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HomeMy WebLinkAboutNCG030027_MONITORING INFO_20190806STORMWATER DIVISION CODING SHEET NCG PERMITS PERMIT NO. DOC TYPE. ❑ HISTORICAL FILE C�MONITORING REPORTS DOC DATE ❑ 000 C) YYYYMMDD Fm,aT*N Dustin A. LaClair Environmental, Health & Safety Manager (336) 503-6538 (office) (336) 503-6562 (fax) dustinlaclair(a)eaton. com July 31, 2019 Division of Water Quality 1617 Mail Service Center Raleigh, North Carolina 27699-1617 Attn: DWQ Central Files Rid.,.} AUG 0 6 2019 CENTItHL FILES DWR SECTION RE: June 2019 Monthly Tier III Discharge Monitoring Report Enclosed is a revised Discharge Monitoring Report for our facility for the month of June 2019. While the laboratory results submitted were complete, incomplete or incorrect information was summarized on the DMR Form. The DMR Form has been updated to reflect all the sampling data from our semi-annual sampling event. I apologize if this caused any confusion. Attached are the analytical results and associated chain of custody for the June 18, 2019 semi-annual Tier III stormwater outfall sampling event, submitted in accordance with Section D of the NPDES Stormwater General Permit No. NCG030000 and Certificate of Coverage No. NCG030027 issued to our facility. Additionally, attached is the applicable Discharge Monitoring Report (DMR) Form provided by the North Carolina Division of Water Quality (NCDWQ). I certify under penalty of law that this document and all attachments were prepared under my direction or supervision in accordance with the system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or other persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fine and imprisonment for knowing violations. Sincere ila. 4V Dustin A. LaClair EHS Manager Attachments Stormwater Discharge Monitoring Report for North Carolina Division of Energy, Mineral and Land Resources General Permit No. NCG030000 Date submitted CERTIFICATE OF COVERAGE NO. NCG03 o 0 2 7 FACILITYNAME Eaton Corporation COUNTY Person PERSON COLLECTING SAMPLES Dustin Laclair LABORATORY PACE National Lab Cert. q ENV375/DW21704/810041 Comments on sample collection or analysis: Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR 2019 SAMPLE PERIOD Q Jan -June ❑ July -Dec or ❑ Monthly' (month) DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA ❑Zero -flow ❑Watersupply [:]SA *Other WS-w; NSW PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4 No discharge this periodj2 - �06tfallNo. .. Date.Sample .Collected' (mo/dd/yr) 24-hour rainfall.: l amount, Inches' _ Total Suspended Solids - P. H, -Total Standard units — Copper 'Total Lead Total Zinc. Non -Polar OW Total Petroleum ' 'Hydrocarbons Total Toxic Organics s Benchmarks 100 mg/L or 50 mg/L4 6.0— 9.0 - 0.010 mg/L 0.075 mg/L 0:126 mg/L 15 mg/L 1 mg/L Parameter Code' - 46529 C0530 00400, 01119 .01051 03094' 00552 - 78141 . Pond (001) 06/18/2019 0.22 7.37 8.5 0.00792 0.002 0.0315 0.806 0.127 Tool Room Trench (005 06/18/2019 0.22 7.11 8.0 0.0148 0.00241 0.0336 1.45 0.033 1 Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceeoance for the same parameter at the same outfall. 'For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 'The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. " See General Permit, Section B, Table 1 to identify the especially sensitive receiving water classifications where the more protective benchmark applies. s Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit Date: 11/1/2018-05/31/2021 SWU-245, last revised 11/1/2018 Page 1 of 3 Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management plan included in the stormwater Pollution Prevention Plan." Dustin LaClair Name (Print name) EHS Manager M till 9 Signature Date Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical format. When results are below the applicable limits, they must be reported in the format. "<XX mg/L" where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. n Nn rlicrhnrnn thic nnrinrl Jz Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches3 New Motor Oil or Hydraulic Oil Usage Non -Polar O&G/ Total Petroleum Hydrocarbons Total Suspended Solids Benchmarks - - - 15 mg/L 100 mg/L or 50 mg/L4 Parameter Code - 46529 NCOIL 00552 CO530 NW rI .1 Footnotes from Part A also apply to Part B Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Permit Date: 1!/1/2018-05/31/2021 SWU-245, last revised 11/1/2018 Page 2 of 3 FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3• HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES Q NO ❑ IF YES, HAVE YOU CONTACTED THE DEMLR REGIONAL OFFICE? YES Q NO ❑ REGIONAL OFFICE CONTACT NAME: Danny Smith Mail an original copv of this DMR, including all "No Discharge" reports within 30 days of receipt of the lab results (or at end of monitoring period in the case of "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am awarmthat,4gre are signifjcdnt penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." of Permittee Permit Date: 11/1/2018-05/31/2021 r,i 31 1019 Date SWU-245, last revised 11/1/2018 Page 3 of 3 aceAnalytical' ANALYTICAL REPORT Nelbnel Centerfor iesting 8lnnawrion July 02, 2019 Eaton Corporation Sample Delivery Group: Samples Received: Project Number: Description: Site: Report To: L1110945 06/20/2019 28091-R Eaton Corp Monthly Stormwater ROXBORO,NC Dustin LaClair 2564 Durham Road Roxboro, NC 27573 Entire Report Reviewed By: 4N dj� Heather J Wagner Project Manager 11 Results relate only tin full. without o the items tested or calibrated and are reponed as rounded values. This test report shall not be reproduced, except written approvaof the l laboratory. Where applicabte, sampling conducted by Pace National/' _ Is performed per guidance proNded In laboratory standard operating procedures: 060302, 060303,and 060304. ,f- TABLE OF CONTENTS ONE LAB NATIONWIDE Cp: Cover Page 1 Tc: Table of Contents 2 Cp ❑ Ss: Sample Summary 3 Cn: Case Narrative 4 Sr: Sample Results 5 JSs 2019-06-18-001 L1110945-01 5 2019-06-18-005 L1110945-02 g Cn Qc: Quality Control Summary 11 SSr Gravimetric Analysis by Method 2540 D-2011 11 Wet Chemistry by Method 1664E 12 QC Metals (ICP) by Method 200.7 13 Volatile Organic Compounds (GC/MS) by Method 624.1 14 GI Pesticides (GC) by Method EPA 608.3 t6 eAl Polychlorinated Biphenyls(GC)by Method EPA-608.3 18 Semi Volatile Organic Compounds (GC/MS) by Method 625.1 19 9 SC GI: Glossary of Terms 24 Al: Accreditations & Locations 25 Sc Sample Chain of Custody 26 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE Eaton Corporation 28091-R L1110945 07/02/19 09:02 2 of 26 SAMPLE SUMMARY ON,E LAB. NATIONWIDE: Collected by Collected dateltime Received dateltime 2019-06-18-001 L111O945-01 W W Colin Betchan 06118/1914:30 06120/19 09:00 r C P Method Batch Dilution Preparation Analysis Analyst Location dale/time dale/lima 1 TC Grbvlmetric Analysis by Method 2540 D2011 WG1301085 1 06/25/1915:23 06/25I1918:15 MMF Mt. Juliet TN Wet Chemistry by Method 1664E WG1304002 1 06129/1911,16 06/30/1911:40 AIW Mt. Juliet, TN Metals gCP) by Method 2003 WG1300332 1 06125/19 02:32 06126/19 03:00 CCE Mt. Juliet, TN Volatile Organic Compounds (GC/MS) by Method 624.1 WG1300040 1 06/2V1919:08 06121/1919:08 TJJ Mt. Juliet, TN Pesticides (GC) by Method EPA 6083 WG1299470 1 06/21/19 07:15 0612311914:26 LEL Mt. Juliet, TN " Cn Polychlorinated Biphenyls (GC)by Method EPA-608.3 W61299470 1 06/21/1907:16 06/24I1908:51 RP Mt. Juliet, TN Semi Volatile Organic Compounds(GC/MS) by Method 625.1 WG1300466 1 06/23/1914:03 06/25/1915:03 AO MI. Juliet, TN Fr] 2019-06-18-005 L111O945-02 WW Collected by Colin Betchan Collected dateltime 06AW914:45 Received date/time 06/20t1909:00 6QC Method Batch Dilution Preparation Analysis Analyst Location date/time date/time GI Gravlmetric Analysis by Method 2540 D 2011 WG1301085 1 06/25/1915:23 06/25/1918:15 MMF Mt. Juliet,TN Wet Chemistry by Method 1664E WG1304002 1 06129/191116 ' 06/30/191140 AIW Mt. Juliet, TN aAl Metals (ICP) by Method 200.7 WG1300332 1 06/25/19 02:32 06/26/19 03,03 CCE Mt. Juliet, TN Volatile Organic Compounds (GOMS) by