text, Table 3, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Note: Results must be reported in numerical format. For example, do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non - numerical format. When results are below the applicable limits, they must be reported in the format, "<XX mg/L", where XX is the numerical value of the detection. limit, reporting limit, etc. in mg/L. Conversely, where fecal coliform results exceed the dilution upper limit, report the result as ">XX". -Note: - if -you report asample value -in excess of the benchmark; you must -implement -Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Permit Date: 11/1/2012-10/31/2017 SWU-248, last revised 10/25/2012 Page 1 of 2 Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. ❑ No discharge this period?2 Outfall Na. Date Sample Collected' (mo/dd/yr} 24•hour rainfall amount, Inches Non -polar O&G/TPH by EPA 1664 (SGT-HEM) Total Suspended Solids pH 9enchmarks =} _ - 15 mg/L 100 mg/L a r SO mg/L 6.0 — 9.0 SU Footnotes from Part A also apply to this Part B Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. FOR PART A AND PART 8 MONITORING RESULTS: • A BENCHMARK £XCEEDANCE TRIGGERS TIER 1 REQUIREMENTS, SEE PERMIT PART 11 SECTION a. • 2 EXCEEDANCES IN A ROW FOR THE SAME PAR A,METFR A'T'I'uF CArtiAC nUTFp,LL Tr{1ruER?Ira 2 o`ytfloc NAIEn:rS "I n` 1—IT nAnr tl "'r1_41� u • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDI:NCt.S FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ® NO IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES a NO ❑ REGIONAL OFFICE CONTACT NAME: _ _ $onia Gfegory Mail on original and one copy of this DMR, includin4 all "No Discharae" reports, within 30 days of_r_ecelpt of the lob results (or at end of monitoring Period In the case of "No nischprue" reports) to: Division of Water Quality Attn: 0WQCentral Files 1617 Mail 5erdce Center Raleigh, North Carolina 27699-1617 QU MUST SIGN THIS CERIE CATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this dorument and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualiI ersonnel properly gather and evaluate the information submitted, Based on my inquiry of the person or persons who manage the system, of those petson,rpdly responsible for gathering the information, the Information submitted is, to the best of my knowledge and belief, true, accurate, and complete am aware a ere_W &8nificaDt penalties for submitting false Information, Including the possibility of fines and Imprisonment for knowing violations." cam/ 7-i5--r'� ignature of Permittee) J r�T (Date) Permit Date: 11/l/2012-10/31/2017 SWU-248, last revised 10/25/2.012 Page 2 of 2 S�nith 5400 Glenwood Avenue, Suite 400 Raleigh, North Carolina 27612 tel: 919-787-5620 fax: 919-781-5730 July 20, 2015 Attention: DWQ Central Files North Carolina Department of Environment and Natural Resources Division of Water Quality 1617 Mail Service Center Raleigh, North Carolina 27699-1617 RECEIVED JUL 2 7 2015 CENTRAL FILES DWR SECTION Subject: Outfall 3 Discharge Monitoring Report - Tier 2 Response Monitoring Period - June 2015 Onslow County Landfill - Permit Number 67-09 Certificate of Coverage Number - NC:G120023 To the Division of Water Quality: CDM Smith Inc., on behalf of Onslow County (County), is submitting two copies of the Stormwater Discharge Monitoring Report for Outfall 3. Samples collected from Outfall 3 during the 2014 semi-annual sampling events had detections of fecal coliform and chemical oxygen demand (COD) above the benchmark values. Stormwater from the outfall is discharged to a former borrow pit and does not leave the property. In response to the benchmark value exceedances, the County implemented Tier 1 and 2 responses. Samples were collected from Outfall 3 on June 3, 2015, and were analyzed for COD, fecal coliform, and total suspended solids. COD was detected at 142 milligrams per liter and fecal coliform was detected at 1,800 colonies per 100 milliliters. The COD and fecal coliform detections were above the benchmark values. Per the Tier 2 response requirements, samples will be collected monthly for all parameters from Outfall 3 until three consecutive sampling events show the parameters are below the benchmark values. Monthly monitoring in accordance with the Tier 2 requirements will continue. The County will maintain a record of the Tier 1 and 2 responses and monitoring results at the landfill. WATER + ENVIRONMENT +TRANSPORTATION + ENERGY + FACILITIES CDM Division of Water Quality July 20, 2015 Page 2 If you have any questions or require further explanation, do not hesitate to call me at (919) 325-3566. Sincerely, Daniel H. Forbes CDM Smith Inc. cc: Scott Bost, Onslow County Mathew Colone, CDM Smith Inc. s 1a Analytical ~,pacelab&c= June 11, 2015 Mr. Dan Forbes CDM 5400 Glenwood Ave Suite 300 Raleigh, NC 27612 RE: Project: Outfall 3 6/3 Pace Project No.: 92252636 Dear Mr. Forbes: Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-M6 Enclosed are the analytical results for sample(s) received by the laboratory on June 03, 2015. The results relate only to the samples included in this report. Results reported herein conform to the most current TN standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. If you have any questions concerning this report, please feel free to contact me. Sincerely, Chris Derouen Christopher.derouen@pacelabs.com Project Manager Enclosures fNCCR� F lge0 A��1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Paces Analytical Services, Inc.. Page 1 of 11 aceAnalytical www.Aacelabs.corrr Project: Outfall 3 613 Pace Project No.: 92252636 Raleigh Certification IDs 6701 Conference Drive, Raleigh, NC 27607 North Carolina Wastewater Certification M 67 Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 Flodda/NELAP Certification M E87648 Massachusetts Certification M M-NCO30 North Carolina Drinking Water Certification #: 37712 CERTIFICATIONS North Carolina Bioassay Certification M 16 North Carolina Drinking Water Certification #: 37731 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 West Virginia Certification #: 356 Urginia/VELAP Certification #: 460222 Pace Analytical services, Inc. 2225 Riverside Dr. Asheville, NC 28604 (828)254-7176 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Paco Analytical Services, Inc.. Page 2 of 11 InciaMnalyfical' wnvw.pacelahscom Project: Outfall 3 613 Pace Project No.: 92252636 Lab ID Sample ID 92252636001 OUTFALL # 3 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 SAMPLE ANAU TE COUNT Anaiytes Method Analysts Reported Laboratory SM 9222D JW1 1 PASI-R SM 2540D RC 1 PASI-R SM 5220D MAB 1 PASI-A REPORT OF LABORArORYANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 3 of 11 acmnalytical ~Pacetabs.com ANALYTICAL RESULTS Project: Outfall 3 6/3 Pace Project No.: 92252636 Pace Analytical Services, Inc. 2225 Riverside Dr, Asheville, NC 28804 (828)254-7176 Sample: OUTFALL # 3 Lab ID: 92252636001 Collected: 06/03/15 10:40 Received: 06/03/15 12:50 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual MBIO 9222D Fecal Coliform RAL Analytical Method: SM 9222D Fecal Coliforms 1800 CFU/100 mL 1.0 1 06/03/15 15A2 2540D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids 49.5 mg/L 12.5 1 06/04/15 08:25 5220D COD Analytical Method: SM 5220D Chemical Oxygen Demand 142 mg1L 25.0 1 06/10/15 12:55 Date: 06111l2015 11:41 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 4 of 11 e aceAinalytical WW..pacelabs.cam Project: Outfall 3 6/3 Pace Project No.: 92252636 QC Batch: RBIO15147 QC Batch Method: SM 9222D Associated Lab Samples: 92252636001 METHOD BLANK: 1476681 Associated Lab Samples: 92252636001 Parameter Units Fecal Coliforrns CFU1100 mL SAMPLE DUPLICATE: 1476682 Parameter Fecal Coliforms QUALITY CONTROL DATA Analysis Method: SM 9222D Analysis Description: 9222D MBIO Fecal Coliform - RAL Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 1.0 06103/1512:17 92252515001 Dup Units Result Result RPD Qualifiers CFU1100 mL ND ND Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (82B)254-7176 Results presented an this page are In the units Indicated by the "Units' column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06111 /2015 11:41 AM without the written consent of Pace Analytical Services, Inc - Page 5 of 11 aceAnalytical w".pecelaUc m QUALITY CONTROL DATA Project: Outfall 3 613 Pace Project No.: 92252636 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QC Batch: RWETI8375 Analysis Method: SM 2540D QC Batch Method: SM 2540D Analysis DescripJon: 2540D Total Suspended Solids Associated Lab Samples: 92252636001 METHOD BLANK: 1474801 Matrix: Water Associated Lab Samples: 92252636001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mg/L ND 2.5 061G4/15 08:20 LABORATORY CONTROL SAMPLE: 1474802 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Suspended Solids mg/L 250 234 94 90-110 SAMPLE DUPLICATE; 1474803 92252516003 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg1L 245 225 9 D6 SAMPLE DUPLICATE: 1474804 92252636001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg1L 49.5 64.0 26 D6 Results presented on this page are In the units Indicated by the "Units" column except where an akemate unit is presented to the right of the result REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06111 /2015 11:41 AM without the written consent of Pace Analytical Services, Inc.. Page 6 of 11 ace Analytical www.paselahs.=n Project: Outfall 3 613 Pace Project No.: 92252636 QC Batch: WETA123206 QC Batch Method: SM 5220D Associated Lab Samples: 92262636001 METHOD BLANK: 1479211 Associated Lab Samples: 92252636001 Parameter Units Chemical Oxygen Demand mg/L LABORATORY CONTROL SAMPLE: 1479212 Parameter Units Chemical Oxygen Demand mg/L Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Analysis Method: SM 5220D Analysis Description: 5220D COD Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 25.0 06110/1512:55 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 750 801 107 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1479213 1479214 MS MSD 92252464002 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Chemical Oxygen Demand mg/L 144 750 750 891 891 100 100 90-110 0 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1479215 1479216 MS MSD 92252155003 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Cont. Result Result % Rec % Rec Limits RPD Qual Chemical Oxygen Demand mg/L 164 750 750 920 920 101 101 90-110 0 Results presented on this page are in the units indicated by the "Units" column except where an altemete unit is presented to the right of the result. REPORT OF LABORA I-ORY ANALYSIS This report shall not be reproduced, except in full. Date: 06111 /2015 11:41 AM without the written consent of Pace Analytical Services, Inc.. Page 7 of 11 • aceAnalytical wwwpaceft&CM QUALIFIERS Project. Outfall 3 613 Pace Project No.: 92252636 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL - Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit. Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyi ether, Styrene, and Vinyl chloride. A separate vial preserved to a pH of 4-5 is recommended in SW646 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current 11;3t of accredited analytes. TNI -The NELAC Institute. LABORATORIES PASI-A Pace Analytical Services - Asheville PASI-R Pace Analytical Services - Raleigh ANALYTE QUALIFIERS D6 The relative percent difference (RPD) between the sample and sample duplicate exceeded laboratory control limits. