NCG030664_Monitoring Report_20191023

.44
October 23, 2019
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
Permit No: NCG030000
Certificate of Coverage: NCG030664
Southwire
12331 Commerce Station Drive
Huntersville, NC 28078
Dear Sir/Madam:
Enclosed is the Semi -Annual Stormwater Discharge Monitoring Report and associated analytical
results for the Southwire Facility.
This report covers required sampling for 2019 July — December Semi -Annual.
Should you have any questions, please contact me at 704-379-9621 or
iamie.mcgrath(a)southwir6.com. Thank you.
Regards,
Jamie McGrath
EHS Manager
Southwire I Huntersville

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aceAnalytical
www.pacelabs.com
October 22, 2019
Jamie McGrath
Southwire
12331 Commerce Station Dr
Huntersville, NC 28078
RE: Project: 2019 Semi -Annual
Pace Project No.: 92449794
Dear Jamie McGrath:
Pace Analytical Services, LLC
205 East Meadow Road - Suite A
Enclosed are the analytical results for sample(s) received by the laboratory on October 16, 2019.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
<�
Taylor Ezell
[e-mail]
[phone]
Project Manager
Enclosures
�Pp ACCpeo
�� 't REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
ME without the written consent of Pace Analytical Services, LLC
Eden, NC 27288
[phone]
Page 1 of 11

aceAnalytical
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Project: 2019 Semi -Annual
Pace Project No.. 92449794
Pace Analytical Services, LLC
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
VirginiaNELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 11

aceAnalytical e
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SAMPLE ANALYTE COUNT
Pace Analytical Services, LLC
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Project:
Pace Project No.:
2019 Semi -Annual
92449794
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92449794001
ROS Outfall #2
EPA 1664E
HH
1
PASI-C
EPA 200.7 Rev 4.4 1994
DS
3
PASI-A
SM 2540D-2011
MJP
1
PASI-A
EPA 9040C
ECH
1
PASI-A
REPORT OF LABORATORY ANALYSIS
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1!,;a'ce Analytical..
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ANALYTICAL RESULTS
Pace Analytical Services, LLC
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Project: 2019 Semi -Annual
Pace Project No.: 92449794
Sample: ROS Outfall #2 Lab ID: 92449794001 Collected: 10/16/19 07:47 Received: 10/16/19 10:14 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No Qual
HEM, Oil and Grease
Analytical Method: EPA 1664B
Oil and Grease
ND mg/L
4.8 1
10/18/19 18:33
200.7 MET ICP
Analytical Method: EPA 200.7 Rev 4.4
1994 Preparation Method: EPA 200.7 Rev 4.4 1994
Copper
ND mg/L
0.0050 1
10/17/19 22:15 10/19/19 20:22 7440-50-8
Lead
ND mg/L
00050 t
10/17/19 22:15 10/19/19 20:22 7439-92-1
Zinc
ND mg/L
0.010 1
10/17/19 22:15 10/19/19 20:22 7440-66-6
2540D TSS, Low -Level
Analytical Method: SM 2540D-2011
Total Suspended Solids
1.2 mg/L
1.0 1
10/19/19 06:23
9040 pH
Analytical Method: EPA 9040C
pH at 25 Degrees C
7.3 Std. Units
0.10 1
10/21/19 16:25 H3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/22/2019 02:56 PM without the written consent of Pace Analytical Services, LLC Page 4 of 11