Method 624.1 WG1300040 1 06/21/1919:29 06/2V1919:29 TJJ Mt. Juliet, TN o Pesticides (GC) by Method EPA 608.3 WG1299470 1 06/21119 0715 06/2311914:38 LEL Mt. Juliet, TN SC Polychlorinated Biphenyls (GC) by Method EPA 608.3 WG1299470 1 06/21/19 07:15 06/24/19 09:05 RP Mt. Juliet, TN Semi Volatile Organic Compounds (GOMS) by Method 6251 WG1300466 1 06/23/1914:03 06/2411914:53 AO Mt. Juliet, TN III .ACCOUNT: - - _ PROJECT: SDG: DATE/TIME: r _ PAGE: I Eaton Corporation 28091-R ,. L1110945 07✓02/19 09:02 3 of 26 i CASE NARRATIVE ONE LAB. NATIONWIDE. All sample aliquots were received at the correct temperature, in the proper containers, with the i Cp appropriate preservatives, and within method specified holding times, unless qualified or notated within the report. Where applicable, all MDL (LOD) and RDL (1-00) values reported for environmental samples Tc have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control are within established criteria except where addressed in this case narrative, a non-conformance form or properly qualified within the sample results. By my digital signature below, I atfinn to the best of my 3S5 knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the quality of the data have been identified by the laboratory, and no information or data have been knowingly withheld that would affect the quality of the data. 6Sr n 4 6Qt. Al �G Heather J Wagner s Project Manager AI 9SC .. ACCOUNT: PROJECT. SDG: DATE/TIME: ._...--- .--- ._ PAGE: Eaton Corporation 28091-R L1110945 07/02/19 09.02 4 of 26 2019-06-18-001 SAMPLE RESULTS 01 Col lected date/lime: 06/1811914:30 ,L1110945 - Additional Information Result Units Analyse pH (On Site) 8.5 su n Temperature Ion-sitCl 25.5 Deg C- i Gravimetric Analysis by Method 2540 D-2011 Result Oualifier MDL RDL Dilution Analysis Batch Analyse mg/I mg/l mg/I date/time Suspended Solids 7,37 Wet Chemistry by Method 1664B 0A62 3.30 1 06/25/201918:15 WG1301085 ONE LAB. NATIONWIDE. Result Oualifier MDL RDL Dilution Analysis Batch Analyte mg/1 mg/l mg/l date/time TPH -Oil&Grease U 0.806 5,56 1 06/30/20191140 WG1304002 Metals (ICP) by Method 200.7 Result Oualifier MDL RDL Dilution Analysis Batch Analyte mg4 mg/1 mg/l dale/time Copper 0.00792 J 0.00700 0.0100 1 06/26/201903:00 WG1300332 " Lead .... .. Ui - ::. 0.00200 '. ':'0.00500 � -1, ' 06/26/201903:00, WG1300332 - ' zinc 0.0315 J 0.00340 0,0500 1 06/26/2019 03:00 WG1300332 Volatile Organic Compounds (GC/MS) by Method 624.1 Result Oualifier MDL RDL Dilution Analysis Batch Analyte mg/l mg/l mg/I date/time Acrolein U 0.00887 0.0500 1 06/21/2019 19:08 WG1300040 Acrylonitrile -' - .. U - 0.00187 0.0100 '::1 06/21RO191908 WG1300040 - - Benzene U 0.000331 0.00100 1 06121/201919:08 WG1300040 Brornodichlorometmne °'D!- .. 0000380 000100 .1 06/21/2019,1908 WG1300040 Bromoform U 0.000469 0.00100 1 06/21/201919:06 WG1300040 Bromomethane 'U - : .0.060866' "0.00500 t 1 06/21/201919:08" ; -WG1300040 - . Carbon tetrachloride ... U .. 0.000379 a00100 1 061211201919:08 WG1300040 Chlorobenzene - , : U - ` " 0.000348 .. 0.00100 1, 06/21/2019ISM -. WG1300040 6hlorotli6romomelhane U 0.000327 0.00100 . 1 06/21/201919:08 WG1300040 _ Chloroettiane . 0 - ... :: " " b.000453` ° 0.00500 1 06121I2019.19.08 :: ....._. v'... 'WG1300040 2-Chloroethyl vinyl ether U 0.00301 0.0500 1 06121/201919:08 WG1300040 Chloroform. - - :0.000339 J ' 0.000324 0.00500 '_ 1...:. 06/21/201919:08 WG1300040 ' Chloromethane U 0.000276 0.00250 1 06/21/201919:08 WG1300040 I:-Dichlorobeniene: :-.,.0 .,.... -0.000349 0.00100 1 ".. 06/21/20191908 7WG1300040 1,3 Dichlorobenzene U 0.000220 0.00100 1 06/21/201919:08 WG1300040 1,4-Dlchlorobenzene U 0.000274 0.00100 t 06I21I201919 08 W61300040 e Dlchlorodifluoromelhane U 0.000551 0.00500 1 061211201919:08 WG1300040 1.1Dichloroethan2 '. U � 0.000259 0.00100 - 1 ` � -O6/21I201919.08 WG7300040 1,2-0Ichloroethane U 0.000361 0.00100 1 06/21/201919:08 WG1300040 147Dlchloroeihene � ��,U :.. , 0.000398 ; .:0.00100 �1 O6I21I20191908 �-WG1300040 ham s-1,2-Dichloroethene U 0.000396 0.00100 1 06/211201919:08 WG1300040 1.2-Dlchloropropane : U 0.000306 , 0.00100 -. 1 > 062V201919,08 - WG1300040 cis-1,3-Dichloropropene U 0.000418 0.00100 1 06/21/201919:08 WG1300040 n._.. .._-.. _ trans-13:D¢Moropropene - .. U : 000041 ., 0.000419 0 _ 0.00100 ._ " : n ._._.. 06I21I20191908 WG1300040 rlhylbenzene U 0.000384 0.00100 1 06/211201919:08 WG1300040 Methylene Chloride U 0.00100 : 0.00500 '1" : Ofi/21/20191908 WG1300040 1,1,2,2-Tetrachloroelhane U 0.000130 0.00100 1 06/21/201919:08 WG1300040 Tr'ylrachloroethene . 0.00187. 0.000372 0.00100 `_7 06/21I201919:08 WG7300040 Toluene U 0.000412 0.00100 1 06/21/2019 19:08 WG1300040 1,1;'1-Trichloroethane U : 0.000319 - - 0,00100 ;L 0621/201919:08- WG1300040 , 1,1,2-Trichloroethane U 0.000383 0.00100 1 06/21/201919:08 WG1300040 ACCOUNT: - PROJECT: SDG: DATE/TIME: _ PAGE: .Eaton Corporation 28091 R .. , L1110945 .07/02/19 09:02 5 of 26 2019-06-18-001 SAMPLE RESULTS - 01 ONE LAB. NATIONWIDE. Collected daleltime: 06118/19 14:30 L1110945 Volatile Organic Compounds (GC/MS) by Method 624.1 Analyze Result mg/I Qualifier MDL mg/I RDL ni Dilution Analysis date/time Batch Trichloroothene 0,000780 J 0,000398 0,00100 1 06/21/201919:08 _ WG1300040 lrichlorofluoromethane U 0.00120 000500 1 06/21/201919.OR WG1300040 Vinyl chloride U 0.000259 0.00100 1 06/21/201919:08 WG1300040 (S) Toluene d8 99.7 80.0 120 061211201919.08 WG1300040 (S)o.o.a-Triquorotoluene 0000 J2 800120 06217201919:08 WG1300040 (5)4-Bromofluorobenzene 79.6 J2 80.0-120 06121201919: 08 WG1300040 (5)1,2-DlcNoroothone d4 996 700-130 06121120191908 WG1300040 Pesticides (GC) by Method EPA 608.3 Result Qualifier MDL RDL Dilution Analysis Batch Analyze moll mg/I mgll date/time Aldrin U 0.00000813 0.0000500 1 06/23/201914:26 WG1299470 Alpha BHC U 0.0000166 0.0000500 1 06/23/2019 14:26 WG1299470 Beta BHC U 0.0000184 0.0000500 1 06/23/201914.26 WG1299470 Delta BHC U 0.0000197 0.0000500 1 06/23/2019 14:26 WG1299470 Gamma BHC U 0,0000176 0.0000500 1 06123/201914:26 WG1299470 Chlordane U 0.0000977 0.000500 1 06/23/2019 14:26 WG1299470 4,4-DDD U 0.0000170 0.0000500 1 06/23/201914.26 WG1299470 4.4-DDE U 0.0000164 0.0000500 1 06/23/261914:26 WG1299470 4.4 DDT U 0.0000177 00000500 1 06/231201914:26 WG1299470 Deform U 0,00000751 0.0000500 1 06/231201914:26 WG1299470 Endosulfan I U 0.0000179 0.0000500 1 06123/201914,26 WG1299470 Endosulfan II U 0,0000176 0.0000500 1 06/23/2019 14:26 WG1299470 Endosulfan sulfate U 0.0000196 0.0000500 1 06/23/2019 14:26 WG1299470 Endrin U 0,0000189 0,0000500 1 06123/201914:26 WGI299470 Endrin aldehyde U 0,0000142 0,0000500 1 06/23/2019 14:26 WG1299470 Endrin ketone U 0,0000170 0.0000500 1 06/23/2019 14:26 WG1299470 Heptachlor U 0.0000108 0.0000500 1 06/23/2019 14:26 WG1299470 Heptachlor epoxide u 0.0000175 0.0000500 1 06/23/201914:26 WG1299470 Hexachlorobereene U 0.0000134 0.0000500 1 06/23/2019 14:26 WG1299470 Methozychlor U 0.0000193 0,0000500 1 06/23/2019 14:26 WG1299470 Toxaphene U 0.000168 0.000500 1 06/23/201914:26 WG1299470 (5) Decachlorobipherri 59.3 100-144 061231201911 WG1299470 (S) Telrochlorri xylene 61A 10.0135 061231201914,26 WG1299470 Polychlorinated Biphenyls (GC) by Method EPA-608.3 Result Qualifier MDL RDL Dilution Analysis Batch Analyze mg/I mg/I mg/I date/time PCB 1016 U 0,000100 0,000500 1 M24/201908:51 WG1299470 PCB 1221 U 0.0000730 0.000500 1 06/24/2019 08:51 WG1299470 PCB 1232 U 0.0000420 0.000500 1 06/24/2019 08:51 WG1299470 PCB 1242 U 0.0000470 0,000500 1 06Q4/201908:51 WG1299470 PCB 1248 U 0.0000860 0,000500 1 06/24/201908:51 WG1299470 PCB 1254 U 0,0000470 0.000500 1 06/241201908:51 WG1299470 PCB 1260 U 0.000120 0.000500 1 06/24/2019 08:51 WG1299470 (S) Demchlorobiphenyl 57.9 10.0144 0612412019 08,51 WG1299470 (S)retrochloro-m-.rylene 566 10.0-135 06124201908.51 WG1299470 Semi Volatile Organic Compounds (GC/MS) by Method 625.1 Analyze Result mg/I Qualifier MDL al RDL mg/1 Dilution Analysis date/time Batch Acenaphthene U 0.000316 0.00100 1 06/25/201915:03 WG1300466 Acenaphthylene U 0.000309 0,00100 1 06/251201915:03 .WG1300466 Anthraceoe U 0.000291 0.00100 1 06/25/201915:03 WG1300466 Benzidine U 0.00432 0,0100 1 06/251201915.03 WG1300466 ACCOUNT: PROJECT: SDG: DATEMME: PAGE: Eaton Corporation 28091R L1110945 07/02/19 09:02 6 of 26 2019 06-18-00.1; SAMPLE RESULTS - 01 ONE LAB. NATioNwloe: ' Collected date/time: 06/1e119 14130 _ L1110945. Semi Volatile Organic Compounds (GC/MS) by Method 625.1 Result Oualifier MDL RDL Dilution Analysis Balch Cp Analyte mg/I mg/I mg/I date/time Benzo(a)anthracene U 0.0000975 000100 1 06125/20191503 WG1300466 z TC Be, nzo(b)fluoranthene-' :U � ` - , 0.0000896 0.00100. 