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06111 /2015 11:41 AM without the written consent of Pace Analytical Services, Inc.. Page 8 of 11 aceAnalj&al e WW'P 0b&= QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Outfall 3 613 Pace Project No.: 92252636 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 288t14 (828)254-7176 Lab ID Sample ID QC Batch Method QC Batch Analytical Method 92252636001 OUTFALL # 3 SM 9222D R131015147 92252636001 OUTFALL # 3 SM 2540D RWETI8375 92252636001 OUTFALL # 3 SM 5220D WETA123206 Analytical Batch Date: 06/11/2015 11:41 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 9 of 11 CHAIN -OF -CUSTODY 1 Analytical Request Document CD The Chaln-d-Custody is a LEGAL DOCUMENT, Ail relevant fields must be wrnpleted accxmalery. awl - Fla._ _ AirF_+CaNlr.+!T!w r A. Alt Sampla Ids Must be uri** T— Ts -!IFNI 0 1 SUMMONED n ■!r■!■■M!■■■■■■r!■■ ■■■■■■■■■■■■ MISSIONIMMMMIIIMMMMMMMM ■■■■!!■!■!■■ ■■!�!!!!■■■■■!■■■■■ ■r■!■■■■■!■■ 0; SON ■rr■!■■■!■■■r■■■■ ■■■■■■■■■M■■ ■�r!!r■■■■r■■■■■ REV _ ■■■■■■!■■!■■ 3;•ir+-K; '.""^i'y �.t�.,�,o yvt y,,,, ykht 'ar'?-s�M ".*h"�'"�4F,- ��'�^ ��Y��.}� rr." .. .�,s:•:a:.' :.�- �`•S�'e�."c"` '." N.•n°.i :'r*,.=�L..�.S;ii'.i°4t•'�•. wh ����� ^'.."w '�`, f ,. F Document Name: Sample Condition Upon Document Revised: May 15, 2015 (jcal' Receipt (SCUR) Page 1 of T Document No.: issuing Authorities: F-RAL-CS-001-rev.03 Pace Raleiah Quality Office Client Name: "Page 2 of 2 is for Intemal Use Only Courier (Circle): Fed Ex UPS USPS Cgenl, Commercial Pace Other Custody Sea Ion CoolerlBox Present: yes no Seats intact: ,d yes no Packing Material: ❑ Bubble Wrap ❑ Bubble Bags e None Ej Other Circle Thermometer Used: IR Gun :122085387 e f Ic Wet (Blue None (� Samples on Ice, cooling process has begun IR Gun � 122065p71 t"emp Correction Factor Add f ct lA C data and Initiate of person examining Corrected Gooier Temp.: 1 1 • C BiolO ical Tissue Is 12rozen: Yes No A B co t Pres ry ti CO Temp should be above freezing to 66C Comments: Chain of Custody Present: WBB ONO OWA 1. Chain of Custodx Filled Out: Y $ ON- ❑WA 2. Chain of Custody Relinquished: Y ❑No OWA 3. Sam ter Name R Signature on COC: Yes ONO ❑NIA 4. Sam les Arrived within Hold Time: LTYT ONO ❑WA 5. Short Hold Time Analysis <72hr : Yes ONO ❑NIA 6. Rush Turn Around Time Requested: ❑Yee I310, ❑WA 7. Sufficient Volume: P90s ONO ❑wA 8. Correct Containers Used: A -as ONO OWA 9. -Pace Containers Used: Yes ONO OWA Containers Intact: eYes ONO ❑NIA 10. Filtered volume received for Dissolved tests ❑Yes ONO ,Q^WA 11. Sample labels match COC: - ff Yeg ONO ❑NrA 12. -Includes dateltimellDlAnal is Matrix: AjaL All containers needing preservation have been checked. ❑No ❑N1A 13. All containers needing preservation are found to be In '�As a s ❑ NO ❑N1A compliance with EPA reoommandallon. 10 exceptions: VOA, ooRrorm, TOC. 080, WI-DRO (water) Yes ONO Samples checked for dechlorinalion: E5as ONO ❑NIA 14. Heads ace In VOA Vials >6mm : ❑YBs ❑No rA 15_ Trip Blank Present: ❑Yes ONO WA 116. Trip Blank Custody Seals Present ❑Yes ONO P<A Pace Trip Blank Lot It if prehased : Client Notiticationl Resolution: Field Data Required? Y I N Person Contacted: DatelTirne: Comments/ Resolution: SCURF /SRF Data: (� i r5 W ® * 92252636 Review:: Dote: Whenever there Is a discrepancy affecting North Carolina compliance samples, a Wpy of this form wilt be sent to the North Carolina DEHNR y I CerUticatlori ofacq ( I.e out of -hold, Inoorrect preservative, out of temp, 92252636 Incorrectccnlalners) _ _ �..— Page 11 of 11 Semi-annual Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG120000 Date submitted June 29, 2015 CERTIFICATE OF COVERAGE NO. NCG12 0 0 2 3 FACILITY NAME Onslow County Land#ill COUNTY Onslow PERSON COLLECTING SAMPLES No Samples Collected LABORATORY Lab Cert. # Comments on sample collection or analysis: Part A: Stormwater Benchmarks and. Monitoring Results. SAMPLE COLLECTION YEAR 2015 SAMPLE PERIOD ❑ Jan -June ❑July -Dec or 0 Monthly) May (month) DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA ❑Zero -flow ❑Water Supply ❑S� X❑OtheC Former Borrow Prt PLEASE REMEMBER TO SIGN ON THE REVERSE ❑X No discharge this period?z Outfall No. Date Sample Collected, (mo/dd/yrj 24-hour rainfall amount, Inches3 Chemical Oxygen Demand Fecal Coliform Total Suspended Solids Benchmarks =__> - - 120 mg/L 1000 count per 100 mL 100 mg/L or 50 mg/L 3 1 Monthly sampling (instead -of semi=annual)_must-begin°with the second -consecutive -benchmark -exceed ance_for.the same_parameter.: at. the:same°outfall:=. z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with-a-checkmark°here: 3 The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. 4 See General Permit text, Table 3, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Note: Results must be reported in numerical format. For example, do not report=Below Detection-Limit;-BDL-,-<PQL; Non -detect; ND; -or -other similar -non -- numerical format. When results are below the applicable limits, they must be reported in the format, "<XX mg/L", where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Conversely, where fecal coliform results exceed the dilution upper limit, report the result as ">XX". Note: If you report a sample value in excess of the benchmark,-youlmust- implement- Tier---1,-Tied,-or--Tier-1responses. -See General Permit -text. Permit Date: 11/1/2012-10/31/2017 SWU-248, last revised 10/25/2012 Page 1 of 2 Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. r+ ❑ No discharge this period: Outfail No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall. . amount, Inches Non -polar O&G/TPH by EPA 1664 (SGT-HEM)' Total Suspended Solids pH Benchmarks ===> _ - 15 mg/L 100 mg/L or 50 mg/L 6.0 — 9.0 SU Footnotes from Part A also apply to this Part B Note: If you report asomple value in excess -of the benchmark;-you:must:implement-Tier`1;=Tierr2;_or-Tier-3:responses.-_'See-General:Permit text. FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS, SEE PERMIT PART ii SECT ION B. • TIER 3: HAS YOUR FArIL!T`! HAD, �I; Pv50RE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFACE? YES ®NO IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ® NO REGIONAL OFFICE CONTACT NAME: Sonia Gregory Mail an oriainal and one copy of this DMA, including all "No Discharge" reports: within-30 days°of receipt of the lab results -for -at end of monitorinq-period- in the case of "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document -and -all -attachments -were prepared under -my direction or supervision°in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry -of the person orpersons-who: manage the system, or. those persons directly responsible for gathering the information, the information submitted is, to the best of my knowtedge-and belief; true; accurate; -and complete: .I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." re of Permittee) 4:;�- G Zvi 5- (Date) Permit Date: 11/1/2012-10/31/2017- -SWU=248, last revised.10/25/2012, Page 2 of 2 CDM Smith 5400 Glenwood Avenue, Suite 400 Raleigh, North Carolina 27612 tel: 919-325-3500 fax: 919-781-5730 July 1, 2015 Attention: DWQ Central Files North Carolina Department of Environment and Natural Resources Division of Water Quality 1617 Mail Service Center Raleigh, North Carolina 27699-1617 Subject: Outfall 3 Discharge Monitoring Report -Tier 2 Response Monitoring Period - May 2015 Onslow County Landfill Certificate of Coverage Number - NCG120023 To the Division of Water Quality: fkeetIVED JUL 06Z.015 cENTL FILES DWR�SECTION CDM.Smith Inc., on behalf of Onslow County (County), is submitting two copies of the Stormwater Discharge Monitoring Report for Outfall 3. Samples collected from Outfall 3 during the 2014 semi-annual sampling events had detections of fecal coliform and chemical oxygen demand above the benchmark values. In response to the benchmark value exceedances, the County implemented Tier 1 and 2 responses. There was no discharge from Outfall 3 in May 2015. Per the Tier II response requirements, samples will be collected monthly for all parameters from Outfall 3 until three consecutive sampling events show the parameters are below the benchmark values. The County will maintain a record of the Tier 1 and 2 responses and monitoring results at the landfill. If you have any questions or require further explanation, do not hesitate to call me at (919) 325-3566. Sincerely, Daniel H. Forbes CDM Smith Inc. cc: Scott Bost, Onslow County Mathew Colone, CDM Smith Inc. 40 WATER + E14VJRONMENT +TRANSPORTATION + ENERGY + FACILITIES Semi-annual Stormwater Discharge-MonitoringAeport- for North Carolina Division of Water Quality General Permit No. NCG120000 Date submitted May 18, 2015 CERTIFICATE OF COVERAGE NO. NCG12 0 0 2 3 FACILITY NAME Onslow County Landfill COUNTY Onslow PERSON COLLECTING SAMPLES Janet Connor LABORATORY Pace Analytical, Inc. Lab Cert. # 37712/37731 Comments on sample collection or analysis: Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR 2015 SAMPLE PERIOD Jan -June ❑ July -Dec or X❑ Monthly' April month DISCHARGING.TO CLASSQORW- ❑HQW- ❑Trout- ❑PNA- ❑Zero-flow ❑Water Supply ❑SA X❑Other Former Borrow Pit _ PLEASE REMEMBER TO SIGN ON THE REVERSE 4 ❑ No discharge this period: Outfall Na. Date Sample Collected' (mo/ Collected' 24-hour rainfall amount, Inches; Chemical Oxygen Demand Fecal Coliform Total` Suspended Solids Benchmarks ===> _ - 120 ..n .;,,.�, L iytii, count per ioo ml 100 mg/L or 50 mg/L 2 4/20/15 0.57 57.0 19.0 13.0 3 4/20/15 0.57 632 15,000 188 I Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameterat-the same outfall. Z For sampling periods with. no discharge -at -any single.outfall,:you:must-still submit this discharge monitoring reportwith-a checkmark here: - 3The total precipitation must be recorded using -data -from --an on=site-rain-gauge: -Unattended--sites may be-eligible-for°a waiver -of the raimgaugerequirement-. 