aceAnalytical
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QUALITY CONTROL DATA
Project: 2019 Semi -Annual
Pace Project No. 92449794
QC Batch: 504574 Analysis Method: EPA 1664E
QC Batch Method: EPA 1664E Analysis Description: 1664 HEM, Oil and Grease
Associated Lab Samples: 92449794001
METHOD BLANK: 2711750 Matrix: Water
Associated Lab Samples: 92449794001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Oil and Grease mg/L ND 5.0 10/18/19 18:28
Pace Analytical Services, LLC
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
LABORATORY CONTROL SAMPLE:
2711751
Spike LCS
LCS
% Rec
Parameter
Units
Conc. Result
% Rec
Limits
Qualifiers
Oil and Grease J
mg/L
40 36.0
90
78-114
MATRIX SPIKE SAMPLE:
2711752
92449509001 Spike
MS
MS
% Rec
Parameter
Units
Result Conc.
Result
% Rec
Limits Qualifiers
Oil and Grease
mg/L
47.2 88.9
43.6
-4 78-114 M1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Project: 2019 Semi -Annual
Pace Project No.: 92449794
QC Batch: 504348
QC Batch Method: EPA 200.7 Rev 4.4 199�
Associated Lab Samples: 92449794001
METHOD BLANK: 2710597
Associated Lab Samples: 92449794001
Parameter
Copper
Lead
Zinc
QUALITY CONTROL DATA
Analysis Method: EPA 200.7 Rev 4 4 1994
Analysis Description: 200.7 MET
Matrix:
Water
Blank
Reporting
Units
Result
Limit
Analyzed Qualifiers
mg/L
ND
0.0050
10/19/1919:55
mg/L
ND
0.0050
10/19/1919:55
mg/L
ND
0.010
10/19/1919:55
Pace Analytical Services, LLC
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
LABORATORY CONTROL SAMPLE:
2710598
Spike
LCS LCS % Rec
Parameter
Units
Conc.
Result % Rec Limits Qualifiers
Copper
mg/L
0.5
0.48 96 85-115
Lead
mg/L
0.5
0.47 94 85-115
Zinc
mg/L
0.5
0.46 93 85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2710599
2710600
MS
MSD
92449710001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits RPD Qual
Copper mg/L
76.3
0.5
0.5
0.58
0.59
100
102
70-130 2
ug/L
Lead mg/L
11.8
0.5
0.5
0.48
0.49
94
96
70-130 2
ug/L
Zinc mg/L
196
0.5
0.5
0.67
0.68
94
98
70-130 2
ug/L
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2710601
2710602
MS
MSD
92449873001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits RPD Qual
Copper mg/L
39.4
0.5
0.5
0.51
0.52
95
96
70-130 1
ug/L
Lead mg/L
ND
0.5
0.5
0.47
0.47
93
93
70-130 0
Zinc mg/L
38.5
0.5
0 5
0.51
0.51
94
95
70-130 1
ug/L
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/22/2019 02:56 PM without the written consent of Pace Analytical Services, LLC
Page 6 of 11

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QUALITY CONTROL DATA
Project: 2019 Semi -Annual
Pace Project No.. 92449794
QC Batch: 504603 Analysis Method: SM 2540D-2011
QC Batch Method: SM 2540D-2011 Analysis Description: 2540D Total Suspended Solids
Associated Lab Samples: 92449794001
METHOD BLANK: 2711853
Associated Lab Samples: 92449794001
Parameter Units
Total Suspended Solids
mg/L
LABORATORY CONTROL SAMPLE:
Parameter
2711854
Units
Total Suspended Solids
mg/L
SAMPLE DUPLICATE: 2711867
Parameter
Units
Total Suspended Solids
mg/L
SAMPLE DUPLICATE: 2711868
Parameter
Units
Total Suspended Solids
mg/L
Pace Analytical Services, LLC
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 1.0 10/19/19 06:21
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
250 248 99 90-110
92449852001 Dup
Result Result
185 207
92449986001 Dup
Result Result
1330 1340
RPD Qualifiers
11 D6
RPD Qualifiers
1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 10/22/2019 02:56 PM without the written consent of Pace Analytical Services, LLC Page 7 of 11

aceAnalytical e
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QUALITY CONTROL DATA
Project: 2019 Semi -Annual
Pace Project No.: 92449794
QC Batch: 504652 Analysis Method: EPA 9040C
QC Batch Method: EPA 9040C Analysis Description: 9040 pH
Associated Lab Samples: 92449794001
SAMPLE DUPLICATE: 2711977
Parameter
pH at 25 Degrees C
SAMPLE DUPLICATE: 2712321
Parameter
pH at 25 Degrees C
92449480001 Dup
Units Result Result RPD Qualifiers
Std. Units 7.0 6.8 2 D6,H3
92449465002 Dup
Units Result Result RPD Qualifiers
Std. Units 7.0 6.9 1 H3
Pace Analytical Services, LLC
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 10/22/2019 02:56 PM without the written consent of Pace Analytical Services, LLC.
Page 8 of 11

25ceAnalyfical'
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QUALIFIERS
Project: 2019 Semi -Annual
Pace Project No : 92449794
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
NO - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
Pace Analytical Services, LLC
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
PQL- Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute
LABORATORIES
PASI-A Pace Analytical Services - Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
D6 The precision between the sample and sample duplicate exceeded laboratory control limits.
H3 Sample was received or analysis requested beyond the recognized method holding time.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/22/2019 02:56 PM without the written consent of Pace Analytical Services, LLC Page 9 of 11

aceAnalytical
www.pacelabs.com
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Analytical Services, LLC
205 East Meadow Road - Suite A
Eden, NC 27266
[phone]
Project:
2019 Semi -Annual
Pace Project No..
92449794
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch Analytical Method Batch
92449794001
ROS Outfall #2
EPA 1664E
504574
92449794001
ROS Outfall #2
EPA 200.7 Rev 4.4 1994
504348 EPA 200.7 Rev 4.4 1994 504398
92449794001
ROS Outfall #2
SM 254OD-2011
504603
92449794001
ROS Outfall #2
EPA 9040C
504652
Date: 10/22/2019 02:56 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC
Page 10 of 11

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