1 O6/25I20191503 � ,WG1300466 � ": - .. �, Ben2o(k)Iluoranthene U 0.000355 0.00100 1 06/2512019 15 03 WG1300466 3 Benzo(g h l)perylene .. U .. :. 0.0 00161 - - 0.00100 1'.. 66/25/20191503.' . WG13004fi6 - ,. l.. .• - SS IPY rene .03 pis 6.660329 0 0,01100 1 06/25/2019 15 03 WG1300466 �. _ - 4Cn Bis(2-chloroethyl)ether U 0.00162 0.0100 1 06125/2019 15 03 WG1300466 Bis"�2-01oroisopropyl)elher U. 0066445 00100 1 66/25/20191503. 'WG1300466.; , 4 Bromophenyl-phenylether U 0000335 0,0100 1 06/25/20191503 WG1300466 .«. _. _.. ne _ -Chlonaphthale 2ro U' .: ... J4 ,' ..s 0 000330 0 00100 :1 O6/25I2019.15 03 _ WG13004666 .. 7. 4 Chlorophenyl-phenylether U 0000303 00100 1 06125/2019 15 03 WG130G466 6QC Chrysenc U :; .0.000332 "6.00100 : 1 06/25/20191503 WG1300466 ' - Dibenz(ah)anthracene U 0000279 000100 1 06/25120191503 WG1300466 33�Dichlolobenzidine U . , � �- 000202 00100 I 1"- O6/25R0191503 WG1300466 GI 24Dinitrotoluene U 0.00165 00100 1 06n5/2019 15 03 WG1300466 26Aimtrotoluene U:� :. 00 0009 - 00100 1 O6/25I20191503 "WG130046fi'' -' aAl 12.Diphenylhydrazine U 0000318 0.0100 1 06/25/201915:03 WG1300466 Fluoranthene U - 0000310 000100 1 06I25I2079 1503 WG1300466 . 9SG Fluorene U 0,000323 000100 1 065/201915.03 WG1300466 Hexetltlorabenzene U � 000 06125/20191503 WG300466 ' _ Hexachloro-1,3-butadiene U 0.000329 0.0100 1 06125/201915:03 WG1300466 .. _.. ..__...,.-- ... rlezachlorocydopentadiene U -? ....., _-_ - ,0.00233 ..-._. ' 0.0100 1 _ 06/25/20191503 WG1300466 -' Hexachloroethane U J4 0,000365 0.0100 1 061251201915:03 WG1300466 IndenO(12 3 ed)pyrene: - U 0.000279 0.00100 1: 06/25/201915 03 " " 'WG1300466- Isophorone U 0.000272 0.0100 1 06/25/201915:03 WG1300466 °-_ Naphthalene �, ' - ��"�' U ... _ ' " . _..___ ;0.000372 ._ _ .__. ' ' 0.00100 ___ :'�1 ._._ 06I25/20191503 - _ _. - �WG1300466 . . ' Nitrobenzene U 0,000367 0.0100 1 06125/201915:03 WG1300466 n-Nilrosodimetnylarnibe U ' -000126 0.0100 1' : ' 06I25/20191503 'WG1300466- n-Nltrosodiphenylamine U 0.00119 0.0100 1 06125/201915:03 WG1300466 n-Nitrosodo-n-propylamine ;. U� � - .: 0.000403 0.0100 1 06/25/20191503 :WG1300466 Phenanthrene U 0.000366 0.00100 1 061251201915:03 WG1300466 Bahzylbutyl phthalate " U - 0.000275 0.00300 T -06/25/201915'.03 WG1300466 Bis(2-ethylhexypphlhalao U 0.000709 0.00300 1 06/25/201915:03 WG1300466 .. .-.._.....__ . _ "Di-r butyl phthalate � .... ........ U - . __ � - 002 0.000266- . .003 0.00300 ...._._ 1 � 06/25I20191503 25/20 � 'WG1300466 ' ' Dlethyl phthalate U 0.000282 0,00300 1 06125/201915:03 WG1300466 r,. - ._._.... ._._... Dimethyl pfithalate - ...._ U - ' _ -.. ` .... __ _ . 0.000283 ....0 __ 06/25/20 .. Di n-octyl phthalate U 0,000278 0.00300 1 06/25/201915:03 WG1300466 Pyreft ne '' : U 0.000330 0.00100 " 1 06/25/2019 1503 ` WG1300466 1,2,4-Trichlorobenzene U J4 0,000355 0.0100 1 061251201915:03 WG1300466 4-Chloro 3 rnethylpho ehl U 0.000263 ' 0.0100 1 - - 06125/201915 03 WG1300466 ; 2-Chlorophenol U 0.000283 0,0100 1 06/25/20191503 WG1300466 2,4-DichlorophenoI U 0000284 _ 00100 :1 .. 06I25I20191503 WG1300466 2,4-Dimethylphenol U 0.000624 0.0100 1 06/25/201915:03 WG1300466 4,6Dlnuro-2-methylphenol U '0.00262 0.0100 1 06R5I201915.03 WG1300466 2,4 Dinitrophenol U 0.00325 0.0100 1 06/25/201915:03 WG1300466 -. . ..ro _ .. 2-Niro phenol t - U .. 0032 0.000320 .:.0.0100 .0 - .. .. _.. 1 .1 -. 06I25/20191503 .. .. W61300466 . 4-Nitrophenol U 0.00201 0.0100 1 06125/201915:03 WG1300466 PentachloroDhenol U ' 0.000313 0.0100 ;: 1 06R51201915'03"" - W61300466' Phenol 0.00176 J 0.000334 0.0100 1 06/25/201915:03 WG1300466 2,4,6-Tnchlorophenol U - 0.000297- U100 1 06/25120191503 WG1300466 (S) 2-Fluorophenol 18.2 10.0-120 0612WO1915.03 WG1300466 (5)Phenol-d5- 11.5 ` . -' 800-424 062-5:03 ----- WG1300466 /SJ Nitrobenzene-d5 337 15.0-314 051251201915,03 WGI300466 (5/7 Fluorob,phenyl 38.7 '' t 22.0-127. 0525120191603 "WG1300466 (SJ24,6-Tribramophenol 53.5 10.0-153 06125120191503 WG1300466 (S)p-Terphenyl-dl4 58.5 29.0-141 A6751019i5:03 WG1300466 ACCOUNT: + ,: PROJECT:, � SDG: ! DATE/TIME:, PAGE: Eaton Corporation28091-R - ! L1110945 07/02/19 09:02 " 7 of 26 2019-06-18-005 SAMPLE RESULTS - 02 ONE LAB. NATIONWIDE. Collected date/time.; 06118119 14:45 L1110946 Additional Information Result Units �P Analyte pH (On Sue) 8 su TC Temperature bri-site) 31,7 Deg C Gravimetric Analysis by Method 2540 D-2011 Ss Result Qualifier MDL RDL Dilution Analysis Batch GCn Analyte Full mg/I mg/Idate/time_._______ Suspended Solids 7,11 0A20 300 1 06125/201918.15 WG1301085 Wet Chemistry by Method 1664B Result Qualifier MDL RDL Dilution Analysis Batch QC Analyte mg/I mgA mg/I date/time TPH- Oil 8Grease U IAS 10.0 7 06I30/201911:40- WG1304002 7G Metals (ICP) by Method 200.7 BAI Result Qualifier MDL RDL Dilution Analysis Batch Analyte mg/I mg/I mg/I date/time Copper____---- 0.0148 0.00700 0.0100-1 06/26/201903:03--_WG1300332---___----_-�_-__--- e$C Lead 0.00241 J 0.00200 0.00500 1 06/26/201903.03 WG1300332 Zinc 0,0336 1 0.00340 0,0500 1 06/26/201903:03 WG1300332 Volatile Organic Compounds (GGMS) by Method 624.1 Analyte Result mg/I Oualifler MDL ri RDL mil Acrolein U 0.00887 0.0500 Acrylonilrile U 0.00187 0.0100 Benzene U 0.000331 0.00100 Bromodichloromethane U 0,000380 0.00100 Bromoform U 0.000469 0,00100 Bromomethane U 0,000866 0.00500 Carbon tetrachloride U 0.000379 0.00100 Chlorobenzene U 0.000348 0.00100 Chlorodibromomethane U 0,000327 0,00100 ChloroeRrane U 0.000453 0,00500 2-Chloroethyl vinyl ether U 0.00301 0,0500 Chloroform U 0.000324 0.00500 Chloromethane U 0.000276 0.00250 12-Dichlorobenzene U 0.000349 MGM 1,3-Dichlorobenzene U 0.000220 0.00100 1,4-Dichlorobenzene U 0.000274 0.00100 Dichlorodifluoromelhane U 0,000551 0.00500 1,1-Dichloroethane U 0.000259 0.00100 1,2-Dichloroethane U 0.000361 0,00100 L1-Dichloroethene U 0.000392 0.00100 trans-1,2-Dichloroethene U 0.000396 0.00100 1 2-Dichloropropene U 0,000306 0,00100 cis-1,3-Dichloropropene U 0,000418 0.00100 trans-1,3 Dichloropropene U 0.000419 0.00100 Ethylbenzene U 0.000384 0.00100 Methylene Chloride U HMO 0.00500 1,1,2,2-Tetrachloroethane U 0.000130 0.00100 Tetrachloroethene U 0,000372 0.00100 Toluene U 0,000412 0,00100 111-Trichloroethane U 0,000319 0,00100 11,2-Trichloroethane U 0,000383 0.00100 ACCOUNT: PROJECT: Eaton Corporation 28091-R Dilution Analysis date/time 1 06/21/2019 19 29 1 06/21/2019 19:29 1 06/21/2019 19:29 1 06/21/2019 19:29 1 06/21/2019 19:29 1 06/21/2019 19:29 1 06/21/2019 19:29 1 06/21/201919,29 1 06121/201919.29 1 06/21/2019 19:29 1 06/211201919:29 1 06/21/2019 19:29 1 06/21/2019 19:29 1 06/21/2019 19:29 1 06/21/2019 19:29 1 06121/201919:29 1 06/21/2019 19:29 1 06/21/201919.29 1 06/21/2019 19:29 1 06/21/2019 19:29 1 06/21/2019 19:29 1 06/21/2019 19:29 1 06/21/2019 19:29 1 06/21/2019 19.29 1 06121/201919:29 1 061211201919:29 1 06/21/2019 19:29 1 06/21/2019 19:29 1 06/21/201919:29 1 06/21/2019 19,29 1 06121/201919:29 SDG: L1110945 Batch WG1300040- WG1300040 WG1300040 WG1300040 WG1300040 WG1300040 WG1300040 WG1300040 WG1300040 WG1300040 WG1300040 WG1300040 WG1300040 WG1300040 WG1300040 WG1300040 WG1300040 WG1300040 WG1300040 WG1300040 WG1300040 WG1300040. WG1300040 WG1300040 WGI300040 WG1360040 WG1300040 WG1300040 WG1300040 WG1300040 WG1300040 DATE, TIME: 07/02/19 09:02 PAGE: 8 of 26 2019-06-18-005 SAMPLE RESULTS 02 bNELAB. NATIONwiCiE Collected date/Iinie: 013/11 19 14.45 - L1110945 - Volatile Organic Compounds (GC/MS) by Method 624.1 Analyze Result Qualifier ni MDL mgll RDL mg/l Dilution Analysis date/time Batch Trichloioolhene U 0.000398 0,00100. 