4 See General Permit text, Table 3, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Note: Results must be reported in numerical format. For example, do not report Below Detection. Limit; BDL, <PQL; Non -detect; -ND; or other similar non= numerical format. When results are below the applicable limits, they -must be -reported in the format:-"<XX me/L", where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Conversely, where fecal coliform results exceed the dilution upper limit, report the result as ">XX". Note: If you report a sample value in excess of the benchmark, you must implement=Tier--1, Tier--2,-or--Tier3 responses. See General-Permit%text. Permit Date: 11/1/2012-10/31/2017 SWU-248, last revised 10/25/2012 Page 1 of 2 Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. ❑ No discharge this period?Z Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches3 Non -polar O&G/TPH by EPA 1664 (SGT-HEM) Total Suspended Solids pH Benchmarks 15 mg/L 100 mg/L or 50 mg/L 6.0 — 9.0 SU (Footnotes from Part A also apply to this Part B Note: if you report a sample value in excess of the benchmark, you must implement Tier .1, Tier Z, or Tier 3 responses. See General Permit text. FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS, SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BFNCHMIARV EXCEEDENCES FOR T Hr SAME PARAMETER AT ANY ONE OUTFALL? YES ®NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES M NO ❑ REGIONAL OFFICE CONTACT NAME: Sonia Gregory Mail an original and one coov of this DMR. includina all "No Discharae" reports, within 30 days of receipt of the lab results for at end of monitorin_q period in the case of "No Discharae" reports! to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU -MUST -SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." ature of Permitteej Permit Date: 11/1/2012-10/31/2017 (Date) SWU-248, last revised 10/25/2012 Page 2 of 2 I CDM Smith 5400 Glenwood Avenue, Suite 400 Raleigh, North Carolina 27612 tel: 919-787-5620 fax: 919-781-5730 May 18, 2015 Attention: DWQ Central Files North Carolina Department of Environment and Natural Resources Division of Water Quality 1617 Mail Service Center Raleigh, North Carolina 27699-1617 RECEIVED MAY 21 2015 owRRAL FILES SECTION Subject: Semi -Annual Discharge Monitoring and Tier Two Sampling Report Monitoring Period - January 1, 2015 to June 30, 2015 Onslow County Landfill Certificate of Coverage Number - NCG120023 To the Division of Water Quality: CDM Smith Inc., on behalf of Onslow County (County), is submitting two copies of the Stormwater Discharge Monitoring Report for the facility referenced above. Samples were collected from Outfalls 2 and 3 on April 20, 2015, after the facility received 0.57 inches of precipitation. Outfall 1 currently receives stormwater runoff from the closed portion of the Subtitle D landfill and was removed from the analytical monitoring requirements following a Division of Water Quality (DWQ) inspection on January 23, 2013. All samples were analyzed for fecal coliform, chemical oxygen demand (COD), and total suspended solids by Pace Analytical Services, Inc. located in Raleigh, North Carolina. Samples collected from Outfall 2 were below the benchmark values and all analytes exceeded the benchmark values in samples collected from Outfall 3: Tier Two monitoring was implemented for Outfall 3 in January 2015 after consecutive detections of COD above the benchmark value. Stormwater from Outfall 3 is discharged to a former borrow pit and does not leave the property. The drainage area for Outfall 3 includes the east slope of the active Subtitle D landfill. Elevated COD at Outfall 3 is a result of washouts on the slope. Per the County's Tier One responses and operations plan, all washouts are repaired and the slope is reseeded as necessary following precipitation events. COD detected above the benchmark value in samples collected from Outfall 3 in April 2015 constitutes the fourth exceedance since the General Permit was issued on November 1, 2012. The DWQ Regional Office Surface Water Supervisor (Ms. Sonia Gregory) was contacted on May 13, 2015, in accordance with the Tier Three requirements. 0 WATER + ENVIRONMENT +TRANSPORTATION + ENERGY + FACILITIES Smith Division of Water Quality May 18, 2015 Page 2 The County will continue monthly monitoring in accordance with the Tier Two requirements until three consecutive sampling events show the analytical parameters are below the benchmark values. The County will maintain a record of the Tier One and Two responses and analytical results at the landfill. If you have any questions or require further explanation, do not hesitate to call me at (919) 325-3566 or by email at forbesd@cdmsmith.com. Daniel H. Forbes CDM Smith Inc. cc: Scott Bost, Onslow County Mathew Colone, CDM Smith Inc. aceAnalytical www.pacefab&mn April 27, 2015 Mr. Dan Forbes CDM 5400 Glenwood Ave Suite 300 Raleigh, NC 27612 RE: Project: Onlsow Co. NPDES 4120 Pace Project No.: 92246203 Dear Mr. Forbes: Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176- Enclosed are the analytical results for sample(s) received by the laboratory on April 20, 2015. The results relate only to the samples included in this report. Results reported herein conform to the most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. If you have any questions concerning this report, please feel free to contact me. Sincerely, Chris Derouen christopher.derouen@pacelabs.com Project Manager Enclosures 'f cOt a a �eORA� REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 1 of 11 acmnalytical www.pacelabe.com Project: Onlsow Co. NPDES 4120 Pace Project No.: 92246203 Raleigh Certification IDs 6701 Conference Drive, Raleigh, NC 27607 North Carolina Wastewater Certification #: 67 Asheville Certification iDs 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification M E87648 Massachusetts Certification M M-NC030 North Carolina Drinking Water Certification M 37712 CERTIFICATIONS North Carolina Bioassay Certification M 16 North Carolina Drinking Water Certification M 37731 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 West Virginia Certification M 356 VirginiaNELAP Certification M 460222 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 2 of 11 /�aceAnalyfical' ! *wwpacebbs.c= i SAMPLE ANALYTE COUNT Project: Onlsow Co. NPDES 4120 Pace Project No.: 92246203 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Lab ID Sample ID Method Analysts Analytes Reported Laboratory 92246203001 OUTFALL 2 SM 9222D JW1 1 PASI-R SM 2540D RC 1 PASI-R SM 5220D MAB 1 PASI-A 92246203002 OUTFALL 3 SM 9222D JW1 1 PASI-R SM 2540D RC 1 PASI-R SM 5220D MAB 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 3 of 11 aceAnalytical. _]7 wwwpacelabs.-, I ANALYTICAL_ RESULTS Project: Onlsow Co. NPDES 4/20 Pace Project No.: 92246203 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Sample: OUTFALL 2 Lab ID: 92246203001 Collected 04/20/15 13:20 Received: 04/20/15 15:55 Matrix: Water Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual MBIO 92220 Fecal Coliform RAL Analytical Method: SM 9222D Fecal Coliforms 19.0 CFU1100 mL 1.0 1 04/20/15 16:10 2540D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids 13.0 mg/L 6.2 1 04121 /15 11 A 5 5220D COD Analytical Method: SM 5220D Chemical Oxygen Demand 57.0 mglL 25.0 1 04/27/15 10:55 Sample: OUTFALL 3 Parameters Lab ID: 92246203002 Collected: 04/20115 1100 Results Units Report Limit OF Received: 04/20/15 15:55 Matrix: Water Prepared Analyzed CAS No. Qual MBIO 9222D Fecal Coliform RAIL Analytical Method: SM 9222D Fecal Coliforms 15000 CFU/100 mL 1.0 1 04/20/15 16:10 2540D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids 188 mg/L 50.0 1 04/21/15 11:16 5220D COD Analytical Method: SM 5220D Chemical Oxygen Demand 632 mglL 25.0 1 04/27/15 10:55 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/27/2015 04:02 PM without the written consent of Pace Analytical Services, Inc.. Page 4 of 11 aceAnalylical j www.pacwabs.com .I Project: Onlsow Co. NPDES 4120 Pace Project No.: 92246203 QC Batch: RBI015030 QC Batch Method: SM 9222D Associated Lab Samples: 92246203001, 92246203002 METHOD BLANK: 1441695 Associated Lab Samples: 92246203001, 92246203002 Parameter Units Fecal Coliforms CFU1100 mL SAMPLE DUPLICATE: 1441696 Parameter Fecal Coliforms QUALITY CONTROL DATA Analysis Method: Analysis Description Matrix: Water Blank Result ND 92246198001 Units Result CFU1100 mL 3000 Reporting SM 9222D 9222D MB10 Fecal Coliform - RAL Limit Analyzed 1.0 04/20/15 16:10 Dup Result RPD 2400 22 Qualifiers Qualifiers Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Results presented on this page are in the units indicated by the "units' column except where an aitamate unit is presented to the right of the resutt. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/27/2015 04:02 PM without the written consent of Pace Analytical Services, Inc.. Page 5 of 11 aceAnalytical e 1 www.pacehiha.cotn I QUALITY CONTROL DATA Project: Onlsow Co. NPDES 4120 Pace Project No.: 92246203 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QC Batch: RWET18251 Analysis Method: SM 2540D QC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids Associated Lab Samples: 92246203001, 92246203002 METHOD BLANK: 1439507 Matrix: Water Associated Lab Samples: 92246203001, 92246203002 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mg1L ND 2.5 04/21/15 11:11 LABORATORY CONTROL SAMPLE: 1439508 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Suspended Solids mglL 250 258 103 90-110 SAMPLE DUPLICATE: 1439509 92245883002 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mglL 489 391 22 D6 SAMPLE DUPLICATE: 1439510 92246203002 Dup Parameter Units Result Result RP❑ Qualifiers Total Suspended Solids mg1L 188 202 7 06 - Results presented on this page are in the units Indicated by the "Units" column except where an altemste unft Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduoed, except in full, Date: 04/27/2015 04:02 PM without the written consent of Pace Analytical Services, Inc.. Page 6 of 11 aceAnalyiical xnvw.pacW'ab&cwn QUALITY CONTROL DATA Project: Onlsow Co. NPDES 4120 Pace Project No.: 92246203 QC Batch: WETA122682 Analysis Method: SM 5220D QC Batch Method: SM 5220D Analysis Description: 5220D COD Associated Lab Samples: 92246203001, 92246203002 METHOD BLANK: 1442592 Matrix: Water Associated Lab Samples: 92246203001, 92246203002 Parameter Chemical Oxygen Demand Blank Reporting Units Result Limit Analyzed Qualifiers mg/L ND 25.0 04127/1510:55 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 LABORATORY CONTROL SAMPLE: 1442593 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Chemical Oxygen Demand mg1L 750 797 106 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1442594 1442595 MS MSD 92246722001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Chemical Oxygen Demand mg/L 84.0 750 750 846 846 102 102 90-110 0 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1442596 1442597 MS MSD 92246195001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Chemical Oxygen Demand mg/L 4010 6000 6000 7460 7460 58 58 90-110 0 M6 Results presented on this page are in the units indicated by the "ltnita" column excopt where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/27/2015 04:02 PM without the written consent of Pace Analytical Services, Inc.. Page 7 of 11 aclmnalydical WW..paaafabs.c= QUALIFIERS Project: Onlsow Co. NPDES 4/20 Pace Project No.: 92246203 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL - Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit. Pace Analytical Services, Inc: 2225 Riverside Dr. Asheville, NC 28804 (828 )254-7176 S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP -Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI -The NELAC Institute. LABORATORIES PASI-A Pace Analytical Services -Asheville PASI-R Pace Analytical Services - Raleigh ANALYTE QUALIFIERS D6 The relative percent difference (RPD) between the sample and sample duplicate exceeded laboratory control limits. M6 Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/27/2015 04:02 PM without the written consent of Pace Analytical Services, Inc.. Page 8 of 11 aceAnalytical wrvw.pecelabs.com QUALITY CONTROL DATA CROSS REFERENCE TABLE Project. Onlsow Co. NPDES 4/20 Pace Project No.: 92246203 Pace Analytical Services, Inc: 2225 Riverside Dr, Asheville, NC 28804 (828)254-7176 Lab ID Sample 113 QC Batch Method QC Batch Analytical Method 92246203001 OUTFALL 2 SM 9222D RBIO/5030 92246203002 OUTFALL 3 SM 9222D R1310/5030 922246203001 OUTFALL 2 SM 2540D RWET/8251 92246203002 OUTFALL 3 SM 2540D RWET/8251 92246203001 OUTFALL 2 SM 5220D WETA/22682 92246203002 OUTFALL 3 SM 5220D WETA/22682 Analytical Batch Date: 04/27/2015 04:02 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 9 of 11 2= race Analytical r''r,`iµY,; ,,.•...,..�j� www.pacela4s.cam j _Lfi %� (I. Cahlerenoe Drive, Raleigh, NC 27607 pki:;(1i) 934498a, lax: (919) 834 8497 . ,yM,CefWG7, NCDW CerW37731 Chain of Custody W.O.