1 06121/201919:29 WG1300040 Trlchlorofluoromemane U U0120 0.00500 1 0612V201919:29 WG1300040 Vinyl chloride U ,' 0.000259 0.00100 _ '1. O6I21I201919'29,-. WG1300040 _- (S) Toluene u8 96.5 80.0-120 06121120797929 WG1300040 /S/o,a,G-Trlfluorotoluene. r 0.000 J2 8D 0-12o 0621/10191929 WG1300040 (S) 4 Bramofluorobenzene 74,4 J2 80.0-120 06/IU201919:29 WG1300040 (S112-Dichloroefhone-o4 99.2. ` .: t + ' " - 70.0d30 _.-.. _ O6/2U20i91929 . W61300040 Pesticides (GC) by Method EPA 608.3 Result Qualifier MDL RDL Dilution Analysis Batch Analyze mgll mgll mg/I date/time Aldrin U 0.00000813 0.0000500 1 061231201914:38 WG1299470 _. Alpha BHC U _._ 00000166 '00000500 .1 ._ 06/23/20191438 - _ WG1299470 Beta BHC U 0,0000184 0,0000500 1 06/23/2019 14 38 WG1299470 Delta BHC U 0.0000197. 0.0000500 .1. 06/23120191436 WG1299470: I . It -_ Gamma BHC _ U .. .. ., 00000176 .. . _ 00000500 1 _ 06/2312019 14 38 WG1299470 Chlordane ' - U ����'��-� - 0.0000977 � � � � 0.000500 .1 ��� 06123/20191438 � �WG1299470 44-DDD U 0.0000170 0.0000500 1 06/23/20191438 WG1299470 4411 - p,. U U 0 00000164 0.00- - ,, - 06l13,14. /20193 • WG1299470 ... . 1 4.4 DDT U 0.0000177 0,0000500 1 06/23/201914:38 WG1299470 Dleldriri - ' U : , O.000OO75i- . 0.0000500. 1; � 06123I20191438 WG1299470 - Endosulfan I U 0.0000179 0.0000500 1 06/23/201914:38 WG1299470 Endosulfan II :. U- 6.0000176 0.0000500 1'. ; 06/23/201914 36 - WG1299470 Endosulfan sulfate U 0,0000196 0,0000500 1 06/23/201914:38 WG129"70 0.00001 -89: -._...� �^ 0.0000500 �-- - - 1 06/2312019.1438 � WG1299470' .. Endrin aldehyde U 0.0000142 0.0000500 1 06/231201914:38 WG1299470 Entlrin ketone �. �.. U � '. - ' - ':0.0000170 :. � 0.0000500 : �4:..: O6/23/201914 36 �: � , WG1299470 Heptachlor U 0.0000108 0.0000500 1 06/23/201914:38 WG1299470 Heptathlar'epoxide U 0.0000175 0.0000500' 1' - 06I23/20191438 - WG1299470 Hexachlorohenzene U 0.0000134 0.0000500 1 061231201914:38 WG1299470 Methoxychlor, ' ' U 0.0000193 0 0000500 , 1 06123/201914 36 WG1299470 Toxaphene U 0.000168 0M0500 1 06/23/201914:38 WG1299470 _ _ .. .. _.. . ._ ._ .._. ocph en. _ (S/Dechlorobibiphyl ..._.. ,_. _ 7 � 56 . '• _..._-. -� ._..._ .... 100744 � _....._. 06/23/20191438 WG1299470 (SJ Telrochlaro-m-xylene 778 10.0-135 06123120191438 WG1299470 orinated Biphenyls (GC) by Method EPA-608.3 Result Qualifier MDL RDL Dilution Analysis Batch Analyze mgn mg/I mgA date/time PCB 1016 U 0.000100 H00500 1 06124/201909:05 WG1299470 PCB 1221 � -U .0.0000730 0.000500 1 6624120190905 WG7299470 PCB 1232 U 0,0000420 0.000500 1 06/24/2019 09:05 WG1299470 PCB 1242 ll , .. 0.0000470 0 000500 1 _ 06/24/2019 09.05 W6299470 PCB 1248 U 0.0000860 0.000500 1 06/241201909:05 WG1299470 PCB 1254 ' - 0.0000470 0.000500' 1- _ 06/24/20190905 `: WG1299470 ' PCB 1260 U 0.000120 0,000500 1 06/24/2019 09:05 WG1299470 SJDecochlorobmhenyl .: 70.1 00-144 0624120I90905 WG1299470 (S)Tetrochloro-m-xylene 65.1 10.0-135 061241201909:05 WG1299470 Semi Volatile Organic Compounds (GC/MS) by Method 625.1 Analyze Result mg/I Qualifier MDL mg/I RDL mg/I Dilution Analysis date/time Balch Acenaphthene U 0,000316 0.00100 1 06124/201914:53 WG1300466 Acenaphthylede � � U � _ �0.000309 _,. _._. 0.001_00 1 _. _ 06R41201914:53_ .� .. .._ .. wG1300466 Antmacene U 0,000291 0,00100 1 06/241201914.53 WG1300466 aenzitlinc "' U ' � 0.00432 0.0100 ''' _:1 '- '06/24/20191453 ACCOUNT:, PROJECT SDGI DATEMME PAGE: Eaton Corporation 1 28091 R L1110945 '; 07/02/19 09.02 ' 9 of 26 I 2019-06-18-005 SAMPLE RESULTS - 02 ONE LAB. NATIONWIDE. !� Collected date/lime:'; 06118/19 14:45 L1110945 Semi Volatile Organic Compounds (GC/MS) by Method 625.1 Result Ouali6er MDL RDL Dilution Analysis Batch Analyte ni mg/I mgll date/time Benzo(a)anthfacene J 0.0000975 0.00100 1 06/24/2019 14:53 WG1300466 Benzo(6)flutimnthene U 0.0000896 0,00100 1 06/241201914:53 WG1300466 Benm(k)fluoranthene U 0,000355 0,00100 1 06/24/201914:53 WG1300466 Benzo(g,h i)perylene J 0.000161 0.00100 1 06/24/201914,53 WG1300466 Senzo(a)pyrene U 0,000340 0.00100 1 06/24/2019 14:53 WG1300466 DIs(2-chlorethoxy)metim e U 0.000329 0,0100 1 06124/201914:53 WG1300466 Bis(2 chloraethylother J 0,00162 0,0100 1 06/24/2019 14:53 WG1300466 Bis(2-chlomisopropyl)ether U 0.000445 0.0100 1 06/241201914:53 WG1300466 4 Bromophenyl-phenylether U 0.000335 0,0100 1 OGJ241201914:53 WG1300466 2-Chloronaphthalene U J4 0,000330 0,00100 1 06/241201914:53 WG1300466 4 Chlarophenyl phenylether U 0.000303 0.0100 1 06/241201914,53 WG1300466 Chrysene J 0.000332 0.00100 1 06/24/2019 14:53 WG1300466 Dibenz(a,h)anthracene U 0.000279 0,00100 1 06/24/2019 14:53 WG1300466 3.3-Dichlorothenzidine U 0,00202 0,0100 1 06/24/201914,53 WG130N66 2A Dlnitroaluene U 0.00165 0.0100 1 06/24/201914.53 WG1300466 2,6 Dinitrotoluene U 0.000279 0,0100 1 06/24/201914.53 WG1360466 1.2-Diphenylhydrazine U 0,000318 0.0100 1 06/24/2019 14:53 WG1300466 Fluoran(hene U 0.000310 0.00100 1 06/24/201914:53 WG1300466 Fluorene a 0.000323 0,00100 1 06/24/2019 14:53 WG1300466 Hexachlorobenzene U 0.000341 0.00100 1 06/24/2019 14:53 WG1300466 Hexachloro 1,3-buladiene U 0,000329 0.0100 1 06/24/201914:53 WG1300466 Hexachlorocyclopentadiene U 0.00233 0.0100 1 06/24/201914:53 WG1300466 Hexachloroelhane U J4 0,000365 0.0100 1 06/24/2019 14:53 WG1300466 Indeno(1,2,3-cd)pyrene J 0.000279 0.00100 1 06/24/2019 14:53 WG1300466 Isophorone U 0.000272 0,0100 1 06/24/201914:53 WG1300466 Naphthalene U 0,000372 0.00100 1 06/24/201914453 WG1300466 Nitrobenzene U 0,000367 0.0100 1 06/24/2019 14:53 WG1300466 n-Ndrosodimethylamine J 0.00126 0.0100 1 06/24/2019 14:53 WG1300466 mNitrosodiphenylamine U 0.00119 0.0100 1 06/24/201914:53 WG1300466 n-Nitrosodim-propylamine U 0.000403 0.0100 1 06/24/2019 14 53 WG1300466 Phenanlhrene U 0.000366 0.00100 1 06/24/201914,53 WG1300466 Benzylbutyl phthalate U 0.o60275 0.00300 1 06/2401914:53 W61300466 Bis(2-ethylhexypphthalate U 0.000709 0.00300 1 06/24/2019 14:53 WG1300466 Ed mbutyl phthalate 0,000310 J 0.000266 0.00300 1 06/24/2019 14:53 WG1300466 Diethyl phthalate J 0.000282 0,00300 1 06/24/201914.53 WGI300466 Dimethyl phthalate U 0.000283 0,00300 1 06/24/2019 14:53 WG1300466 Di-n-octyl phthalate U 0.000278 0.00300 1 06/24201914:53 WG1300466 Pyrene U 0.000330 0,00100 1 06124/201914:53 WG1300466 1.24-Trichlombenzene U J4 0.000355 0,0100 1 06124/201914,53 WG1300466 4-Chlorc, 3 nethylphenol U 0.000263 0.0100 1 06/24/201914.53 WG1300466 2-Chlorophenol U 0,000263 0.0100 1 06/2412019 14 53 WG1300466 2 4-Dichlorophenol U 0.000284 0.0100 1 06/24/2019 14:53 WG1300466 2,4-Dimethylphenol U 0.000624 0.0100 1 06124/201914:53 WG1300466 4,6-Dinitm-2-methylphenol J 0.00262 0.0100 1 06124/201914:53 WG1300466 2,4-Dinitrophcnol U 0.00325 0.0100 1 06/24/2019 14:53 WG1300466 2-Nitropher l U 0,000320 0.0100 1 06/24/201914,53 WG1300466 4 Nincamnol U 0.00201 0.0100 1 06/241201914:53 WG1300466 Pentachlorophenol J 0.000313 0.0100 1 06/24/2019 14:53 WG1300466 Phenol 0,00164 J 0,000334 0.0100 1 06/24/2019 14:53 WG1300466 2,4,6-Trichlorophenol; U 0,000297 0.0100 1 0624/201914,53 WG1300466 (S)1-Fluorophenol 19.3 10.0-120 0612412019 14 53 WG1300466 (S)Phenol-d5 12.8 8.00-424 061241201914.53 WG1300466 (S) Nitrobenzene-d5 33.6 15,0-314 061241201914:53 WG1300466 (S)2-Fluorobiphenyl 39.3 22.0-127 061Z47201914:53 WG1300466 (S)2.4,6-Tabromophenol 54.0 100-153 06124120191453 WG1300466 (S)p-Terphenyl 614 573 29.0-141 06124120191453 WG1300466 ICp eTc 3S$ 4Cn aQC FI a[Al 9Sc ACCOUNT: PROJECT: SDG' DATE/TIME' PAGE' Eaton Corporation 28091-R L1110945 07/02/19 09.02 10 of 26 WG1301085 QUALITY CONTROL SUMMARY ONELABNATIONWIDE G ravlmetrlc Analysis by Method 2540_D_2011__ — -------'------L7110945-01;Oi=J�- Method Blank (MB) 1 Cp (MB) R3424936-1 06/25/19 18:15 7 TC MB Result MB Qualifier M8 MOIL M ROL Analyze mgfl mgfl mgfl Suspended Solids U 0.350 2,50 aSs L1110831-01 Original Sample (OS) • Duplicate (DUP) 4Cn (OS) L1110831-01 06/25/19 18:15 • (DUP) R3424936-3 06/25/19 18:15 Sr Original Result DUP Result Dilution DUP RPD DUP Qualifier DUPtRPD Limis Analyte mgfl mgfl % % Suspended Solids 58.8 61.2 1 4.00 5 7GI L1110911-01 Original Sample (OS) • Duplicate (DUP) (OS) L1110911-01 06125/1918:15 - (DUP) R3424936-4 06/25/19 18:15 aAl Original Result DUP Result Dilution DUPRPD DUP DUP Qualifier LimitsPD Analyte mg/I mg/I % % z Suspended Solids 2L2 22.6 1 6.39 P1 5 SC Laboratory Control Sample (LCS) (LCS) R3424936-2 06/25/19 18:15 Spike Amount LCS Result LCS Red. Rec. Limits LCS Qualifier Analyte mgfl mgfl % % Suspended Solids 773 780 101 85.0-115 ACCOUNT:.. .. .. - . PROJECT ..- _. .... SDG:: .. , DATE/TIME 28091-R - - L1110945 07/02/19, 0902 _ _ -_. 11 of.. .. _. PAGE :Eaton Corporation 26 WG1304002 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE. y1 Wet Chemistry by Method 1664B L7110945-01,02 Method Blank (MB) (MB) R3426189-1 06/3011911.40 RP Result MB Oualifier MB MDL MB RDL Analyte mg/1 mg4 mg/l TC rea TPH - Oil & Gse U 0,725 5,00 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) 1Lia) rcs4min7-L Ub/surly 11:4U • 1L(.JU) N34Gbin-3 U6/30/191140 Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rea. Limits LCS Qualifier LCSD Oualifier RPD Analyte mg/I mg/I mg/I % % % % ___.—______—____ TPH - Oil & Grease 20.0 22.1 23.9 ill 720 64.0-132 7,g3 RPD Limits 34 ACCOUNT: PROJECT: SDG: Eaton Corporation 26091-R L1110945 DATEFrIME: 07/02/19 09:02 PAGE: 12 of 26 WG1300332 QUALITY "CONTROL SUMMARY ONE LAB NATIONWIDE Metals (ICP). by Method 200.7-"'- Method Blank (MB) CD (MB) R3424691-1 06/26/19 02.18 ME Result MR Qualifier ME MOIL ME ROL z Analyze mg/I mgA mg/I TC Copper U - 0.00700 0.0100 _. � Lead.. U 0.00200 '_ 0.00500 Zinc U 0,00340 0.0500 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3424691-2 06/26/19 02:21 • (LCSD) R3424691-3 06/26/19 02:24 Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec Limits LCS Qualifier LCSD Qualifier RED RED Limits Analyte mgA mgA mgA % % % % % Copper 1.00 1.01 0.978 101 97.8 85.0-115 2.80 20 Lead .'._. _-�,...1.00� _'-� 7.02 1--'0.994. 102 "'99.4 '850115- Zinc 1.00 0.995 0.973 99.5 97.3 85.0-115 2.23 20 L1110970-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L1110970-01 06/26/19 02:27 • (MS) R3424691-5 06/26/19 02:32 • (MSD) R3424691-6 06/26/19 02:35 Spike Amount Original Result MS Result MSD Result MS Rec MSD Rec. Dilution Rec. Limits MS Qualifer MSD Qualifier RPD RPD Limits Analyte mg/I al mgA mg/I % % % % % Copper 1.00 NO 0.967 0.978 96.7 97.8 1 70.0-130 1.18 20 Lead - - -1.00 AND , 1.0Y. _ ° 1.01. 101 -. - �. 101 - .11 „_ 70 0-130.0.0756. QO .. Zinc 1.00 NO 0.980 0.979 97.5 97.4 1 70.0-130 0.0258 20 L1111035-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L1111035-01 06/26/19 02:38 • (MS) R3424691-7 06/26/19 0240 • (MSD) R3424691-8 06/26/19 0243 Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Oualifier MSD Qualifier RPD RPD Limits Analyse mg/I mg/I mg4 mg/I % % % % % Copper 1.00 NO 0.972 0.996 97.2 99.6 1 70.0-130 2.49 - - --4.30 20 Lead .1.00 - NO -... 0.991 _. -. 1.03 . ; _ � 99.1. „ .. .103 :- ., i ..., 70.0-130 - - � �20 Zinc 1.00 NO 0.962 1.00 96.2 100 1 70.0-130 4.06 20 ACCOUNT: ' '' ` 'PROJECT - . SDG: DATE/TIME: _ 'PAGE: "'- 13 of 26 Eaton Corporation ' ""28091-R - L1110945 - '07/02/19 09,02 WG1300040 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE. �6 Volatile Organic Compounds (GC/MS) by Method 624.1 1-1110945-01,02 Method Blank (MB) (MD) R3423681-1 06/21/1917.02 MB Result MB Ouahfier MB MDL MB RDL Analyte mg/I mgn mg/I Acrolein U 0.00887 0,0500 Acrylonitrlle U 0,00187 0.0100 Benzene U 0.000331 0.00100 Bromodichloro methane U 0,000380 0.00100 Bromoform U 0.000469 0.00100 Bromomethane U 0,000866 0.00500 Carbon tetrachloride U 0,000379 0.00100 Chlorobenzene U 0.000348 0.00100 Chlorodibromomethane U 0.000327 0.00100 Chloroethane U 0.000453 0.00500 2-Chloroethyl vinyl ether U 0.0030i 0.0500 Chloroform U 0.000324 0.00500 Chloromethane U 0.000276 0.00250 i,2-Dichlorabenzene U 0,000349 0.00100 i.3 Dichlorobenzene U 0,000220 0,00100 1,4-Dichlorobenzene U 0.000274 0.00100 Dlchlorodifluoromethane U 0.000551 0,00500 1,1-Dichloroethane U 0,000259 000100 1,2-Dichloroethane U 0,000361 0.00100 11-Dichloroethene U 0,000398 0.00100 trans-1,2-Dichloroethene U 0.000396 0.00100 1,2-Dichloroprop8ne U 0,000306 0.00100 cis-1,3-Dichloropropene U 0.000418 0,00100 trans-1,3-Dichloropropene U 0,000419 0.00100 Ethylbenzene U 0.000384 0.00100 Methylene Chloride U 0,00100 0.00500 11 2.2-Tetrachloroethane U 0.000130 0,00100 Tetrachloroethene U 0.000372 0.00100 Toluene U 0.000412 0.00100 1,1.1-Trichloroethane U 0.000319 0.00100 11.2-Trichloroethane U 0.000383 0,00100 Trichloroethene. U 0,000398 0.00100 TrichloroRuoromethane U 0,00120 0.00500 Vinyl chloride U 0.000259 0.00100 (S Toluene-0 102 80.0-120 (Sa,o,o-Trilluorotoluene 0.000 J2 800-120 (S) 4-BromoAuorobenzene 83.2 80.0-120 (S)12-Dichloroethane-d4 97.6 70,0-130 ACCOUNT: PROJECT: Eaton Corporation 28091-R SDG: L1110945 DATEITIME: 07/02/19 09.02 PAGE: 14 of 26 WG1300040 QUALITY"CON.TROL SUMMARY oNeLAe.rAnoNwloE Volatile organic Compounds.(6C/MS) by .Method 624.1 - 1.1110945=01.02 _=--- Laboratory Control Sample (LCS) Cp (LCS) R3423681-2 06/21/1917:23 Spike Amount LCS Result LCS Rec. Rec. Limits LCS Oualifier 2 Analyte mg/I mg/I % % TC Acrolein 0.125 0.118 94.6 60.0-140 Acrylonitrile _ - 0.125 0.159 127'- .: 60.0-140 Benzene 0.0250 0.0255 102 65.0-135 ;Bromotl¢hloromethane. 0.0250-'0.0243 ' 972 '700135- Bromo(orm 0.0250 0.0287 115 700130 Cn Bromomethane - 0.0250 -0.0157 627 .. 150185 5 Carbon tetrachloride 0.0250 0.0239 957 700130 _ Sr _ ..-... - _ - -. Yhlorobenzene _,_- 0.0256 - _ -0.0266 166 �'650-135: Chlorodibromomethane 0.0250 0.0264 114 700135 iChloroethane . " - .; 0.0250 ..- 0.0145 ... •. 579_. -." ._40.0160--- 2-Chloroethyl vinyl ether 0.125 0.116 930 0100-225 Chloroform ._. "0.0250 0.0224: "895 70.0-135- Chloromethane 0.0250 0.0326 130 0100-205 1,2-6lchlorobenzene 0.0250 0.0222 ." 650135- 1,3-Dmhlorobenzene 0.0250 0:0223 -�888 892 700130 14-Dichlorobenzene Dichlorodinuoromethane 0.6250 0.0250 0.0225 0.0235 -899 940 -650135 490-155 9 1,1-Dichloroethane- 0.0250. 0.0246:."' 985 .. 900130:.- 1.2-Dichloroethane 0.0250 0.0264 105 70.0-130 1d-Dichloroethene 0.0250. 0.0187. 74.7 --50.0-150 trans-1,2-Dichloroethene 0.0250 0.0226 90.4 70.0-130 4,2;Dichloropropane 0.0250: _..0.0257 103"- 35.0-165: - - - cis-1,3-Dichloropropene 0.0250 0.0274 110 25.0-175 .trans l,3-Dichloropropene " - 0.0250 0.0292 .117 - -50.0-150 Ethylbenzene 0.0250 0.0243 97.0 60.0-140 Me[hylene.Chloride. .0.0250 �. O0223 789.1 -- 600140.- 1,1,2,2-Tetrachloroethane 0.0250 0.0266 106 60.0-140 _ Tetrachloroethene - 0.0250... 0.0306 122 .. 70.0-130 Toluene 0.0250 0.0256 102 70.0-130 :1,1,1-Trichloroethane. - 0,0250, 0,0226 - 90.4- " .. 700-130 1,1,2-Trichloroethane 0.0250 0.0260 104 70.0-130 _ Tdchloroethene" - -" 0.0250_ "0.0269- 167 65.0-135-- Trichlorolluoromethane 0.0250 0.0188 75.1 50.0-150 _ Vinyl chloride. " -- 0.0250." 0.0204 81.5- `500195 (S) Toluene-u8 101 80.0-120 (S)a,a,a-Tiiflup/otaluene ". 0:000 800.120J2'. (S)4-Bromo(luorobenzene 84.5 80.0-120 _(S)q2-Dichloroethane a4 -" '< 105- 70.0-130 .. ACCOUNT_ - - 'PROJECT: -" .SDG: DATE/TIME PAGE: '.' - 07/02/19 09.02 5 0126 Eaton Corporation �28091 R ' - - L1110945.. - - .. _ _ . WG1299470 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE. Pesticides (GC) by Method EPA 608.3 L1110945-01,02 Method Blank (MB) (MB) R3423788-2 06/23/1911,32 MB Result MB Qualifier MB MDL MB RDL Analyte mg/I mg4 mg/I Aldrin U 0.00000813 0.0000500 Alpha BHC U 0.0000166 0.0000500 Beta BHC U 0,0000184 0,0000500 Delta BHC U 0.0000197 0,0000500 Gamma BHC U 0.0000176 0.0000500 4,4-DDD U 0.0000170 0.0000500 4,4-DDE U 0.0000164 0.0000500 4,4-DDT U 0.0000177 0.0000500 Dieldrin U 0.00000751 0.0000500 Endosulfan I U 0.0000179 0.0000500 Endosulfan II U 0,0000176 0.0000500 Endosulfan sulfate U 0,0000196 0.0000500 Endrin U 0.0000189 0,0000500 Endrin aldehyde U 0,0000142 00000500 Endrin ketone U 0.0000170 0,0000500 Heptachlor U 0.0000108 0.0000500 Heptachlor epoxide U 0.0000175 0.0000500 Hexachlorobenzene. U 0.0000134 0.0000500 Methoxychlor U 0.0000193 0.0000500 Chlordane U 0.0000977 0.000500 Toxaphene U 0.000168 0.000500 (S) Decochlorobiphenyl 43.1 10.0-144 (S) Te(rachloro-m-xylene 89.5 10.0-135 Laboratory Control Sample (LCS) (LCS) R3423788-1 06/23/19 1119 Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier Analyte mg/I mg/I % % Aldrin 0,00100 0,000961 96.1 42.0-140 Alpha BHC 0.00100 0.00115 115 37.0-140 Beta BHC 0.00100 0.00106 106 17 0-147 Delta BHC 0.00100 0.00113 113 19.0-140 Gamma BHC 0,00100 0.00112 112 32.0-140 4,4-DDD 0.00100 0.00106 106 3t0-141 4,4-DDE 0.00100 0.000948 94.8 30.0-145 4,4-DDT 0.00100 0.000866 86.6 25.0-160 Dleldrin 0,00100 0.00107 107 36.0-146 Endosulfan 1 0.00100 0.00103 103 45.0-153 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Eaton Corporation 28091-R L1110945 07/02/19 09:02 16 of 26 WG1299470 QUALITY CONTROL SUMMARY _ ONE LAB. NATIONWIDE_ Pesticloes (GC)by..Methoo EPA 608:3 --L1110945 Laboratory Control Sample (LCS) Cp (LCS) R3423788-1 06/23/19 11:19 Spike Amount LCS Result LCS Rec. Rec. Limits LCS OualiBer z Analyte mg4 mg/I % % TC Endosulfan II MOM 0.00100 Endosulfan sulfate - 0.00100 0.00110 100 110 1,00-202 26.0-144' _ a SS Endrin 0.00100 0.00108 108 30.0-147 Endnnaldehyde. -. 