# lesuits To: y:LD M H �uoo G f��u�d /�✓e Ifoo QArP1 e111 kk a12 96 5 — 35 t R _.77% - Q7? A I by (signature): 62, s' BIII To: CD— Project Reference: C ti Project Number: Purchase Order M, �ndard Report Delivery ❑ Rush Report Delivery (wlsurcharge) —Rush projects we Subject to prior approval by the Laboratory Requested Due Date: .1:.? cn,. �:+:l�x•:.it�•f Will, rt YtUi t.i f� sit) 1 rt e�i�w}t � K � S � 'f tJ` i{'q. �,�aJ ♦ G�� l rYj > "'7,; w•.•rrw r�,}Y• - h{. < � 1 �A1 1 ��/�. { .'«�;.g_r 5ti t •S W. l ,ur v::�p ..�r^ Y�. t �' J 1 1 ..,.. .1.. ..y.:.,; Y.,.�_ ,...•; :.y.. � - a 1 ' * 15 y„ ,� •�- ! - ' � � � : / i 1' 15 +} ?-•i,..: i J ', .� 1 r t rteli' i5had by signature) R efved Twa*tur D e Time Reli Utshad by (signature) Received D e lime ,Rollnqulshed by (signature) Reoelved by (slgnature) Date Time Reoelpt Condltbns (L U Only) ❑ 4t2°C ❑ Temp: °C Res. Chlorine: ❑ Absent ❑ Present ❑ rtla Add preserv. <2? ❑ Yes ❑ No ❑ nla Base preserv. >12? ❑ Yes ❑ No ❑ rda Page 10 of 11 A Document Name: Sample Condition ' I Document No.: Document Revised: April 04. 2013 Page_1 of 2 Issuina Authorities: Client Name:�,47!(`/` re,Received: Huntersville n Asheville EdenRaleigh rier._1Circle�: Fed Ex UPS USPS Client Commercial Pace . Other Ay Seal on Cooler/Box Present: ❑ yes no Seats intact: E yes Q no ng.Ntaterial., (3 Bubble Wrep B to Bags 0 None n Other i Thermometer Used: IR Gun :122005387T d of Ice: Wet Blue None Samples on ice. cooling process has begun IR Gurn B 6�71 'Temp Correction Factor: Ad S trac Data and Initials of person exam n ng i} "f,CorrecEed Cooler Temp.: C _C. Biological Tissue is Frozen: Yea No WA oo ! Pr e oA l -Temp should be above freezing to e C Comments: check: Cheln of Custody f�re$ent: Yea ❑No ❑MIA 1: .Chain of Cuslad FII1ed put: q- [)No ❑WA 2. s ; p± Chain of Custody Retin Unshed: s ❑No ❑WA 3. Sam ter Name & Si nature on COC: eyes ❑No ❑NIA 4. Samptes Arrived within Hold Time: Yes ON. ❑NIA 6. Short Hold Time Analysis <72hr : Yos ONO ❑NIA e. Rush Turn Around Time Requested: Dyes o UNIA 7. Sufficient Volume: XY.. ON. ❑WA S. Correct Containers Used: f {Yes CINo I]WA J. Pace Containers Used: / Yes ONO ❑NIA Containers Intact: es ONo ❑NIA W Filtered volume -resolved for Dissolved tests ❑Yes ONO WA i i . Sample. Labels match COC: ❑wA 12. -Includes date/time/ID/Analysis Matrix: �YQ All containers needing preservation have been checked. ❑ ❑A 13. M oontalners needing preservation are found to be In es C7No 0WA compliance with EPA reoommendation, V "ptbns: VOA, W torm, Toc, odG, WWR4 twater) ONo metes checked for dechlorination: Yes ❑No CIMA 14, Heads 'ace in VOA Vials >6mm : ❑Yea ❑No NIA 16. drip Blank Present: ❑Yes ❑Nv 9 tIA i6. Trip Blank Custody Seals Present ❑Yes ❑No NIA Pace Trip Blank Lot # if purchased): _ _- Client Notification/ Resolutlon: Field Data Required? Y J N Person Contacted, _ Dateliime: Comments/ Resolution: SCURF,lSRI Date: Cr Review:: Note: Whenever there Is a discrepancy a;rnctirC, North Garollna compllance samples, a copy of this tosm will be sent to tr,ti North :;arollna DEHNR Certification Office (I.e .oat of hold, l n rec! ,resar-rlva, out of ternn. lncorrect oow-nem, WO#:92246203 IIIII! Illl lull1111111 Page 11 of 1'l Semi-annual Stormwatelr Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG120000 Date submitted April 28 _2015 CERTIFICATE OF COVERAGE NO. NCG12 0 0 2 3 FACILITY NAME Onslow County Landfill COUNTY Onslow PERSON COLLECTING SAMPLES Mark Darwin LABORATORY Pace Anal tical Inc. Lab Cert. # 37712/37731 Comments on sample collection or analysis: - Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR 2015 SAMPLE PERIOD ❑ Jan -June ❑ July -Dec or X❑ Monthly' March (month) DISCHARGING TO CLASS ❑ORW ❑HQW- [:]Trout- E]PNA- Elzero-flow ❑Water Supply ❑SA X❑Other_ Former Borrow Pit PLEASE REMEMBER TO SIGN ON THE REVERSE 4 0 No discharge thisperiod?z Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches3 Chemical Oxygen Demand Fecal Coliform Total Suspended Solids Benchmarks =__> - - 120 mg/L 1000 count per 100 mL 100 mg/L or, 50 mg/L 4 3 3/27/15 0,4 065 3,200 55.0 1 Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark-exceedance for the same-parameterat the same-outfall. z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. 4 See General'Permit text, Table 3, identifying the especially-sensitive.-receiving-water°classifications;where:the,more: protective :benchmark,applies. Note: Results must be reported in numerical format. For example, do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, -or other similar non - numerical format. When results are below the applicable limits, they must be reported in the format. "<XX mx/L", where XX is the numerical value of the detection limit, reporting limit, etc: in mg/L. Conversely, -where fecal coliform-resultsexceed the dilution -upper -limit, report the result-as`">XX". Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See -General Permit text. Permit Date: 11/1/2012-10/31/2017 SWU-248, last revised 10/25/2012 Page 1 of 2 Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. ❑ No discharge this period?' Outfall No. Date Sample Collected) (mo/dd/yr) 24-hour rainfall amount, IncheS3 Non -polar O&G/TPH by EPA 1664 (SGT-HEM) Total Suspended Solids PH Benchmarks 15 mg/L 100 mg/1 or 50 mg/L" 6.0 -- 9.0 5U Footnotes from Part A also apply to this Part B Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. FOR PART A AND PART B MONITORING RESULTS: A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDANCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an oriainal and one copy of this DMR. including all "No Discharge" reports, within 30 days of receipt of the lab results for at end of monitoring Period in the case of "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "i certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the Information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. am aware that there are significant penalties fo submitting false information, including the possibility of fines and imprisonment for knowing violations." (s ature of Permitteel (Date) Permit Date: 11/1/2012-10/31/2017 SWU-248, last revised 10/25/2012 Page 2 of 2 CDM Smith 5400 Glenwood Avenue, Suite 400 Raleigh, North Carolina 27612 tel: 919-787-5620 fax: 919-781-5730 April 28, 2015 Attention: DWQ Central Files North Carolina Department of Environment and Natural Resources Division of Water Quality 1617 Mail Service Center Raleigh, North Carolina 27699-1617 RECEIVED MAY 0 5 &j CENTRAL FILES DWR SECTION Subject: Outfall 3 Discharge Monitoring Report - Tier 2 Response Monitoring Period - March 2015 Onslow County Landfill Certificate of Coverage Number - NCG120023 To the Division of Water Quality. CDM Smith Inc., on behalf of Onslow County (County), is submitting two copies of the Stormwater Discharge Monitoring Report for Outfall 3. Samples collected from Outfall 3 during the 2014 semi-annual sampling events had detections of fecal coliform and chemical oxygen demand above the benchmark values. In response to the benchmark value exceedances, the County implemented Tier 1 and 2 responses. Samples were collected from Outfall 3 on March 27, 2015, and were analyzed for chemical oxygen demand (COD), fecal coliform, and total suspended solids. COD was detected at 865 milligrams per liter and fecal coliform was detected at 3,200 colonies per 100 milliliters. The COD and fecal coliform detections were above the benchmark values. Per the Tier II response requirements, samples will be collected monthly for all parameters from Outfall 3 until three consecutive sampling events show the parameters are below the benchmark values. Monthly monitoring in accordance with the Tier II requirements will continue. The County will maintain a record of the Tier 1 and 2 responses and monitoring results at the landfill. i� WATER + E14VIRONMENT +TRANSPORTATION + ENERGY + FACILITIES CDM Division of Water Quality April 28, 2015 Page 2 if you have any questions or require further explanation, do not hesitate to call me at (919) 325-3566. Sincerely, Daniel H. Forbes CDM Smith Inc. cc. Scott Bost, Onslow County Mathew Colone, CDM Smith Inc. acEAnalytical www.pacekbs.com April 08, 2015 Mr. Dan Forbes CDM 5400 Glenwood Ave Suite 300 Raleigh, NC 27612 RE: Project: Onslow Co Outfall 003 3127 Pace Project No.: 92243077 Dear Mr. Forbes: Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Enclosed are the analytical results for sample(s) received by the laboratory on March 27, 2015. The results relate only to the samples included in this report. Results reported herein conform to the most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. If you have any questions concerning this report, please feel free to contact me. Sincerely, Chris Derouen chdstopher.derouen@pacelabs.com Project Manager Enclosures asp pccR�r� ,j5 TNI 9eORA�� REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 1 of 11 acmnalytical e w w.pscelabs.= Project: Onslow Co Outfali 003 3127 Pace Project No.: 92243077 Raleigh Certification IDs 6701 Conference Drive, Raleigh, NC 27607 North Carolina Wastewater Certification #: 67 Asheville Certification IN 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87648 Massachusetts Certification #: M-NCO30 North Carolina Drinking Water Certification #: 37712 CERTIFICATIONS North Carolina Bioassay Certification #: 16 North Carolina Drinking Water Certification #: 37731 North Carolina Wastewater Certification #: 40 South Carolina Certification M 99030001 West Virginia Certification #: 356 VirginiaNELAP Certification #: 460222 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 REPORT OF LABORATORYANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 2 of 11 aceAnalytrcale' x�rw.pecelabtaom SAMPLE ANALYTE COUNT Project: Onslow Co Outfall 003 3127 Pace Project No.: 92243077 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Analyses Lab ID Sample ID Method Analysts Reported Laboratory 92243077001 OUTFALL 3 SM 9222D JW1 1 PASI-R SM 2540D RC 1 PASI-R SM 5220D MAB 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reprodjjced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 3 of 11 a aceAnalytical www.pecelabs.tom ANALYTICAL RESULTS Pace Anatytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Project: Onslow Co Outfall 003 3127 Pace Project No.: 92243077 Sample: OUTFALL 3 Lab ID: 92243077001 Collected: 03/27/15 09:45 Received: 03/27115 12:15 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual MBIO 9222D Fecal Coliform RAL Analytical Method: SM 9222D Fecal Coliforms 3200 CFU1100 mL 1.0 1 03/27/15 14:03 2540D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids 55.0 mg/L 25.0 1 03/31/15 10:29 5220D COD Analytical Method: SM 5220D Chemical Oxygen Demand 865 mg/L 25.0 1 04/07/15 09:15 Date: 04/08/2015 12:55 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced. except in full, without the written consent of Pace Analytical Services, Inc.. Page 4 of i 1 aceAnalytrcal ewnxpacafahs.cam Project: Onslow Co Outfall 003 3127 Pace Project No.: 92243077 QC Batch: RBIO14975 QC Batch Method: SM 9222D Associated Lab Samples: 92243077001 METHOD BLANK: 1428070 Associated Lab Samples: 92243077001 Parameter Units Fecal Coliforms CFU1100 mL SAMPLE DUPLICATE: 1428071 Parameter Units Fecal Coliforms CFU1100 mL QUALITY CONTROL DATA Analysis Method: SM 9222D Analysis Description: 9222D MBIO Fecal Coliform - RAL Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 1.0 03/2711514:03 92243077001 Dup Result Result 3200 3200 RPD