6,00106 -0.00102- - _102 - 560-128- a Endnnketone 0.00100 0.00109 109 540142 Cn :Heptachlor - O.o0100 0.0010o 100 34.0-140 ss Heptachlor epoxide 0,00100 0.00106 106 37.0-142 _ r 'Hexachlorobenzene,: 0,60100 0.000964`_-.'_964 '.-35;0-120. _ Methoxychlor 0.00100 0.00102 102 440160 /SJbecaclilorobiphenyl. —45.8 104144- fS) Tet(ochloro-m-xylene 94.3 10.0-135 7G1 aAl 9Sc .ACCOUNT'. PROJECT: SOG: _. DATE(TIME: PAGE: Eaton Corporation--28091-R L1110945, _ 07/02/19 09:02 - 17 of 26 WG1299470 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE. Polychlorinated 61phenyls (GC) by Method EPA-608.3 L1110945-01,02 Method Blank (MB) (ME) R34239U1-1 Ufi713/1916:30 MB Result MB Qualifier MB MDL MB RDL Analyte mg/I mg/1 mg/l PCB 1260 U 0.000120 0000500 PCB 1016 U 0.000100 0.000500 PCB 1221 U 0,0000730 0.000500 P061232 U 0.0000420 0.000500 PCB 1242 U 0.00(00470 0.000500 PCB 1248 U 0.0000860 0.000500 PCB 1254 U 0.0000470 0.000500 (S) Decochlorobiphenyl 56,1 10 0-144 (S) retrachloro-m-xylene 710 10 0-135 Laboratory Control Sample (LCS) (L(-S) H3423901-2 0623/19 1545 Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier Analyte mg/1 Mel % % PCB 1260 0.00250 0,00192 76.8 8.00-140 PCB 1016 0.00250 0.00219 87.6 50.0-140 (S) Decochlorobiphenyl 44.9 10,0444 (A7etrochloro-m-xylene 94.9 10.0-135 L111O533-02 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L1110533-02 06/24/19 08:10 • (MS) R3423999-1 06/24/19 08.24 • (MSD) R3423999-2 06/24/19 08:38 Spike Amount Original Result MS Result MSD Result MS Rec MSD Rec Dilution Rec Limits Analyze mg/I mg/1 mg/I mg/I % % PCB 1260 0.00250 NO 0,00137 0D0133 548 53.2 1 8.00-140 PCB 1016 0.00250 NO 0.00197 MOM 78.8 75.6 1 50.0-140 (S) Decochlorobiphenyl 374 35.4 100-144 (A Tetrochloro-m-xylene 62..4 60.3 10.0-135 MS Qualifier MSD Qualifier RPD RPD Limits % % ----2.96 38_-- 4.15 36 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE' Eaton Corporation 28091-R L1110945 07/02/19 09'02 18 of 26 WG1300466. QUALITY CONTROL SUMMARY ONE _LAB. NATIONWIDE. _ _- -- - Semi Volatile Organic .Compounds (GC/MS) by Method 625.1 ---'-11110945-01;02 __--s - ----- -__ - Method Blank (MB) CP (MB) R3424171-2 06/2411913:52 MB Result MB Oualater MB MDL MB RDL z Analyte mg/I mg/I mg/I TC Acenaphthene U Acenaphthylene. - U 0.000316 - .0.000309 0.00100 0.00100.: $5 Anthracene U 0.000291 0.00100 _ Azobenzene- - �lU "0.000318 0.0100 -- Benzidme U 0,00432 0.0100 Cn Benzo(a)anthracene U_ :0.0000975,. 0.00100. 5 Benzo(b)tluoranthene U 0,0000996 0.00100 Benzo(k)Fldoranthene U - ' 0.000355 - - 0.00100 - " - 8enzo(g,h,i)perylene U 0.000161 0.00100 8... o(a)pyrene U '_ .0.000340 -0.00100- Bis(2-chlorethoxy)methane U -' 0,000329 _ - 0.0100 'Bis(2 chloroethyl)ether U - .0.00162 - - 0.0100 Bis(2 chloroisopropyl)ether U 0.000445 0.0100 4-Bromophenyl-phenylether ., .0 � --0.000335 .0.0100- 2-Chloronaph halene U 0.000330 0.00100 _ AI 4-Chlorophenyl-phenylether U ` '. Chrysene U - �0.000303 0.000332 0.0100_. 0.00100 Dibenz(a h)anthracene U 0.000279 _ 0.00100. - 33-Dichlorobenzidine U 0,00202 0.0100 2,4-Dinitrotoluene U 0.00165 0.0100 2,6-Dinitrotcluene U 0.000279 0.0100 Fluoranthene:, _ U - - - 0.000310 0.00100- Fluorene U 0.000323 0,00100 Hexachlorobenzene U. 0.000341 - 0..0600 _ - - Hexachloro-1.3-butadiene U 0.000329 0.0100 _ Hexachlorocyclopentadiene. U. _ 0.00233 :0.0100 Hexachloroethane U 0.000365 0.0100 hdeno(1,2,3-cd)pyrene U _ 0.000279 0.00100 .. .. .. .. - ... - Isophorone U 0.000272 0,0100 Naphthalene ', .,..U:: - : :0.000372 0,00100 Nitrobenzene U o.000367 0.0100 m-Nitrosodimethylamine U- - 0.00126 0.0100.- n-Nitrosodiphenylamine U 0.00119 - 0.0100 - n-Nitrosodi-n-propylamine .. . U-' .-0.000403 0.0100, - -` Phenanthrene U 0.000366 0.00100 Benzylbutylphthalate U ". 0.000275 0.00300 - - Bis(2-ethylhexyl)phthalate U 0.000709 0.00300 Di-ri-butyl phthalate .U - � _ - 0.000266 0.00300 Diethyl phthalate U 0,000282 0.00300 .Dimethyl phthalata Ll .. - - - .. .. 0.000283 0.00300 ACCOUNT::- `'. - .PROJECT:" -: ""` '6DG: T' DATE/TIME. .. 'PAGE: Eaton Corporation .. - - 28091-R'.: '..-L1110945 '. .. .- ... 07/02/19 09:02 , ,_ - 19 of 26 WG1300466 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE. Semi Volatile Organic Compounds (GC/MS) by Method 625.1 1-7110945.01,02 Method Blank (MB) (MB).R3424121-2 Ob/24/191352 MB Result Di-n-octyl phthalate U Pyrene U 1,24-Trichlorobenzene U 4 Chloe 3-methylphenol U 2-Chlorophenol U 2,4-Dichlorophenol U 2,4-Dimethylphenol U 4,6-Dinitro-2-methylphenol U 24-Dinitrophenol U 2-Nitrophenol U 4-Nitrophenol U Pentachlorophenol U Phenol U 2,4,6-Trichlorophenol U (S) Nitrobenzene-d5 497 (S) 2-Fluorobiphenyl 64.0 (S)p-Terphenybdl4 83.6 (5) Phenol-d5 16.5 (S) 2-Fluorophenol 27.7 (S) 2,4,6-Tobromophenol 74.5 MB Qualifier Laboratory Control Sample (LCS) MB MDL mgA 0.000278 0.000330 0000355 0,000263 0.000283 0.000284 0.000624 0.00262 0,00325 0.000320 0.00201 0.000313 0.000334 0.000297 MB RDL mg/I 000300 0.00100 0.0100 0.0100 0.0100 0.0100 00100 HIM 0.0100 0.0100 0.0100 0.0100 0,0100 0.0100 15 0-314 22 0-127 29 0 141 8.00-424 10.0-120 10 0-153 (L6) H34241 /1-1 Ob/24/19 Analyfe 13:32 Spike Amount mg/I LCS Result mg/I LCS Rec. % Rec. Limits LCS Qualifier % Acenaph;hene 0.0500 0.0350 70.0 47.0-145 Acenaphthvlene 0,0500 0.0367 73.4 33.0-145 Anthracene 0.0500 0.0379 75.8 27.0-133 Azobenzene 0,0500 0.0395 79.0 37.0-125 Benzidine 0,100 0.0190 19.0 100-120 Benzo(a)anthracene 0.0500 0.0417 63.4 33.0-143 Benzo(b)fluoranthene 0.0500 0.0422 84.4 24.0-159 Benzo(k)fluoranthene 0,0500 0.0407 81.4 11.0-162 Benzo(g,h,i)perylene 0,0500 0.04M 82.0 1.00-219 Benzo(a)pyrene 0.0500 0.0417 83A 17.0-163 Bis(2-chlorethoxy(methane 0.0500 0.0294 58.8 1.00-219 "nis(2-chloroethype;her 0.0500 00673 135 33.0-185 Bis(2-chloroisopropypether 0.0500 0.0305 610 36.0-166 ACCOUNT: PROJECT: SDG: Eaton Corporation 28091-R L111O945 DATE/TIME: 07/02/19 09,02 PAGE: 20 of 26 WG130046.6 QUALITY CONTROL SUMMARY-- ONE LAB. NATIONWIDE _ - - - - =- Semi Volatile. Organic Compounds (GC/MS) . 6y Method'_625-t _ - L7110945.01;02...--- .. - - - Laboratory Control Sample (LCS) Cp (LCS) R3424171-1 06/24/19 13:32 Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier 2 Analyte mgA mg/1 % % TC 4-Bromophenyl-phenylether ,0.0500 0.0369 .. 73.8 - 53 0127 2-Chlcronaphthalene 0.0500 0.0299 59.8 600-120 J4 ,4-Chloropheal -phenylether. 0.0500 0.0359 71.8 250-158- Chysene 0.0500 0.0381 76.2 170168- _ _ ;Dibenz(a,h)anthracene ' 0.0500 '. '.0.0397 . 79.4-.-7.00-227, . - - - n 33-Dichlorobenzidine 0.100 0.0895 99.5 1.00 262 s 2;4-Dimtro:oluene.. '0.0500 '0.0414, - 82.8 - - 390139 - Sr 2,6-Dimtrotoluene 0.0500 0.0395 79.0 500-156 -- :Fluoranthene: : 0.0409 - - 81.8' --260137- - -- Fluorene 0.0500 0.0373 74.6 59 0 121 _ .0.0500 Mexachlorobenzene . -'-0.0500 "0.0385' . 77.0' .: -' 1.00:152�- 7GI Hexachloro-1.3-butadiene 0.0500 0.0129 25.8 240120 _ Hexachlororyclopentadiene-0.0500 :-., -0.0131 :. -26.2 100-120 Hexachloroethane 0.0500 0.0143 286 400120 J4 !Indenol1,2,3-cd)pyrene. 0.0500 :0.0414 :826 - 1.00171.. Isophorone 0.0500 0.0306 61.2 210-196 _ _ _ _ _ aSC Naphthalene ', 0.0500. ..' -0.0267 - 53A 270-133- - Nitrobenzene 0.0500 0.0292 58.4 35.0.180 n-Nitrosodimethylamine 0.0500 -0.0213 426 10.0-120- n-Nitrosodiphenylamine 0.0500 0.0384 76.8 44.0-120 _ n-Nihosodi-n-propylamine: :0.0500 : 0.0314 '628 - - 1.00-230- Phenanthrene 0.0500 0.0375 75.0 54.0-120 'Benzylbuiyl phthalate .:0.0500 0.0408' - 81.6 .1.00-152- 8is(2-ethylhexyl)phthalate 0.0500 0.0398 79.6 8.00-158 Di-h-butyl phthalate 0.0500 .. .. .. ... 0.0428 .. ' 85 6 _ Diethyl phthalate 0.0500 0.0426 85.2 1.00-120 'Dimethyl phthalate :0.0500' 0.0407: - -. 81.4. '1.00-120'- Di-n-octyl phthalate 0MOD 0.0412 82.4 4.00-146 IPyrene '... 0.0500 - 0.0392. ,.78.4 - '52.0-120.- 1,2A-Trichlorobenzene 0.0500 0.0200 40.0 44.0-142 J4 4-Chloro-3-methylphenol,0.0500 0.0359 7i8 22 0-147. - - - - 2-Chlorophenol 0.0500 0.0271 54.2 23.0-134 2,4-DIChIoroRhenol. _:. .' 0.0500-.:.0.0314 : 62.8 - - 39.0-135� 2,4-Dimethylphenol 0.0500 0.0324 64.8 32.0-120 _ 4,6-Dinitro 2-methylphenol - 0.0500. . 0.04831 - 96.6 1.00181.- 2,4-Dinitrophenol 0.0500 0.0552 110 _ _ ..29.0-182 1,00-191 . 2-Nitrophenol -: .0.0500. _:0.0350 70.0 4-Nitrophenol 0.0500 0.0195 39.0 1.00-132 Pemachlorophenol 0,0500 - 0,0446. - : 89.2 14 017fi- Phenol 0.0500 0.0115 23.0 5,00-120 ACCOUNT - :PROJECT: SDP: .... DATEMME: PAGE:. ' Eaton Corporation �- � '"28091R - L1110945 '. __ 07/02/1909:02 21'of 26 _ WG1300466 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE. !IR Seml Volatile Organic Compounds (GC/MS) by Method 625.1 L1110945.01,02 Laboratory Control Sample (1-CS) (LCS( R3424171-1 06/24/1913:32 Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier Analyte mg/I fill % % 2.4,6-Trichloraphen0l 0.0500 0.0395 79.0 37.0-144 (S) Nitrobenzene-d5 52,2 15.0-314 (5)2-Fluorobiphenyl 589 22..0-127 (S)p-7erphenyl-d14 788 29,0-141 (S)Phenol45 23.4 800-424 (S) 2-Fluorophenol 33.9 10.0-)20 (S) 2.4,6-Tribromophenol 93,5 10.0-153 L1111094-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (US) L1111094-01 Ub/24/1917:16 • (MS) P3424171-3 06/24/19 17:37 • (MSD) R3424171-4 06/24/19 17,57 -- Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits Analyte mg/l mg/I mg/1 mg/I -___-.... % % % % % Acenaphthene 0.0500 U 0,0359 ----- 0,0329 _._________.__-__.__ 71.8 65.3 1 47.0-145 8.72 48 Acenaphthylene 0.0500 U 00372 0.0342 74A 68.4 1 33.0-145 SRO 74 Anthracene 0,0500 U 0.0381 0.0369 76.2 73.8 1 27.0-133 3.20 66 Benzo(a)anthracene 0.0500 U 0.0414 0,0407 82.8 814 1 33.0-143 1,71 53 Benzo(b)Fluoramhene 0.0500 U 0.0440 0,0433 88.0 86.6 1 24.0-159 1.60 71 1,2-Diphenylhydrazine 00500 U 0.0404 0,0375 80.8 750 1 18.0-156 745 34 Benzo(k)fiuoranthene 0.0500 U 0.0426 0.0412 852 824 1 11.0-162 334 63 Benzo(g,h,i(perylene 0,0500 U 0.0409 0.0390 81.8 78.0 1 1,00-219 476 97 3enzo(a)pvrene 0.0500 U 0.0430 0-0420 86.0 84.0 1 17.0-163 2.35 72 Bis(2-chlorethoxy(methane 0.0500 a 0.0289 0,0273 STS 54.6 1 33.0-184 5,69 54 Bis(2-chloroethyl)ether 0,0500 U 0.0444 0.0587 88.8 117 1 12.0-158 27.7 i08 Benzibine 0,100 U 0.0323 0.0473 32.3 47.3 1 1,00-120 37.7 40 Bis(2-chloroisopropyi)ether 0.0500 U 0,0309 0.0301 61.8 60.2 1 360-166 2.62 76 4-Bromophenyl-phenylether 0.0500 U 0,0390 0,0372 78.0 74A 1 53 0-127 4,72 43 2-Chloronaphthalene 0,0500 U 0,0308 0.0280 61.6 56.0 1 60.0-120 J6 9.52 24 4-Chlorophenyl-phenylether 0,0500 U 0,0386 0.0357 77.2 71l 1 25-0-158 7.81 61 Chrysene 0.0500 U 0.0386 0.0378 7T2 75S 1 170-168 2.09 87 Dibenz(ah)anthracene 00500 U 0.0396 0.0386 79.2 77.2 1 1,00-227 2,56 126 3,3-Dichlorobenzidine 0.100 U 0,0817 0,0858 81.7 85.8 1 1.00-262 4.90 108 2.4-Dinitrotoluene 0,0500 U 0.0415 0,0389 83.0 77.8 1 39.0-139 6,47 42 2,6-Dinitrotoluene 0.0500 U 0.0410 0,0384 82.0 76.8 1 50.0-158 6.55 48 Fluoranthene 0.0500 U 0,0413 0.0397 82.6 794 1 26.0-137 3,95 66 Fluorene 0.0500 U 0.0388 0.0358 77.6 71.6 1 59.0-121 8,04 38 Hexachlorobenzene 0,0500 U 0.0418 0.0400 83.6 80.0 1 1,00-152 4A0 55 Hexachlcro-1,3-hutadiene 0.0500 U 0.0151 0.0112 30.2 22.4 1 24.0-120 J6 29.7 62 Hexachlorocyclopentabiene 0.0500 U 0,0195 0.0150 39.0 30.0 1 10.0-146 26.1 34 ACCOUNT: PROJECT: SDG: Eaton Corporation 28091-R L1110945 DATE/TIME: 07/02/19 09:02 PAGE'. 22 of 26 WG1300466 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE Seml Volatile Orga Nc Compounds GC/MS) by.Method_625.1._. - --L7110945-01,02. - _ L1111094-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) - CP (OS) L1111094-01 06/24/19 17:16 - (MS) R3424171-3 06/24/1917:37 - Spike Amount Original Result MS Result Analyte mg/I mg/I mg/I (MSD) R3424171-4 06/24/1917:57 MSD Result MS Rec. mg/1 % MSD Rec. % Dilution Rec. Limits % MS Qualifier MSD Oualifier RPD % RPD Limits % Hexachloroethane 0,0500 U 0.0160 0.0128 32.0 25.6 1 MIA-120 J6 J6 22.2 52 Indeno(1,2,3-cd)pyrene. 0.0500. U 0.0389 0.0372 77.8 74.4 1 - 1.00-171 .4.47. 99 - Isophorone 0.0500 U 0.0305 0.0287 61.0 57.4 1 21"0-196 _ 6.08 93 .Naphthalene 0.0500: - :.0 0.0261 0.0248 '52.2 49.6 1 21:0:133 5.11 '65 Nitrobenzene 0.0500 U 0,0292 0.0275 584 55.0 1 35"0-180 6,00 62 n-Nitrosodimethylamine 0.0500 U -.. 0.0208 0.0197 41.6 39.4 -1 100-120 - 5.43 40 . n-Nitrosodiphenylamine D0500 U 0.0405 0.0388 BID 77.6 1 16.0-160 4.29 28 h-Nitrosodi-n-propylamine ""0,0500 U. .0.0311 0.0297 622 59.4 1 1.00-230 � � - 4.61 Phenanthrene a0500 U 0.0381 0.0366 76.2 73.2 1 54.0-120 4,02 39 Benzylbutyl phthalate .. 0.0500 U". 0.0429 OD419 85.8 83.8 1 1.00-152, ,2.36 60 Bis(2-ethylheayl)phthalate 0.0500 U 0.0414 GD411 82.8 82.2 1 8.00-158 0727 82 Di-n-butyl phthalate 0.0500 U:.. - 0.0434- 0,0431 86.8 86.2 -- 4' 1.00-120_. .. ""0.694 - 47 Diethyl phthalate 0.0500 U 0.0425 0.0410 85.0 82.0 - 1 1.00-120 3.59 100 Dimethyl phthalate 0,0500 - - U 0,0411 - 0.0387 .82.2 : 77.4 . �. 1 1.00-120.. - " 6D2 183 Di-n-octyl phthalate 0.0500 U 0.0424 0.0412 84.8 824 1 4DO-146 2,87 69 Pyrene" " 0.0500 .0 - - 0.0403' . 0.697 80 6 .79.4- 1. 52.0-120. .. 1,50 49 r 2 n T. whi-non,ono n n5nn 11 00209 0.0181 41.8 36.2 1 44.0-142 J6 J6 14A 50 4-Chioro 3 methylphenol 0.0500 U. 0.0350 0.03A 70.0- - 64.2 '- .1 _ ..22.0-147 - . -' _ - 8,64 73 2-Chorophenol 0.0500 U 0,0298 0.0273 59.6 54.6 1 23.0-134 876 61 2,4-Dichlorophenol 0.0500 U 0,0314 - 6.0363 - 62.8 66.6 - 1 39.0-135 3:57 - ' 50 2,4-Dimethylphenol 0.0500 U 0.0322 0.0304 644 60.8 1 32.0-120 575 58 4,6-Dinitro-2:methylphenol :: 0.0500 U 0.0443 0.0465 .88.6 93D 1 1.00-181 -4.85 203 2 4-Dinitrophenol 0.0500 U 0.0517 0.0523 103 105 1 1.00-191 115 132 .2-Nitrophenol'... 0.0500 U' -0.0348 0.0333 69.6fi6.6 L -,. 29.0-162 .. 44155 4-Nitrophenol 0,0500 U 0.0158 0.0169 31.6 33.8 1 1.00-132 6,73 _ - 131 Pentachlorophenol 0.0500 U 0.0429 '- ODOR' 85.8 '.85.6" 1 -14.0-176 � 0233 86 Phenol 0.0500 U 0.0115 0.0111 23D 22.2 1 5.00-120 3.54 64 2,4,6-Tr ., 0.0500 U' 0.0393: 0.0377' 78.6 " 75.4 ..1 '37D-144' " 416, -58 (S) Nifrobenzen"5 53.5 50.6 15.0-314 (S)2-Fluoroblphenyl 72.3- 66.2- 21.0117. (S)p-Terphenyl-dN 80.6 80.2 29.0-141 _(S)Phenol-d5 .. .2414 22.1 '8.00424. _. (S) 2-Fluorophenol 38.0 34.7 10.0-120 (S)2,4,6-Tribromophenof _ - 95.0 `870-_ 10.6453. ACCOUNT: Eaton. Corporation . PROJECT: SDG: 28091-R" - - LIIIO945. DATE/TIME: . 07/N/19 09:02; PAGE: 23 of 26 GLOSSARY OF TERMS ONE LAB. NATIONWIDE. 