Qualifiers 0 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result REPORT OF LABORATORYANALYSIS This report shall not be reproduced, except in full, Date: 04/08/2015 12:55 PM without the written consent of Pace Analytnml Services, Inc.. Page 5 of 11 aceAnalytical www.pecelabs.com QUALM' CONTROL DATA Project: Onslow Co Outfali 003 3127 Pace Project No.: 92243077 QC Batch: RWETI8190 Analysis Method: SM 2540D QC Batch Method: SM 2540D Analysis Description: 25400 Total Suspended Solids Associated Lab Samples: 92243077001 METHOD BLANK: 1422958 Matrix: Water Associated Lab Samples: 92243077001 Blank Reporting Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 26804 (828)254-7176 Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mg1L ND 2.5 03/31/15 10:21 LABORATORY CONTROL SAMPLE: 1422959 Spike l_CS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Suspended Solids mg/L 250 260 104 90-110 SAMPLE DUPLICATE: 1422960 92242952001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 1010 1020 1 SAMPLE DUPLICATE: 1422961 92242961002 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 164 154 6 D6 Results presented on this page are in the units Indicated by the -Units' column except where an alternate unit is presented to the right of the result REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. Date: 04/08/2015 12:55 PM without the written consent of Pace Analytical Services, Inc.. Page 6 of 11 acoAnalytical e www,pac&Ws.com QUALITY CONTROL DATA Project: Onslow Co Outfall 003 3127 Pace Project No.: 92243077 QC Batch: WETA122438 Analysis Method: SM 52200 QC Batch Method: SM 5220D Analysis Description: 5220D COD Associated Lab Samples: 92243077001 METHOD BLANK: 1426252 Associated Lab Samples: 92243077001 Parameter Units Chemical Oxygen Demand mg1L LABORATORY CONTROL SAMPLE: 1426253 Parameter Units Chemical Oxygen Demand mg/L Pace Anatytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7178 Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 25.0 04/07/15 09:15 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 750 727 97 90-110 MATRIX SPIKE R MATRIX SPIKE DUPLICATE: 1426254 1426255 MS MSD 92243731001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD , Qual Chemical Oxygen Demand mg/L ND 750 7511 759 759 101 101 90-110 0 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1426256 1426257 MS MSD 92243286001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Chemical Oxygen Demand mg1L 221 750 750 923 923 94 94 90-110 0 Results presented an this page arc in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/08/2015 12:55 PM without the written consent of Pace Analytical Services, Inc.. Page 7 of 11 WeAna,(Xical www.pmlahs.cam QUALIFIERS Project: Onslow Co Outfall 003 3127 Pace Project No.: 92243077 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit. Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (628)254-7176 S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. LABORATORIES PAST -A Pace Analytical Services - Asheville PAST-R Pace Analytical Services - Raleigh ANALYTE QUALIFIERS D6 The relative percent difference (RPD) between the sample and sample duplicate exceeded laboratory control limits. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. Date: 04/08/2015 12:55 PM without the written consent of Pace Analytical Services, Inc.. Page 8 of 11 aceAnalytrcal o www.pacelabs.com QUALITY CONTROL DATA CROSS REFERENCE TABLE Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Project: Onslow Co Outfall 003 3/27 Pace Project No.: 92243077 Analytical Lab ID SamPle ID QC Batch Method QC Batch Analytical Method Batch 92243077001 OUTFALL 3 SM 9222D R810/4975 92243077001 OUTFALL 3 SM 2540D RWET/8190 92243077001 OUTFALL 3 SM 52200 WETA/22438 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04108/201512:55 PM without the written consent of Pace Analytical Services, Inc.. Page 9 of 11 :' aceAnal�/�ical' umnr —1" is ma CHAIN -OF -CUSTODY / Analytical Request Document The Chain-otCusmdy is a LEGAL DOCUMENT.An relevant Adds must be cdmptetad a=wately. Section A Section S Seatton C Page: of Roges[red Caen! Iniormcoon: Rapired P-)w Intom-k— ImWm lntom�on: �Cmmpar>r Repoa Toc Attentlon: 18 8 4 9,01 To: Company Name: ::: ? Fo �•cu�aoaaracir LM f— NPDES i GROUNDWATER I' DRINKING WATER eAe yd r UST = RCRA OTHER EmailTa, PurhaseOrder No.; Phana: - ;S.- 356M Fait Prcyept Name: C SKd'i oeaGott -: ; Regu�stedDuel}atelTA:: Pr*ctKumber. Pace Pro&91. Rao!u►st+ AnacyslsFy_tdvedQr#tt), ::-:• �k;` .. cation D Matrix Cod&$ r grarodQenlViDimatSon Au ter cooE COLLECTED Prsservatives •>r: - - - 0l4YftWater DW Mier— WT g U waste wear ww Prod= P eow+wrrt START oornoarra EMpCRA9 Uj Sca 5oad SL 3 � z SAMPLE ID al OL aifflCb (A-2.0.9r r! A r� AR W Sample 10s MUST BE LINSQUEu�e U OthX OT V J w O m V m a n Qc rL Q 9 6Q f 1 x Q ca s• = W m III: , API = y u 3 O i 7 ritac a 2 Z Z O .: 4 IX Pace Project NO./ Lab I.D. GATE Ti V1e 7C ey • 2-: t :4 GYM 2- 3 5. 71 �16Diii0►iALCQM6AENTS -• R61 NQUiSliE)BY1.AFF!LiAT10M RATE TIME ';;',' ACCEPTEUBYlAI!f?L1H7Tatf:>:�: ,` A7E ; ' 7tuE:?; SASNPLECONDi170F[5 �RIGII�..j_ :sAI tOL it'tuwirr hka':slcirA E s� � a z m F PRINT flame of SAMPLER: ~ " `A! ¢ UP - y DATE S1Qned SIGNATURE Of SAMPLER: (MMlDDlYI'); / %�• j c/0i " wt-t N'= By armors ctis fan you am axapinp PsDw* Na- = Cay =S'nun.:sm' AN AG•ral a :0 Lw Chords. 0: 15% por morm bf any i1re:;az w Fold u1:M 3d eeri. ' F ALL-"20rev.07, 15-May-2007 Document Name: Sample Condition Upon Document Revised: April 04, 2013 aCeAnalyNcal' Receipt (SCUR) Page 1 of 2 J "'""�' "'"°' Document No.: I Issuing Authorities: Client Name: CID" Where Received: Hunlersville Asheville Cj Eden R leigh Courier(Clrclo): Fed Ex UPS USP3 Client Commercial Other Custody Seat on Cooler/Box Present. 0 yes ;E' no Seals intact: 4 yes n no Packing Material: El Bubble Wrap s VNona Other Circle Thermometer Used: IR Gun :122065387T of Ice: Wet Blue None Samples on Ice, 000ling process has begun IR Gun Ba 5371 Temp Correction Factor: Add A cl Wbtract-')C Date and Initials of peroon examining Corrected Cooler Temp.: i C Biological Tissue is Frozen: Yea tta NIA co chock: t s P t Temp. should be above keezing to 6140 C Ontnient8: Chdin of CUSIOdy Present: 6Yes ❑Na ❑WA 4. Chain of Custod rFllled Out: Yes ❑No ❑WA 2. Chain of Custody Relinquished: Yes ❑No ©N/A 3. Sampler Name 8 Signature on COC: Yes ❑Na ❑NIA 4. Samples {arrived Mthln Hold Time: AYes ❑No ❑NIA J.. Short Hold Time Anal is < 2hr : Yes OHO ❑NIA 6. Rush Turn Around Time Re crested: ❑Yes Na C]WA 7. Sufficient Volume: Yes ONO ❑WA 8. Correct Containers Used: Yes ❑No ❑WA 8. -Pace Containers Used; Yes ONO ❑WA Containers Intact: es ❑No ON/A 10. Filtered volume -received for Dissolved lasts ❑Yes ❑No NIA 11. Sample Labels match COG: Yea QNo Or,IIA 12. -includes dateltlmeADIAnaI sis Matrix All containers neading'preservatlon have been checked. as ❑No ❑Wq 13. AA eontafners needing preservation are found to be in as ❑No ❑NIA comp larme with EPA recommendation. emptlora: VOh coiiform,loc. C&G,WI-DRO(Water) Yes ONo Sam les checked for dechiorinatlon: es ❑No pwA 14. Headspace In VOA Vials >6mm): ores ONO 014A 15. Trip Blank Present: ❑Yes ONO YJWA ((AWA 18. Trip Blank Custody Seals Present ❑Yes ❑No Pace Trip Blank Lot # If purchased)' Client Notification/ Resolution: Field Data Required? Y 1 N Person Contacted- Date/Time: Comments/ Resolution: SCURF/SRF Review:; Date: Note: Whenever there Is a discrepancy affecting North Carollnb oompltanco samples, a copy of this form will be sent to the North Corolins DEHNR Certification-Ofiice ( Le out of hold, Incorrect preservallo, out of temp, Inoorred containers) Ir Oti92243-077 ltl8ll��hl�lai4lll,llhl; , { 1112263 17- s Page 11 of_11 Semi-annual Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG120000 Date submitted _ _ _ . _March 11, 2015 r' CERTIFICATE OF COVERAGE NO. NCG12 0 0 2 3 FACILITY NAME Onslow County Landfiil COUNTY Onslow PERSON COLLECTING SAMPLES No Samples Collected LABORATORY Lab Cert. # Comments on sample collection or analysis: Part A: Stormwater Benchmarks and Monitoring Results Z SAMPLE COLLECTION YEAR 2015 SAMPLE PERIOD ❑ Jan -June ❑ July -Dec or X❑ Monthly' February (month) DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA ❑Zero -flow ❑Water Supply ❑SA X❑Other Former Borrow Pit PLEASE REMEMBER TO SIGN ON THE REVERSE 4 ❑X No discharge this period?z Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches3 Chemical Oxygen Demand Fecal Coliform Total Suspended Solids Benchmarks 120 MgJ L 1000 count per 100 mL 100 mg/L or 50 mg/L' 3 __pm J L_1 1 Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. 2 For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. 4 See General Permit text, Table 3, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Note: Results must be reported in numerical format. For example, do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non - numerical format. When results are below the applicable limits, they must be reported in the format, "<XX mg/L", where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Conversely, where fecal coliform results exceed the dilution upper limit, report the result as ">XX". Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier Z, or Tier 3 responses. See General Permit text. Permit Date: 11/1/2012-10/31/2017 SWU-248, last revised 10/25/2012 Page 1 of 2 Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > SS gal of new oil per month. [],No discharge this period?z Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches Non -polar O&G/TPH by EPA 1664 (SGT-HEM) Total Suspended Solids pH Benchmarks =__> _ 15 mg/L 100 mg/L or 50 mg/L4 6.0 - , 9.0 SU Footnotes from Part A also apply to this Part B Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART It SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUiREMENT& SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDANCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO IF YES, HAVE YOU CUNTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an original and one coov of this DMR, including all "No Discharge" reports, within 30 days of receipt of the lab results (or at end of monitorinq period in the case of "No Discharae" reports) to: Division of Water Quality Attn: DWQ Centrai Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." b/ • (Signature of Permittee) Permit Date: 11/1/2012-10/31/2017 (Date) SWU-248, last revised 10/25/2012 Page 2 of 2 ,I CDM Smith 5400 Glenwood Avenue, Suite 400 Raleigh, North Carolina 27612 tel: 919-787-5620 fax: 919-781-5730 March 11, 2015 Attention: DWQ Central Files North Carolina Department of Environment and Natural Resources Division of Water Quality 1617 Mail Service Center Raleigh, North Carolina 27699-1617 Subject: Outfall 3 Discharge Monitoring Report - Tier 2 Response Monitoring Period - February 2015 Onslow County Landfill Certificate of Coverage Number - NCG120023 To the Division of Water Quality: RECEIVED MAR 16 2015 CENTRAL FILES DINR SECTION CDM Smith Inc., on behalf of Onslow County (County), is submitting two copies of the Stormwater Discharge Monitoring Report for Outfall 3. Samples collected from Outfall 3 during the 2014 semi-annual sampling events had detections of fecal coliform and chemical oxygen demand above the benchmark values. In response to the benchmark value exceedances, the County implemented Tier 1 and 2 responses. There was no discharge from Outfall 3 in February 2015. Per the Tier 11 response requirements, samples will be collected monthly for all parameters from Outfall 3 until three consecutive sampling events show the parameters are below the benchmark values. The County will maintain a record of the Tier 1 and 2 responses and monitoring results at the landfill. If you have any questions or require further explanation, do not hesitate to call me at (919) 325-3566. Sincerely, �P���.