0 Guide to Reading and Understanding Your Laboratory Report Thp information below, is designed to better explain the various terms used In your report of analytical results from the Laboratory. This is not intended as a comprehensive explanation. and if you have additional questions please contact your project representative. Abbreviations and Definitions MDL Method Detection Limit. ND Not detected at the Reporting Limit (or MDI. where applicable). RDL Reported Detection Limit Rec. Recovery. RPD Relative Percent Difference. SDG Sample Delivery Group. Surrogate (Surrogate Standard)- Analves added to every blank, sample, Laboratory Control Sample/Duplicate and (5) Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be detected in all environmental media. U Not detected at the Reporting Limit (or MDL where applicable). Artiste The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analytes reported. If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the Dilution standard or if concentrations of analytes In the sample are higherihan the highest limit ofconcentratlon that the laboratory can accurately report, the sample may be diluted for analysis. Ira value different than 1 is used in this field, the result reported has already been corrected for this factor. These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal Limits for the method and analyte being reported Successful QC Sample analysis will target all analytes recovered or duplicated within these ranges. Original Sample The non -spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control sample. The Original Sample may not be included within the reported SDG. This column provides a letter and/or number designation that corresponds to additional information concerning the result Qualifier reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable. The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was Result no measurable result returned for a specific analyze, the result In this column may state "ND" (Not Detected) or "BDL" (Below Detectable Levels). The information in the results column should always be accompanied by either an MDL (Method Detection Limit) or RDL (Reporting Detection Limit)that defines the lowest value that the laboratory could detect or report for this analyte. Uncertainty (Radiochemistry) Confidence level of 2 sigma. g A brief discussion about the included sample results. including a discussion of any non -conformances to protocol Case Narrative (Cn) observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report. Quality Control This section of the report includes the results of the laboratory quality control analyses required by procedure or Summary (Oc) analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not being performed on your samples typically, but on laboratory generated material. This Is the document created in the field when your samples were initially collected. This is used to verify the time and Sample Chain of date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This Custody (Sc) chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the samples from the time of collection until delivery to the laboratory for analysis. 'Phis section of your report will provide the results of all testing performed on your samples. These results are provided Sample Results (Sr) by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for each sample will provide the name and method number for the analysis reported. Sample Summary (Ss) This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and times of preparation and/or analysis. Qualifier Description J The identification of the analyze is acceptable; the reported value is an estimate. J2 Surrogate recovery limits have been exceeded; values are outside lower control limits. J4 The associated batch OC was outside the established quality control range for accuracy. J6 The sample matrix interfered with the ability to make any accurate determination; spike value is low. P1 RPD value not applicable for sample concentrations less than 5 times the reporting limit. ACCOUNT: PROJECT: SDG'. DATE/TIME: PAGE'. Eaton Corporation 28091 R L1110945 07/02/19 09:02 24 of 26 ACCREDITATIONS & LOCATIONS ONE LAB. NATIONWIDE, Pace National is the only environmental laboratory accredited/certifled to support your work nationwide from one location. One phone call, one point of comact, one laboratory. No other lab is as accessible or prepared to handle your needs throughout the country. Our capacity and capability from our single location laboratory is comparable to the collective totals of the network laboratories In our Industry. The most significant benefit to our one location design Is the design of our laboratory campus. The model Is conducive to accelerated productivity, decreasing tum-around time, and preventing cross contamination, thus protecting sample integrity. Our locus on premium quality and prompt service allows us to be YOUR LAB OF CHOICE. Not all certifications held by the laboratory are applicable to the results reported In the attached report. Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace National. State Accreditations Alabama 40660 Alaska California _ _...._... 2932 Coloratlo iN00003 Connecticut PH0197 Florida - .. _ _..E87487 _.-.-._.__..— ----. .__ Georgia NELAP -,_ _--_._-__-- Georgia' - 923 _ --_-___— Illinois 1uvuua Indiana C-TN-01 Iowa 364 Kansas E10277 Kentucky "--__——_--__ 90010_---__—_ ------ Kentucky 2 16 Louisiana A130792 Louisiana' _ LA180010 Maine TN0002 Maryland 324 Massachusetts M TNO03 Michigan _ 9958 Minnesota 047 999-395 Mississippi TN00003 _ Missouri 340 Montana CERT0086 Third Party Federal Accreditations Nebraska NE OS-15-05 Nevada TN 03_-2002-34-_-- _ New Hampshire ---- — — -- -- New Jersey-NEtAP _—_ _ 2975 -- ------ _ _ . TN002 New Mexico' n/a New York------- North Carolina _ 11742 Env375 Noah Confirm _-- DW21704 _ Carolina' _ 41 _North North Dakota _ R 140 Ohio-VAP -- CL0069 Oklahoma Oregon TN200002 68 02979 _Pennsylvania Rhode Island LA000356 South Carolina 84004 South Dakota n/a Tennessee " 2006 Texas _ T104704245-18-15 Texas' LA80152 Utah TN00003 Vermont VT2006 Virginia 460132 Washington C847 West Vlrgamin 233 Wisconsin 9980939910 Wyoming A2LA A2LA-ISO 17025 1461.01 AIHA LAP,LLC EMIAP 100789 A2tA-ISO 17025° 1461.02 DOD 1461.01 Canada 1461.01 USDA P330-15 00234 _ CPA-Crypto TN00003 'Drinking Water 2 Underground Storage Tanks ° Aquatic Toxicity 'ChemlcaVMlcrobiological "Mold "Wastewater Ilia Accreditation not applicable Our Locations Pace National has sixty-four client support centers that provide sample pickup and/or the delivery of sampling supplies. If you would like assistance from one of our support offices, please contact our main office. Pace National performs all testing at our central laboratory. WA MT NO OR MN T ID SD T W v r MI T T IA T hN NE T IL Ili OH UT T CO T T _ CA 1(S r.10 T Po, t T •• N t TAz NIA UK AR ._._ T MS AL• GA IF Tx � LA _ AK T HI ACCOUNT: PROJECT: - SDG: Eaton Corporation .. 28091.R L1110945 DATE7TIME:. PAGE: 67/02/19 09'D2 25 of 26 : Billing Information: - • -, i^Analysis/Container% Preservative " - Chain of Page c Eatori or oration •, P'. _ . 2564 Durham - NA Financial Services Center 1009 Pres PO$ox 818024.�- .-'x-' cnk _ CBARdljrllC81- �r'-`'+ a5 _ , ,�.'7 G ,, - 7 - Y� F `' •v, p. ': ` t'Y.ez r, — "-* "1"i. "' s ° e *^� . Road'- Cleveland, OH 44181-8024 • `"fPx"'b "'pe^"'°"'" Roxboro, NC 27573 .. f 3, . 1 "t • 't5 , w•--- _, £ D ? i an. ---t '� ^• q A 29 -.- _ ' Ilsast waon ad❑. 'Q: MW tluFel TN 1111I Phvix Tse Q Report to Dustin CaClair " v Email To dustlnlaclalr@eaton.com "'""' •• .. }4 Project ' City/Stale Description. Eaton Corp Semi -Annual Stormwater'- Collected, .. Phone: Client Project IX - "' I lab Project ,-: yy qg rq vi�R' t7- m nw • Fax. - 28091-R 3 EATONRNC 28091SWIZ n ' -y(print)- � f d 4Z ws�"�'' u'.. r,'Z• a =- a '' F21� Collected by SiteJFaOlity lox POIX • ROXBORQNC - 9 148703 a+ a oE~-{ ¢ key ;n,� rr •g3 - Acctnum; EATONRNC-`^�' Collected by (signature):.:. ` 4 • _ ��jjjr �t ,t , a - Rush? (lab MUST Be Notified) Quotex ' _ a Day ._Five DaV'".. ." 2§+J gyp( ' E;Y E Q m'.E.' y,s= € gcEy �O o•i `-t' V, �. r*dyyf� 9Op 'y2 . �. 'Q. E. y,� s"�`N5 .i T h4 Templa�teTT99987r y. Pref 686424"'�` Py yN-NYt,•,-.�V-F'V, Immedietel - _Same - Next Day 5Day (Rad Only) 'Date Results Needed D. cC .I x. UI. Yd�-' v� O. #' - s S& BIn . 87 eath11 nCr�w 3Bg ..YTwo Packed onJce N_ Y _X 10 DaY,(Rad DnlY) ,e„INO 'three Dqy lof OEa•.-O O p0��, �0_.' Our .z'- -a�>-71.E-_ 4 eZ" _ , PB ' Sample ID Comp/Grab. 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Time Received by (Signature) - Trip Blank Received' a No 7•c+ ���.�W Y� � � Relinquished by: (Signature) Date Time: Received by (Signanue) - - ' s,e �C'Botties Pece ed .r Temp; --- If preservation required by Login Oate(rme- Relinquished by: (Signature) , _ _ Date - Time , Received for lab by (Signature) i Date ,_.<-t1•+F Time ,y^ Hold..� a sd3yr -•°