+.cX %� � � S•t,�,y� Daniel H. Forbes CDM Smith Inc. cc: Scott Bost, Onslow County Mathew Colone, CDM Smith Inc. A WATER + ENVIRONMENT +TRANSPORTATION + ENERGY + FACILITIES Semi-annual Stormwater Discha[ge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG120000 Date submitted March 6. 2015 CERTIFICATE OF COVERAGE No. NCG12 120023 FACILITY NAME Onslow County Landfill COUNTY OnSlow PERSON COLLECTING SAMPLES No Samples Collected LABORATORY Lab Cert. # Comments on sample collection or analysis: Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR 2015 SAMPLE PERIOD ❑ Jan -June ❑ July -Dec or X❑ Monthly' January month DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA ❑Zero -flow ❑Water Supply ❑SA X❑Other Former Borrow Pit PLEASE REMEMBER TO SIGN ON THE REVERSE ❑X No discharge this period?z Outfall No. Date Sample Collected (mo/dd/yr) 24-hour rainfall amount, Inches' Chemical Oxygen Demand Fecal Coliform Total Suspended Solids Benchmarks =_=> _ - 120 mg/L 1000 count per 100"mL 100 mg/L or 50 mg/L4 3 1 Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. 2 For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. See General Permit text, Table 3, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Note: Results must be reported in numerical format. For example, do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non - numerical format. When results are below the applicable limits, they must be reported in the format, "<XX mg/L", where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Conversely, where fecal coliform results exceed the dilution upper limit, report the result as ">XX". Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier.2, or Tier 3 responses. See General Permit text. Permit Date: 11/1/2012-10/31/2017 SWU-248, last revised 10/25/2012 Page 1 of 2 Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. ❑ No discharge this period?? Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches3 Non -polar O&G/TPH by EPA 1664 (SGT-HEM) Total Suspended Solids pH Benchmarks ===> _ - 15 mg/L 100 mg/L or 50 mg/L4 6.0 -- 9.0 SU Footnotes from Part A also apply to this Part 8 Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 1, or Tier 3-responses. See General Permit text. FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART -II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALI_ TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES ❑ NO IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an original and one copy of this DMR, including all "No Discharae" reports, within 30 days of receipt of the lab results (or at end of monitoring period in the case of "No Discharae" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." l� Z45>/_37- (Date) Permit Date: 11/l/2012-10/31/2017 SWU-248, last revised 10/25/2012 Page 2 of 2 �CDIIA Smith 5400 Glenwood Avenue, Suite 400 Raleigh, North Carolina 27612 tel: 919-787-5620 fax: 919-781-5730 March 6, 2015 Attention: DWQCentral Files North Carolina Department of Environment and Natural Resources Division of Water Quality 1617 Mail Service Center Raleigh, North Carolina 27699-1617 Subject: Outfall 3 Discharge Monitoring Report - Tier 2 Response Monitoring Period - January 2015 Onslow County Landfill Certificate of Coverage Number - NCG120023 To the Division of Water Quality: RECE/ E!o MAR. 16 2015 CENTp,AL Ff DwR SECTS E ON CDM Smith Inc., on behalf of Onslow County (County), is submitting two copies of the Stormwater Discharge Monitoring Report for Outfall 3. Samples collected from Outfall 3 during the 2014 semi-annual sampling events had detections of fecal coliform and chemical oxygen demand above the benchmark values. In response to the benchmark value exceedances, the County implemented Tier 1 and 2 responses. There was no discharge from Outfall 3 in January 2015. Per the Tier II response requirements, samples will be collected monthly for all parameters from Outfall 3 until three consecutive sampling events show the parameters are below the benchmark values. The County will maintain a record of the Tier 1 and 2 responses and monitoring results at the landfill. If you have any questions or require further explanation, do not hesitate to call me at (919) 325-3566. Sincerely, Daniel H. Forbes CDM Smith Inc. cc: Scott Bost, Onslow County Mathew Coione, CDM Smith Inc. A• �1 WATER + ENVIRONMENT +TRANSPORTATION + ENERGY + FACILITIES S°m'"en 5400 Glenwood Avenue, Suite 300 Raleigh, North Carolina 27612 tel: 919-787-S620 fax: 919-781-5730 February 4, 2015 Attention: DWQ Central Files North Carolina Department of Environment and Natural Resources Division of Water Quality 1617 Mail Service Center Raleigh, North Carolina 27699-1617 Subject: Semi -Annual Discharge Monitoring Report Monitoring Period - July 1, 2014 to December 31, 2014 Onslow County Landfill Certificate of Coverage Number - NCG120023 To the Division of Water Quality: RECEIVED FEB 0 9 2015 CENTRAL FILES DWR SECTION CDM Smith Inc., on behalf of Onslow County (County), is submitting two copies of the Stormwater Discharge Outfall Monitoring Report for the above referenced facility. Samples were collected from Outfalls 2 and 3 on December 22, 2014, after receiving 0.24 inches of precipitation. Outfall 1 currently receives stormwater runoff from the closed portion of the Subtitle D landfill and was removed from the analytical and qualitative monitoring requirements following a Division of Water Quality inspection on January 23, 2013. Samples collected from Outfalls 2 and 3 were analyzed for chemical oxygen demand (COD), fecal coliform, and total suspended solids by PRISM Analytical Services, Inc. located in Raleigh, North Carolina. Samples collected from Outfall 2 were below the benchmark values. Fecal coliform and COD were detected in samples collected from Outfall 3 above the benchmark values. Samples collected from Outfall 3 during the January 1 through June 30, 2014, monitoring period also had detections of fecal coliform and COD above the benchmark values. In accordance with the General Permit, the County has implemented the Tier 1 and 2 response actions. The Tier 1 response has been documented and filed at the landfill. Per the Tier II response actions, samples will be collected monthly for all parameters from Outfa.11 3 until three consecutive sampling events show the parameters are below the benchmark values. The County will maintain a record of the Tier II response and monitoring results at the landfill. �~d WATER + ENVIRONMENT + TRANSPORTATION + ENERGY + FACILITIES Smith Division of Water Quality February 4, 2015 Page 2 If you have any questions or require further explanation, do not hesitate to call me at (919) 325-3566. Sincerely, Daniel H. Forbes CDM Smith Inc. Attachments cc: Scott Bost, Onslow County Mathew Colone, CDM Smith Inc. STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT GENERAL PERMIT NO. NCGI20000 SAMPLES COLLECTED DURING=CALENDAWYEAR: 2014- CERTIFICATE OF COVERAGE NO. NCG120023 (This monitoring report is due at the Division no later than 30 days4rom4he date the facility receives the sampling results from the laboratory.) FACILITY NAME Onslow County Landfill COUNTY Onslow PERSON COLLECTING SAMPLES Mark Darwin (CDM Smith Inc.) PHONE NO. 910 989-2107 CERTIFIED LABORATORY Pace Analytical Services, Inc. Lab # 37712 Lab # PLEASE SIGN ON THE REVERSE 4 Part A: Specific Monitoring Requirements Outfall No. Date Sample Collected, molddl r 00340 31616 00530 Chemical Oxygen Demand, m Fecal Coliform, # per 100 ml Total Suspended Solids, m L Benchmark - 120 1000 colonies 100 2 12/22/14 119 256 10.7 3 12/22/14 302 3,300 139 Note: if you report a sampled value in excess of the benchmark value, you must implement Tier 1 or Tier 2 responses. See General Permit text. Does this facility perform Vehicle Maintenance --Activities-using more than-55-gallons-of new motor oil per month? -_ yes- -XX no - (if yes, complete Part B) Part B: Vehicle Maintenance Activity � onitoring =Re uirements- Outfall No. Date Sample Collected, molddl r 00556 00530 00400 Oil and Grease, m L Total Suspended Solids, mgfL pH, Standard units New Motor Oil Usage, Average annual allmo Benchmark - 30 100 6.0 — 9.0 - Note: if you report a sampled value in excess of the benchmark value, or outside the benchmark range for pH-, you must implement Tier; l-or Tier,2 responses. See General Permit text. STORM EVENT CHARACTERISTICS: Date 12/22/14 (first event -sampled) - Total Event Precipitation (inches): 0.24- Date (list each additional event sampled -this -reporting period; and -rainfall amount) - Total Event Precipitation (inches): -Mail-Original and°one'copy to: Attn: DWQ Central Files NCDENRI DWQ 1617 Mail Service Center Raleigh,NC 276994617 SWU-248-102107 Page 1 of 2 STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." 00 (Signature of Permittee) (Date) S W U-248-102107 Page 2 of 2 aceAnalytical. www pecelabscom January 06, 2015 Aaron Weisefenning CDM Smith 5400 Glenwood Ave Raleigh, NC 27612 RE: Project: Onslow 12122 Pace Project No.: 92230703 Dear Aaron Weisefenning: Pecs Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Enclosed are the analytical results for sample(s) received by the laboratory on December 22, 2014. The results relate only to the samples included in this report. Results reported herein conform to the most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. If you have any questions concerning this report, please feel free to contact me. Sincerely, Chris Derouen Christopher.derouen@pacelabs.com Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report shalt not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 1 of 11 aiteAnalytieal wmpecelab&com Project: Onslow 12122 Pace Project No.: 92230703 Raleigh Certification Ms 6701 Conference Drive, Raleigh, NC 27607 North Carolina Wastewater Certification M 67 Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87648 Massachusetts Certification M M-NCO30 North Carolina Drinking Water Certification M 37712 CERTIFICATIONS North Carolina Bioassay Certification M 16 North Carolina Drinking Water Certification #: 37731 North Carolina Wastewater Certification M 40 South Carolina Certification M 99030001 West Virginia Certification M 356 Virginia/VELAP Certification #: 460222 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 2 of 11 aceAnalytical wwwpecelebs.cam SAMPLE ANALYTE COUNT Project: Onslow 12/22 Pace Project No.: 92230703 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Lab ID Sample ID Method Analysts An alytes Reported Laboratory 92230703001 OUTFALL 3 SM 9222D JW1 1 PASI-R SM 2540D RC 1 PASI-R SM 5220D JTJ 1 PASI-A 92230703002 OUTFALL 2 SM 9222D JW1 1 PASI-R SM 2540D RC 1 PASi-R SM 5220D JTJ 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 3 of 11 aceAnalytical" ' www.pacelabs.aom ANALYTICAL RESULTS Project. Onslow 12122 Pace Project No.: 92230703 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Sample: OUTFALL 3 Lab ID: 92230703001 Collected: 12/22/14 11:30 Received: 12/22/14 14:05 Matrix: Water Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual MBIO 92220 Fecal Coliform RAL Analytical Method: SM 9222D Fecal Coliforms 3300 CFU1100 mL 1.0 1 12/22/14 14:46 2540D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids 139 mg/L 25.0 1 12/29/14 14A2 5220D COD Analytical Method: SM 5220D Chemical Oxygen Demand 302 mg1L 25.0 1 01/06/15 11:00 Sample: OUTFALL 2 Lab ID: 92230703002 Collected: 12/22/14 11:35 Received: 12/22/14 14:05 Matrix: Water Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual MBIO 92220 Fecal Coliform RAIL Analytical Method: SM 9222D Fecal Coliforms 256 CFU1100 mL 2.0 2 12/22/14 14A6 2540D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids 10.7 mg1L 4.2 1 12/29/14 14:43 5220D COD Analytical Method: SM 5220D Chemical Oxygen Demand 119 mglL 25.0 1 01/06/15 11:00 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. Date: 01/06/2015 05:57 PM without the written consent of Pace Analytical Services, Inc.. Page 4 of 11 aceAnalytical A wwwparewmcom Project: Onslow 12122 Pace Project No.: 92230703 QC Batch: RBI014686 QC Batch Method: SM 9222D Associated Lab Samples: 92230703001, 92230703002 METHOD BLANK: 1360029 Associated Lab Samples: 92230703001, 92230703002 Parameter Units Fecal Coliforms CFU1100 mL SAMPLE DUPLICATE: 1360030 Parameter Units Fecal Coliforms CFU1100 mL QUALITY CONTROL DATA Analysis Method: SM 9222D Analysis Description: 9222D MBIO Fecal Coliform - RAL Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 1.0 12/22/1414:46 92230684001 Dup Result Result 73.0 57.0 RPD Qualifiers 25 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Results presented on this page are In the units Indicated by the "Units' column except where an alternate unit Is presented to the right of the resuft. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. Date: 01 /06/2015 05:57 PM without the written consent of Pace Analytical Services, Inc.. Page 5 of 11 aceAnalytical. ,www.pacelabs.mm QUALITY CONTROL DATA Project. Onslow 12122 Pace Project No.: 92230703 QC Batch: RWETf7783 Analysis Method: SM 2540D QC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids Associated Lab Samples: 92230703001, 92230703002 METHOD BLANK: 1360376 Matrix: Water Associated Lab Samples: 92230703001, 92230703002 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mglL ND 2.5 12/29/14 14:37 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 LABORATORY CONTROL SAMPLE: 1360377 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Suspended'Solids mg1L 250 246 98 90-110 SAMPLE DUPLICATE: 1360378 92230684002 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mglL 58.0 62.0 7 SAMPLE DUPLICATE: 1360379 92230721001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mglL 66.7 58.3 13 D6 Results presented on this page are in the units Indicated by the "Units' column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /06/2015 05:57 PM without the written consent of Pace Analytical Services, Inc.. Page 6 of 11 aceAnalyfical ' www.pecelebs.c= Project: Onslow 12122 Pace Project No.: 92230703 QC Batch: WETA121490 QC Batch Method: SM 5220D Associated Lab Samples: 92230703001, 92230703002 METHOD BLANK: 1363590 Associated Lab Samples: 92230703001, 92230703002 Parameter Units Chemical Oxygen Demand mg1L LABORATORY CONTROL SAMPLE: 1363591 Parameter Units Chemical Oxygen Demand mg1L QUALITY CONTROL DATA Analysis Method: SM 5220D Analysis Description: 5220D COD Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 25.0 0110611511:00 Spike LCS Conc. Result 750 746 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1363592 MS MSD 92230352001 Spike Spike Parameter Units Result Conc. Conc. Chemical Oxygen Demand mg/L 5120 15000 15000 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 LCS % Rec % Rec Limits Qualifiers 99 90-110 1363593 MS MSD MS MSD % Rec Result Result % Rec % Rec Limits RPD Qual 13700 13600 57 57 90-110 1 M6 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1363594 1363595 MS MSD 92230565001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Chemical Oxygen Demand mg1L 141 750 750 831 836 92 93 90-110 1 Results prevented on this page are In the units Indicated by the "Units- column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. Date: 01 /06/2015 05:57 PM without the written consent of Pace Analytical Services, Inc.. Page 7 of 11 aceAnalytica! • www.pacelabs.m n QUALIFIERS Project. Onslow 12/22 Pace Project No.: 92230703 DEFINITIONS Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 OF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of the sample aliquot, or moisture content. NO - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL - Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit. S - Surrogate 1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Acid preservation may not be appropriate for 2-Chloroethyivinyl ether, Styrene, and Vinyl chloride. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. LABORATORIES PASI-A Pace Analytical Services -Asheville PASI-R Pace Analytical Services - Raleigh ANALYTE QUALIFIERS D6 The relative percent difference (RPD) between the sample and sample duplicate exceeded laboratory control limits. M6 Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01l06/2015 05:57 PM without the written consent of Pace Analytical Services, Inc.. Page 8 of 11 aceAnalXical. ' ivww.pacelab&com QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Onslow 12122 Pace Project No.: 92230703 Lab ID Sample ID QC Batch Method QC Batch 92230703001 OUTFALL 3 SM 9222D RB10l4686 92230703002 OUTFALL 2 SM 9222D RB1014686 92230703001 OUTFALL 3 SM 2540D RWETl7783 92230703002 OUTFALL 2 SM 2540D RWETl7783 92230703D01 OUTFALL 3 SM 5220D WETA121490 92230703002 OUTFALL 2 SM 5220D WETA121490 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Analytical Method Analytical Batch Date: 01/06/2015 05:57 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 9 of 11 f "dceAnaocaf Wwwasoel bmm Section A Required Ciifxil Irdo Trod n: CHAIN -OF -CUSTODY f Analytical Request Document The Chain-of-Cus" is a LEGAL DOCUMENT. Ap ralevam fields must be =n*rtad accurst*. Section D Section C Requires Project Infaansaon: Invoice irdbr nmion: a m m is 4 Papa: of t t To: Ate:110M 1 tS tS ti ti 1 tS s �, y y P Copy To: Company Name: REGULATORY AGENCY Aedrosw. r NPDES r- GROUNDWATER F DRINKING WATER 5 usr f RCRA r oTttEx Empil 70: PreUtasa Order Nw. P= Ouse Phone: Fax Projoel Name: P Stte Loeatiorl s, 3 U 15� SrA Requested Due Date fAT: ProJed Number Paco p MOP f: Regsfeated Analysts Filtered {YJirij Section D hiattix Codes wquvea caerd tnrmreUM rcarmx r cciof Ddrift weOw br s C COLLECTED Aresena0ives i= we V%FT Weafa Water ww V mproduct COMPOSM STARr coupc$n E1WgrtA6 yVj p sowsatd SL $ Q ey SAMPLE ID � = „ W c wp (AZ 04/r) AM AR p ru a z Q 9 } `o $ample i0s MUST K UNME Ticauo TS O 0. m to U Ottror OT X 0O U a On 8 4 y C p = r e m �.L �3 070 t OATS TIME awTE Tim y c z z x= v � z �' z m 20 �` Pace Project NoJ Lab I.D. t UTV, 3 k 1 1 141�r k k Oct 2 3 4 S 6 T B. 9 10 11 t2 ADWT*"LCOAtMaM tiELINgWSItiEC i3YIAFFiLu4TM DATE TIME ActRgrN DATE Tam SAmpLE CONDrnONS ( VA40�' C►? ORIGINAL sAstPLERNAMEAND SIGNATURE, � g �a Z "+ 1"IT Namo or SAMPLFc , E aZ c DATE Signori i SIGNATURE of SAMPLER: �'�' t }" J m y E q N 'rreoaunt NOW ay %%V V a.s rum you era accepbW Pxe s NET 30 say payaxrt term: sea aRearg m Itte cr"M of J.S% Per berm for arty'+.*= mt avd wvD 30 wYs. F-ALL43-020rev.07. 7SMay-2007 r 40 f Document Name: Sample Condition -Receipt SCUR Document No.: Document Revised: April 04, 2013 . - - Page 1 of 2 Issuing Authorities:. Pace Asheville Quality Office Client Name: . Where Received: Huntersville Asheville Eden A Raleigh Courier (Circle): Fed Ex UPS USPS pho - Commercial Pace . Other_ _ Custody Seal on CoolerlBox present: ye& Seals intact: yes El no Packing Material: ❑ Bubble Wrap Bubble Bags 0 None' Other Circle Thermometer Used: I pun :i22Q65387 ype of Ice: Blue None n Somplason Ice, aoolingprocess has bogun iR Gun Bac N: 22085371 'temp Correction Factor: Add 1 ubtract , C Correoted Cooler Temp.:...._.. C Biological Tissue Is Frozen; Yes no NIA Temp, should be above freezing to 610 Comments: pate and Initials of per on e: am ng check nt P� ° u ` Chdln of Custody Present: 9IYea ❑No OVA 1. Chaln of Custody Filled Out: fhYos ONO ❑NIA 2. Chaln of Custody Relln wished: yss ONO ❑N.A 3. Sampler Name & Signature on COC: Yes ON. ❑wA 4. Samples Arrived within Hold lime: 4yes ❑No ❑wA 5.- Short Hold Tim Anai sis' <2hr : Yea ON, ❑WA 8. Rush Turn Around Time Requested: ❑Yea No ❑wA 7. Sufftclent Volume: VYes ❑No ❑N!A 8. Correct Containers Used: -Pace Containers Used: Byes ONO ` Yss ❑No DIVA ❑wA 9. Containers intact: 6YOO ❑No ❑WA 10. Filtered volume -received for Dissolved tests OYes f3tlo qfVA 11. Sample Labels match COG. -includes dateldme/lDlAnal sis Matrix: IljYee 1.7No 1/ ❑WA 12. Arl containers needing preservation have been checked. All containers needing preservation are found to be In compliance with EPA recommendation. exceptions; VOA, peliform, TOC, 0&0. WI -PRO crater) ]Yes ❑No rC%1es ONO lr Yes ONO OWA DIVA 13. Samples checked for dechlorination: iiVes ONO ❑NrA 14. Meads ace in VOA Vials ( >6mm): Yes ONO ONJA 15. Trip Blank Present: Trip Blank Custody Seats Present Pace Trip Blank Lot# if purchased): ❑yes ONO Dyes ONO �NrA VWA 18. Client NotiFloationl Resolution: Field Data Required? Y 1 N Person Contacted: DatelTime: Commehisi Resolution: SCURF 1SRF pate: r A , Review:: Note: Whenever there Is a disoreparwy affecting North Ca Itna compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Cfflce (i,e out of hold, incorrect preservative, out of temp. Incorrect containers) WO#:92230703 92230703 Page 11 of 11 � CDM Smith 5400 Glenwood Avenue, Suite 300 Raleigh, North Carolina 27612 tel: 919-787-5620 fax: 919-781-5730 July 10, 2014 Attention: DWQ Central Files North Carolina Department of Environment and Natural Resources Division of Water Quality 1617 Mail Service Center Raleigh, North Carolina 27699-1617 Subject: Semi -Annual Discharge Monitoring Report Monitoring Period —January 1, 2014 to June 30, 2014 Onslow County Landfill Certificate of Coverage Number - NCG120023 To the Division of Water Quality: RECEIVED JUL 15 2054 CEN`fRAL FILES DWQIBOG CDM Smith Inc., on behalf of Onslow County, is submitting two copies of the Stormwater Discharge Outfall Monitoring Report for the above referenced facility. The facility received 1.53 inches of precipitation on May 16, 2014. Samples were collected from Outfalls 2 and 3 and analyzed for fecal coliform, chemical oxygen demand, and total suspended solids. Outfall 1 currently receives stormwater runoff from the closed portion of the Subtitle D landfill and was removed from the analytical and qualitative monitoring following a Division of Water Quality inspection on January 23, 2013. If you have any questions or require further explanation, do not hesitate to call me at (919) 787-5620, Sincerely, Daniel H. Forbes CDM Smith Inc. Attachments cc: Scott Bost, Onslow County Mathew Colone, CDM Smith Inc. 40 WATER + ENVIRONMENT +TRANSPORTATION + ENERGY + FACILITIES STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT GENERAL PERMIT NO. NCG120000 SAMPLES COLLECTED DURING CALENDAR YEAR: 2014 -CERTIFICATE-OF_COVERAGE=NO: NCG120023 - -(This monitoring -report is -due at.the=Division=no later than 30 days from the date the facility receives the sampling results from the laboratory.) FACILITY NAME Onslow County Landfill COUNTY Onslow -PERSON-COLLECTING.SAMPI,ES_ Aaron -Weis fennin CDM Smith Inc:) PHONE NO. (910) 989-2107 CERTIFIED LABORATORY ENCO Laboratories Lab # 591 Lab # PLEASE SIGN ON THE REVERSE 4 Part A: Specific Monitoring Requirements Outfall No. Date Sample Collected, mo/dd/ r 00340 31616 00530 Chemical Oxygen Demand, m gLL Fecal Coliform, # per 100 ml Total Suspended Solids, m Benchmark - 120 1000 colonies 100 2 5/16/14 28 <2420 4.4 3 5/16/14 250 <2420 91 Note: If you report a sampled value in excess of the benchmark value, you must implement Tier I or Tier 2 responses. See General Permit text. Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? _ yes _XX_no (if yes, complete Part B) Part B: Vehicle Maintenance Activity Monitoring Requirements Outfall No: Date Sample Collected, mo/dd/ r 00556 00530 00400 Oil and Grease, m Total Suspended Solids, m pH, Standard units New Motor Oil Usage, Average annual al/mo Benchmark - 30 100 6.0 — 9.0 - Note: If you report a sampled value in excess of the benchmark value, or outside the benchmark range for pH, you must implement Tier I or Tier 2 responses. See General Permit text. STORM EVENT CHARACTERISTICS: -Date_ 5/16/14- -(first-event,sampled). Total--Event-P-recipitation (inches): 1.53 Date (list each additional event sampled this reporting period, and rainfall amount) Total Event Precipitation (inches): Mail Original and one copy to: Attn: DWQ Central Files NCDENR/ DWQ 1617 Mail Service Center Raleigh, NC 27699-1617 S WU-248-102107 Page] of 2 STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Permittee) (Date) SWU-248-102107 Page 2 of 2 Environmental Conservation Laboratories, Inc. 102-A Woodwinds Industrial Court Cary NC, 27511 Phone: 919.467.3090 FAX: 919.467.3515 Monday, June 2, 2014 CDM Smith, Inc. (CD004) Attn: Dan Forbes 5400 GLENWOOD AVE SUITE 300 RALEIGH, NC 27612- RE:. Laboratory Results for Project Number: [none], Project Name/Desc: Onslow County NPDES ENCO Workorder(s): C405428 Dear Dan Forbes, Enclosed is a copy of your laboratory report for test samples received by our laboratory on Friday, May 16, 2014. Unless otherwise noted in an attached project narrative, all samples were received in acceptable condition and processed in accordance with the referenced methods/procedures. Results for these procedures apply only to the samples as submitted. The analytical results contained in this report are in compliance with NELAC standards, except as noted in the project narrative. This report shall not be reproduced except in full, without the written approval of the Laboratory. This report contains only those analyses performed by Environmental Conservation Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from outside organizations will be reported under separate cover. If you have any questions or require further information, please do not hesitate to contact me. Sincerely, Chuck Smith Project Manager Enclosure(s) (9 �eo www.encolabs.com The total number of pages in this report, including this page is 11. (� �Go www.encolabs.com SAMPLE SUMMARY/LABORATOKY CHRONICLE Client 1D: Dutlall 2 Lab ID: C40S428-01 Sampled: 05/16/14 11:50 Received: 05/16/14 14:40 Parameter Hold Date/Time(s) Prop Date/Tlme(s) Analysis Date/Time(s) Colilert 18 05/16/14 17:50 05/17/14 15:39 05/16/14 17:35 5/17/2014 11:50 SM 2540D-1997 05/23/14 05/21/14 11:47 5/21/2014 11:47 SM 5220D-1997 06/13/14 05/20/14 10:32 5/20/2014 17:58 Client ID: Outfall 3 Lab ID: C405428-02 Sampled: 05/16/14 12:20 Received: 05/16/14 14:40 Parameter Hold Date/Tlme(s) _ _ __ -.-Prep Date/Time(s)_ _Analysis Date/Time(s) Cglilert 18 Y 05/16/14 18:20 �05/17/14 15:39 05/16/14 17:35 5/17/2014 11:50 SM 2540D-1997 05/23/14 05/21/14 11:47 5/21/2014 11:47 SM 5220D-1997 06/13/14 05/20/14 10:32 5/20/2014 17:58 Page 2 of l l (� �eo www.encolabs.com NORTH CAROLINA SWS SAMPLE DE ga0N SUMMARY lient ID: Outfall 2 Lab ID: C405428-01 Analyte Results flag OF MDL MRL NC SWSL Units Method Notes Chemical Oxygen Demand 28 1 10 10 NE mg/L SM 5220D-1997 Total Suspended Solids 4.4 1 1.0 1.0 NE mg/L SM 254OD-1997 lient 10. Outfall 3 Lab ID: C405428-02 Analyte Results Flag DF MDL MRL NC SWSL Units Method Notes Chemical Oxygen Demand 250 1 10 10 NE mg/L SM 5220D-1997 Total Suspended Solids 91 1 1.0 1.0 NE mg/L SM 254OD-1997 Page 3 of l 1 Ce NS' �■ www.enoolabs.Lwm ANALYTICAL BESULTS Description: Outfall 2 Lab Sample I0: C405428-01 Received: 05/16/14 14!40 Matrix: Surface Water Sampled: 05/16/14 11:50 Work Order: C405428 Project: Onslow County NPDES Sampled By: Aaron Weispfenning Classical Chemistry Parameters ^ - ENCO Cary cerjrAed anaVe (NC 5911 Resufts an units X FIDL H& t SWSS ]mod Anal�rsed Ift Chemical Oxygen Demand [ECL-0035] 28 mg/L 1 10 10 NE SM 5220D-1997 05/20/14 17:58 loc ^ Total Suspended Solids [ECL-0159] ^ 4.4 mglL 1 1.0 1.0 NE SM 2540D-1997 OSJ21/14 11:47 MMR Page 4 of 11 Description: Outfall 2 Matrix: Surface Water Project: Onslow County NPDE5 Microbiological Parameters ^ - ENCO Cary certfred a-W [NC 5911 AnaMe T—CM Humberl Wiform, Fecal [ECL-00381 ^ Lab Sample ID: C405428-01 Sampled: 05/16/ 14 11: 50 Sampled By: Aaron Weispfenning (� �(20 www.encolabs.com Received: 05/ 16/ 14 14 :40 Work Order: C405428 >2420 MPN/100 mL 1 1.0 Colllert 18 05/17/14 11:50 ASC This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 5 of 11 Description: Outfal 13 Matrix: Surface Water Project: Onslow County NPDES Lab Sample ID: C405428-02 Sampled: 05/16/ 14 12:20 Sampled By: Aaron Weispfenning �G-O- www.encolabs.com Received: 05 / 16/ 14 14:40 Work Order: C405428 Classical Chemistry Parameters ^ ENCO Cary -,Ytified a -Ate ANC 591] Anabft jCAS Number? Resu E[g9 U& PIE ML MRL NC Sws Method Analyzed ft Mgt= Chemical Oxygen Demand [ECL-0035] 250 mg/L 1 10 10 NE SM 5220D-1"7 05/20/14 17:5B 30C n Total Suzpended Solids [ECL-0169] 91 mg/L 1 LO 1.0 NE SM 2540D-1997 05/21/14 11:47 MMR Page 6 of I I (� �Ge) www.encolabs.com Description: Outfall 3 Lab Sample ID: C405428-02 Received: 05/16/14 14:40 Matrix: Surface Water Sampled: 05/16/14 12:20 Work order: C405428 Project: Onslow County NPDES Sampled By: Aaron Weispfenning Microbiological Parameters A - ENQ7 Cary c_bfied arralyte [NC 591] AnaNte ICAS Numbed Results EIJg Units 9E MU NC SWSL Meth AnalZmd fy Mgt= Colifomr, Fecal [ECL-00381 ^ >2420 MPN/100 mL 1 1.0 Colllert 18 05/17/14 11:50 PSC This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 7 of 11 (9 �eo www.encolabs.com QUALITY CONTROL Classical Chemistry Parameters - Quality Control Batch 4E20006 - Same Blank (4E20006-BLK1) Prepared: 05/20/2014 10:32 Analyzed: 05/20/2014 17:58 Spike Source %REC RPD Analyte Result Flag MRL Units Level Result %REC Limits RPD Limit Notes Chemical Oxygen Demand 10 U 10 mg/L LCS (4E20006-BSI) Prepared: 05/20/2014 10:32 Analyzed: 05/20/2014 17:58 IAnallyte,Result Spike Source %REC RPD Flag MRL Units Level Result %REC Limits RPD Limit Notes Chemical Oxygen Demand 490 10 rrg/L 500 98 90-110 Matrix Spike (4E20006-MS1) Prepared: 05/20/2014 10:32 Analyzed: 05/20/2014 17:58 Source: C402318-01 IAnalyte Spike Source %REC RPD Result Flag MRL Units Level Result %REC Limits RPD Limit Notes Chemical Oxygen Demand 16000 200 mg/L 10000 69W 89 90-110 QM-05 Matrix Spike Dup (4E20006-MS01) Prepared: 05/20/2014 10:32 Analyzed: 05/20/2014 17:58 Source: C402318-01 IAnalyte Spike Source %REC RPD Result Flag MRL Units Level Result %REC Limits RPD Limit Notes Chemical Oxygen Demand 17000 2D0 mg/L 10000 6900 97 90-110 5 10 Batch 4E21016 - NO PREP Blank (4E21016-BLKI) Prepared & Analyzed: OS/21/2014 11:47 Spike Source %"C RPb Analyte Result Flag MRL Units Level Result %REC Limits RPD Limit Notes Total Suspended Solids 1.0 U 1.0 LCS(4E21OL6-BSI) Analyte Result Flag MRL Total Suspended Solids Duplicate (4E21016-DUP1) Source: C406029-02 99 1.0 Analyte Result Flag MRL Total Suspended Solids 4000 1.0 Duplicate (4E21016-DUP2) Source: C406029-03 mg/L Prepared & Analyzed: 05/21/2014 11:47 Spike Source %REC RPD Units Level Result %REC Limits RPD Limit Notes mg/L 100 99 80-120 Prepared & Analyzed: 05/21/2014 11:47 Spike Source %REC RPO Units Level Result %REC Limits RPD Limit Notes mg/L 4000 0 10 Prepared & Analyzed: 05/21/2014 11:47 Spike Source %REC RPO Analyte Result Flag WILL Units Level Result %REC Limits RPD Limit Notes Total Suspended Solids 4200 1.0 mg/L 4400 3 10 Microbiological Parameters - Quality Control Batch 4E14020 - NO PREP Page 8 of 11 Microbiological parameters - Quality Control &trh 4E19010 - NO PREP Duplicate (41E19020-DUPI) Source: C405536-02 CemNL" www.encolabs.com QUALITY CONTROL Prepared: 05/16/2014 14:08 Analyzed: 05/17/2014 11:50 Spike Source %REC RPD IAnalyte Result Flag MRL Units Level Result %REC Limits RPD Limit Notes Coliform, Fecal 6.3 1.0 WN1100 3.1 68 25 QR-04 mL Page 9 of 11 www.encolabs.com FLAGS/NOTES AND DEFINITIONS B The analyte was detected in the associated method blank. D The sample was analyzed at dilution. J The reported value is between the laboratory method detection limit (MDL) and the laboratory method reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable. U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation data and moisture content, where applicable. E The concentration indicated for this analyte is an estimated value above the calibration range of the instrument. This value is considered an estimate. MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is based on the low point of the calibration curve, when applicable, sample preparation factor, dilution factor, and, in the case of soil samples, moisture content. QM-05 The spike recovery was outside acceptance limits for the MS and/or MSD due to matrix interference. The LCS and/or LCSD were within acceptance limits showing that the laboratory is in control and the data is acceptable. QR-04 Duplicate precision outside acceptance limits due to low analyte concentration. Page 10 of I I ENVIRONMENTAL CONSERVATION LABORATORIES CHAIN -OF -CUSTODY RECORD www.encolabs.com 10775 Central Port Dr. 4610 Executive Park Court, Suite 111 102-A Woodwinds Industrial Cit. + Orlando, FL 32824 Jacksonville, FL 32216.6069 ' Cary, NC 27511 II 1 (407826-5314 Fax (407) 85-6945 (904)96-07 Fax(904)296(919)467-3090 Fax(919)47-3515 oaga f ll Client Name r- M Smith Inc { Project Number Requested Analyses Requested Turnaround Times Note: Rush requests subject to acceptance by the facility Standard _Expedited Due N _ — [C,',r �i �1 u- C� � i%I Address U - ., I] Projec Name, - scCl Onsl w hunt NPDES CityIST(Zrp RALEIGH NC 27612- PO # I Billing Into Tel . 32-5-35Bu A Fax Reporting Contact Dan Forbes Sampler ) Name, Affiliation {Print) tn!' ,s n.r��a �UI`'1 .S r.�t` Billing Contact Accounts Payable— Sampler(sj Sign ure l Site Location 1 Time Zone Lab Wprkori. -, r4 Preservation (See Codes) (Combine as necessary) Item # Sample ID (Field IdentlfiCation) Collection Date Collection Time Comp I Grab Matrix (see codes) loW # of Containers Sample Comments -16'I� lc�D V �' I 3 X X — , Total # of Containers Sample Ka Prepared By Date/Time Relinquished B "1 elDaterrime Received � Data/Time CommenlsrSpeaial Reporting Requirements Relinquish y V Date/Time eceived'By Date7rime Relinquished By Date/Time Rece' ed By Dalerrime Cooler #'s & Temps on Receipt I Condition U Receipt { Acceptable Unacceptable Alatt X : OW-Groenowaler SD -Soil DW-Drinking Water SE -Sediment SW-Surlace Water WW-Wastewater A -Air O-Other (detail in comments) Preservation: I -Ice H-HCI N-HNO3 S-H2SO4 NO-NaOH 0-Other (detail In comments) Note: All samples submitted to ENCO Labs are in accordance with the terms and conditions listed on the reverse of this form. unless prior written agreements eKist